CN106690325A - Walnut oil soft capsule with high oxidation resistance and preparation method of walnut oil soft capsule - Google Patents
Walnut oil soft capsule with high oxidation resistance and preparation method of walnut oil soft capsule Download PDFInfo
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- CN106690325A CN106690325A CN201611042630.0A CN201611042630A CN106690325A CN 106690325 A CN106690325 A CN 106690325A CN 201611042630 A CN201611042630 A CN 201611042630A CN 106690325 A CN106690325 A CN 106690325A
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Abstract
The invention discloses a walnut oil soft capsule with high oxidation resistance. The walnut oil soft capsule comprises a capsule shell and contents, wherein the capsule shell is made from the following raw material components in parts by weight: 40-60 parts of gelatin, 3-5 parts of vitamin E, 3-5 parts of vitamin C, 0.01-0.05 part of tween-80, 0.5-1 part of a plastifier, 5-10 parts of glucose and 40-60 parts of purified water; and the contents are made from the following raw material components in parts by weight: 70-90 parts of walnut oil, 5-10 parts of vitamin E, 3-5 parts of sesamol and 0.01-0.05 part of tween-80. The walnut oil soft capsule with high oxidation resistance provided by the invention has high oxidation resistance, and the problems that walnut oil health-care products are easy to have oxidative deterioration in the processing and storing course and the walnut oil health-care products are not suitable for being stored for a long term are solved. In addition, the invention further discloses a preparation method of the walnut oil soft capsule with high oxidation resistance.
Description
Technical field
The invention belongs to health products preparing technical field, and in particular to a kind of strong anti-oxidation walnut oil soft capsule and its system
Preparation Method.
Background technology
It is a kind of nutritious health food containing the trace element such as abundant calcium, phosphorus and mineral matter in walnut.Walnut
In contain substantial amounts of walnut oil, account for the half of walnut kernel gross mass, wherein the linoleic acid for containing, leukotrienes etc. for reduce people
Body blood fat, prevention coronary sclerosis have good effect, and with continuing to develop for modern science, the yield of walnut oil is year by year
Increase, wherein the walnut oil for the purpose of culinary art is most commonly seen.
Soft capsule be it is a kind of by liquid medicine or juicy fruit body medicine it is appropriately processed after be sealed in soft capsule material
Capsule.In recent years, in the market has engendered the soft capsule products of walnut oil, is convenient for carrying, transports and eats.Yet with
Containing abundant unrighted acid in walnut oil, make it that oxidation deterioration easily occur in processing and storage, it is unfavorable
In the long-term preservation of walnut oil health products, therefore, it is necessary to develop a kind of walnut oil soft capsule with strong anti-oxidation.
The content of the invention
A kind of strong anti-oxidation walnut oil soft capsule that the present invention is provided, with stronger inoxidizability, solves walnut
Easily there is oxidation deterioration in oil health care product, be unfavorable for that the long-term preservation of walnut oil health products is asked in processing and storage
Topic.
A kind of strong anti-oxidation walnut oil soft capsule that the present invention is provided, including capsule shells and content, the capsule shells
It is made up of the raw material components of following weight portion：Gelatin 40-60 parts, vitamin E 3-5 parts, vitamin C 3-5 parts, Tween-80
0.01-0.05 parts, plasticizer 0.5-1 parts, glucose 5-10 parts, purified water 40-60 parts；The wherein weight portion of gelatin and purified water
Ratio is 1:1；
The content is made up of the raw material components of following weight portion：Walnut oil 70-90 parts, vitamin E 5-10 parts, sesame
Numb phenol 3-5 parts, Tween-80 0.01-0.05 parts；
Wherein, the mass ratio of the capsule shells and content is 1:0.5~1.
Preferably, in above-mentioned strong anti-oxidation walnut oil soft capsule, the capsule shells by following weight portion raw material components
It is made：It is 50 parts of gelatin, 5 parts of vitamin E, 5 parts of vitamin C, 0.01 part of Tween-80,0.8 part of plasticizer, 8 parts of glucose, pure
Change 50 parts of water；
The content is made up of the raw material components of following weight portion：80 parts of walnut oil, 8 parts of vitamin E, sesamol 3
Part, 0.01 part of Tween-80；
Wherein, the mass ratio of the capsule shells and content is 1:1.
Preferably, the plasticizer is one kind of glycerine, xylitol or mannitol.
Present invention also offers a kind of preparation method of strong anti-oxidation walnut oil soft capsule, following steps are specifically included：
Step 1, weighs raw material
Step 1.1, weighs the raw material of following weight portion respectively：Gelatin 40-60 parts, vitamin E 3-5 parts, vitamin C 3-
5 parts, Tween-80 0.01-0.05 parts, plasticizer 0.5-1 parts, glucose 5-10 parts, purified water 40-60 parts；Wherein gelatin with it is pure
The weight ratio for changing water is 1:1；
Step 1.2, weighs the raw material of following weight portion respectively：Walnut oil 70-90 parts, vitamin E 5-10 parts, sesamol
3-5 parts, Tween-80 0.01-0.05 parts；
Wherein, the raw material gross mass ratio weighed in the raw material gross mass and step 1.2 that are weighed in step 1.1 is 1:0.5-
1；
Step 2, prepares one layer of glue
Step 2.1, the purified water mixing of the gelatin that will be weighed in step 1.1, plasticizer and half quality, is heated to 80-
90 DEG C, gelatin and plasticizer is all dissolved, obtain gelatin solution；Glucose and second half quality during step 1.1 is weighed
Purified water mixing, be heated to 80-90 DEG C, make glucose all dissolve, obtain glucose solution；
Step 2.2, institute's gelatine solution is mixed with glucose solution, then in vacuum be -0.10~-0.05MPa,
Temperature after solution bubble-free, is cooled to 50-60 DEG C persistently to be stirred under the conditions of 80-90 DEG C；It is subsequently adding title in step 1.1
Vitamin E, vitamin C and the Tween-80 for taking, in vacuum be -0.10~-0.05MPa, temperature be 50-60 DEG C under the conditions of hold
Continuous stirring 10-15min, obtains one layer of glue；
Step 3, prepares content
Walnut oil, vitamin E, sesamol and the Tween-80 that will be weighed in step 1.2 are well mixed, vacuum be 0~
0.06MPa, temperature are subsequently cooled to room temperature persistently to stir 10-15min under conditions of 30-40 DEG C, obtain content；
Step 4, prepares individual layer capsule
The one layer of glue for preparing and the content of preparation are input into capsule machine, according to a conventional method after pelleting treatment, in 20-
Dried process under the conditions of 30 DEG C, until capsule moisture is less than 5%, that is, obtains individual layer capsule；
Step 5, prepares double-deck capsule
Step 5.1, individual layer capsule is placed in the acetum that concentration is 0.1mol/L, soaks 10-15min, Ran Houyong
Purified water immersion, cleaning, drain away the water, and obtain acid treatment capsule；
Step 5.2, acid treatment capsule is placed in soak, then in vacuum be -0.10~-0.05MPa, normal temperature bar
Persistently stirred under part, after solution bubble-free, be standing and soak for 20-30min, drained away the water, then dried under the conditions of 20-30 DEG C
Treatment, that is, obtain strong anti-oxidation walnut oil soft capsule；
Wherein, in every liter of soak the mannitol containing 10g and 10g sucrose, solvent is purified water.
Compared with prior art, a kind of strong anti-oxidation walnut oil soft capsule that the present invention is provided has following beneficial effect
Really：
(1) with very strong inoxidizability：Vitamin E, vitamin C and grape are with the addition of in the preparing raw material of capsule shells
Sugar, these three materials are respectively provided with reproducibility, can stop that oxygen enters in content with the oxygen reaction in air；
Tween-80, vitamin E, sesamol increased the viscosity of walnut oil, be that walnut oil covers one layer of antioxidant guarantor
Sheath, even if penetrating into a small amount of oxygen from capsule shells, it is also possible to prevent the oxidized phenomenon of unrighted acid in walnut oil.
(2) glucose of addition increased the fragility of capsule shells, while increased the adhesive between different molecular, make molecule
Between spacing it is small, as the oxygen barrier layer of internal layer；By acid soak, make the gelatin partial hydrolysis of individual layer capsule surface, form one
Layer micropore, then soaks through in the soak containing mannitol and sucrose, and sucrose molecule and mannitol molecule enter these micropores
In, one layer of crackling sugar-coat of rear formation to be dried, as the oxygen barrier layer of outer layer；In addition, by true in two-layer capsule shells preparation process
Manage in vacancy so that two-layer capsule shells laminating degree is high, the material that two-layer shell is used in addition is different, intermolecular gap rule is different,
Also can extend oxygen by the time, the inoxidizability of walnut oil capsule is increased indirectly.
(3) plasticizer loading that walnut oil capsule of the invention is used is relatively low, meets national standard, and safety non-toxic is compared
For the emulsifying agent added in conventional vitamin E soft capsule preparation process, consumption greatly reduces, less than soft capsule gross mass
1/100。
Specific embodiment
With reference to specific embodiment, the present invention is described in detail, but should not be construed as limitation of the invention.
A kind of strong anti-oxidation walnut oil soft capsule that the present invention is provided, including capsule shells and content, the capsule shells
It is made up of the raw material components of following weight portion：Gelatin 40-60 parts, vitamin E 3-5 parts, vitamin C 3-5 parts, Tween-80
0.01-0.05 parts, plasticizer 0.5-1 parts, glucose 5-10 parts, purified water 40-60 parts；The wherein weight portion of gelatin and purified water
Ratio is 1:1；
The content is made up of the raw material components of following weight portion：Walnut oil 70-90 parts, vitamin E 5-10 parts, sesame
Numb phenol 3-5 parts, Tween-80 0.01-0.05 parts；
Wherein, the mass ratio of the capsule shells and content is 1:0.5~1.
Preferably, the plasticizer is one kind of glycerine, xylitol or mannitol.
It should be noted that the walnut oil is the walnut oil extracted by conventional method, its extracting method includes pressure
Squeezing method, extraction method and supercritical extraction etc., such as, with reference to Li Shuguo etc., refine production technology of walnut oil and its oxidation be steady
Qualitatively study, Chinese oil, 2003,28 (10)：27-30.
It should be noted that all compounds that the present invention is used, such as sesamol (3,4- methylenedioxyphenol), telling
Temperature 80 etc., should all use commercially available food grade compounds.
Strong anti-oxidation walnut oil soft capsule of the invention belongs to health products, walnut oil in the content of walnut oil soft capsule
Fragrance do not have because addition sesamol the reason for and be affected, sensory evaluation is good；
Instructions of taking is for once a day, a 2g can take the cycle, if Time of Administration is more than three according to own situation regulation
Individual month, then should cut out 1-4 weeks, then could continue to take.
Meanwhile, based on same inventive concept, present invention also offers a kind of system of strong anti-oxidation walnut oil soft capsule
Preparation Method, specifically includes following steps：
Step 1, weighs raw material
Step 1.1, weighs the raw material of following weight portion respectively：Gelatin 40-60 parts, vitamin E 3-5 parts, vitamin C 3-
5 parts, Tween-80 0.01-0.05 parts, plasticizer 0.5-1 parts, glucose 5-10 parts, purified water 40-60 parts；Wherein gelatin with it is pure
The weight ratio for changing water is 1:1；
Step 1.2, weighs the raw material of following weight portion respectively：Walnut oil 70-90 parts, vitamin E 5-10 parts, sesamol
3-5 parts, Tween-80 0.01-0.05 parts；
Wherein, the raw material gross mass ratio weighed in the raw material gross mass and step 1.2 that are weighed in step 1.1 is 1:0.5
~1；
Step 2, prepares one layer of glue
Step 2.1, the purified water mixing of the gelatin that will be weighed in step 1.1, plasticizer and half quality, is heated to 80-
90 DEG C, gelatin and plasticizer is all dissolved, obtain gelatin solution；Glucose and second half quality during step 1.1 is weighed
Purified water mixing, be heated to 80-90 DEG C, make glucose all dissolve, obtain glucose solution；
Step 2.2, institute's gelatine solution is mixed with glucose solution, then in vacuum be -0.10~-0.05MPa,
Temperature after solution bubble-free, is cooled to 50-60 DEG C persistently to be stirred under the conditions of 80-90 DEG C；It is subsequently adding title in step 1.1
Vitamin E, vitamin C and the Tween-80 for taking, in vacuum be -0.10~-0.05MPa, temperature be 50-60 DEG C under the conditions of hold
Continuous stirring 10-15min, obtains one layer of glue；
Step 3, prepares content
Walnut oil, vitamin E, sesamol and the Tween-80 that will be weighed in step 1.2 are well mixed, vacuum be 0~
0.06MPa, temperature are subsequently cooled to room temperature persistently to stir 10-15min under conditions of 30-40 DEG C, obtain content；
Step 4, prepares individual layer capsule
The one layer of glue for preparing and the content of preparation are input into capsule machine, according to a conventional method after pelleting treatment, in 20-
Dried process under the conditions of 30 DEG C, until capsule moisture is less than 5%, that is, obtains individual layer capsule；
Step 5, prepares double-deck capsule
Step 5.1, individual layer capsule is placed in the acetum that concentration is 0.1mol/L, soaks 10-15min, Ran Houyong
Purified water immersion, cleaning, drain away the water, and obtain acid treatment capsule；
It should be noted that purified water immersion, the purpose of cleaning treatment are thoroughly to remove the acetic acid remained in capsule shells, behaviour
It is first to soak 10-15min with purified water as step, then rinses 15-20min with purified water, finally drain away the water again, obtains
Acid treatment capsule；
Step 5.2, acid treatment capsule is placed in soak, then in vacuum be -0.10~-0.05MPa, normal temperature bar
Persistently stirred under part, after solution bubble-free, be standing and soak for 20-30min, drained away the water, then dried under the conditions of 20-30 DEG C
Treatment, that is, obtain strong anti-oxidation walnut oil soft capsule；
Wherein, in every liter of soak the mannitol containing 10g and 10g sucrose, solvent is purified water.
Preferably, the strong anti-oxidation walnut oil soft capsule that the present invention is provided, including following examples：
Embodiment 1
A kind of strong anti-oxidation walnut oil soft capsule, including capsule shells and content, the capsule shells are by following weight portion
Raw material components be made：50 parts of gelatin, 5 parts of vitamin E, 5 parts of vitamin C, 0.01 part of Tween-80,0.8 part of glycerine, grape
Sugared 8 parts, 50 parts of purified water；The content is made up of the raw material components of following weight portion：80 parts of walnut oil, 8 parts of vitamin E,
3 parts of sesamol, 0.01 part of Tween-80；Wherein, the mass ratio of the capsule shells and content is 1:1.Specifically according to following
It is prepared by step：
Step 1, weighs raw material
Step 1.1, weighs the raw material of following weight portion respectively：50 parts of gelatin, 5 parts of vitamin E, 5 parts of vitamin C, tell
- 80 0.01 parts of temperature, 0.8 part of glycerine, 8 parts of glucose, 50 parts of purified water；
Step 1.2, weighs the raw material of following weight portion respectively：80 parts of walnut oil, 8 parts of vitamin E, 3 parts of sesamol, tell
- 80 0.01 parts of temperature；
The raw material gross mass ratio weighed in the raw material gross mass and step 1.2 that are wherein weighed in step 1.1 is 1:1；
Step 2, prepares one layer of glue
Step 2.1, the purified water mixing of the gelatin that will be weighed in step 1.1, glycerine and half quality, is heated to 80 DEG C,
Gelatin and glycerine is all dissolved, obtain gelatin solution；The purified water of glucose and second half quality during step 1.1 is weighed
Mixing, is heated to 80 DEG C, glucose is all dissolved, and obtains glucose solution；
Step 2.2, institute's gelatine solution is mixed with glucose solution, then in vacuum be -0.10~-0.05MPa,
Temperature after solution bubble-free, is cooled to 50 DEG C persistently to be stirred under the conditions of 80 DEG C；It is subsequently adding the dimension weighed in step 1.1
Raw element E, vitamin C and Tween-80, in vacuum be -0.10~-0.05MPa, temperature for 50 DEG C under the conditions of persistently stir
10min, obtains one layer of glue；
Step 3, prepares content
Walnut oil, vitamin E, sesamol and the Tween-80 that will be weighed in step 1.2 are well mixed, vacuum be 0~
0.06MPa, temperature are subsequently cooled to room temperature persistently to stir 10min under conditions of 35 DEG C, obtain content；
Step 4, prepares individual layer capsule
The one layer of glue for preparing and the content of preparation are input into capsule machine, according to a conventional method after pelleting treatment, in 25
Dried process under the conditions of DEG C, until capsule moisture is less than 5%, that is, obtains individual layer capsule；
Step 5, prepares double-deck capsule
Step 5.1, individual layer capsule is placed in the acetum that concentration is 0.1mol/L, soaks 10min, then with purifying
Water immersion, cleaning, drain away the water, and obtain acid treatment capsule；
Step 5.2, acid treatment capsule is placed in soak, then in vacuum be -0.10~-0.05MPa, normal temperature bar
Persistently stirred under part, after solution bubble-free, be standing and soak for 20min, drained away the water under nitrogen protective condition, then in 25 DEG C of bars
Dried process under part, that is, obtain strong anti-oxidation walnut oil soft capsule；Wherein, in every liter of soak the mannitol containing 10g and
The sucrose of 10g, solvent is purified water.
Embodiment 2
A kind of strong anti-oxidation walnut oil soft capsule, including capsule shells and content, the capsule shells are by following weight portion
Raw material components be made：60 parts of gelatin, 3 parts of vitamin E, 4 parts of vitamin C, 0.03 part of Tween-80,0.5 part of xylitol, Portugal
Grape sugar 5 parts, 60 parts of purified water；The content is made up of the raw material components of following weight portion：70 parts of walnut oil, vitamin E 5
Part, 0.03 part of Tween-80；Wherein, the mass ratio of the capsule shells and content is 1:1.Specifically according to following steps system
It is standby：
Step 1, weighs raw material
Step 1.1, weighs the raw material of following weight portion respectively：60 parts of gelatin, 3 parts of vitamin E, 4 parts of vitamin C, tell
- 80 0.03 parts of temperature, 0.5 part of xylitol, 5 parts of glucose, 60 parts of purified water；
Step 1.2, weighs the raw material of following weight portion respectively：70 parts of walnut oil, 5 parts of vitamin E, 5 parts of sesamol, tell
- 80 0.03 parts of temperature；
The raw material gross mass ratio weighed in the raw material gross mass and step 1.2 that are wherein weighed in step 1.1 is 1:0.5；
Step 2, prepares one layer of glue
Step 2.1, the purified water mixing of the gelatin that will be weighed in step 1.1, xylitol and half quality, is heated to 90
DEG C, gelatin and mannitol is all dissolved, obtain gelatin solution；Glucose and second half quality during step 1.1 is weighed
Purified water mixes, and is heated to 90 DEG C, glucose is all dissolved, and obtains glucose solution；
Step 2.2, institute's gelatine solution is mixed with glucose solution, then in vacuum be -0.10~-0.05MPa,
Temperature after solution bubble-free, is cooled to 55 DEG C persistently to be stirred under the conditions of 90 DEG C；It is subsequently adding the dimension weighed in step 1.1
Raw element E, vitamin C and Tween-80, in vacuum be -0.10~-0.05MPa, temperature for 55 DEG C under the conditions of persistently stir
10min, obtains one layer of glue；
Step 3, prepares content
Walnut oil, vitamin E, sesamol and the Tween-80 that will be weighed in step 1.2 are well mixed, vacuum be 0~
0.06MPa, temperature are subsequently cooled to room temperature persistently to stir 10min under conditions of 40 DEG C, obtain content；
Step 4, prepares individual layer capsule
The one layer of glue for preparing and the content of preparation are input into capsule machine, according to a conventional method after pelleting treatment, in 30
Dried process under the conditions of DEG C, until capsule moisture is less than 5%, that is, obtains individual layer capsule；
Step 5, prepares double-deck capsule
Step 5.1, individual layer capsule is placed in the acetum that concentration is 0.1mol/L, soaks 15min, then with purifying
Water immersion, cleaning, drain away the water, and obtain acid treatment capsule；
Step 5.2, acid treatment capsule is placed in soak, then in vacuum be -0.10~-0.05MPa, normal temperature bar
Persistently stirred under part, after solution bubble-free, be standing and soak for 25min, drained away the water, then the dried process under the conditions of 25 DEG C,
Obtain strong anti-oxidation walnut oil soft capsule；Wherein, in every liter of soak the mannitol containing 10g and 10g sucrose, solvent
It is purified water.
Embodiment 3
A kind of strong anti-oxidation walnut oil soft capsule, including capsule shells and content, the capsule shells are by following weight portion
Raw material components be made：55 parts of gelatin, 5 parts of vitamin E, 4 parts of vitamin C, 0.05 part of Tween-80,0.6 part of mannitol, Portugal
Grape sugar 10 parts, 55 parts of purified water；The content is made up of the raw material components of following weight portion：90 parts of walnut oil, vitamin E
10 parts, 4 parts of sesamol, 0.05 part of Tween-80；Wherein, the mass ratio of the capsule shells and content is 1:1.Specifically according to
It is prepared by following steps：
Step 1, weighs raw material
Step 1.1, weighs the raw material of following weight portion respectively：55 parts of gelatin, 5 parts of vitamin E, 4 parts of vitamin C, tell
- 80 0.05 parts of temperature, 0.6 part of mannitol, 10 parts of glucose, 55 parts of purified water；
Step 1.2, weighs the raw material of following weight portion respectively：90 parts of walnut oil, 10 parts of vitamin E, 4 parts of sesamol, tell
- 80 0.05 parts of temperature；
Wherein, the raw material gross mass ratio weighed in the raw material gross mass and step 1.2 that are weighed in step 1.1 is 1:
0.75；
Step 2, prepares one layer of glue
Step 2.1, the purified water mixing of the gelatin that will be weighed in step 1.1, mannitol and half quality, is heated to 85
DEG C, gelatin and mannitol is all dissolved, obtain gelatin solution；Glucose and second half quality during step 1.1 is weighed
Purified water mixes, and is heated to 85 DEG C, glucose is all dissolved, and obtains glucose solution；
Step 2.2, institute's gelatine solution is mixed with glucose solution, then in vacuum be -0.10~-0.05MPa,
Temperature after solution bubble-free, is cooled to 55 DEG C persistently to be stirred under the conditions of 85 DEG C；It is subsequently adding the dimension weighed in step 1.1
Raw element E, vitamin C and Tween-80, in vacuum be -0.10~-0.05MPa, temperature for 55 DEG C under the conditions of persistently stir
12min, obtains one layer of glue；
Step 3, prepares content
Walnut oil, vitamin E, sesamol and the Tween-80 that will be weighed in step 1.2 are well mixed, vacuum be 0~
0.06MPa, temperature are subsequently cooled to room temperature persistently to stir 15min under conditions of 35 DEG C, obtain content；
Step 4, prepares individual layer capsule
The one layer of glue for preparing and the content of preparation are input into capsule machine, according to a conventional method after pelleting treatment, in 25
Dried process under the conditions of DEG C, until capsule moisture is less than 5%, that is, obtains individual layer capsule；
Step 5, prepares double-deck capsule
Step 5.1, individual layer capsule is placed in the acetum that concentration is 0.1mol/L, soaks 12min, then with purifying
Water immersion, cleaning, drain away the water, and obtain acid treatment capsule；
Step 5.2, acid treatment capsule is placed in soak, then in vacuum be -0.10~-0.05MPa, normal temperature bar
Persistently stirred under part, after solution bubble-free, be standing and soak for 30min, drained away the water, then the dried process under the conditions of 20 DEG C,
Obtain strong anti-oxidation walnut oil soft capsule；Wherein, in every liter of soak the mannitol containing 10g and 10g sucrose, solvent
It is purified water.
In order to prove effect of the invention, the walnut oil soft capsule of embodiment 1-3 has been carried out storage experiment by us respectively
With anti-oxidant experimental verification, concrete outcome is as follows：
First, influence (storage experiment) of the storage temperature to peroxide value POV
The peroxide value of embodiment 1-3 is determined with reference to GB5009.227-2016 (measure of peroxide value in food)
(POV)。
Before storage, the POV of embodiment 1-3 and walnut oil is respectively 3meq/kg, 3.5meq/kg, 3meq/kg and 6meq/
kg；After storage 1 month, POV measure is carried out to the sample preserved under the conditions of 5 DEG C, 15 DEG C and 30 DEG C respectively, as a result as shown in table 1,
After 5 DEG C, 15 DEG C and 30 DEG C are preserved 1 month, the POV changes of embodiment 1-3 are not obvious.Illustrate at normal temperatures, embodiment
The walnut oil soft capsule of 1-3 is respectively provided with good inoxidizability.
The POV of the different temperatures of table 1
2nd, anti-oxidant experiment
The peroxide value of embodiment 1-3 is determined referring again to GB5009.227-2016 (measure of peroxide value in food)
POV。
The sample of embodiment 1-3 and commercially available walnut oil soft capsule is placed in 60 DEG C of insulating boxs, each a period of time surveys
The POV of random sample product, calculates the time needed for POV reaches 12meq/kg, and on the basis of the POV of commercially available walnut oil soft capsule, meter
Antioxidative Factors PF is calculated, wherein PF=(sample P OV reach 12meq/kg needed for time)/(commercially available walnut oil soft capsule POV reaches
Time to needed for 12meq/kg), as a result as shown in table 2.As shown in Table 2, under the same terms, embodiment 1-3 it is anti-oxidant because
Sub- PF improves more than 5 times compared with walnut oil, illustrates by after the packaging of double-deck capsule shells, the inoxidizability of walnut oil is obvious
Improve.
The Antioxidative Factors PF of the different samples of table 2
, but those skilled in the art once know basic creation although preferred embodiments of the present invention have been described
Property concept, then can make other change and modification to these embodiments.So, appended claims are intended to be construed to include excellent
Select embodiment and fall into having altered and changing for the scope of the invention.
Obviously, those skilled in the art can carry out various changes and modification without deviating from essence of the invention to the present invention
God and scope.So, if these modifications of the invention and modification belong to the scope of the claims in the present invention and its equivalent technologies
Within, then the present invention is also intended to comprising these changes and modification.
Claims (4)
1. a kind of strong anti-oxidation walnut oil soft capsule, it is characterised in that including capsule shells and content, the capsule shells by with
The raw material components of lower weight portion are made：Gelatin 40-60 parts, vitamin E 3-5 parts, vitamin C 3-5 parts, Tween-80 0.01-
0.05 part, plasticizer 0.5-1 parts, glucose 5-10 parts, purified water 40-60 parts；The wherein weight ratio of gelatin and purified water
It is 1:1；
The content is made up of the raw material components of following weight portion：Walnut oil 70-90 parts, vitamin E 5-10 parts, sesamol
3-5 parts, Tween-80 0.01-0.05 parts；
Wherein, the mass ratio of the capsule shells and content is 1:0.5~1.
2. strong anti-oxidation walnut oil soft capsule according to claim 1, it is characterised in that the capsule shells are by following heavy
The raw material components for measuring part are made：50 parts of gelatin, 5 parts of vitamin E, 5 parts of vitamin C, 0.01 part of Tween-80, plasticizer 0.8
Part, 8 parts of glucose, 50 parts of purified water；
The content is made up of the raw material components of following weight portion：80 parts of walnut oil, 8 parts of vitamin E, 3 parts of sesamol, tell
- 800.01 parts of temperature；
Wherein, the mass ratio of the capsule shells and content is 1:1.
3. strong anti-oxidation walnut oil soft capsule according to claim 1 and 2, it is characterised in that the plasticizer is sweet
One kind of oil, xylitol or mannitol.
4. the preparation method of strong anti-oxidation walnut oil soft capsule according to claim 1, it is characterised in that specifically include
Following steps：
Step 1, weighs raw material
Step 1.1, weighs the raw material of following weight portion respectively：Gelatin 40-60 parts, vitamin E 3-5 parts, vitamin C 3-5 parts,
Tween-80 0.01-0.05 parts, plasticizer 0.5-1 parts, glucose 5-10 parts, purified water 40-60 parts；Wherein gelatin and purified water
Weight ratio be 1:1；
Step 1.2, weighs the raw material of following weight portion respectively：Walnut oil 70-90 parts, vitamin E 5-10 parts, sesamol 3-5
Part, Tween-80 0.01-0.05 parts；
Wherein, the raw material gross mass ratio weighed in the raw material gross mass and step 1.2 that are weighed in step 1.1 is 1:0.5~1；
Step 2, prepares one layer of glue
Step 2.1, the purified water mixing of the gelatin that will be weighed in step 1.1, plasticizer and half quality, is heated to 80-90 DEG C,
Gelatin and plasticizer is all dissolved, obtain gelatin solution；The purifying of glucose and second half quality during step 1.1 is weighed
Water mixes, and is heated to 80-90 DEG C, glucose is all dissolved, and obtains glucose solution；
Step 2.2, institute's gelatine solution is mixed with glucose solution, then in vacuum be -0.10~-0.05MPa, temperature
Persistently to be stirred under the conditions of 80-90 DEG C, after solution bubble-free, 50-60 DEG C is cooled to；It is subsequently adding in step 1.1 what is weighed
Vitamin E, vitamin C and Tween-80, in vacuum be -0.10~-0.05MPa, temperature be 50-60 DEG C under the conditions of persistently stir
10-15min is mixed, one layer of glue is obtained；
Step 3, prepares content
Walnut oil, vitamin E, sesamol and the Tween-80 that will be weighed in step 1.2 are well mixed, vacuum be 0~
0.06MPa, temperature are subsequently cooled to room temperature persistently to stir 10-15min under conditions of 30-40 DEG C, obtain content；
Step 4, prepares individual layer capsule
The one layer of glue for preparing and the content of preparation are input into capsule machine, according to a conventional method after pelleting treatment, in 20-30 DEG C
Under the conditions of dried process, until capsule moisture be less than 5%, that is, obtain individual layer capsule；
Step 5, prepares double-deck capsule
Step 5.1, individual layer capsule is placed in the acetum that concentration is 0.1mol/L, soaks 10-15min, then with purifying
Water immersion, cleaning, drain away the water, and obtain acid treatment capsule；
Step 5.2, acid treatment capsule is placed in soak, then under vacuum is -0.10~-0.05MPa, normal temperature condition
Lasting stirring, after solution bubble-free, is standing and soak for 20-30min, drains away the water, then at drying under the conditions of 20-30 DEG C
Reason, that is, obtain strong anti-oxidation walnut oil soft capsule；
Wherein, in every liter of soak the mannitol containing 10g and 10g sucrose, solvent is purified water.
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| CN111557446A (en) * | 2020-06-05 | 2020-08-21 | 王素荣 | Health-care capsule for middle-aged and old people and preparation method thereof |
| CN112808234A (en) * | 2020-12-31 | 2021-05-18 | 徐州工程学院 | Method for preparing multilayer structure charcoal bag by using biological resources and charcoal bag prepared by same |
| CN112890197A (en) * | 2021-03-10 | 2021-06-04 | 湖南文理学院 | Fish oil product with health promotion effect |
| CN114306273A (en) * | 2022-01-11 | 2022-04-12 | 新昌辽远科技有限公司 | Multilayer hollow capsule and preparation method thereof |
| CN115299607A (en) * | 2022-07-20 | 2022-11-08 | 广东润源中天生物科技有限公司 | Fish oil soft capsule and preparation method thereof |
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| CN115299607A (en) * | 2022-07-20 | 2022-11-08 | 广东润源中天生物科技有限公司 | Fish oil soft capsule and preparation method thereof |
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