CN106561655A - Thermal insulation nutritional diatomite doped plant anti-freezing agent and preparation method thereof - Google Patents

Thermal insulation nutritional diatomite doped plant anti-freezing agent and preparation method thereof Download PDF

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Publication number
CN106561655A
CN106561655A CN201611027024.1A CN201611027024A CN106561655A CN 106561655 A CN106561655 A CN 106561655A CN 201611027024 A CN201611027024 A CN 201611027024A CN 106561655 A CN106561655 A CN 106561655A
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CN
China
Prior art keywords
parts
kieselguhr
freezing agent
plant
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611027024.1A
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Chinese (zh)
Inventor
马海英
邓万宇
马雷鸣
姜斌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui New Vision Landscaping Engineering Co Ltd
Original Assignee
Anhui New Vision Landscaping Engineering Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui New Vision Landscaping Engineering Co Ltd filed Critical Anhui New Vision Landscaping Engineering Co Ltd
Priority to CN201611027024.1A priority Critical patent/CN106561655A/en
Publication of CN106561655A publication Critical patent/CN106561655A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G13/00Protecting plants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/44Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing at least one carboxylic group or a thio analogue, or a derivative thereof, and a nitrogen atom attached to the same carbon skeleton by a single or double bond, this nitrogen atom not being a member of a derivative or of a thio analogue of a carboxylic group, e.g. amino-carboxylic acids
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C1/00Ammonium nitrate fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity

Abstract

The invention discloses a thermal insulation nutritional diatomite doped plant anti-freezing agent and a preparation method thereof. The anti-freezing agent is prepared from the following raw materials in parts by weight: 2 to 3 parts of starch, 7 to 12 parts of polylactic acid, 2 to 4 parts of diatomite, 3 to 6 parts of sorbitan fatty acid ester, 8 to 15 parts of chloroform, 25 to 35 parts of water, 5 to 10 parts of corn protein flour, 1 to 2 parts of ammonium nitrate, 1 to 3 parts of glucose, 2 to 4 parts of amino acid, 4 to 6 parts of glycerin, 1 to 2 parts of sodium dodecyl sulfate, 2 to 5 parts of magnesium chloride, and 2 to 5 parts of urea. Corn protein flour is soaked in glucose and amino acid, through the adhesive effect of polylactic, the anti-freezing agent is adhered on the plants, the anti-freezing agent has a thermal insulation effect, moreover, glucose and amino acid can prominently increase the contents of sugar and free amino acids in plants, the anti-freezing agent can protect cells and effectively reduce the damage of freezing to plants, and the viscosity of the anti-freezing agent is increased through the addition of diatomite and starch.

Description

A kind of kieselguhr doping Plant antifreezer of insulation nutrition and preparation method thereof
Technical field
The present invention relates to a kind of Plant antifreezer, and in particular to a kind of kieselguhr of insulation nutrition doping Plant antifreezer and Its preparation method.
Background technology
Below 0 DEG C, plant often occurs cell injury or the phenomena of mortality to Wintering Period temperature.Plant is main at present prevents One of jelly measure is exactly to spray antifreezing agent, and antifreezing agent is called antifreeze, is applied to green plantss are significantly improved on all kinds of plants And each planting fruit-trees, the disease-resistant low-temperature resistance of nursery stock, the freezing tolerance of cold spell in later spring, it is effectively prevented early late frost and attacks, it is to avoid or mitigate By freeze injury.Chemical anti-freezing product species on market is a lot, but frost-resistant principle can substantially divide three classes, and one is inducer type, profit Induced with growth hormone etc. and in plant body, produce anti-freeze gene, strengthen freezing tolerance;Two is by spraying chemical agent, being formed Protecting film, makes nursery stock to a certain extent from freeze injury;Three is to apply nutrient substance, strengthens cell wall thickness or Cytoplasm is dense Degree, improves nursery stock freezing tolerance.
Luan Zengle exists《The preparation of Plant antifreezer》In, using Q resins and glucose etc., it is prepared for a kind of plant antifreeze Agent, but its insulation cryoprotective effects is notable not enough, at the same time, the degraded of resin and recycles problem, is not also solved Certainly.
The content of the invention
Think deeply based on more than, the present invention is intended to provide a kind of insulation cryoprotective effects are good, auxotype, environment-friendly type plant it is antifreeze Agent, and preparation method thereof.
The technical problem to be solved is realized using following technical scheme:
The kieselguhr doping Plant antifreezer of a kind of insulation nutrition, it is characterised in that be made up of the raw material of following weight portion:
Starch 2-3, polylactic acid 7-12, kieselguhr 2-4, sorbitan fatty ester 3-6, chloroform 8-15, water 25-35, it is beautiful Rice gluten powder 5-10, ammonium nitrate 1-2, glucose 1-3, aminoacid 2-4, glycerol 4-6, dodecyl sodium sulfate 1-2, magnesium chloride 2- 5, carbamide 2-5.
A kind of kieselguhr doping Plant antifreezer and preparation method thereof of described insulation nutrition, it is characterised in that be by Following steps are made:
A. sorbitan fatty ester is dissolved in chloroform, under homogenous disperse machine high-speed stirred, is added thereto to 8- 15 parts of water, after emulsifying 10-30min, adds polylactic acid, is placed in the dissolving of constant temperature oscillation shaking table;After polylactic acid is completely dissolved, after Continuous stirring and emulsifying 20-40min, obtains uniform white emulsion;
B. Zein powder, starch, kieselguhr are added in remaining water, add glucose, aminoacid, glycerol, dodecane Base sodium sulfonate, after being uniformly dispersed, soaks 30-60min, obtains mixing suspension;
C. mixing suspension obtained by step b is mixed with white emulsion obtained by step a, after stirring, adds magnesium chloride, urine Element, ammonium nitrate, mix homogeneously obtain final product Plant antifreezer.
Kieselguhr doping Plant antifreezer of described a kind of insulation nutrition and preparation method thereof, it is characterised in which makes It is nebulization with method, Plant antifreezer is diluted 500-800 times and is sprayed on before cooling needs antifreeze plant leaf surface, flower, bud And Fruiting branches.
The invention has the beneficial effects as follows:Polylactic acid can form layer protecting film in plant surface, play that cold-resistant is antifreeze, subtract The effect of few transpiration dehydration, while the production process of polylactic acid is pollution-free, and product be able to can be made after degraded with biodegradation For vegetable fertilizer, the circulation in nature is realized;Zein powder is soaked in glucose, aminoacid, and by poly- breast The bonding effect of acid is attached on plant, not only can reach the effect of insulation, and wherein glucose, aminoacid can be dramatically increased The content of sugar, free amino acid in plant body is so as to increase the concentration of the activity and Cell sap of cytoplasma membrane ATP enzymes, right Cell has protective effect, effectively reduces impact of the freeze injury to plant;Cooperation with the addition of kieselguhr, starch etc., enhance the plant The viscosity of thing antifreezing agent.
Specific embodiment
With reference to embodiment, the specific embodiment of the present invention is further described.
Embodiment
The kieselguhr doping Plant antifreezer of a kind of insulation nutrition, it is characterised in that be by the raw material system of following weight portion Into:
Starch 3, polylactic acid 12, kieselguhr 4, sorbitan fatty ester 6, chloroform 15, water 35, Zein powder 10, nitre Sour ammonium 2, glucose 3, aminoacid 4, glycerol 6, dodecyl sodium sulfate 2, magnesium chloride 5, carbamide 5.
A kind of kieselguhr doping Plant antifreezer and preparation method thereof of described insulation nutrition, it is characterised in that be by Following steps are made:
A. sorbitan fatty ester is dissolved in chloroform, under homogenous disperse machine high-speed stirred, is added thereto to 8- 15 parts of water, after emulsifying 10-30min, adds polylactic acid, is placed in the dissolving of constant temperature oscillation shaking table;After polylactic acid is completely dissolved, after Continuous stirring and emulsifying 20-40min, obtains uniform white emulsion;
B. Zein powder, starch, kieselguhr are added in remaining water, add glucose, aminoacid, glycerol, dodecane Base sodium sulfonate, after being uniformly dispersed, soaks 30-60min, obtains mixing suspension;
C. mixing suspension obtained by step b is mixed with white emulsion obtained by step a, after stirring, adds magnesium chloride, urine Element, ammonium nitrate, mix homogeneously obtain final product Plant antifreezer.
Kieselguhr doping Plant antifreezer of described a kind of insulation nutrition and preparation method thereof, it is characterised in which makes It is nebulization with method, Plant antifreezer is diluted 500-800 times and is sprayed on before cooling needs antifreeze plant leaf surface, flower, bud And Fruiting branches.
The present invention technical parameter be:Antifreezing effect >=7 day.

Claims (3)

1. it is a kind of insulation nutrition kieselguhr doping Plant antifreezer, it is characterised in that be made up of the raw material of following weight portion:
Starch 2-3, polylactic acid 7-12, kieselguhr 2-4, sorbitan fatty ester 3-6, chloroform 8-15, water 25-35, it is beautiful Rice gluten powder 5-10, ammonium nitrate 1-2, glucose 1-3, aminoacid 2-4, glycerol 4-6, dodecyl sodium sulfate 1-2, magnesium chloride 2- 5, carbamide 2-5.
2. kieselguhr doping Plant antifreezer and preparation method thereof of a kind of insulation nutrition according to claim 1, which is special Levy and be, be made up of following steps:
A. sorbitan fatty ester is dissolved in chloroform, under homogenous disperse machine high-speed stirred, is added thereto to 8- 15 parts of water, after emulsifying 10-30min, adds polylactic acid, is placed in the dissolving of constant temperature oscillation shaking table;After polylactic acid is completely dissolved, after Continuous stirring and emulsifying 20-40min, obtains uniform white emulsion;
B. Zein powder, starch, kieselguhr are added in remaining water, add glucose, aminoacid, glycerol, dodecane Base sodium sulfonate, after being uniformly dispersed, soaks 30-60min, obtains mixing suspension;
C. mixing suspension obtained by step b is mixed with white emulsion obtained by step a, after stirring, adds magnesium chloride, urine Element, ammonium nitrate, mix homogeneously obtain final product Plant antifreezer.
3. kieselguhr doping Plant antifreezer and preparation method thereof of a kind of insulation nutrition according to claim 2, which is special Levy and be, its using method is nebulization, Plant antifreezer is diluted 500-800 times and is sprayed on before cooling needs antifreeze plant Blade face, flower, bud and Fruiting branches.
CN201611027024.1A 2016-11-22 2016-11-22 Thermal insulation nutritional diatomite doped plant anti-freezing agent and preparation method thereof Pending CN106561655A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611027024.1A CN106561655A (en) 2016-11-22 2016-11-22 Thermal insulation nutritional diatomite doped plant anti-freezing agent and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611027024.1A CN106561655A (en) 2016-11-22 2016-11-22 Thermal insulation nutritional diatomite doped plant anti-freezing agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106561655A true CN106561655A (en) 2017-04-19

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107018992A (en) * 2017-05-12 2017-08-08 和县正林苗木专业合作社 A kind of crops anti-icing fluid and preparation method
CN108668757A (en) * 2018-05-30 2018-10-19 贵州卡农云服务有限公司 A kind of Winter protection method of Queensland nut

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103922840A (en) * 2014-04-04 2014-07-16 李美凤 Compound plant anti-freezing agent and preparation method thereof

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103922840A (en) * 2014-04-04 2014-07-16 李美凤 Compound plant anti-freezing agent and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107018992A (en) * 2017-05-12 2017-08-08 和县正林苗木专业合作社 A kind of crops anti-icing fluid and preparation method
CN108668757A (en) * 2018-05-30 2018-10-19 贵州卡农云服务有限公司 A kind of Winter protection method of Queensland nut

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Application publication date: 20170419