CN106727906A - A kind of concocting method of bark of ash medicine materical crude slice - Google Patents
A kind of concocting method of bark of ash medicine materical crude slice Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/51—Gentianaceae (Gentian family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/22—Anacardiaceae (Sumac family), e.g. smoketree, sumac or poison oak
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/51—Gentianaceae (Gentian family)
- A61K36/515—Gentiana
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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Abstract
The invention discloses a kind of concocting method of bark of ash medicine materical crude slice, belong to Chinese medicine preparation technical field.Because bark of ash is extremely bitter, processed using art methods, although bark of ash bitter taste weakens, but gentiopicroside in different morphological leaf is substantially reduced.In order to gentiopicroside in different morphological is reduced in solving the problems, such as concocting process, this root of hair is according to bark of ash own characteristic, the concocting method of offer, not only so that the content of active ingredient gentiamarin is significantly improved in bark of ash, and the content of flavone compound is increased simultaneously, enhance bark of ash anti-inflammatory, antibacterial, antalgic and sedative, liver protecting, oxidation resistant effect, and weaken significantly by the bark of ash bitter taste that concocting method of the present invention is processed, also give out the delicate fragrance of valerian.
Description
Technical field
The invention belongs to Chinese medicine preparation technical field, specifically a kind of concocting method of bark of ash medicine materical crude slice.
Background technology
Bark of ash is the root of gentianaceae plant bark of ash Gent iana m acrophy l laPall..Its taste is pungent, hardship, it is mild-natured,
Return stomach, liver, gallbladder channel, the effects such as with wind-damp dispelling, stopping numbness pain, reducing the asthenic fever, clearing away damp-heat, be conventionally used to arthralgia pain due to rheumatism, muscle arteries and veins contraction,
The illness such as joint is ached, apoplexy hands and feet caused by paralysis and osteopyrexia and fever, infantile malnutrition generates heat, jaundice with damp-heat pathogen.Modern study shows, bark of ash
With the effect such as anti-inflammatory, analgesia, calm, antipyretic and liver protection, central nervous system and immune system can be adjusted, be widely used in rheumatism
The treatment of disease, cardiovascular and cerebrovascular disease, the nervous system disease, anal and intestinal disease and skin disease etc..
Research finds that its principle active component of bark of ash is gentiamarin.Gentiamarin is secoiridoid methods of glycosides,
Due to being influenceed by ethylidene ether structure, the amount in medicinal material can be influenceed by different Processing methods conditions.Glycoside in Chinese medicine into
Point under the uniform temperature and damp condition can by cell in corresponding enzyme decompose, so containing aminoglycoside frequently with frying, steam, dry
The method being exposed to the sun suppress or destructive enzyme activity, be used to prevent the reduction of active principle in medicinal material containing glycoside.Bark of ash tradition
Concocting method have be exposed to the sun, dry in the shade, frying, wine fry.Number of patent application：2011100990879 disclose a kind of " bark of ash prepared slices of Chinese crude drugs
Preparation method " preparation method comprises the following steps：Washing, cover, dry in the shade, wash, infiltrate, cut into slices, dry, cool down and wrap
Fill, the method feature is：Simply, conveniently, and can greatly improve the drug effect of bark of ash, shorten preparation time, reduces cost,
But either traditional concocting method or concocting method disclosed in the patent do not occur it is related improve flavone compound and
The report of gentiopicroside in different morphological.
The content of the invention
It is an object of the invention in view of the shortcomings of the prior art, there is provided a kind of concocting method of bark of ash medicine materical crude slice.
In order to realize the purpose of the present invention, the present invention is realized by following technical method：
A kind of concocting method of bark of ash medicine materical crude slice, specifically includes following steps：
(1), after by fresh common smoketree branchlet and leaf, fresh day floral leaf of ancient India, fresh papaya leaf washing, 1-3 is compared according to weight:2-4:2-5 is mixed
Close, add the alcoholic strength of 1.5 times of its gross weight to smash rear juice extractor to pieces for 11 degree of beer and squeeze the juice, separate juice filter residue, obtain mixed juice
Liquid, filter residue are standby；Bark of ash raw medicinal herbs is taken, is cut into slices after washing, slice thickness is 3mm, and above-mentioned filter residue then is uniformly coated on into the Qin
Macrophylla is fitted into gauze bag behind surface, then gauze bag is put into the ceramic vessel for filling 10% glycerine, water proof heating 30min, so
Bark of ash thin slice is rinsed into 20-30s with 2-4 DEG C of cold water of temperature afterwards, bark of ash sheet surface moisture is blotted with blotting paper, then by bark of ash
Thin slice puts into vexed profit in the glass container of the mixing juice equipped with 0.8 times of its weight, in vexed profit to container in 30 DEG C of environment
Without mixing juice residual, dry naturally, it is standby；
(2), fresh bark of ash leaf, fresh Swertia patens leaf, fresh rough gentian leaf are smashed to pieces respectively, 1-4 is compared according to weight:3-6:After 5-8 mixing
1 times of alcoholic strength of its gross weight is added for 52 degree of white wine, small fire decocts 15min, filtering, the bark of ash after (1) filtrate and step are processed
Thin slice is by weight 1:Put into after 1.5 mixing in closed container, closed vexed profit to filtrate is sucked completely in 35 DEG C of environment,
Take out, dry naturally, obtain final product bark of ash medicine materical crude slice.
Papaya leaf is the leaf of Caricaceae plant papaya Carica papaya L..
Day floral leaf of ancient India is the leaf of malvaceae plant Buddhist smallpox Urena procumbens L. [U.sinuata L.].
Common smoketree branchlet and leaf is Anacardiaceae plant ash colourea smoketree Cotinus coggygria Scop.var.cinerea Engl.
With the branches and leaves of hair leaf smoke tree Cotinus coggygria Scop.pubescens Engl..
Swertia patens leaf leaf is gentianaceae plant two point Swertia patens leaf Swertia bimaculata (Sieb.et Zucc.)
The leaf of Hook.Thoms.ex.
Bark of ash leaf is the leaf of gentianaceae plant bark of ash Gent iana m acrophy l laPall..
Rough gentian leaf is the leaf of gentianaceae plant rough gentian Gentiana scabra Bunge.
The beneficial effects of the present invention are：The bark of ash obtained by concocting method of the invention not only increases flavonoids
The content of compound and gentiamarin, enhances bark of ash anti-inflammatory, antibacterial, antalgic and sedative, liver protecting, oxidation resistant effect, Er Qiejing
Processing is crossed, bark of ash bitter taste weakens significantly, also gives out the delicate fragrance of valerian.
Specific embodiment
Further describe the present invention by the following examples, it should be understood that these embodiments are only used for illustration
Purpose, is not limited to the present invention.
Embodiment 1
A kind of concocting method of bark of ash medicine materical crude slice, specifically includes following steps：
(1), after by fresh common smoketree branchlet and leaf, fresh day floral leaf of ancient India, fresh papaya leaf, washing, 1 is compared according to weight:2:2 mixing, add
The alcoholic strength of 1.5 times of its gross weight is smashed rear juice extractor to pieces and is squeezed the juice for 11 degree of beer, separates juice filter residue, must mix juice, filter residue
It is standby；Bark of ash raw medicinal herbs is taken, is cut into slices after washing, slice thickness is 3mm, after above-mentioned filter residue then is uniformly coated on into bark of ash surface
It is fitted into gauze bag, then gauze bag is put into the ceramic vessel for filling 10% glycerine, water proof heating 30min, then with temperature 2
Bark of ash thin slice is rinsed 20s by DEG C cold water, and bark of ash sheet surface moisture is blotted with blotting paper, is then put into bark of ash thin slice and is equipped with
Vexed profit in the glass container of the mixing juice of 0.8 times of its weight, without mixing juice residual in vexed profit to container in 30 DEG C of environment,
Naturally dry, it is standby；
(2), fresh bark of ash leaf, fresh Swertia patens leaf, fresh rough gentian leaf are smashed to pieces respectively, 1 is compared according to weight:3:It is added after 5 mixing
1 times of alcoholic strength of gross weight is 52 degree of white wine, and small fire decocts 15min, and filtering, the bark of ash thin slice after (1) filtrate is processed with step is pressed
Weight compares 1:Put into after 1.5 mixing in closed container, closed vexed profit is sucked completely to filtrate in 35 DEG C of environment, takes out,
Naturally dry, obtain final product bark of ash medicine materical crude slice.
Embodiment 2
A kind of concocting method of bark of ash medicine materical crude slice, specifically includes following steps：
(1), after by fresh common smoketree branchlet and leaf, fresh day floral leaf of ancient India, fresh papaya leaf washing, 3 are compared according to weight:3:4 mixing, add
The alcoholic strength of 1.5 times of its gross weight is smashed rear juice extractor to pieces and is squeezed the juice for 11 degree of beer, separates juice filter residue, must mix juice, filter residue
It is standby；Bark of ash raw medicinal herbs is taken, is cut into slices after washing, slice thickness is 3mm, after above-mentioned filter residue then is uniformly coated on into bark of ash surface
It is fitted into gauze bag, then gauze bag is put into the ceramic vessel for filling 10% glycerine, water proof heating 30min, then with temperature 4
Bark of ash thin slice is rinsed 30s by DEG C cold water, and bark of ash sheet surface moisture is blotted with blotting paper, is then put into bark of ash thin slice and is equipped with
Vexed profit in the glass container of the mixing juice of 0.8 times of its weight, without mixing juice residual in vexed profit to container in 30 DEG C of environment,
Naturally dry, it is standby；
(2), fresh bark of ash leaf, fresh Swertia patens leaf, fresh rough gentian leaf are smashed to pieces respectively, 2 are compared according to weight:3:It is added after 4 mixing
1 times of alcoholic strength of gross weight is 52 degree of white wine, and small fire decocts 15min, and filtering, the bark of ash thin slice after (1) filtrate is processed with step is pressed
Weight compares 1:Put into after 1.5 mixing in closed container, closed vexed profit is sucked completely to filtrate in 35 DEG C of environment, takes out,
Naturally dry, obtain final product bark of ash medicine materical crude slice.
Embodiment 3
A kind of concocting method of bark of ash medicine materical crude slice, specifically includes following steps：
(1), after by fresh common smoketree branchlet and leaf, fresh day floral leaf of ancient India, fresh papaya leaf washing, 3 are compared according to weight:4:5 mixing, add
The alcoholic strength of 1.5 times of its gross weight is smashed rear juice extractor to pieces and is squeezed the juice for 11 degree of beer, separates juice filter residue, must mix juice, filter residue
It is standby；Bark of ash raw medicinal herbs is taken, is cut into slices after washing, slice thickness is 3mm, after above-mentioned filter residue then is uniformly coated on into bark of ash surface
It is fitted into gauze bag, then gauze bag is put into the ceramic vessel for filling 10% glycerine, water proof heating 30min, then with temperature 3
Bark of ash thin slice is rinsed 25s by DEG C cold water, and bark of ash sheet surface moisture is blotted with blotting paper, is then put into bark of ash thin slice and is equipped with
Vexed profit in the glass container of the mixing juice of 0.8 times of its weight, without mixing juice residual in vexed profit to container in 30 DEG C of environment,
Naturally dry, it is standby；
(2), fresh bark of ash leaf, fresh Swertia patens leaf, fresh rough gentian leaf are smashed to pieces respectively, 3 are compared according to weight:5:It is added after 7 mixing
1 times of alcoholic strength of gross weight is 52 degree of white wine, and small fire decocts 15min, and filtering, the bark of ash thin slice after (1) filtrate is processed with step is pressed
Weight compares 1:Put into after 1.5 mixing in closed container, closed vexed profit is sucked completely to filtrate in 35 DEG C of environment, takes out,
Naturally dry, obtain final product bark of ash medicine materical crude slice.
Test example
The bark of ash raw medicinal herbs of 900g Tianshui cities product is taken, is cut into slices after washing, slice thickness is 3mm, experiment sets 9 treatment
Group, 3 test groups, numbering 1-3,6 control groups, numbering 4-9 divides equally to each treatment group the bark of ash thin slice after section, often
100g is organized, concrete operations are：
Test group 1：Bark of ash thin slice is processed according to the concocting method of embodiment 1.
Test group 2：Bark of ash thin slice is processed according to the concocting method of embodiment 2.
Test group 3：Bark of ash thin slice is processed according to the concocting method of embodiment 3.
Control group 4：(1) bark of ash thin slice is processed according to the step of embodiment 3 only.
Control group 5：(2) bark of ash thin slice is processed according to the step of embodiment 3 only.
Control group 6：Tradition is fried：Fried to surface color intensification with slow fire or moderate heat during bark of ash thin slice is put into hot pot
Control group 7：Traditional wine is fried：Bark of ash thin slice is braised through with yellow rice wine, per 10g medicinal materials yellow rice wine 10g, put in hot pot with text
Fire is fried to surface color and deepened.
Control group 8：Traditional wine is steamed：Bark of ash thin slice is mixed thoroughly with yellow rice wine, per 10g medicinal materials yellow rice wine 10g, heating in pot is put and is steamed
Thoroughly (10min), put after taking-up in baking oven in 100 DEG C of dryings.
Control group 9：Traditional milk steams：Bark of ash thin slice is mixed thoroughly with fresh milk, heating in pot is put and is steamed thoroughly (10min), taken out
After put in baking oven in 100 DEG C of dryings.
Assay method：The bark of ash that above-mentioned control group takes before 10g is processed and after processing respectively with every group of test group carries out total Huang
The measure of ketone compounds, gentiopicroside in different morphological, the assay method uses high performance liquid chromatography, and said determination method is this
The technology that art personnel should know；Measurement result is as shown in table 1.
Table 1
As shown in Table 1, compared with control group, the bark of ash flavone compound after the processing of test group 1-3 concocting methods
Content and gentiopicroside in different morphological increase before relatively processing, and other control groups 4-9 is by bark of ash flavonoid after processing
Thing content and gentiopicroside in different morphological decline, therefore it will be apparent that, concocting method of the invention enhances bark of ash anti-inflammatory, antibacterial, town
Pain calmness, liver protecting, oxidation resistant effect.
Claims (1)
1. a kind of concocting method of bark of ash medicine materical crude slice, it is characterised in that specifically include following steps：
(1), after by fresh common smoketree branchlet and leaf, fresh day floral leaf of ancient India, fresh papaya leaf washing, 1-3 is compared according to weight:2-4:2-5 mixes, plus
The alcoholic strength for entering 1.5 times of its gross weight is smashed rear juice extractor to pieces and is squeezed the juice for 11 degree of beer, separates juice filter residue, must mix juice, filter
Slag is standby；Bark of ash raw medicinal herbs is taken, is cut into slices after washing, slice thickness is 3mm, and above-mentioned filter residue then is uniformly coated on into bark of ash surface
It is fitted into gauze bag afterwards, then gauze bag is put into the ceramic vessel for filling 10% glycerine, water proof heating 30min, then with temperature
Bark of ash thin slice is rinsed 20-30s by 2-4 DEG C of cold water of degree, and bark of ash sheet surface moisture is blotted with blotting paper, then throws bark of ash thin slice
Enter the vexed profit in the glass container of the mixing juice equipped with 0.8 times of its weight, without mixing in vexed profit to container in 30 DEG C of environment
Juice is remained, and is dried naturally, standby；
(2), fresh bark of ash leaf, fresh Swertia patens leaf, fresh rough gentian leaf are smashed to pieces respectively, 1-4 is compared according to weight:3-6:Added after 5-8 mixing
1 times of alcoholic strength of its gross weight is 52 degree of white wine, and small fire decocts 15min, filtering, the bark of ash thin slice after (1) filtrate and step are processed
By weight 1:Put into after 1.5 mixing in closed container, closed vexed profit is sucked completely to filtrate in 35 DEG C of environment, takes
Go out, dry naturally, obtain final product bark of ash medicine materical crude slice.
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Application publication date: 20170531 |