CN106689242A - Sterilization herbicide and preparation method thereof - Google Patents

Sterilization herbicide and preparation method thereof Download PDF

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Publication number
CN106689242A
CN106689242A CN201611098561.5A CN201611098561A CN106689242A CN 106689242 A CN106689242 A CN 106689242A CN 201611098561 A CN201611098561 A CN 201611098561A CN 106689242 A CN106689242 A CN 106689242A
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China
Prior art keywords
parts
sulphur
chinese
asarum
kuh
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CN201611098561.5A
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Chinese (zh)
Inventor
贺艺
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Qinzhou Xinghuo Planning Office
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Qinzhou Xinghuo Planning Office
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Priority to CN201611098561.5A priority Critical patent/CN106689242A/en
Publication of CN106689242A publication Critical patent/CN106689242A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/501,3-Diazoles; Hydrogenated 1,3-diazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/72Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
    • A01N43/80Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms five-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,2
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/72Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
    • A01N43/84Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms six-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,4
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/02Sulfur; Selenium; Tellurium; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/48Zingiberaceae [Ginger family], e.g. ginger or galangal

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental Sciences (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Wood Science & Technology (AREA)
  • Dentistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a sterilization herbicide and a preparation method thereof. The sterilization herbicide is prepared from the following ingredients in parts by mass: 10-20 parts of trifluoro-bentranil, 5-7 parts of a formaldehyde solution, 15-25 parts of benzothiazole metribuzin, 4-8 parts of imazapic, 5-7 parts of herba violae, 7-9 parts of saltpetre, 1-3 parts of sulphur, 4-8 parts of radix saposhnikoviae, 4-8 parts of rhizoma curcumae longae, 4-8 parts of fructus schisandrae, 4-8 parts of herba asari, 4-8 parts of radix sophorae flavescentis, 5-7 parts of officinal magnolia bark and 7-9 parts of hydrogen peroxide. The invention provides an environment-friendly herbicide which is obvious in weeding effect, free from harmful ingredient residue in soil, and easily available in raw materials, thereby being an ideal herbicide with a sterilization function.

Description

A kind of bactericidal and herbicidal agent and preparation method thereof
Technical field
The present invention relates to herbicide field, in particular to a kind of bactericidal and herbicidal agent and preparation method thereof.
Background technology
Current China pesticide species are aging, and based on high-toxic pesticide, the kind of efficient, ultra high efficiency and safety only accounts for agriculture The 15% of medicine sum.In order to reduce the adverse effect to environment, agricultural chemicals must exempt to low toxicity, efficient, low-residual and enhancing crop The directions such as epidemic disease resistance are developed, simultaneously because the generation of pest and disease damage resistance, it is also necessary to develop preferable Mixed Pharmacy to be applied to Agricultural production, excellent mixture, it is possible to reduce agricultural chemicals single dose consumption, reduction spray number of times, enhancing crop immunity, reach thing half The purpose of work(times.
Trifluoro grass piperazine is a kind of Triazinone herbicide researched and developed by BASF, ISO agricultural chemicals common names technology committee in 2014 Member can have approved its new active component common name according to agricultural chemicals common name outline (CPCN), and it has to various crop weeds Kill except effect well.AC 263222 is also a kind of new of BASF AG's production, wide spectrum, the special weeding of efficient peanut Agent, its absorbability is strong, has good preventive effect to single, double cotyledon weeds, can not only well kill weeds aerial part, and Also there is stronger preventive effect to the root and stem of weeds underground part.Chinese herbal medicine is windproof, kuh-seng, the bark of official magnolia, turmeric, the fruit of Chinese magnoliavine, asarum, Contain fungicide active ingredient in Chinese violet, it is extracted after, plant source Fungicidal substance can be obtained in its extract, be added to herbicide and mix In agent, enhancing crop immunity can be played, certain prevention effect is played to peanut disease.Do not have trifluoro in the prior art Careless piperazine, AC 263222 and windproof, kuh-seng, the bark of official magnolia, turmeric, the fruit of Chinese magnoliavine, asarum, the report of Chinese violet mixture application.
The content of the invention
The invention provides a kind of bactericidal and herbicidal agent and preparation method thereof, the invention provides the environmentally friendly weeding of kind Agent, bactericidal and herbicidal effect substantially, is remained in soil without harmful components, and raw material are easy to get, and is kind ideal possess sterilized work( The herbicide of energy.
To achieve the above object, the present invention provides following technical scheme:
A kind of bactericidal and herbicidal agent and preparation method thereof, is made up of following mass fraction formula components:Trifluoro grass piperazine 10-20 Part, formalin 5-7 parts, 15-25 parts of benzene thiazole humulone, AC 263222 4-8 parts, Chinese violet 5-7 parts, nitre 7-9 parts, sulphur 1- 3 parts, windproof 4-8 parts, turmeric 4-8 parts, fruit of Chinese magnoliavine 4-8 parts, asarum 4-8 parts, kuh-seng 4-8 parts, bark of official magnolia 5-7 parts, hydrogen peroxide 7-9 Part.
Further:It is made up of following mass fraction formula components:10 parts of piperazine of trifluoro grass, 5 parts of formalin, benzene thiazole humulone 15 parts, 4 parts of AC 263222,5 parts of Chinese violet, 7 parts of nitre, 1 part of sulphur, windproof 4 parts, 4 parts of turmeric, 4 parts of the fruit of Chinese magnoliavine, 4 parts of asarum, 4 parts of kuh-seng, 5 parts of the bark of official magnolia, 7 parts of hydrogen peroxide.
Further:It is made up of following mass fraction formula components:15 parts of piperazine of trifluoro grass, 6 parts of formalin, benzene thiazole humulone 20 parts, 6 parts of AC 263222,6 parts of Chinese violet, 8 parts of nitre, 2 parts of sulphur, windproof 6 parts, 6 parts of turmeric, 6 parts of the fruit of Chinese magnoliavine, 6 parts of asarum, 6 parts of kuh-seng, 6 parts of the bark of official magnolia, 8 parts of hydrogen peroxide.
Further:It is made up of following mass fraction formula components:20 parts of piperazine of trifluoro grass, 7 parts of formalin, benzene thiazole humulone 25 parts, 8 parts of AC 263222,7 parts of Chinese violet, 9 parts of nitre, 3 parts of sulphur, windproof 8 parts, 8 parts of turmeric, 8 parts of the fruit of Chinese magnoliavine, 8 parts of asarum, 8 parts of kuh-seng, 7 parts of the bark of official magnolia, 9 parts of hydrogen peroxide.
Further:Preparation method of the present invention has following steps:
Step one, the Chinese herbal medicine Chinese violet that will be weighed, nitre, windproof, turmeric, the fruit of Chinese magnoliavine, asarum, each 90-100g of kuh-seng, plus Enter in the 5-8 times of water of quality, after slow fire boils 2-3 hour, filtering to remove the dregs of a decoction obtains 300-500g supernatants excessively;
Step 2, by trifluoro grass piperazine, AC 263222, Chinese herbal medicine concentrate, be well mixed i.e. Herbicidal mixtures;
Step 3, will Herbicidal mixtures in above-mentioned steps add surplus stock after insert in fiberizer, defibrination 3-5 is small When, it is made pasty state;
Step 4, the pasty mixture that will be obtained in above-mentioned steps are inserted and refinement homogenization are carried out in homogenizer, are set Homogenization pressure is 12-18Mpa, and homogenizing temperature is 25-30 DEG C;
Step 5:Herbicide after above-mentioned steps homogeneous is filled in polybag, is sealed.
The beneficial effects of the invention are as follows:
1st, the invention provides environmentally friendly herbicide is planted, bactericidal and herbicidal effect is obvious;
2nd, remained without harmful components in soil, raw material are easy to get, be kind of the ideal herbicide for possessing sterilizing function.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based in the present invention Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all Belong to the scope of protection of the invention.
Embodiment one:
A kind of bactericidal and herbicidal agent is made up of following mass fraction formula components:10-20 parts of piperazine of trifluoro grass, formalin 5-7 Part, 15-25 parts of benzene thiazole humulone, AC 263222 4-8 parts, Chinese violet 5-7 parts, nitre 7-9 parts, sulphur 1-3 parts, it is windproof 4-8 parts, Turmeric 4-8 parts, fruit of Chinese magnoliavine 4-8 parts, asarum 4-8 parts, kuh-seng 4-8 parts, bark of official magnolia 5-7 parts, hydrogen peroxide 7-9 parts.
Embodiment two:
A kind of bactericidal and herbicidal agent is made up of following mass fraction formula components:10 parts of piperazine of trifluoro grass, 5 parts of formalin, benzene 15 parts of thiazole humulone, 4 parts of AC 263222,5 parts of Chinese violet, 7 parts of nitre, 1 part of sulphur, windproof 4 parts, 4 parts of turmeric, 4 parts of the fruit of Chinese magnoliavine, 4 parts of asarum, 4 parts of kuh-seng, 5 parts of the bark of official magnolia, 7 parts of hydrogen peroxide.
Embodiment three:
A kind of bactericidal and herbicidal agent is made up of following mass fraction formula components:15 parts of piperazine of trifluoro grass, 6 parts of formalin, benzene 20 parts of thiazole humulone, 6 parts of AC 263222,6 parts of Chinese violet, 8 parts of nitre, 2 parts of sulphur, windproof 6 parts, 6 parts of turmeric, 6 parts of the fruit of Chinese magnoliavine, 6 parts of asarum, 6 parts of kuh-seng, 6 parts of the bark of official magnolia, 8 parts of hydrogen peroxide.
Example IV:
A kind of bactericidal and herbicidal agent is made up of following mass fraction formula components:20 parts of piperazine of trifluoro grass, 7 parts of formalin, benzene 25 parts of thiazole humulone, 8 parts of AC 263222,7 parts of Chinese violet, 9 parts of nitre, 3 parts of sulphur, windproof 8 parts, 8 parts of turmeric, 8 parts of the fruit of Chinese magnoliavine, 8 parts of asarum, 8 parts of kuh-seng, 7 parts of the bark of official magnolia, 9 parts of hydrogen peroxide.
Embodiment five:
A kind of preparation method preparation method of bactericidal and herbicidal agent comprises the following steps:
Step one, the Chinese herbal medicine Chinese violet that will be weighed, nitre, windproof, turmeric, the fruit of Chinese magnoliavine, asarum, each 90-100g of kuh-seng, plus Enter in the 5-8 times of water of quality, after slow fire boils 2-3 hour, filtering to remove the dregs of a decoction obtains 300-500g supernatants excessively;
Step 2, by trifluoro grass piperazine, AC 263222, Chinese herbal medicine concentrate, be well mixed i.e. Herbicidal mixtures;
Step 3, will Herbicidal mixtures in above-mentioned steps add surplus stock after insert in fiberizer, defibrination 3-5 is small When, it is made pasty state;
Step 4, the pasty mixture that will be obtained in above-mentioned steps are inserted and refinement homogenization are carried out in homogenizer, are set Homogenization pressure is 12-18Mpa, and homogenizing temperature is 25-30 DEG C;
Step 5:Herbicide after above-mentioned steps homogeneous is filled in polybag, is sealed.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each implementation method is only wrapped Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should Specification an as entirety, the technical scheme in each embodiment can also be formed into those skilled in the art through appropriately combined May be appreciated other embodiment.

Claims (5)

1. a kind of bactericidal and herbicidal agent, it is characterised in that:It is made up of following mass fraction formula components:
Trifluoro grass 10-20 parts of piperazine, formalin 5-7 parts, 15-25 parts of benzene thiazole humulone, AC 263222 4-8 parts, Chinese violet 5-7 Part, nitre 7-9 parts, sulphur 1-3 parts, windproof 4-8 parts, turmeric 4-8 parts, fruit of Chinese magnoliavine 4-8 parts, asarum 4-8 parts, kuh-seng 4-8 parts, thickness It is plain 5-7 parts, hydrogen peroxide 7-9 parts.
2. a kind of bactericidal and herbicidal agent according to claim 1, it is characterised in that:By following mass fraction formula components group Into:
10 parts of piperazine of trifluoro grass, 5 parts of formalin, 15 parts of benzene thiazole humulone, 4 parts of AC 263222,5 parts of Chinese violet, 7 parts of nitre, sulphur 1 part of sulphur, windproof 4 parts, 4 parts of turmeric, 4 parts of the fruit of Chinese magnoliavine, 4 parts of asarum, 4 parts of kuh-seng, 5 parts of the bark of official magnolia, 7 parts of hydrogen peroxide.
3. a kind of bactericidal and herbicidal agent according to claim 1, it is characterised in that:By following mass fraction formula components group Into:
15 parts of piperazine of trifluoro grass, 6 parts of formalin, 20 parts of benzene thiazole humulone, 6 parts of AC 263222,6 parts of Chinese violet, 8 parts of nitre, sulphur 2 parts of sulphur, windproof 6 parts, 6 parts of turmeric, 6 parts of the fruit of Chinese magnoliavine, 6 parts of asarum, 6 parts of kuh-seng, 6 parts of the bark of official magnolia, 8 parts of hydrogen peroxide.
4. a kind of bactericidal and herbicidal agent according to claim 1, it is characterised in that:By following mass fraction formula components group Into:
20 parts of piperazine of trifluoro grass, 7 parts of formalin, 25 parts of benzene thiazole humulone, 8 parts of AC 263222,7 parts of Chinese violet, 9 parts of nitre, sulphur 3 parts of sulphur, windproof 8 parts, 8 parts of turmeric, 8 parts of the fruit of Chinese magnoliavine, 8 parts of asarum, 8 parts of kuh-seng, 7 parts of the bark of official magnolia, 9 parts of hydrogen peroxide.
5. a kind of a kind of preparation method of bactericidal and herbicidal agent according to claim 1, it is characterised in that:Including following step Suddenly:
Step one, the Chinese herbal medicine Chinese violet that will be weighed, nitre, windproof, turmeric, the fruit of Chinese magnoliavine, asarum, each 90-100g of kuh-seng, add 5- In 8 times of water of quality, after slow fire boils 2-3 hour, filtering to remove the dregs of a decoction obtains 300-500g supernatants excessively;
Step 2, by trifluoro grass piperazine, AC 263222, Chinese herbal medicine concentrate, be well mixed i.e. Herbicidal mixtures;
Step 3, will Herbicidal mixtures in above-mentioned steps add surplus stock after insert in fiberizer, defibrination 3-5 hours, It is made pasty state;
Step 4, the pasty mixture that will be obtained in above-mentioned steps are inserted and refinement homogenization are carried out in homogenizer, set homogeneous Pressure is 12-18Mpa, and homogenizing temperature is 25-30 DEG C;
Step 5:Herbicide after above-mentioned steps homogeneous is filled in polybag, is sealed.
CN201611098561.5A 2016-12-04 2016-12-04 Sterilization herbicide and preparation method thereof Pending CN106689242A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611098561.5A CN106689242A (en) 2016-12-04 2016-12-04 Sterilization herbicide and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201611098561.5A CN106689242A (en) 2016-12-04 2016-12-04 Sterilization herbicide and preparation method thereof

Publications (1)

Publication Number Publication Date
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105638727A (en) * 2014-11-24 2016-06-08 武汉鸿信通科技有限公司 Herbicide
CN105941512A (en) * 2016-06-01 2016-09-21 山东省花生研究所 Formula of herbicide with fungicidal function and preparation method of herbicide

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105638727A (en) * 2014-11-24 2016-06-08 武汉鸿信通科技有限公司 Herbicide
CN105941512A (en) * 2016-06-01 2016-09-21 山东省花生研究所 Formula of herbicide with fungicidal function and preparation method of herbicide

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Application publication date: 20170524