CN106747905A - A kind of Plant antifreezer with disinsection efficiency and preparation method thereof - Google Patents

A kind of Plant antifreezer with disinsection efficiency and preparation method thereof Download PDF

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Publication number
CN106747905A
CN106747905A CN201611014103.9A CN201611014103A CN106747905A CN 106747905 A CN106747905 A CN 106747905A CN 201611014103 A CN201611014103 A CN 201611014103A CN 106747905 A CN106747905 A CN 106747905A
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CN
China
Prior art keywords
plant
amino acid
antifreezer
pla
glucose
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611014103.9A
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Chinese (zh)
Inventor
马海英
邓万宇
马雷鸣
姜斌
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Anhui New Vision Landscaping Engineering Co Ltd
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Anhui New Vision Landscaping Engineering Co Ltd
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Publication date
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Priority to CN201611014103.9A priority Critical patent/CN106747905A/en
Publication of CN106747905A publication Critical patent/CN106747905A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05C—NITROGENOUS FERTILISERS
    • C05C9/00—Fertilisers containing urea or urea compounds
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/36—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a singly bound oxygen or sulfur atom attached to the same carbon skeleton, this oxygen or sulfur atom not being a member of a carboxylic group or of a thio analogue, or of a derivative thereof, e.g. hydroxy-carboxylic acids
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/647—Triazoles; Hydrogenated triazoles
    • A01N43/653—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/44—Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Environmental Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Organic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of Plant antifreezer with disinsection efficiency and preparation method thereof, it is characterised in that be made up of the raw material of following weight portion：Herba Menthae powder 13, PLA 5 11, camphor 12, sorbitan fatty ester 36, chloroform 8 15, water 25 35, corn protein powder 5 10, triapenthenol 12, glucose 13, amino acid 24, glycerine 46, dodecyl sodium sulfate 12, magnesium chloride 25, urea 25.The present invention soaks corn protein powder in glucose, amino acid; and the bonding effect by PLA is attached on plant; the effect of insulation can not only be reached; wherein glucose, amino acid can dramatically increase the content of sugar in plant, free amino acid; there is protective effect to cell, influence of the freeze injury to plant is effectively reduced；By adding camphor etc., make the Plant antifreezer that there is the effect of desinsection.

Description

A kind of Plant antifreezer with disinsection efficiency and preparation method thereof
Technical field
The present invention relates to a kind of Plant antifreezer, and in particular to a kind of Plant antifreezer and its preparation with disinsection efficiency Method.
Background technology
Below 0 DEG C, plant often occurs cell injury or the phenomena of mortality to Wintering Period temperature.Current plant is main to be prevented One of jelly measure is exactly to spray antifreezing agent, and antifreezing agent is called antifreeze, is applied to that green plants can be significantly improved on all kinds of plants And each planting fruit-trees, the disease-resistant low-temperature resistance of nursery stock, the freezing tolerance of cold spell in later spring, effectively prevent early late frost from attacking, it is to avoid or mitigate By freeze injury.The chemical anti-freezing product species of in the market is a lot, but frost-resistant principle can substantially divide three classes, and one is inducer type, profit Induced with growth hormone etc. and anti-freeze gene is produced in plant, strengthen freezing tolerance；Two is by spraying chemical agent, being formed Diaphragm, makes nursery stock to a certain extent from freeze injury；Three is to apply nutriment, and enhancing cell wall thickness or cytoplasm are dense Degree, improves nursery stock freezing tolerance.
Luan Zengle exists《The preparation of Plant antifreezer》In, using Q resins and glucose etc., it is prepared for a kind of plant antifreeze Agent, but its insulation cryoprotective effects is notable not enough, at the same time, the degraded of resin and recycles problem, is not also solved Certainly.
The content of the invention
Think deeply based on more than, the present invention is intended to provide a kind of insulation cryoprotective effects are good, auxotype, environment-friendly type plant it is antifreeze Agent, and preparation method thereof.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of Plant antifreezer with disinsection efficiency, it is characterised in that be made up of the raw material of following weight portion：
Herba Menthae powder 1-3, PLA 5-11, camphor 1-2, sorbitan fatty ester 3-6, chloroform 8-15, water 25-35, it is beautiful Rice gluten powder 5-10, triapenthenol 1-2, glucose 1-3, amino acid 2-4, glycerine 4-6, dodecyl sodium sulfate 1-2, magnesium chloride 2- 5, urea 2-5.
Described a kind of Plant antifreezer with disinsection efficiency and preparation method thereof, it is characterised in that be by following step Suddenly it is made：
A. sorbitan fatty ester is dissolved in chloroform, under homogenous disperse machine high-speed stirred, is added thereto to 8- 15 parts of water, after emulsification 10-30min, adds PLA, is placed in the dissolving of constant temperature oscillation shaking table；After PLA is completely dissolved, after Continuous stirring and emulsifying 20-40min, obtains uniform white emulsion；
B. corn protein powder, Herba Menthae powder, camphor are added in remaining water, add glucose, amino acid, glycerine, dodecane Base sodium sulfonate, after being uniformly dispersed, soaks 30-60min, obtains mixing suspension；
C. step b gained mixing suspensions are mixed with step a gained white emulsions, after stirring, adds triapenthenol, chlorine Change magnesium, urea, it is well mixed to obtain final product Plant antifreezer.
A kind of described Plant antifreezer with disinsection efficiency and preparation method thereof, it is characterised in that its application method It is spray-on process, Plant antifreezer is diluted 500-800 times and is sprayed on before cooling needs antifreeze plant leaf surface, flower, bud and fruit branch Position.
The beneficial effects of the invention are as follows：PLA can form layer protecting film in plant surface, play that cold-resistant is antifreeze, subtract The effect of few transpiration dehydration, while the production process of PLA is pollution-free, and product be able to can be made with biodegradation after degraded It is vegetable fertilizer, realizes the circulation in nature；Corn protein powder is soaked in glucose, amino acid, and by poly- breast The bonding effect of acid is attached on plant, can not only reach the effect of insulation, and wherein glucose, amino acid can be dramatically increased The content of sugar, free amino acid in plant, so that increase the activity of cytoplasma membrane ATP enzymes and the concentration of cell liquid, it is right Cell has protective effect, effectively reduces influence of the freeze injury to plant；By adding camphor etc., there is the Plant antifreezer and kill The effect of worm.
Specific embodiment
With reference to embodiment, specific embodiment of the invention is further described.
Embodiment
A kind of Plant antifreezer with disinsection efficiency, it is characterised in that be made up of the raw material of following weight portion：
Herba Menthae powder 3, PLA 11, camphor 2, sorbitan fatty ester 6, chloroform 15, water 35, corn protein powder 10, suppression Bud azoles 2, glucose 3, amino acid 4, glycerine 6, dodecyl sodium sulfate 2, magnesium chloride 5, urea 5.
Described a kind of Plant antifreezer with disinsection efficiency and preparation method thereof, it is characterised in that be by following step Suddenly it is made：
A. sorbitan fatty ester is dissolved in chloroform, under homogenous disperse machine high-speed stirred, is added thereto to 8- 15 parts of water, after emulsification 10-30min, adds PLA, is placed in the dissolving of constant temperature oscillation shaking table；After PLA is completely dissolved, after Continuous stirring and emulsifying 20-40min, obtains uniform white emulsion；
B. corn protein powder, Herba Menthae powder, camphor are added in remaining water, add glucose, amino acid, glycerine, dodecane Base sodium sulfonate, after being uniformly dispersed, soaks 30-60min, obtains mixing suspension；
C. step b gained mixing suspensions are mixed with step a gained white emulsions, after stirring, adds triapenthenol, chlorine Change magnesium, urea, it is well mixed to obtain final product Plant antifreezer.
A kind of described Plant antifreezer with disinsection efficiency and preparation method thereof, it is characterised in that its application method It is spray-on process, Plant antifreezer is diluted 500-800 times and is sprayed on before cooling needs antifreeze plant leaf surface, flower, bud and fruit branch Position.Technical parameter of the invention is：Antifreezing effect >=7 day.

Claims (3)

1. a kind of Plant antifreezer with disinsection efficiency, it is characterised in that be made up of the raw material of following weight portion：
Herba Menthae powder 1-3, PLA 5-11, camphor 1-2, sorbitan fatty ester 3-6, chloroform 8-15, water 25-35, it is beautiful Rice gluten powder 5-10, triapenthenol 1-2, glucose 1-3, amino acid 2-4, glycerine 4-6, dodecyl sodium sulfate 1-2, magnesium chloride 2- 5, urea 2-5.
2. a kind of Plant antifreezer with disinsection efficiency according to claim 1 and preparation method thereof, it is characterised in that It is made up of following steps：
A. sorbitan fatty ester is dissolved in chloroform, under homogenous disperse machine high-speed stirred, is added thereto to 8- 15 parts of water, after emulsification 10-30min, adds PLA, is placed in the dissolving of constant temperature oscillation shaking table；After PLA is completely dissolved, after Continuous stirring and emulsifying 20-40min, obtains uniform white emulsion；
B. corn protein powder, Herba Menthae powder, camphor are added in remaining water, add glucose, amino acid, glycerine, dodecane Base sodium sulfonate, after being uniformly dispersed, soaks 30-60min, obtains mixing suspension；
C. step b gained mixing suspensions are mixed with step a gained white emulsions, after stirring, adds triapenthenol, chlorine Change magnesium, urea, it is well mixed to obtain final product Plant antifreezer.
3. a kind of Plant antifreezer with disinsection efficiency according to claim 2 and preparation method thereof, it is characterised in that Its application method is spray-on process, 500-800 times of Plant antifreezer dilution is sprayed on before cooling need antifreeze plant leaf surface, Flower, bud and Fruiting branches.
CN201611014103.9A 2016-11-18 2016-11-18 A kind of Plant antifreezer with disinsection efficiency and preparation method thereof Pending CN106747905A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611014103.9A CN106747905A (en) 2016-11-18 2016-11-18 A kind of Plant antifreezer with disinsection efficiency and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201611014103.9A CN106747905A (en) 2016-11-18 2016-11-18 A kind of Plant antifreezer with disinsection efficiency and preparation method thereof

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Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1709379A (en) * 2005-06-03 2005-12-21 季荣生 Anti-freeze bacteriostat and production method
CN102515948A (en) * 2011-12-09 2012-06-27 大千生态景观股份有限公司 Plant antifreezer and its preparation method
CN103539536A (en) * 2013-10-09 2014-01-29 新疆高冠土壤研究所 Plant antifreeze containing ribitol substances
CN103570442A (en) * 2012-08-03 2014-02-12 天津春之韵园艺工程技术发展有限公司 Formula of antifreezing agent for vertical greening plants and preparation method of antifreezing agent
CN103875672A (en) * 2013-12-20 2014-06-25 西北农林科技大学 Walnut early frost anti-freezing agent
CN103922840A (en) * 2014-04-04 2014-07-16 李美凤 Compound plant anti-freezing agent and preparation method thereof
CN104286026A (en) * 2014-08-29 2015-01-21 徐州万国生物能源有限公司 Plant antifreezing agent
CN104817405A (en) * 2015-05-20 2015-08-05 张达燕 Plant antifreezing agent
CN105145662A (en) * 2015-09-18 2015-12-16 王素敏 Application method of tree crop cold damage protection liquid

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1709379A (en) * 2005-06-03 2005-12-21 季荣生 Anti-freeze bacteriostat and production method
CN102515948A (en) * 2011-12-09 2012-06-27 大千生态景观股份有限公司 Plant antifreezer and its preparation method
CN103570442A (en) * 2012-08-03 2014-02-12 天津春之韵园艺工程技术发展有限公司 Formula of antifreezing agent for vertical greening plants and preparation method of antifreezing agent
CN103539536A (en) * 2013-10-09 2014-01-29 新疆高冠土壤研究所 Plant antifreeze containing ribitol substances
CN103875672A (en) * 2013-12-20 2014-06-25 西北农林科技大学 Walnut early frost anti-freezing agent
CN103922840A (en) * 2014-04-04 2014-07-16 李美凤 Compound plant anti-freezing agent and preparation method thereof
CN104286026A (en) * 2014-08-29 2015-01-21 徐州万国生物能源有限公司 Plant antifreezing agent
CN104817405A (en) * 2015-05-20 2015-08-05 张达燕 Plant antifreezing agent
CN105145662A (en) * 2015-09-18 2015-12-16 王素敏 Application method of tree crop cold damage protection liquid

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
孙绍曾编著: "《新编实用日用化学品制造技术》", 31 October 1996 *

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Application publication date: 20170531