CN106968106A - A kind of low soft flocks non-dust cloth procedure for producing of super abrasive - Google Patents

A kind of low soft flocks non-dust cloth procedure for producing of super abrasive Download PDF

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Publication number
CN106968106A
CN106968106A CN201710403813.9A CN201710403813A CN106968106A CN 106968106 A CN106968106 A CN 106968106A CN 201710403813 A CN201710403813 A CN 201710403813A CN 106968106 A CN106968106 A CN 106968106A
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water
dye vat
temperature
producing
soft flocks
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CN201710403813.9A
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Chinese (zh)
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CN106968106B (en
Inventor
蒋宪清
段俊丽
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Huge Ultra-Clean Science And Technology (suzhou) Co Ltd Of Dragon
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Huge Ultra-Clean Science And Technology (suzhou) Co Ltd Of Dragon
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/38Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06BTREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
    • D06B1/00Applying liquids, gases or vapours onto textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing or impregnating
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06CFINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
    • D06C7/00Heating or cooling textile fabrics
    • D06C7/02Setting
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06HMARKING, INSPECTING, SEAMING OR SEVERING TEXTILE MATERIALS
    • D06H7/00Apparatus or processes for cutting, or otherwise severing, specially adapted for the cutting, or otherwise severing, of textile materials
    • D06H7/22Severing by heat or by chemical agents
    • D06H7/221Severing by heat or by chemical agents by heat
    • D06H7/223Severing by heat or by chemical agents by heat using ultrasonic vibration
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/10Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
    • D06M13/184Carboxylic acids; Anhydrides, halides or salts thereof
    • D06M13/207Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatment Of Fiber Materials (AREA)

Abstract

The present invention carries out three immersions, diversified decontamination dust removal, it is ensured that the dustless property of cloth processed using UF water, RO water and DI water;Basic agent is added in UF water, then acid medicine is added in RO water again, can be neutralized before and after both, without additionally carrying out pickling with acid solutions such as acetic acid again;Appropriate organic stabilizer is added in UF water, RO water, it is ensured that the stability of fabric, prevent from carrying out secondary pollution in subsequent step, and can prevent the corrosion of alkalescence or acid solution.

Description

A kind of low soft flocks non-dust cloth procedure for producing of super abrasive
Technical field
The invention belongs to non-dust cloth field, more particularly to it is a kind of low soft flocks non-dust cloth procedure for producing of super abrasive.
Background technology
Non-dust cloth is a kind of chemical cloth for being widely used in the medical semiconductor equipment of electron-optical, the cleaning to itself Degree, absorbability, dust removal, wearability have in very high requirement, current row generally using terylene non-dust cloth or to wash brocade compound Ultra-fine non-dust cloth.The competitively priced but dust removing effects of terylene non-dust cloth are general, and rough surface easily abrades sophisticated product surface.And Polyester-nylon composite superfine fibre non-dust cloth absorbability, dust removal performance are excellent, and surface exquisiteness is difficult scratch sophisticated product surface, but price Costliness, greatly increases product cost, therefore is not widely adopted yet.
Patent CN104074044 discloses a kind of ultra-fine non-dust cloth of blending, and it is employed many times in the water-washing process of fabric The mode arranged while washing can prevent the mode for cloth processed of contamination, but it is cleaned merely with RO water, relatively simple water Washing method, and need repeatedly to can be only achieved preferable dustless property.
The content of the invention
To make up the deficiencies in the prior art, the invention provides a kind of low soft flocks non-dust cloth procedure for producing of super abrasive, including Refine, be dehydrated, shaping, cutting and clean five steps, it is characterised in that the specific steps of the refining are as follows successively:
1.1 enter UF water:Fabric is put into dye vat, UF water is added in dye vat, the bath raio of the UF water is 1:8~1:10, temperature It is controlled in 55 ~ 75 DEG C, 10 ~ 15min of operation immersion;
1.2 Automatic Dosing:, start Automatic Dosing, refining agent and 0.5 ~ 1.5g/L that dosages distribution is 1.0-2.0g/L NaOH, medicament control is added and constantly stirred during dosing in 10min;
1.3 heating:Dye vat temperature is risen to 90 ~ 100 DEG C, the speed of heating is 2 ~ 3 DEG C/Min, is incubated 25-30 minutes;
1.4 cooling:Dye vat temperature is down to normal temperature, cooling rate is 1.0 ~ 2.0 DEG C/Min, to normal temperature after carry out 10min overflow Stream;
1.5 discharge opeing:Water in dye vat is drained, draining mode is now moved using cloth;
1.6 enter RO hot water:RO water is added in dye vat, the bath raio of the RO water is 1:8~1:10, water temperature is controlled at 60 ~ 70 DEG C;
1.7 Automatic Dosing:Citric acid and 0.1 ~ 0.2g/L moisture absorbing and sweat releasing agent of the dosages distribution for 0.5 ~ 2.0g/L, medicament control Add and constantly stirred during dosing in 10min
1.8 heating:Dye vat temperature is risen to 75 ~ 85 DEG C, the speed of heating is 2 ~ 3 DEG C/Min, is incubated 20-30 minutes.
1.9 cooling:Dye vat temperature is down to normal temperature, cooling rate is 1.0 ~ 2.0 DEG C/Min, to normal temperature after carry out 10 ~ 20min overflow;
2.0 discharge opeing:Water in dye vat is drained, draining mode is now moved using cloth;
2.1 enter DI water:DI water, the bath raio 1 of the DI water are added in dye vat:10~1:15, normal temperature operation immersion 15min;
2.2 overflows, discharge opeing:10 ~ 15min of overflow, it is then that the water in dye vat is drained, draining mode is now moved using cloth;
2.3 repeat steps 2.1 and 2.2, refining terminates.
Embodiments in accordance with the present invention, dissolve organic stabilizer in advance in the UF water and RO water.
The dosage of organic stabilizer in embodiments in accordance with the present invention, the UF water is 0.5-1.5g/L, the RO water In organic stabilizer dosage be 0.1-0.2g/L.
Embodiments in accordance with the present invention, the condition of the dehydration is:700 ~ 800 turns/min of rotating speed, 20 ~ 35 minutes time.
Embodiments in accordance with the present invention, the forming machine that the sizing is selected is 7 sections, another plus 4 preheating rollers, with natural Gas combustion heating, whole controllable base weight, thickness and breadth, the actual conditions of sizing are as follows:
Temperature:185 ~ 195 DEG C, main frame speed:20 ~ 25 meters/min;
It is upper super:It is 18 ~ 23 meters/min, lower super:20 ~ 22 meters/min, left hairbrush:15 ~ 20 meters/min, right hairbrush:15 ~ 20 meters/min;
170 meters of breadth of sizing, wind speed 600 ~ 800;
Manufactured finished product fabric physical parameter is:Base weight:130 ~ 135 g/m2, breadth:167 ~ 172cm, thickness:It is more than 0.3mm, water absorption:More than 250ml/m2.
Embodiments in accordance with the present invention, described cut is carried out by the way of ultrasonic wave hilted broadsword or flanging.
Embodiments in accordance with the present invention, cleaning includes cleaning and dried, and wherein drying condition is:The heat that 45 ~ 55 DEG C of temperature 10 ~ 15min of wind, temperature is 10 ~ 15min of cold wind of normal temperature.
Embodiments in accordance with the present invention, can also include the vapor for being passed through flowing between step 2.0 and step 2.1, Under the steam atmosphere of flowing, gaseous state cleaning is carried out to fabric.
Advantages of the present invention is as follows:
(1)The present invention using UF water, RO water and DI water carry out three times soak, diversified decontamination dust removal, it is ensured that cloth processed it is dustless Property;
(2)Basic agent is added in UF water, then acid medicine is added in RO water again, can be neutralized before and after both, without Additionally carry out pickling with acid solutions such as acetic acid again;
(3)Appropriate organic stabilizer is previously added in UF water, RO water(Rather than added simultaneously with medicament), it is ensured that fabric Stability, prevent from carrying out secondary pollution in subsequent step, and can prevent alkalescence or acid solution corrosion.
(4)Under the steam atmosphere of flowing, fabric is placed under high temperature under wet environment, can take away organic substance, and water Steam can go deep into fabric various pieces, and cleaning effect is uniform.
Embodiment
The low soft flocks non-dust cloth procedure for producing of a kind of super abrasive that the present invention is provided, including refine, be dehydrated, shaping, cutting and Clean five steps, it is characterised in that the specific steps of the refining are as follows successively:
1. refining
1.1 enter UF water:Fabric is put into dye vat, UF water is added in dye vat, the bath raio of the UF water is 1:8~1:10, temperature It is controlled in 55 ~ 75 DEG C, operation immersion 10 ~ 15min, and the UF water and dissolves in the dosage of organic stabilizer for 0.5-1.5g/ L;
1.2 Automatic Dosing:Start Automatic Dosing, refining agent and 0.5 ~ 1.5g/L that dosages distribution is 1.0-2.0g/L NaOH, medicament control is added and constantly stirred during dosing in 10min;
1.3 heating:Dye vat temperature is risen to 90 ~ 100 DEG C, the speed of heating is 2 ~ 3 DEG C/Min, is incubated 25-30 minutes;
1.4 cooling:Dye vat temperature is down to normal temperature, cooling rate is 1.0 ~ 2.0 DEG C/Min, to normal temperature after carry out 10min overflow Stream;
1.5 discharge opeing:Water in dye vat is drained, draining mode is now moved using cloth;
1.6 enter RO hot water:RO water is added in dye vat, the bath raio of the RO water is 1:8~1:10, water temperature is controlled at 60 ~ 70 DEG C, and And it is 0.1-0.2g/L that the dosage of organic stabilizer is dissolved in the RO water;
1.7 Automatic Dosing:Citric acid and 0.1 ~ 0.2g/L moisture absorbing and sweat releasing agent of the dosages distribution for 0.5 ~ 2.0g/L, medicament control Add and constantly stirred during dosing in 10min
1.8 heating:Dye vat temperature is risen to 75 ~ 85 DEG C, the speed of heating is 2 ~ 3 DEG C/Min, is incubated 20-30 minutes.
1.9 cooling:Dye vat temperature is down to normal temperature, cooling rate is 1.0 ~ 2.0 DEG C/Min, to normal temperature after carry out 10 ~ 20min overflow;
2.0 discharge opeing:Water in dye vat is drained, draining mode is now moved using cloth;After this, it can include being passed through flowing Vapor, under the steam atmosphere of flowing, to fabric carry out gaseous state cleaning.
2.1 enter DI water:DI water, the bath raio 1 of the DI water are added in dye vat:10~1:15, normal temperature operation immersion 15min;
2.2 overflows, discharge opeing:10 ~ 15min of overflow, it is then that the water in dye vat is drained, draining mode is now moved using cloth;
2.3 repeat steps 2.1 and 2.2, refining terminates.
2. dehydration
The condition of the dehydration is:700 ~ 800 turns/min of rotating speed, 20 ~ 35 minutes time.
3. sizing
The forming machine that the sizing is selected is 7 sections, another plus 4 preheating rollers, is heated with combustion of natural gas, whole controllable base Weight, thickness and breadth, the actual conditions of sizing are as follows:
Temperature:185 ~ 195 DEG C, main frame speed:20 ~ 25 meters/min;
It is upper super:It is 18 ~ 23 meters/min, lower super:20 ~ 22 meters/min, left hairbrush:15 ~ 20 meters/min, right hairbrush:15 ~ 20 meters/min;
170 meters of breadth of sizing, wind speed 600 ~ 800;
Manufactured finished product fabric physical parameter is:Base weight:130 ~ 135 g/m2, breadth:167 ~ 172cm, thickness:It is more than 0.3mm, water absorption:More than 250ml/m2.
4. cut
Described cut is carried out by the way of ultrasonic wave hilted broadsword or flanging.
5. it is clean
Cleaning includes cleaning and dried, and wherein drying condition is:10 ~ 15min of hot blast of 45 ~ 55 DEG C of temperature, temperature is normal temperature 10 ~ 15min of cold wind.
The final products that method for making according to the present invention is obtained have following parameter property:0.3um ↑≤100/ft3, Base weight:135 ± 10 g/m2, thickness:>0.3mm, water absorption:>250ml/m2, delustring time<5s, LPC--0.5um ↑≤500 / cm3, fiber--100um ↑≤4/cm3, calcium and magnesium sodium potassium plasma content in 0.2PPM once;In the husky skin of 1000 mesh After being rubbed 10 times on paper, fiber departs from without fracture without obvious soft flocks, and its wearability is superpower, meets semiconductor and panel production The wiping demand of industry.
Finally it should be noted that:Obviously, above-described embodiment is only intended to clearly illustrate example of the present invention, and simultaneously The non-restriction to embodiment.For those of ordinary skill in the field, it can also do on the basis of the above description Go out other various forms of changes or variation.There is no necessity and possibility to exhaust all the enbodiments.And thus drawn Among the obvious changes or variations that Shen goes out is still in protection scope of the present invention.

Claims (8)

1. a kind of low soft flocks non-dust cloth procedure for producing of super abrasive, including refine, be dehydrated, shaping, cutting and clean five steps, its It is characterised by that the specific steps of the refining are as follows successively:
1.1 enter UF water:Fabric is put into dye vat, UF water is added in dye vat, the bath raio of the UF water is 1:8~1:10, temperature It is controlled in 55 ~ 75 DEG C, 10 ~ 15min of operation immersion;
1.2 Automatic Dosing:, start Automatic Dosing, refining agent and 0.5 ~ 1.5g/L that dosages distribution is 1.0-2.0g/L NaOH, medicament control is added and constantly stirred during dosing in 10min;
1.3 heating:Dye vat temperature is risen to 90 ~ 100 DEG C, the speed of heating is 2 ~ 3 DEG C/Min, is incubated 25-30 minutes;
1.4 cooling:Dye vat temperature is down to normal temperature, cooling rate is 1.0 ~ 2.0 DEG C/Min, to normal temperature after carry out 10min overflow Stream;
1.5 discharge opeing:Water in dye vat is drained, draining mode is now moved using cloth;
1.6 enter RO hot water:RO water is added in dye vat, the bath raio of the RO water is 1:8~1:10, water temperature is controlled at 60 ~ 70 DEG C;
1.7 Automatic Dosing:Citric acid and 0.1 ~ 0.2g/L moisture absorbing and sweat releasing agent of the dosages distribution for 0.5 ~ 2.0g/L, medicament control Add and constantly stirred during dosing in 10min;
1.8 heating:Dye vat temperature is risen to 75 ~ 85 DEG C, the speed of heating is 2 ~ 3 DEG C/Min, is incubated 20-30 minutes;
1.9 cooling:Dye vat temperature is down to normal temperature, cooling rate is 1.0 ~ 2.0 DEG C/Min, to normal temperature after carry out 10 ~ 20min Overflow;
2.0 discharge opeing:Water in dye vat is drained, draining mode is now moved using cloth;
2.1 enter DI water:DI water, the bath raio 1 of the DI water are added in dye vat:10~1:15, normal temperature operation immersion 15min;
2.2 overflows, discharge opeing:10 ~ 15min of overflow, it is then that the water in dye vat is drained, draining mode is now moved using cloth;
2.3 repeat steps 2.1 and 2.2, refining terminates.
2. the low soft flocks non-dust cloth procedure for producing of super abrasive according to claim 1, it is characterised in that:In the UF water and RO Organic stabilizer is dissolved in water in advance.
3. the low soft flocks non-dust cloth procedure for producing of super abrasive according to claim 2, it is characterised in that:Having in the UF water The dosage of machine stabilizer is 0.5-1.5g/L, and the dosage of the organic stabilizer in the RO water is 0.1-0.2g/L.
4. the low soft flocks non-dust cloth procedure for producing of super abrasive according to claim 1, it is characterised in that:The condition of the dehydration For:700 ~ 800 turns/min of rotating speed, 20 ~ 35 minutes time.
5. the low soft flocks non-dust cloth procedure for producing of super abrasive according to claim 1, it is characterised in that:What the sizing was selected Forming machine is 7 sections, another plus 4 preheating rollers, is heated, whole controllable base weight, thickness and breadth, shaped with combustion of natural gas Actual conditions it is as follows:
Temperature:185 ~ 195 DEG C, main frame speed:20 ~ 25 meters/min;
It is upper super:It is 18 ~ 23 meters/min, lower super:20 ~ 22 meters/min, left hairbrush:15 ~ 20 meters/min, right hairbrush:15 ~ 20 meters/min;
170 meters of breadth of sizing, wind speed 600 ~ 800;
Manufactured finished product fabric physical parameter is:Base weight:130 ~ 135 g/m2, breadth:167 ~ 172cm, thickness:It is more than 0.3mm, water absorption:More than 250ml/m2.
6. the low soft flocks non-dust cloth procedure for producing of super abrasive according to claim 1, it is characterised in that:It is described to cut using super Sound wave hilted broadsword or the mode of flanging are carried out.
7. the low soft flocks non-dust cloth procedure for producing of super abrasive according to claim 1, it is characterised in that:Cleaning include cleaning and Drying, wherein drying condition is:10 ~ 15min of hot blast of 45 ~ 55 DEG C of temperature, temperature is 10 ~ 15min of cold wind of normal temperature.
8. the low soft flocks non-dust cloth procedure for producing of super abrasive according to claim 1, it is characterised in that:In step 2.0 and step The vapor for being passed through flowing can also be included between rapid 2.1, under the steam atmosphere of flowing, gaseous state cleaning is carried out to fabric and is walked Suddenly.
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108950839A (en) * 2018-08-08 2018-12-07 龙钜超洁净科技(苏州)有限公司 A kind of production method for removing the ultra-fine wiping non-dust cloth of white mark
CN108977984A (en) * 2018-08-08 2018-12-11 龙钜超洁净科技(苏州)有限公司 A kind of production method of the wear-resisting plain weave non-dust cloth of high wiping
CN109023630A (en) * 2018-08-08 2018-12-18 龙钜超洁净科技(苏州)有限公司 A kind of production method of the ultra-fine non-dust cloth of high wiping
CN111705402A (en) * 2020-06-18 2020-09-25 龙钜超洁净科技(苏州)有限公司 Preparation method of low-static low-impedance wiping dust-free cloth
CN111705403A (en) * 2020-06-18 2020-09-25 龙钜超洁净科技(苏州)有限公司 Preparation method of soft wear-resistant purification wiping dust-free cloth

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CN1807730A (en) * 2006-02-10 2006-07-26 郑志皇 Dustless cloth manufacturing method
CN101507587A (en) * 2009-03-19 2009-08-19 厦门市捷瑞静电设备有限公司 Anti-static dust-free wiping cloth and preparation method thereof
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108950839A (en) * 2018-08-08 2018-12-07 龙钜超洁净科技(苏州)有限公司 A kind of production method for removing the ultra-fine wiping non-dust cloth of white mark
CN108977984A (en) * 2018-08-08 2018-12-11 龙钜超洁净科技(苏州)有限公司 A kind of production method of the wear-resisting plain weave non-dust cloth of high wiping
CN109023630A (en) * 2018-08-08 2018-12-18 龙钜超洁净科技(苏州)有限公司 A kind of production method of the ultra-fine non-dust cloth of high wiping
CN111705402A (en) * 2020-06-18 2020-09-25 龙钜超洁净科技(苏州)有限公司 Preparation method of low-static low-impedance wiping dust-free cloth
CN111705403A (en) * 2020-06-18 2020-09-25 龙钜超洁净科技(苏州)有限公司 Preparation method of soft wear-resistant purification wiping dust-free cloth

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