CN105941512A - Formula of herbicide with fungicidal function and preparation method of herbicide - Google Patents

Formula of herbicide with fungicidal function and preparation method of herbicide Download PDF

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Publication number
CN105941512A
CN105941512A CN201610382496.2A CN201610382496A CN105941512A CN 105941512 A CN105941512 A CN 105941512A CN 201610382496 A CN201610382496 A CN 201610382496A CN 105941512 A CN105941512 A CN 105941512A
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herbicide
chinese herbal
herbal medicine
gram
homogenizing
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CN105941512B (en
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曲明静
路兴涛
高华援
陈建洪
鞠倩
李晓
姜晓静
杨珍
焦坤
江晨
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Shandong Peanut Research Institute
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Shandong Peanut Research Institute
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/50—1,3-Diazoles; Hydrogenated 1,3-diazoles
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
    • A01N43/84—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms six-membered rings with one nitrogen atom and either one oxygen atom or one sulfur atom in positions 1,4
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Pest Control & Pesticides (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a formula of a herbicide with the fungicidal function and a preparation method of the herbicide. The herbicide is prepared from herbicide triaziflam, herbicide imazapic and Chinese herbs with the fungicidal function, wherein the Chinese herbs include radix saposhnikoviae, radix sophorae flavescentis, officinal magnolia bark, rhizoma curcumae longae, Chinese magnoliavine fruits, herba asari and herba corydalis bungeanae. The herbicide is prepared through the steps of Chinese herb concentration treatment, raw material blending, grinding, homogenizing, filling and the like. The herbicide with the fungicidal function is environmentally friendly, obvious in fungicidal and herbicidal effect, free of harmful ingredient residues in soil and ideal, and raw materials are easy to obtain.

Description

A kind of Herbicidal composition possessing sterilizing function and preparation method thereof
Technical field
The invention belongs to Weed in peanut field and techniques of pest control field, be specifically related to a kind of weeding possessing sterilizing function Agent prescription and preparation method.
Background technology
China's pesticide species is aging at present, and based on high-toxic pesticide, the kind of efficient, ultra high efficiency and safety only accounts for agriculture The 15% of medicine sum.In order to reduce the adverse effect to environment, pesticide must be exempted to low toxicity, efficient, low-residual and enhancing crop The directions such as epidemic disease resistance are developed, simultaneously because the generation of pest and disease damage resistance, it is also necessary to develop preferable Mixed Pharmacy to be applied to agriculture Industry produces, excellent mixture, it is possible to reduce pesticide single dose consumption, minimizing spray medicine number of times, enhancing crop immunity, reaches thing half The purpose of merit times.
Trifluoro grass piperazine is a kind of Triazinone herbicide researched and developed by BASF, ISO pesticide common name technology committee member in 2014 Can have approved its new active component common name according to pesticide common name outline (CPCN), various crop weeds are all had very by it Good kills except effect.The one that AC 263222 also produces for BASF AG is novel, wide spectrum, efficient peanut herbicides special, In it, absorption is strong, single, double cotyledon weeds is all had good preventive effect, can not only well kill weeds aerial parts, and right The root of weeds underground part and stem also have stronger preventive effect.Chinese herbal medicine Radix Saposhnikoviae, Radix Sophorae Flavescentis, Cortex Magnoliae Officinalis, Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis, thin Containing fungicide active ingredient in pungent, Herba Violae, extracted after, its extract can obtain plant source Fungicidal substance, add weeding to In agent mixture, enhancing crop immunity can be played, peanut disease is played certain prevention effect.Prior art does not has by Trifluoro grass piperazine, AC 263222 and Radix Saposhnikoviae, Radix Sophorae Flavescentis, Cortex Magnoliae Officinalis, Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis, Herba Asari, the report of Herba Violae mixture application.
Summary of the invention
The technical problem to be solved is to invent a kind of Herbicidal composition possessing sterilizing function and preparation method, uses In the various weeds of removal Peanut Fields, Semen arachidis hypogaeae sprout term disease also there is is certain prevention effect, be finally reached and improve peanut yield Purpose.
For solving above-mentioned technical problem, the present invention realizes by following technical solution:
A kind of Herbicidal composition possessing sterilizing function and preparation method, it is characterised in that this formula be the trifluoro grass piperazine with 20%, The AC 263222 of 98% and the Chinese herbal medicine Radix Saposhnikoviae of sterilization, Radix Sophorae Flavescentis, Cortex Magnoliae Officinalis, Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis, Herba Asari, Herba Violae composition.Warp Cross Chinese herbal medicine concentration, proportioning raw materials, defibrination, homogenizing and fill step to be prepared from.
The consumption on described every mu of ground of Herbicidal composition is: trifluoro grass piperazine 10-15g, the AC 263222 50-of 98% of 20% 65g, Chinese herbal medicine Radix Saposhnikoviae 90-100 gram, Radix Sophorae Flavescentis 90-100 gram, Cortex Magnoliae Officinalis 90-100 gram, 90-100 gram of Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis 90- 100 grams, Herba Asari 90-100 gram, Herba Violae 90-100 gram.
Described preparation method comprises the steps:
Chinese herbal medicine concentration: by the Chinese herbal medicine Radix Saposhnikoviae weighed, Radix Sophorae Flavescentis, Cortex Magnoliae Officinalis, Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis, Herba Asari, each 90-of Herba Violae 100g, adds in the water of 5-6 times of quality, and after slow fire boils 5-6 hour, filtering to remove medicinal residues obtains 300-400g supernatant excessively； Gained supernatant is Chinese herbal medicine concentrated solution.
Proportioning raw materials: weigh trifluoro grass piperazine 10-15g, the AC 263222 50-65g of 98% of 20%, Chinese herbal medicine concentrated solution 300-400g, mix homogeneously i.e. Herbicidal mixtures.
Defibrination: the Herbicidal mixtures in above-mentioned steps is inserted in fiberizer, defibrination 3-4 hour, make pasty state.
Homogenizing: the pasty mixture obtained in above-mentioned steps is inserted in homogenizer and carry out refining homogenizing process, homogenizing is set Pressure is 12-18Mpa, and homogenizing temperature is 25-30 DEG C.
Fill: the herbicide after above-mentioned steps homogenizing is filled in plastic bag, sealing.
After peanut seeding earthing, every bag is watered 50 kilograms, is uniformly sprayed onto on soil, then overlay film.
Beneficial effects of the present invention:
The invention provides a kind of environmentally friendly herbicide possessing sterilizing function, be mainly used in soil treatment, herbicidal effect is obvious, Having sterilizing function concurrently, remain without harmful components in soil, raw material is easy to get, and is a kind of ideal bactericidal and herbicidal agent.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described, but these examples are not limiting as the model of the present invention Enclose.In addition any change that the present invention is done by those of ordinary skill in the related art, without departing from the essence of the present invention, all incites somebody to action Equivalence falls in claims of the present invention limited range.
Embodiment 1
Weigh Chinese herbal medicine Radix Saposhnikoviae 90 grams, Radix Sophorae Flavescentis 90 grams, Cortex Magnoliae Officinalis 90 grams, 100 grams of Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis 100 grams, Herba Asari 95 grams, Herba Violae 90 grams adds in the water of 5 times of quality, and after slow fire boils 5 hours, filtering to remove medicinal residues obtains 300g supernatant excessively；Gained Supernatant is Chinese herbal medicine concentrated solution.
Proportioning raw materials: weigh trifluoro grass piperazine 10g, the AC 263222 65g of 98% of 20%, Chinese herbal medicine concentrated solution 300g, Mix homogeneously i.e. Herbicidal mixtures.
Defibrination: the Herbicidal mixtures in above-mentioned steps is inserted in fiberizer, defibrination 3 hours, make pasty state.
Homogenizing: the pasty mixture obtained in above-mentioned steps is inserted in homogenizer and carry out refining homogenizing process, homogenizing is set Pressure is 18Mpa, and homogenizing temperature is 30 DEG C.
Fill: the herbicide after above-mentioned steps homogenizing is filled in plastic bag, sealing.
After peanut seeding earthing, every bag is watered 50 kilograms, is uniformly sprayed onto on soil, then overlay film.
Comparison plot, sows by the same way, applies fertilizer, waters and field management that other are identical.
During harvesting peanut, test group reaches 85.6% to the preventive effect of Peanut Fields malignant weed Rhizoma Cyperi, prevents Amaranthus retroflexus Except effect reaches 95.2%, Semen arachidis hypogaeae sprout term disease (stem rot, root rot) prevention effect is reached 45.6%, every mu of results flower Raw 421kg；Unprocessed field results Semen arachidis hypogaeae 335kg/ mu, experimental group volume increase 25.6%, process field and be significantly better than untreated field.
Embodiment 2
Weigh Chinese herbal medicine Radix Saposhnikoviae 100 grams, Radix Sophorae Flavescentis 95 grams, Cortex Magnoliae Officinalis 95 grams, 90 grams of Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis 100 grams, Herba Asari 90 grams, Herba Violae 100 grams adds in the water of 6 times of quality, and after slow fire boils 6 hours, filtering to remove medicinal residues obtains 400g supernatant excessively；Gained Supernatant is Chinese herbal medicine concentrated solution.
Proportioning raw materials: weigh trifluoro grass piperazine 15g, the AC 263222 60g of 98% of 20%, Chinese herbal medicine concentrated solution 400g, Mix homogeneously i.e. Herbicidal mixtures.
Defibrination: the Herbicidal mixtures in above-mentioned steps is inserted in fiberizer, defibrination 4 hours, make pasty state.
Homogenizing: the pasty mixture obtained in above-mentioned steps is inserted in homogenizer and carry out refining homogenizing process, homogenizing is set Pressure is 15Mpa, and homogenizing temperature is 30 DEG C.
Fill: the herbicide after above-mentioned steps homogenizing is filled in plastic bag, sealing.
After peanut seeding earthing, every bag is watered 50 kilograms, is uniformly sprayed onto on soil, then overlay film.
Comparison plot, sows by the same way, applies fertilizer, waters and field management that other are identical.
During results, test group reaches 83.4% to the preventive effect of Peanut Fields malignant weed Rhizoma Cyperi, and Amaranthus retroflexus is prevented and kill off effect Fruit reaches 93.2%, Semen arachidis hypogaeae sprout term disease (stem rot, root rot) prevention effect reaches 35.3%, every mu of ground results Semen arachidis hypogaeae 410kg；Unprocessed comparison field results Semen arachidis hypogaeae 340kg, test group volume increase 20.6%.

Claims (3)

1. Herbicidal composition possessing sterilizing function and preparation method thereof, it is characterised in that this formula is the trifluoro grass with 20% The Chinese herbal medicine Radix Saposhnikoviae of piperazine, the AC 263222 of 98% and sterilization, Radix Sophorae Flavescentis, Cortex Magnoliae Officinalis, Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis, Herba Asari, Herba Violae group Become；It is prepared from through Chinese herbal medicine concentration, proportioning raw materials, defibrination, homogenizing and fill step.
2. according to claim 1, described Herbicidal composition be every mu use 20% trifluoro grass piperazine 10-15g, the first imidazoles of 98% Nicotinic acid 50-65g, Chinese herbal medicine Radix Saposhnikoviae 90-100 gram, Radix Sophorae Flavescentis 90-100 gram, Cortex Magnoliae Officinalis 90-100 gram, 90-100 gram of Rhizoma Curcumae Longae, five Taste 90-100 gram, Herba Asari 90-100 gram, Herba Violae 90-100 gram.
3., according to claim 1, described preparation method comprises the steps:
Chinese herbal medicine concentration: by the Chinese herbal medicine Radix Saposhnikoviae weighed, Radix Sophorae Flavescentis, Cortex Magnoliae Officinalis, Rhizoma Curcumae Longae, Fructus Schisandrae Chinensis, Herba Asari, each 90-of Herba Violae 100g, adds in the water of 5-6 times of quality, and after slow fire boils 5-6 hour, filtering to remove medicinal residues obtains 300-400g supernatant excessively, Gained supernatant is Chinese herbal medicine concentrated solution；
Proportioning raw materials: weigh trifluoro grass piperazine 10-15g, the AC 263222 50-65g of 98% of 20%, Chinese herbal medicine concentrated solution 300- 400g, mix homogeneously i.e. Herbicidal mixtures；
Defibrination: the Herbicidal mixtures in above-mentioned steps is inserted in fiberizer, defibrination 3-4 hour, make pasty state；
Homogenizing: being inserted by the pasty mixture obtained in above-mentioned steps in homogenizer and carry out refining homogenizing process, arranging homogenization pressure is 12-18Mpa, homogenizing temperature is 25-30 DEG C；
Fill: the herbicide after above-mentioned steps homogenizing is filled in plastic bag, sealing.
CN201610382496.2A 2016-06-01 2016-06-01 A kind of Herbicidal composition and preparation method thereof having sterilizing function Active CN105941512B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106577898A (en) * 2016-12-14 2017-04-26 安徽扬子化工有限公司 Chinese herbal medicine antibacterial weedicide special for agriculture and forestry and preparation method
CN106689242A (en) * 2016-12-04 2017-05-24 钦州市星火计划办公室 Sterilization herbicide and preparation method thereof
CN107047643A (en) * 2016-12-12 2017-08-18 安徽常泰化工有限公司 A kind of Chinese herbal medicine antibacterial type herbicide and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1947522A (en) * 2005-10-14 2007-04-18 中国医学科学院药用植物研究所 Botany resource disinfectants for agricultural use an dits prepn. method
CN104222157A (en) * 2014-09-09 2014-12-24 山东省农作物种质资源中心 Compound herbicide suitable for planting sesban and alfalfa in Huang-Huai-Hai region

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1947522A (en) * 2005-10-14 2007-04-18 中国医学科学院药用植物研究所 Botany resource disinfectants for agricultural use an dits prepn. method
CN104222157A (en) * 2014-09-09 2014-12-24 山东省农作物种质资源中心 Compound herbicide suitable for planting sesban and alfalfa in Huang-Huai-Hai region

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106689242A (en) * 2016-12-04 2017-05-24 钦州市星火计划办公室 Sterilization herbicide and preparation method thereof
CN107047643A (en) * 2016-12-12 2017-08-18 安徽常泰化工有限公司 A kind of Chinese herbal medicine antibacterial type herbicide and preparation method thereof
CN106577898A (en) * 2016-12-14 2017-04-26 安徽扬子化工有限公司 Chinese herbal medicine antibacterial weedicide special for agriculture and forestry and preparation method

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