CN106729068A - A kind of external application energy gauging that can be helped for sleep and preparation method thereof - Google Patents
A kind of external application energy gauging that can be helped for sleep and preparation method thereof Download PDFInfo
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Abstract
The invention provides a kind of external application energy gauging that can be helped for sleep and preparation method thereof, the external application energy gauging includes that the raw material of volumes below part is made:7.5 8 parts of 9.5 9.9 parts of 50 51 parts of Lavender, cus-cus essential oil or Basil Essential, 11 11.4 parts of valerian essential oil, oil of Cymbopogon winterianus or Cananga odorata quintessence oil, Chinese juniper another name for oil 13.5 14 parts and 6.7 7.3 parts of marjoram essential oil.The external application energy gauging has significant effect at aspects such as treatment insomnia, mood placating and pain of alleviation;The preparation method has that process is simple, easy-operating advantage.
Description
Technical field
The invention belongs to health product technology field, and in particular to a kind of external application energy gauging that can be helped for sleep and its preparation side
Method.
Background technology
Sleep be life necessary to process, be body restore, integrate and consolidating memory important step, be that health can not
The important component for lacking.But influence the factor of ortho more and more in actual life, such as noise or illumination ring
Pain that border, travelling at a high speed across zone, daytime and the replacing worked at night and some diseases cause etc..Sleep insufficiency
Can not only influence brain right mind, influence normal body to develop, can also trigger various diseases.
The method for the treatment of insomnia at present is mainly to be taken artificial synthesized calmness and hypnotic drug or is treated using physics
Method.Although calm and hypnotic drug can make one to enter sleep state, after wakeing up it is possible that it is dizzy, weak, sleepy and/
Or the phenomenon such as lassitude;Although physical therapy side effect is smaller, inconvenient operation, and relatively costly.
The content of the invention
In order to solve the above mentioned problem of prior art presence, the invention provides a kind of external application energy gauging that can be helped for sleep
And preparation method thereof, the external application energy gauging has significant effect at aspects such as treatment insomnia, mood placating and pain of alleviation.
Additionally, it is raw material that the external application energy gauging uses plants essential oil, with green, safety and compared to the secondary work of calm and sleeping class medicine
With small advantage.
The technical solution adopted in the present invention is:A kind of external application energy gauging that can be helped for sleep, including volumes below part
Raw material is made:Lavender 50-51 parts, cus-cus essential oil or Basil Essential 9.5-9.9 parts, 11-11.4 parts of valerian essential oil, perfume
Thatch essential oil or 6.7-7.3 parts of Cananga odorata quintessence oil 7.5-8 parts, 13.5-14 parts of Chinese juniper another name for oil and marjoram essential oil.
Preferably, the raw material of the external application energy gauging, including volumes below part is made:50 parts of Lavender, cus-cus
Essential oil or 8 parts of 9.5 parts of Basil Essential, 11 parts of valerian essential oil, oil of Cymbopogon winterianus or Cananga odorata quintessence oil, 14 parts of Chinese juniper another name for oil and marjoram essence
7.3 parts of oil.
Preferably, the raw material of the external application energy gauging, including volumes below part is made:51 parts of Lavender, cus-cus
Essential oil or 7.5 parts of 9.9 parts of Basil Essential, 11.4 parts of valerian essential oil, oil of Cymbopogon winterianus or Cananga odorata quintessence oil, Chinese juniper another name for oil 13.5 parts and horse
6.7 parts of Yu Lan essential oils.
In order that effect of the external application energy gauging is more notable, preferred technical scheme is, the external application energy gauging, including
The raw material of volumes below part is made:50.5 parts of Lavender, cus-cus essential oil or 9.7 parts of Basil Essential, valerian essential oil 11.2
7.8 parts of part, oil of Cymbopogon winterianus or Cananga odorata quintessence oil, Chinese juniper another name for oil 13.8 parts and 7 parts of marjoram essential oil.
It should be noted that the cus-cus essential oil and Basil Essential, the effect for playing is close, and other essential oils collocation
Also close, the two can be replaced mutually;
Similarly, the Chinese juniper another name for oil and marjoram essential oil can also play close effect.
To ensure effect and purity of Lavender, in the present invention, the Lavender is made of following methods:
A, by lavender flower freeze-drying after, crush and cross 80-200 mesh sieves, obtain distillating material;
B, distillation treatment is carried out to distillating material, the steam pressure in still-process is 0.1-0.2MPa, and temperature is 120-
140 DEG C, distillation time is 0.5-1.5h, obtains distillate;
C, distillate is carried out into water-oil separating, take upper oil phase;
D, upper oil phase is carried out into revolving treatment, isolate dulcet grease, and using anhydrous sodium sulfate to described
Dulcet grease is dried, and obtains the Lavender.
The Lavender obtained using the above method, with purity is high, the significant advantage of effect.
To improve the recovery rate of Lavender, preferred technical scheme is, in stepb, after the completion of distillation, by residue
Bottoms add water and carry out ultrasonic wave or Microwave Extraction, and during the extract solution that will be obtained adds the distillate.Namely
Say, bottoms are extracted again one time, and the efficiency extracted is lifted using ultrasonic wave or microwave, clothing is smoked so as to improve
The utilization rate of the showy flowers of herbaceous plants piece.
Further, in stepb, bottoms and the mass ratio of addition water are 1:4-6, Extracting temperature is 80-90
DEG C, extraction time is 1-3h.
To ensure the effect of freeze-drying, in step A, by lavender flower subzero 25 DEG C in subzero 20-, vacuum is
Freeze-drying 4-6 hours under 0.06-0.08MPa, 80-200 mesh sieves are crushed and crossed after freeze-drying, obtain distillating material.
The Lavender higher to obtain purity, preferred technical scheme is, in step D, vacuum during revolving is
0.07-0.08MPa, temperature is 30-40 DEG C.
Present invention also offers a kind of preparation method of the external application energy gauging, each raw material is well mixed, you can obtain
The external application energy gauging.
For ease of understanding the present invention, raw material of the present invention is analyzed below:
Lavender can be purified, pacify soul, mitigate angry and used-up sensation, and making one can be with even-tempered and good-humoured
Ground is to life.
Cus-cus essential oil can mosquito repellent catch up with fly, antipruritic antibacterial, while can centre of equilibrium nerve, sedation effect is good, can
Allow people's spirit and QI cleaning, the diseases such as big pressure, anxiety, insomnia and worry can be improved.
Basil Essential can relieve pain, ease pain, and can improve dysmenorrhoea;Gastrointestinal disease can be treated, such as abdominal distension, constipation, pregnant woman dislikes
The heart;Being capable of anti-spasm, sterilization;Can stimulate circulation;Simultaneously have refresh oneself, set the mind at rest, anti-depression, treatment headache and partially
Effect of headache;Neural fatigue and pressure can be alleviated, mood, dispelling fatigue is rouse oneself, loosen nerve.
Valerian essential oil can resist spasm, promote lymphatic system toxin expelling;Can mitigate pain, dispelling fatigue, loosen nerve,
Depressurize and sleeping.
Oil of Cymbopogon winterianus can mitigate headache, antimigraine and neuralgia;Weak or patient body is can assist in take good care of;Can
The psychology for providing infant's safety is consoled;Mood can be purified and improved, the depressed mood of solution is expressed.
Cananga odorata quintessence oil can balance hormone, reduce blood pressure, anti-spasm, chest enlarge, hair care;Chronic ache can be alleviated;Energy
Enough treatment apositia, be short of breath, palpitaition, insomnia, the symptom such as nervous and melancholy.
There is Chinese juniper another name for oil cooling blood and hemostasis, wind-dispelling to manage wet, refrigerant convergence, profit blood vessels, nourish strong, intelligence development of allaying excitement, beneficial blood
The effectiveness such as hidroschesis and moistening dryness for relaxing bowels.
Marjoram essential oil can adjust the menstrual cycle, mitigate dysmenorrhoea;Myalgia can be alleviated, improved varication, promoted
Enter blood circulation, reduce hypertension;The anxiety that can releive and pressure, reinforcing soul and warm mood etc..
The compatibility principle of the external application energy gauging is:Lavender collocation vetivert or Basil Essential can effectively pacify
Comfort mood, dispelling fatigue and mitigate effect of pain, Cananga odorata quintessence oil or oil of Cymbopogon winterianus collocation marjoram essential oil can be played and more had
The adjustment blood pressure of effect, pain of alleviation, the effect of promotion sleep, valerian essential oil and the oil collocation of Chinese juniper another name for can loosen nerve, depressurize
And it is sleeping:Various essential oils are reasonably combined, not only significantly improve respective effect, while also acting independent or a part of component
Irrealizable effect when sharing, has significant effect at aspects such as treatment insomnia, mood placating and pain of alleviation.
Beneficial effects of the present invention are:
1st, the invention provides a kind of external application energy gauging that can be helped for sleep, the external application energy gauging is in treatment insomnia, peace
The aspects such as mood and pain of alleviation are comforted with significant effect.Additionally, it is raw material that the external application energy gauging uses plants essential oil, tool
Have the advantages that green, safe and small compared to calm and sleeping class drug side-effect.
2nd, present invention also offers a kind of preparation method of the external application energy gauging, the preparation method is simple to operation,
Each raw material is well mixed and can obtain the external application energy gauging, obtained external application energy gauging low cost can be by most people
Group receives.
Specific embodiment
With reference to embodiment, present disclosure is further illustrated.It should be appreciated that implementation of the invention is not limited to
In the following examples, any formal accommodation and/or change made to the present invention fall within the scope of the present invention.
In the present invention, if not refering in particular to, all of part, percentage are unit of weight, and all of equipment and raw material etc. are
It is commercially available or the industry is conventional.Method in following embodiments, unless otherwise instructed, is the routine of this area
Method.
Embodiment 1
A kind of external application energy gauging that can be helped for sleep, including the raw material of volumes below is made:Lavender 50mL, vertivazulene
Careless essential oil 9.5mL, valerian essential oil 11mL, Cananga odorata quintessence oil 8mL, Chinese juniper another name for oil 13.5mL and marjoram essential oil 7.3mL.
Wherein, the Lavender is made of following methods:
A, by lavender flower at subzero 20 DEG C, vacuum is freeze-drying 4 hours, powder after freeze-drying under 0.08MPa
Broken and 200 mesh sieves excessively, obtain distillating material;
B, distillation treatment is carried out to distillating material, the steam pressure in still-process is 0.1MPa, temperature is 140 DEG C, is steamed
The time is evaporated for 0.5h, obtains distillate;After the completion of distillation, remaining bottoms are added water carries out ultrasonic wave or microwave is carried
Take, bottoms are 1 with the mass ratio of addition water:6, Extracting temperature is 80 DEG C, and extraction time is 3h, obtains extract solution, and
The extract solution that will be obtained is added in the distillate;
C, distillate is carried out into water-oil separating, take upper oil phase;
D, upper oil phase is carried out into revolving treatment, vacuum during revolving is 0.07MPa, temperature is 40 DEG C, has been isolated
The grease of fragrance, and the dulcet grease is dried using anhydrous sodium sulfate, obtain the Lavender.
The preparation method of the external application energy gauging:Each raw material is well mixed, you can obtain the external application energy gauging.
Embodiment 2
A kind of external application energy gauging that can be helped for sleep, including the raw material of volumes below is made:Lavender 51mL, vertivazulene
Careless essential oil 9.9mL, valerian essential oil 11.4mL, Cananga odorata quintessence oil 7.5mL, Chinese juniper another name for oil 14mL and marjoram essential oil 6.7mL.
Wherein, the Lavender is made of following methods:
A, by lavender flower at subzero 25 DEG C, vacuum is freeze-drying 6 hours, powder after freeze-drying under 0.06MPa
Broken and 80 mesh sieves excessively, obtain distillating material;
B, distillation treatment is carried out to distillating material, the steam pressure in still-process is 0.2MPa, temperature is 120 DEG C, is steamed
The time is evaporated for 1.5h, obtains distillate;After the completion of distillation, remaining bottoms are added water carries out ultrasonic wave or microwave is carried
Take, bottoms are 1 with the mass ratio of addition water:4, Extracting temperature is 90 DEG C, and extraction time is 1h, obtains extract solution, and
The extract solution that will be obtained is added in the distillate;
C, distillate is carried out into water-oil separating, take upper oil phase;
D, upper oil phase is carried out into revolving treatment, vacuum during revolving is 0.08MPa, temperature is 30 DEG C, has been isolated
The grease of fragrance, and the dulcet grease is dried using anhydrous sodium sulfate, obtain the Lavender.
The preparation method of the external application energy gauging:Each raw material is well mixed, you can obtain the external application energy gauging.
Embodiment 3
A kind of external application energy gauging that can be helped for sleep, including the raw material of volumes below is made:Lavender 50.5mL, sieve
Strangle essential oil 9.9mL, valerian essential oil 11.3mL, oil of Cymbopogon winterianus 7.6mL, Chinese juniper another name for oil 13.5mL and marjoram essential oil 7.3mL.
Wherein, the Lavender is made of following methods:
A, by lavender flower subzero 20, vacuum is freeze-drying 5 hours under 0.08MPa, is crushed after freeze-drying
And 160 mesh sieves are crossed, obtain distillating material;
B, distillation treatment is carried out to distillating material, the steam pressure in still-process is 0.15MPa, temperature is 140 DEG C, is steamed
The time is evaporated for 0.5h, obtains distillate;After the completion of distillation, remaining bottoms are added water carries out ultrasonic wave or microwave is carried
Take, bottoms are 1 with the mass ratio of addition water:6, Extracting temperature is 90 DEG C, and extraction time is 1.5h, obtains extract solution,
And in the extract solution addition distillate that will be obtained;
C, distillate is carried out into water-oil separating, take upper oil phase;
D, upper oil phase is carried out into revolving treatment, vacuum during revolving is 0.08MPa, temperature is 37 DEG C, has been isolated
The grease of fragrance, and the dulcet grease is dried using anhydrous sodium sulfate, obtain the Lavender.
The preparation method of the external application energy gauging:Each raw material is well mixed, you can obtain the external application energy gauging.
Embodiment 4
A kind of external application energy gauging that can be helped for sleep, including the raw material of volumes below is made:Lavender 51mL, sweet basil
Essential oil 9.5mL, valerian essential oil 11.3mL, oil of Cymbopogon winterianus 8mL, Chinese juniper another name for oil 13.7mL and marjoram essential oil 7.3mL.
Wherein, the Lavender is made of following methods:
A, by lavender flower at subzero 25 DEG C, vacuum is freeze-drying 4 hours, powder after freeze-drying under 0.07MPa
Broken and 200 mesh sieves excessively, obtain distillating material;
B, distillation treatment is carried out to distillating material, the steam pressure in still-process is 0.1MPa, temperature is 130 DEG C, is steamed
The time is evaporated for 1h, obtains distillate;After the completion of distillation, remaining bottoms are added water carries out ultrasonic wave or Microwave Extraction,
Bottoms are 1 with the mass ratio of addition water:4, Extracting temperature is 80 DEG C, and extraction time is 2.5h, obtains extract solution, and will
The extract solution for obtaining is added in the distillate;
C, distillate is carried out into water-oil separating, take upper oil phase;
D, upper oil phase is carried out into revolving treatment, vacuum during revolving is 0.07MPa, temperature is 35 DEG C, has been isolated
The grease of fragrance, and the dulcet grease is dried using anhydrous sodium sulfate, obtain the Lavender.
The preparation method of the external application energy gauging:Each raw material is well mixed, you can obtain the external application energy gauging.
Embodiment 5
A kind of external application energy gauging that can be helped for sleep, including the raw material of volumes below is made:Lavender 50.5mL, sieve
Strangle essential oil 9.7mL, valerian essential oil 11.2mL, Cananga odorata quintessence oil 7.8mL, Chinese juniper another name for oil 13.8mL and marjoram essential oil 7mL.
Wherein, the Lavender is made of following methods:
A, by lavender flower at subzero 22 DEG C, vacuum is freeze-drying 5 hours, powder after freeze-drying under 0.07MPa
Broken and 140 mesh sieves excessively, obtain distillating material;
B, distillation treatment is carried out to distillating material, the steam pressure in still-process is 0.15MPa, temperature is 130 DEG C, is steamed
The time is evaporated for 1h, obtains distillate;After the completion of distillation, remaining bottoms are added water carries out ultrasonic wave or Microwave Extraction,
Bottoms are 1 with the mass ratio of addition water:5, Extracting temperature is 85 DEG C, and extraction time is 2h, obtains extract solution, and incite somebody to action
To extract solution add the distillate;
C, distillate is carried out into water-oil separating, take upper oil phase;
D, upper oil phase is carried out into revolving treatment, vacuum during revolving is 0.075MPa, temperature is 35 DEG C, has been isolated
The grease of fragrance, and the dulcet grease is dried using anhydrous sodium sulfate, obtain the Lavender.
The preparation method of the external application energy gauging:Each raw material is well mixed, you can obtain the external application energy gauging.
Embodiment 6
In order to prove that the external application energy gauging for helping for sleep, to the therapeutic effect having a sleepless night, is made using the embodiment of the present invention 5
Standby external application energy gauging, has carried out the following test of pesticide effectiveness.Subject Population is divided into four groups, A groups according to sex and age:Female
Property, 30-49 Sui;B groups:Women, 50-70 Sui;C groups:Male, 30-49 Sui;D groups:Male, 50-70 Sui;Every group of 100 people.Experiment
Sleep is first 30 minutes daily for person, and energy essential oil 0.2ml uniform applications obtained in Example 5 are after temple, ear-lobe, ear or neck
The positions such as portion.It is continuous to use 20 days, sleep improvement situation is counted, statistics is as shown in table 1.
Table 1 is to different crowd sleep improvement situation statistical form
Group | Experiment number | Improvement number | Improvement ratio |
A groups | 100 | 93 | 93% |
B groups | 100 | 90 | 90% |
C groups | 100 | 97 | 97% |
D groups | 100 | 91 | 91% |
Statistics shows that being slept using the crowd more than 90 percent of the external application energy gauging is improved, additionally,
Crowd's sleep improvement rate of 30-49 Sui, the crowd's sleep improvement rate higher than 50-70 Sui.
Model case:
1st, Zhang, man, 60 years old, usually difficulty falling asleep, dreaming often and waking easily had difficulty in going to sleep after waking up, vexed irritability, with it is forgetful,
Nervous, belly turgor, abundant expectoration and the symptom such as be hard and dry.The external application energy gauging prepared using the present embodiment 5, sleeps first 30 points daily
Clock smears 0.2ml after temple, ear-lobe, ear or the position such as neck, and continuous to use 20 days, sleep quality has clear improvement, respectively
Symptom has mitigated, while day person, memory is significantly improved.
2nd, Zhang, female, 58 years old, while with anxiety, depression.The external application for helping for sleep prepared using the present embodiment 3
Can gauging, sleep smear within first 30 minutes 0.2ml after temple, ear-lobe, ear or the position such as neck daily, it is continuous using after 10 days,
The patient sleeps are obviously improved, and depression also has larger alleviation, has no adverse reaction.
3rd, Wu, female, 36 years old, because residence is near high-speed railway rail, night was often waken up by train sound, is difficult to again after waking up
Fall asleep, while with mood agitation and Anemia.The external application energy gauging for helping for sleep prepared using the present embodiment 5, daily
Sleep and smear within first 30 minutes 0.2ml after temple, ear-lobe, ear or the position such as neck, continuous using after 25 days, its sleep quality is bright
Aobvious to improve, mood is irritated and Anemia disappears, without other adverse reactions.
4th, Liu, female, 30 years old, work taken up needed daytime and night-time shifts, and biological clock is chaotic, often insomnia.Use
The present embodiment 5 prepare the external application energy gauging for helping for sleep, sleep daily first 30 minutes smear 0.2ml after temple, ear-lobe, ear
Or the position such as neck, continuous using after 20 days, insomnia is eased.
5th, Sun, man, 37 years old, difficulty falling asleep, dreaming often and waking easily, mood agitation has difficulty in going to sleep after waking up, and is made using the present embodiment 5
The standby external application energy gauging for helping for sleep, sleeps smear within first 30 minutes 0.2ml after temple, ear-lobe, ear or the portion such as neck daily
Position, continuous using after 15 days, sleep is returned to normal.
It should be noted last that, the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although ginseng
The present invention is described in detail according to preferred embodiment, should be understood that and be the foregoing is only specific implementation of the invention
Mode, the protection domain being not intended to limit the present invention, it is all within the spirit and principles in the present invention, done any repair
Change, equivalent, improvement etc., should be included within the scope of the present invention.
Claims (10)
1. a kind of external application energy gauging that can be helped for sleep, it is characterised in that the raw material including volumes below part is made:Lavender essence
Oily 50-51 parts, cus-cus essential oil or Basil Essential 9.5-9.9 parts, 11-11.4 parts of valerian essential oil, oil of Cymbopogon winterianus or Cananga odorata quintessence oil
6.7-7.3 parts of 7.5-8 parts, 13.5-14 parts of Chinese juniper another name for oil and marjoram essential oil.
2. external application energy gauging according to claim 1, it is characterised in that the raw material including volumes below part is made:Smoke clothing
8 parts of 9.5 parts of 50 parts of careless essential oil, cus-cus essential oil or Basil Essential, 11 parts of valerian essential oil, oil of Cymbopogon winterianus or Cananga odorata quintessence oil, Chinese juniper wood
7.3 parts of 14 parts of essential oil and marjoram essential oil.
3. external application energy gauging according to claim 1, it is characterised in that the raw material including volumes below part is made:Smoke clothing
7.5 parts of 9.9 parts of 51 parts of careless essential oil, cus-cus essential oil or Basil Essential, 11.4 parts of valerian essential oil, oil of Cymbopogon winterianus or Cananga odorata quintessence oil,
6.7 parts of 13.5 parts of Chinese juniper another name for oil and marjoram essential oil.
4. external application energy gauging according to claim 1, it is characterised in that the raw material including volumes below part is made:Smoke clothing
9.7 parts of 50.5 parts of careless essential oil, cus-cus essential oil or Basil Essential, 11.2 parts of valerian essential oil, oil of Cymbopogon winterianus or Cananga odorata quintessence oil 7.8
Part, Chinese juniper another name for oil 13.8 parts and 7 parts of marjoram essential oil.
5. external application energy gauging according to claim 1, it is characterised in that the Lavender uses following methods system
Into:
A, by lavender flower freeze-drying after, crush and cross 80-200 mesh sieves, obtain distillating material;
B, distillation treatment is carried out to distillating material, the steam pressure in still-process is 0.1-0.2MPa, and temperature is 120-140
DEG C, distillation time is 0.5-1.5h, obtains distillate;
C, distillate is carried out into water-oil separating, take upper oil phase;
D, upper oil phase is carried out into revolving treatment, isolate dulcet grease, and have perfume (or spice) to described using anhydrous sodium sulfate
The grease of taste is dried, and obtains the Lavender.
6. external application energy gauging according to claim 5, it is characterised in that in stepb, after the completion of distillation, will be remaining
Bottoms add water carries out ultrasonic wave or Microwave Extraction, and in the extract solution addition distillate that will be obtained.
7. external application energy gauging according to claim 6, it is characterised in that in stepb, bottoms with add water
Mass ratio is 1:4-6, Extracting temperature is 80-90 DEG C, and extraction time is 1-3h.
8. external application energy gauging according to claim 5, it is characterised in that in step A, by lavender flower in subzero 20-
Subzero 25 DEG C, vacuum is freeze-drying 4-6 hours under 0.06-0.08MPa, 80-200 mesh sieves to be crushed and crossed after freeze-drying,
Obtain distillating material.
9. external application energy gauging according to claim 5, it is characterised in that in step D, vacuum during revolving is 0.07-
0.08MPa, temperature is 30-40 DEG C.
10. the preparation method of any external application energy gaugings of claim 1-4, it is characterised in that be well mixed each raw material, i.e.,
Can obtain the external application energy gauging.
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109006880A (en) * | 2018-08-21 | 2018-12-18 | 湖州稻草娃生物科技有限公司 | A kind of culicifuge promoting sleep |
CN109316462A (en) * | 2018-09-06 | 2019-02-12 | 温州医科大学附属第医院 | A kind of pillow Chinese materia medica preparation pharmaceutical carrier and preparation method thereof |
CN109646670A (en) * | 2019-01-30 | 2019-04-19 | 刘奇 | Bee venom essential oil |
WO2019175550A1 (en) * | 2018-03-12 | 2019-09-19 | Unex Designs Ltd | Calming composition |
CN110354187A (en) * | 2019-08-02 | 2019-10-22 | 汉萃(天津)生物技术有限公司 | A kind of plant extract composition improving sleep |
CN110613805A (en) * | 2019-10-18 | 2019-12-27 | 成都瑞事吉事商贸有限公司 | Compound essential oil with calming and sleep-aiding effects and preparation method thereof |
CN111388572A (en) * | 2020-04-13 | 2020-07-10 | 北京中医药大学 | Compound essential oil and preparation method, preparation and application thereof |
CN112891469A (en) * | 2019-12-04 | 2021-06-04 | 杨春辉 | Compound essential oil for improving sleep quality |
CN113082171A (en) * | 2021-04-23 | 2021-07-09 | 花安堂生物科技集团有限公司 | Composition and sleep-aiding product containing black spruce extract |
CN113509528A (en) * | 2021-04-23 | 2021-10-19 | 花安堂生物科技集团有限公司 | Composition and sleep-aiding product containing magnolia sieboldii extract |
-
2016
- 2016-12-23 CN CN201611206951.XA patent/CN106729068A/en active Pending
Non-Patent Citations (3)
Title |
---|
人面桃花旗舰店: "桧木精油——阿里山的神木传奇", 《HTTPS://WWW.MEIPIAN.CN/7VX2AAE》 * |
林波: "《初级芳香保健师培训教程》", 30 June 2011, 中国物资出版社 * |
精油之恋网: "老年人治疗失眠的精油配方", 《HTTP://WWW.JY94.COM/NEWS/87_1248.HTML》 * |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2019175550A1 (en) * | 2018-03-12 | 2019-09-19 | Unex Designs Ltd | Calming composition |
CN109006880A (en) * | 2018-08-21 | 2018-12-18 | 湖州稻草娃生物科技有限公司 | A kind of culicifuge promoting sleep |
CN109316462A (en) * | 2018-09-06 | 2019-02-12 | 温州医科大学附属第医院 | A kind of pillow Chinese materia medica preparation pharmaceutical carrier and preparation method thereof |
CN109646670A (en) * | 2019-01-30 | 2019-04-19 | 刘奇 | Bee venom essential oil |
CN110354187A (en) * | 2019-08-02 | 2019-10-22 | 汉萃(天津)生物技术有限公司 | A kind of plant extract composition improving sleep |
CN110613805A (en) * | 2019-10-18 | 2019-12-27 | 成都瑞事吉事商贸有限公司 | Compound essential oil with calming and sleep-aiding effects and preparation method thereof |
CN112891469A (en) * | 2019-12-04 | 2021-06-04 | 杨春辉 | Compound essential oil for improving sleep quality |
CN111388572A (en) * | 2020-04-13 | 2020-07-10 | 北京中医药大学 | Compound essential oil and preparation method, preparation and application thereof |
CN113082171A (en) * | 2021-04-23 | 2021-07-09 | 花安堂生物科技集团有限公司 | Composition and sleep-aiding product containing black spruce extract |
CN113509528A (en) * | 2021-04-23 | 2021-10-19 | 花安堂生物科技集团有限公司 | Composition and sleep-aiding product containing magnolia sieboldii extract |
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Application publication date: 20170531 |