CN106758199A - A kind of pre-treatment processing technology of silk flosssilk wadding - Google Patents
A kind of pre-treatment processing technology of silk flosssilk wadding Download PDFInfo
- Publication number
- CN106758199A CN106758199A CN201611216166.2A CN201611216166A CN106758199A CN 106758199 A CN106758199 A CN 106758199A CN 201611216166 A CN201611216166 A CN 201611216166A CN 106758199 A CN106758199 A CN 106758199A
- Authority
- CN
- China
- Prior art keywords
- silk
- weight
- percentage
- formula
- refining
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/262—Sulfated compounds thiosulfates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to textile technology field, the pre-treatment processing technology of specifically a kind of silk flosssilk wadding.A kind of pre-treatment processing technology of silk flosssilk wadding, including refining, bleaching process flow and neutralization, plus soft technology flow, it is characterised in that：Specific processing technology is as follows：Refining, bleaching process；Neutralize, add soft technology.Compared with the existing technology, employ the synthetic operation system of biotechnology and chemicals technology, new processing route is devised, on the basis of refining, one step of bleaching are completed, the use for reducing chemical assistant is realized, reduce treatment temperature, process time is shortened, water, electricity, the consumption of vapour equal energy source is considerably reduced, discharge of wastewater is reduced, production capacity and product quality are effectively improved, has truly accomplished clean manufacturing, energy-saving and emission-reduction.
Description
Technical field
The present invention relates to textile technology field, the pre-treatment processing technology of specifically a kind of silk flosssilk wadding.
Background technology
Silk floss is that the floating silk on a kind of damaged cocoon and cocoon shell surface is raw material (including continuous, the double palace silk flosses of pelettes etc.), by essence
Practice, dissolve silk gum, garnetting fiber and be made.Its warmth retention property is good, can make clothing wadding and is used by wadding.The white silk of silk floss in traditional handicraft
Drift process includes degumming, bleaching twice technique.Degumming and bleaching are to be completed in two self-contained process respectively, therefore operation is numerous
Multiple, equipment flowing water line length, energy consumption is big；The activity duration is long again, and silk is de- to damage big, low production efficiency；Containing a large amount of in its working solution
Alkali, bleaching agent, silk it is de- etc., the wastewater environment of discharge is seriously polluted, and intractability is high.
Although degumming, bleaching twice technique to be merged into the technique of step completion in the prior art, exist and use
Chemical assistant it is many, the contaminated wastewater of discharge is serious, and the removal effect of impurity in silk floss after processing, grease is undesirable, silk
De- loss is big, and fibre damage is serious, and silk floss color and luster is partially yellow, and the problems such as pliability is relatively low, therefore the factory for really using now is simultaneously
Seldom.
For example：A kind of disclosed patent of invention " manufacture method of pelettes silk quilt " (application number 201410585989.7),
Working solution is according to 1 in above invention:25~30 bath raio, the continuous piece that will be extracted is put into refining agent, is protected at 97 DEG C~99 DEG C
Micro- fluidized state is held 110~160 minutes, wherein the refining agent is made up of the following ingredients represented with concentration expressed in percentage by weight：
0.1%~0.2% Na2CO3,0.3%~0.5% waterglass, 0.32%~0.48% AEO,
0.08%~0.12% alkyl phenol ethylene oxide condensation product and water composition, complicated component, process time is long, and the de- loss of silk is big,
Fibre damage is serious, and treatment effect is general.
The content of the invention
The present invention employs the synthetic operation system of biotechnology and chemicals technology to overcome the deficiencies in the prior art,
New processing route is devised, on the basis of refining, one step of bleaching are completed, the use for reducing chemical assistant is realized, reduced
Treatment temperature, shortens process time, considerably reduces water, electricity, the consumption of vapour equal energy source, reduces discharge of wastewater, effectively carries
Production capacity high and product quality, have truly accomplished clean manufacturing, energy-saving and emission-reduction.
To achieve the above object, design a kind of pre-treatment processing technology of silk flosssilk wadding, including refining, bleaching process flow and in
With, plus soft technology flow, it is characterised in that：Specific processing technology is as follows：
(1) refining, bleaching process flow：
(1) configuration refining by a certain percentage, bleaching working solution, in addition silk floss scouring machine；
(2) floss silk fibre is put into, floss silk fibre is 1 with the weight ratio of refining, bleaching working solution：30~50；
(3) refining, bleaching working solution are warming up to 75~90 DEG C, are incubated 60~90 minutes；
(4) floss silk fibre after treatment is dehydrated, is washed, be dehydrated standby；
(2) neutralize, add soft technology flow：
(1) configuration by a certain percentage is neutralized, adds soft working solution, in addition silk floss scouring machine；
(2) floss silk fibre after dehydration is added, floss silk fibre and the weight ratio for neutralizing, adding soft working solution are 1：35~40；
(3) soak 30~60 minutes at room temperature；
(4) floss silk fibre after treatment is dehydrated, is dried.
Described refining, the formula of bleaching working solution and percentage by weight are：Compound formulation is 0.3~2%；Refining agent is
0.1~1%；100% hydrogen peroxide is 0.3~1.5%；Water is 95.5~99.3%.
Described compound formulation is the one kind in clear silk treasured 100T, clear silk treasured 600N, is studied by Shanghai City textile science
The product of institute's production；The formula and percentage by weight of described clear silk treasured 100T be：Boratex is 30%；Ammonium carbonate is 20%；
Sodium chloride is 50%；The formula and percentage by weight of described clear silk treasured 600N be：Ammonium oxalate is 20%；Sodium oxalate is 20%；
Disodium hydrogen phosphate is 20%；Sodium sulphate is 40%.
During described refining agent is net fibroin DW-205, net fibroin DW-206, net fibroin DW-351, net fibroin DW-301
One kind, by the product that Shanghai City Spinning Science Institute produces；The formula and percentage by weight of described net fibroin DW-205
For：Lauryl alcohol sodium sulfovinate is 20%；Xylene sulphonic acid sodium is 5%；Water is 75%；The formula of described net fibroin DW-206
And percentage by weight is：Sldium lauryl sulfate is 18%；Glycol distearate is 10%；Water is 72%；Described net silk
The formula and percentage by weight of plain DW-351 be：Cocounut oil acyl both sexes base diethyl acid disodium is 25%；Propylene glycol oleate is 5%；
Water is 70%；The formula and percentage by weight of described net fibroin DW-301 be：Cocoamidopropyl betaine is 10%；Water is
90%.
Described neutralization, plus the formula and percentage by weight of soft working solution be：Softening agent is 0.06~0.2%；Glacial acetic acid
It is 0.1~0.5%；Water is 99.3~99.84%.
Described softening agent is the one kind in TG-928, TG-320, TG-409, is given birth to by Shanghai City Spinning Science Institute
The product of product；The formula and percentage by weight of described TG-928 be：Dimethyl silicone polymer is 20%；Water is 80%；It is described
TG-320 formula and percentage by weight be：Stearic acid polyoxyethylene (20) ether is 5%；Hexadecanol polyoxyethylene (20) ether is
5%；Water is 90%；The formula and percentage by weight of described TG-409 be：Lanonol polyoxyethylene (30) ether is 30%；Water is
70%.
The present invention compared with the existing technology, employs the synthetic operation system of biotechnology and chemicals technology, devises
New processing route, on the basis of refining, one step of bleaching are completed, realizes the use for reducing chemical assistant, reduces treatment
Temperature, shortens process time, considerably reduces water, electricity, the consumption of vapour equal energy source, reduces discharge of wastewater, effectively improves production capacity
And product quality, truly accomplish clean manufacturing, energy-saving and emission-reduction.
Specific embodiment
A kind of pre-treatment processing technology of silk flosssilk wadding, including refining, bleaching process flow and neutralization, plus soft technology flow, its
It is characterised by：Specific processing technology is as follows：
(1) refining, bleaching process flow：
(1) configuration refining by a certain percentage, bleaching working solution, in addition silk floss scouring machine；
(2) floss silk fibre is put into, floss silk fibre is 1 with the weight ratio of refining, bleaching working solution：30~50；
(3) refining, bleaching working solution are warming up to 75~90 DEG C, are incubated 60~90 minutes；
(4) floss silk fibre after treatment is dehydrated, is washed, be dehydrated standby；
(2) neutralize, add soft technology flow：
(1) configuration by a certain percentage is neutralized, adds soft working solution, in addition silk floss scouring machine；
(2) floss silk fibre after dehydration is added, floss silk fibre and the weight ratio for neutralizing, adding soft working solution are 1：35~40；
(3) soak 30~60 minutes at room temperature；
(4) floss silk fibre after treatment is dehydrated, is dried.
Refining, the formula of bleaching working solution and percentage by weight are：Compound formulation is 0.3~2%；Refining agent be 0.1~
1%；100% hydrogen peroxide is 0.3~1.5%；Water is 95.5~99.3%.
Compound formulation is the one kind in clear silk treasured 100T, clear silk treasured 600N, is produced by Shanghai City Spinning Science Institute
Product；The formula and percentage by weight of described clear silk treasured 100T be：Boratex is 30%；Ammonium carbonate is 20%；Sodium chloride
It is 50%；The formula and percentage by weight of described clear silk treasured 600N be：Ammonium oxalate is 20%；Sodium oxalate is 20%；Phosphoric acid hydrogen
Disodium is 20%；Sodium sulphate is 40%.
Refining agent is the one kind in net fibroin DW-205, net fibroin DW-206, net fibroin DW-351, net fibroin DW-301,
By the product that Shanghai City Spinning Science Institute produces；The formula and percentage by weight of described net fibroin DW-205 be：Month
Cinnamic alcohol ether sodium sulfovinate is 20%；Xylene sulphonic acid sodium is 5%；Water is 75%；The formula and weight of described net fibroin DW-206
Measuring percentage is：Sldium lauryl sulfate is 18%；Glycol distearate is 10%；Water is 72%；Described net fibroin DW-
351 formula and percentage by weight be：Cocounut oil acyl both sexes base diethyl acid disodium is 25%；Propylene glycol oleate is 5%；Water is
70%；The formula and percentage by weight of described net fibroin DW-301 be：Cocoamidopropyl betaine is 10%；Water is
90%.
Neutralize, plus soft working solution formula and percentage by weight be：Softening agent is 0.06~0.2%；Glacial acetic acid be 0.1~
0.5%；Water is 99.3~99.84%.
Softening agent is the one kind in TG-928, TG-320, TG-409, by the product that Shanghai City Spinning Science Institute produces
Product；The formula and percentage by weight of described TG-928 be：Dimethyl silicone polymer is 20%；Water is 80%；Described TG-
320 formula and percentage by weight be：Stearic acid polyoxyethylene (20) ether is 5%；Hexadecanol polyoxyethylene (20) ether is 5%；
Water is 90%；The formula and percentage by weight of described TG-409 be：Lanonol polyoxyethylene (30) ether is 30%；Water is
70%.
In the case where shop equipment is not changed, a step solves degumming, kiering, bleaching processing to present invention process, simplifies
Technological process, reduces technological temperature, substantially reduces the working time.As shown in table 1, existing process is useless with present invention process discharge
Water test data compares.
Table 1
| Project | Unit | Existing process | Present invention process |
| PH value | 10~11 | 9~10 | |
| Temperature | ℃ | 98~110 | 75~90 |
| Soaking time | Minute | 110~160 | 60~90 |
| Technique total used time | Minute | 150~200 | 90~120 |
The shortening of present invention process working time, the floss silk fibre reduced in the process of scouringing and bleaching is damaged, and reduces weight-loss ratio,
Improve the whiteness of floss silk fibre after scouringing and bleaching.As shown in table 2, existing process and present invention process silk floss semi-finished product physical index pair
Compare data.
Table 2
| Detection project | Existing process | Present invention process |
| Whiteness (W10) | 75~80 | 81~85 |
| Weight-loss ratio | ≤13 | ≤7 |
Embodiment 1
Material：Pelettes is continuous.
Equipment：Silk floss scouring machine.
Refining, the formula of bleaching working solution：Hydrogen peroxide (100%) is 9g/L；Clear silk treasured 100T is 5g/L；Net fibroin DW-
206 is 1.5g/L.
Neutralize, add the formula of soft working solution：Glacial acetic acid is 5g/L；TG-928 is 2g/L.
Technological process：
(1) by the refining of above-mentioned recipe configuration, bleaching working solution；
(2) pelettes silk floss is put into, the continuous weight ratio with refining, bleaching working solution of pelettes is 1：40, temperature is 50 DEG C；
(3) refine, bleaching working solution is warming up to 90 DEG C, is incubated 60 minutes；
(4) the pelettes silk floss after treatment is carried out into discharge opeing, dehydration, liquid carrying rate is 80%；
(5) the pelettes silk floss after dehydration is washed at room temperature, washing time is 30 minutes；
(6) the pelettes silk floss after washing is dehydrated, liquid carrying rate is 80%；
(7) by the pelettes silk floss after dehydration be put into neutralization, plus soft working solution in, pelettes it is continuous with neutralize, plus soft working solution weight
Amount is than being 1：40, normal temperature, soak time is 30 minutes；
(8) the pelettes silk floss after treatment is dehydrated, liquid carrying rate is 80%；
(9) the pelettes silk floss after dehydration is dried, drying temperature is 80 DEG C, drying time is 5 hours, drying is to containing tide
Rate is less than 15%.
Embodiment 2
Material：Double palaces are continuous.
Equipment：Silk floss scouring machine.
Refining, the formula of bleaching working solution：Hydrogen peroxide (100%) is 3g/L；Clear silk treasured 100T is 1g/L；Net fibroin DW-
301 is 0.5g/L.
Neutralize, add the formula of soft working solution：Glacial acetic acid is 1g/L；TG-409 is 2g/L.
Technological process：
(1) by the refining of above-mentioned recipe configuration, bleaching working solution；
(2) double palaces silk flosses are put into, the continuous weight ratio with refining, bleaching working solution in double palaces is 1：50, temperature is 60 DEG C；
(3) refine, bleaching working solution is warming up to 80 DEG C, is incubated 90 minutes；
(4) by treatment after double palace silk flosses carry out discharge opeing, dehydration, liquid carrying rate is 100%；
(5) by dehydration after double palaces silk floss washed at room temperature, washing time be 30 minutes；
(6) by washing after double palace silk flosses be dehydrated, liquid carrying rate is 100%；
(7) by dehydration after double palace silk flosses be put into neutralization, plus soft working solution in, double palaces it is continuous with neutralize, plus soft working solution weight
Amount is than being 1：40, normal temperature, soak time is 30 minutes；
(8) by treatment after double palace silk flosses be dehydrated, liquid carrying rate is 60%；
(9) by dehydration after double palace silk flosses dried, drying temperature be 80 DEG C, drying time be 5 hours, drying to containing tide
Rate is less than 15%.
Each data after embodiment 1 and embodiment 2 are processed are as shown in table 3.
Table 3
| Embodiment | Whiteness | Weight-loss ratio (%) | Oil content (%) |
| 1 | 83 | 5 | 0.9 |
| 2 | 85 | 7 | 1 |
| Existing process | 75 | 12 | 1.5 |
Wherein, the quality requirement in national standard (GB/T 24252-2009) to silk quilt Grade A is：Oil content：≤
1.5%.
Method of testing：Whiteness：GB/T 7973-2003；Weight-loss ratio：Silk floss is placed in insulating box at 105 DEG C and dries to perseverance
Weight, weighs after balance 24h.
Weight-loss ratio=[(m0-m1)/m0] × 100%, in formula, m0It is silk floss original dry mass；m1It is silk flosssilk wadding dry mass after treatment.
Oil content=m0/m1× 100%, silk floss is dried into the m that weighs0, it is placed in the leaching pipe of Soxhlet grease extractor, with
Petroleum ether is extractant, is extracted in the water-bath of 70-75 degree 2 hours, then steams the extractant in the mixed liquor in flask
Hair falls, then is dried 1 hour in 105 degree of insulating boxs, obtains pupal fat dry weight m1。
Claims (6)
1. the pre-treatment processing technology of a kind of silk flosssilk wadding, including refining, bleaching process flow and neutralization, plus soft technology flow, it is special
Levy and be：Specific processing technology is as follows：
（One）Refining, bleaching process flow：
（1）Configuration refining by a certain percentage, bleaching working solution, in addition silk floss scouring machine；
（2）Floss silk fibre is put into, floss silk fibre is 1 with the weight ratio of refining, bleaching working solution：30~50；
（3）Refining, bleaching working solution are warming up to 75~90 DEG C, 60~90 minutes are incubated；
（4）Floss silk fibre after treatment is dehydrated, is washed, be dehydrated standby；
（Two）Neutralize, add soft technology flow：
（1）Configuration by a certain percentage is neutralized, adds soft working solution, in addition silk floss scouring machine；
（2）The floss silk fibre after dehydration is added, floss silk fibre and the weight ratio for neutralizing, adding soft working solution are 1：35~40；
（3）Soak 30~60 minutes at room temperature；
（4）Floss silk fibre after treatment is dehydrated, is dried.
2. the pre-treatment processing technology of a kind of silk flosssilk wadding according to claim 1, it is characterised in that：Described refining, bleaching
The formula and percentage by weight of working solution be：Compound formulation is 0.3 ~ 2%；Refining agent is 0.1 ~ 1%；100% hydrogen peroxide be 0.3 ~
1.5%；Water is 95.5 ~ 99.3%.
3. the pre-treatment processing technology of a kind of silk flosssilk wadding according to claim 2, it is characterised in that：Described compound formulation is
One kind in clear silk treasured 100T, clear silk treasured 600N；The formula and percentage by weight of described clear silk treasured 100T be：Boratex is
30%；Ammonium carbonate is 20%；Sodium chloride is 50%；The formula and percentage by weight of described clear silk treasured 600N be：Ammonium oxalate is 20%；
Sodium oxalate is 20%；Disodium hydrogen phosphate is 20%；Sodium sulphate is 40%.
4. the pre-treatment processing technology of a kind of silk flosssilk wadding according to claim 2, it is characterised in that：Described refining agent is net
One kind in fibroin DW-205, net fibroin DW-206, net fibroin DW-351, net fibroin DW-301；Described net fibroin DW-205
Formula and percentage by weight be：Lauryl alcohol sodium sulfovinate is 20%；Xylene sulphonic acid sodium is 5%；Water is 75%；Described is net
The formula and percentage by weight of fibroin DW-206 be：Sldium lauryl sulfate is 18%；Glycol distearate is 10%；Water is
72%；The formula and percentage by weight of described net fibroin DW-351 be：Cocounut oil acyl both sexes base diethyl acid disodium is 25%；Propane diols
Oleate is 5%；Water is 70%；The formula and percentage by weight of described net fibroin DW-301 be：Cocoamidopropyl betaine
It is 10%；Water is 90%.
5. the pre-treatment processing technology of a kind of silk flosssilk wadding according to claim 1, it is characterised in that：It is described neutralization, plus soft
The formula and percentage by weight of working solution be：Softening agent is 0.06 ~ 0.2%；Glacial acetic acid is 0.1 ~ 0.5%；Water be 99.3 ~
99.84%。
6. the pre-treatment processing technology of a kind of silk flosssilk wadding according to claim 5, it is characterised in that：Described softening agent is
One kind in TG-928, TG-320, TG-409；The formula and percentage by weight of described TG-928 be：Dimethyl silicone polymer
It is 20%；Water is 80%；The formula and percentage by weight of described TG-320 be：Stearic acid polyoxyethylene（20）Ether is 5%；16
Alcohol polyoxyethylene（20）Ether is 5%；Water is 90%；The formula and percentage by weight of described TG-409 be：Lanonol polyoxyethylene
（30）Ether is 30%；Water is 70%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611216166.2A CN106758199B (en) | 2016-12-26 | 2016-12-26 | A kind of pre-treatment processing technology of silk floss |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611216166.2A CN106758199B (en) | 2016-12-26 | 2016-12-26 | A kind of pre-treatment processing technology of silk floss |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106758199A true CN106758199A (en) | 2017-05-31 |
| CN106758199B CN106758199B (en) | 2019-02-15 |
Family
ID=58925772
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611216166.2A Active CN106758199B (en) | 2016-12-26 | 2016-12-26 | A kind of pre-treatment processing technology of silk floss |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106758199B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107604631A (en) * | 2017-08-12 | 2018-01-19 | 浙江同辉纺织股份有限公司 | A kind of refining white technique of silk floss satin |
| CN113564730A (en) * | 2021-08-31 | 2021-10-29 | 冯志伟 | Cold water spinning formula |
| CN115821568A (en) * | 2022-12-23 | 2023-03-21 | 合肥市东方美捷分子材料技术有限公司 | Flexible pretreatment process for pure cotton gauze |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS591768A (en) * | 1982-06-08 | 1984-01-07 | ヘンケル・コマンデイトゲゼルシヤフト・アウフ・アクテイ−ン | Chemicals and method of refining natural silk yarn |
| CN1208094A (en) * | 1998-08-10 | 1999-02-17 | 邹荣顺 | Pongee fabric and the tussah processing technique thereof |
| CN102206875A (en) * | 2011-05-18 | 2011-10-05 | 南充银海丝绸有限公司 | Method for separating and refining silk reeling leftovers |
| CN102560696A (en) * | 2011-11-29 | 2012-07-11 | 湖州市农业科学研究院 | Production method of natural colorful mulberry silk floss |
| CN103628145A (en) * | 2012-08-27 | 2014-03-12 | 南充银海丝绸有限公司 | Frison fixation bleaching refining process |
| CN103898734A (en) * | 2014-03-24 | 2014-07-02 | 苏州润弘贸易有限公司 | Preparation method of silk wadding blended fabric scouring agent |
| CN104695199A (en) * | 2015-02-11 | 2015-06-10 | 海门市润圣纺织品有限公司 | Tussah spun silk textile as well as manufacturing method and application thereof |
-
2016
- 2016-12-26 CN CN201611216166.2A patent/CN106758199B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS591768A (en) * | 1982-06-08 | 1984-01-07 | ヘンケル・コマンデイトゲゼルシヤフト・アウフ・アクテイ−ン | Chemicals and method of refining natural silk yarn |
| CN1208094A (en) * | 1998-08-10 | 1999-02-17 | 邹荣顺 | Pongee fabric and the tussah processing technique thereof |
| CN102206875A (en) * | 2011-05-18 | 2011-10-05 | 南充银海丝绸有限公司 | Method for separating and refining silk reeling leftovers |
| CN102560696A (en) * | 2011-11-29 | 2012-07-11 | 湖州市农业科学研究院 | Production method of natural colorful mulberry silk floss |
| CN103628145A (en) * | 2012-08-27 | 2014-03-12 | 南充银海丝绸有限公司 | Frison fixation bleaching refining process |
| CN103898734A (en) * | 2014-03-24 | 2014-07-02 | 苏州润弘贸易有限公司 | Preparation method of silk wadding blended fabric scouring agent |
| CN104695199A (en) * | 2015-02-11 | 2015-06-10 | 海门市润圣纺织品有限公司 | Tussah spun silk textile as well as manufacturing method and application thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107604631A (en) * | 2017-08-12 | 2018-01-19 | 浙江同辉纺织股份有限公司 | A kind of refining white technique of silk floss satin |
| CN113564730A (en) * | 2021-08-31 | 2021-10-29 | 冯志伟 | Cold water spinning formula |
| CN115821568A (en) * | 2022-12-23 | 2023-03-21 | 合肥市东方美捷分子材料技术有限公司 | Flexible pretreatment process for pure cotton gauze |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106758199B (en) | 2019-02-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106758199B (en) | A kind of pre-treatment processing technology of silk floss | |
| CN105002730A (en) | Low-temperature dyeing and finishing technology of cottonette | |
| CN103469563B (en) | A kind of method for refining of real silk fabric | |
| CN104099670A (en) | Method for degelatinizing hemp fiber with biological enzyme degelatinizing method combined with chemical degelatinizing method | |
| CN108950867B (en) | Production process of high-strength anti-wrinkle spunlace non-woven fabric | |
| CN105256384A (en) | Method for oxidation degumming of ramie under weak acid condition | |
| CN104278336B (en) | Method for manufacturing bassinas silk quilt | |
| CN104278335A (en) | Hemp pretreatment technology | |
| CN107956143A (en) | A kind of production method of new pure natural dyed fabric | |
| CN106087075A (en) | A kind of production method of the bamboo fiber of good spinnability | |
| CN110629554A (en) | Preparation of cotton hydrophilic softening agent used in high-temperature cylinder | |
| CN106968106A (en) | A kind of low soft flocks non-dust cloth procedure for producing of super abrasive | |
| CN106192419A (en) | A kind of fabric softener and preparation method thereof | |
| CN104480542A (en) | Production technology for flax fiber | |
| CN106995958B (en) | A kind of hemp, cotton blended knitted yarn preparation method | |
| CN103255484B (en) | Refined and degummed cotton stalk bark fiber and preparation method thereof | |
| CN102703994A (en) | Process for combining flax enzyme and chemical degumming with bleaching | |
| CN106592199B (en) | A kind of continuous oxygen bleaching refining agent and preparation method thereof | |
| CN103194907A (en) | Pretreatment process for cotton knitted fabric low-temperature scouring and bleaching one bath two steps and washing deoxygenation one bath one step method | |
| WO2018010355A1 (en) | Dyeing method for polyester/cationic dyeable polyester/nylon/spandex fabric | |
| CN102691113A (en) | Sodium chlorite-hydrogen peroxide bleaching integrated bath process of flax | |
| CN102634421A (en) | Clothes washing agent and preparation method thereof | |
| CN102995159A (en) | Method for improving elasticity of linen fabric | |
| CN104195777B (en) | A kind of improve the method for color depth after natural colorful mulberry silk fabric degumming | |
| CN107829317B (en) | A kind of high-efficiency activated dyestuff loose colour remover and its padding process |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 200082 No. 988, Pingliang Road, Shanghai, Yangpu District Patentee after: SHANGHAI TEXTILE RESEARCH INSTITUTE Co.,Ltd. Address before: 200082 No. 988, Pingliang Road, Shanghai, Yangpu District Patentee before: SHANGHAI TEXTILE Research Institute |
|
| CP01 | Change in the name or title of a patent holder | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200605 Address after: 314100 Dong shou (Miao Jia Cun), dayunji Town, Jiashan County, Jiaxing City, Zhejiang Province Patentee after: JIASHAN JIASHENG SILK SPINNING Co.,Ltd. Address before: 200082 No. 988, Pingliang Road, Shanghai, Yangpu District Patentee before: SHANGHAI TEXTILE RESEARCH INSTITUTE Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| CP01 | Change in the name or title of a patent holder |
Address after: 314100 Dongshou (Miaojia Village), dayunji Town, Jiashan County, Jiaxing City, Zhejiang Province Patentee after: Jiashan Jiasheng Silk Textile Co.,Ltd. Address before: 314100 Dongshou (Miaojia Village), dayunji Town, Jiashan County, Jiaxing City, Zhejiang Province Patentee before: JIASHAN JIASHENG SILK SPINNING Co.,Ltd. |
|
| CP01 | Change in the name or title of a patent holder |