CN106666005A - Moringa seed tea and preparation method thereof - Google Patents

Moringa seed tea and preparation method thereof Download PDF

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Publication number
CN106666005A
CN106666005A CN201710012029.5A CN201710012029A CN106666005A CN 106666005 A CN106666005 A CN 106666005A CN 201710012029 A CN201710012029 A CN 201710012029A CN 106666005 A CN106666005 A CN 106666005A
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China
Prior art keywords
moringa seeds
tea
moringa
preparation
moringa seed
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CN201710012029.5A
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Chinese (zh)
Inventor
丁雄
华帅
陈海丰
段柱标
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Xishuangbanna Tropical Botanical Garden of CAS
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Xishuangbanna Tropical Botanical Garden of CAS
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Priority to CN201710012029.5A priority Critical patent/CN106666005A/en
Publication of CN106666005A publication Critical patent/CN106666005A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23FCOFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F3/00Tea; Tea substitutes; Preparations thereof
    • A23F3/34Tea substitutes, e.g. matè; Extracts or infusions thereof

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a preparation method of moringa seed tea. The preparation method comprises the following steps: adding moringa seeds into ethyl alcohol and water in sequence, and carrying out microwave extraction to prepare a moringa seed ethyl alcohol extract and a water extract; taking beta-cyclodextrin as an inclusion material, mixing the moringa seed ethyl alcohol extract with the beta-cyclodextrin, carrying out ultrasonic treatment with ultrasonic waves, then carrying out refrigeration or freezing and suction filtering, washing with absolute ethyl alcohol, and carrying out settling and drying to obtain a moringa seed tea inclusion complex; mixing the moringa seed water extract with the moringa seed tea inclusion complex, adding a diluent and an adhesive, and preparing the moringa seed tea in an extrusion molding manner. The invention further discloses the moringa seed tea prepared based on the preparation method. The contents of nutritional components and active components of the moringa seed tea are increased, the taste of the original moringa seed tea is improved, and the treating effect and the acceptance degree of the moringa seed tea are enhanced.

Description

A kind of moringa seeds tea and preparation method thereof
Technical field
The invention belongs to food processing field, specifically, is related to a kind of moringa seeds tea and preparation method thereof.
Background technology
Moringa is the tropical plants of Moringaceae Moringa, in addition to containing protein, aminoacid, vitamins and other nutritious components, Also containing polysaccharide and flavonoid isoreactivity composition, with blood sugar lowering, blood pressure lowering, the effect such as cholesterol, hepatoprotective, cardioprotection is reduced (He Yanpei, Wang Qian, Kong Lingyu. the progress of Moringa. scientific observation [J], 2013,2:87-89.).Mainly take at this stage Mode is to swallow fecula, or soaked when tea-drinking is used, or Jing is simply extracted and is prepared into other preparations, and not only utilization rate is low, weak curative effect, And cause the great wasting of resources.
The content of the invention
In view of this, the present invention is low for existing moringa seeds tea active component dissolution rate, the not good problem of tea mouthfeel of immersion, There is provided a kind of moringa seeds tea and preparation method thereof.
In order to solve above-mentioned technical problem, the invention discloses a kind of preparation method of moringa seeds tea, comprises the following steps:
1) moringa seeds are added in ethanol, microwave extraction prepares moringa seeds ethanol extraction;
2) moringa seeds after is extracted ethanol add water, microwave extraction that moringa seeds tea extract is obtained;
3) with beta-schardinger dextrin-to include material, moringa seeds ethanol extraction is mixed with beta-schardinger dextrin-, using supersound process, Cold preservation afterwards or freezing, sucking filtration, with absolute ethanol washing 2-3 time, precipitates drying, obtains final product moringa seeds tea bag compound;
4) moringa seeds water extract and moringa seeds tea bag compound are mixed, and adds diluent and binding agent, by extruding The mode of molding, prepares moringa seeds tea.
Further, step 1) in the mass ratio of moringa seeds and water be 1:8-1:12, the volumetric concentration of ethanol is 50%- 80%.
Further, step 1) and step 2) in the microwave extraction time be 3-7 minutes, microwave extraction power be 0.5- 1.5KW, microwave extraction number of times is 1-3 time.
Further, step 3) in the mass ratio of beta-schardinger dextrin-and Moringa seed extract be 1:1-1:3.
Further, step 3) in sonication times be 40-90 minutes, ultrasonic power is 100-500W;Cold preservation or Cooling time is 60-240 minutes.
Further, step 4) in diluent be mass ratio be 1:1-4:1 ethyl cellulose and Microcrystalline Cellulose Mixture;Binding agent is the ethyl cellulose ethanol solution that mass-volume concentration is 3-5%;The quality consumption of diluent is Moringa 2-5 times of seed water extract;The quality consumption of binding agent is diluent, moringa seeds water extract and moringa seeds tea bag compound quality The 1%-10% of total amount.
The invention also discloses a kind of moringa seeds tea prepared by above-mentioned preparation method.
Compared with prior art, the present invention can be obtained including following technique effect:
1) present invention adopts microwave extraction technology, improves nutritional labeling and active constituent content in moringa seeds tea, while Also the extraction for moringa seeds searches out scientific and reasonable method;
2) inclusion technique is adopted, greatly improves dissolubility of the alcohol soluble substance in water;
3) slow release method is adopted, composition in moringa seeds tea is progressively discharged;
4) present invention improves the nutritional labeling and active component content of moringa seeds tea, improves the mouthfeel of former moringa seeds tea, So as to improve the curative effect and acceptance level of moringa seeds tea.
Certainly, the arbitrary product for implementing the present invention it is not absolutely required to while reaching all the above technique effect.
Specific embodiment
Embodiments of the present invention are described in detail below in conjunction with embodiment, thereby to the present invention how application technology handss Section come solve technical problem and reach technology effect realize that process can fully understand and implement according to this.
The invention discloses a kind of preparation method of moringa seeds tea, comprises the following steps:
1) it is 1 according to mass volume ratio:8-1:It is micro- during moringa seeds are added volumetric concentration for the ethanol of 50%-80% by 12 Ripple extracts 3-7 minutes, wherein, the power of microwave is 0.5-1.5KW, is extracted 1-3 time, prepares moringa seeds ethanol extraction;
2) by step 1) the moringa seeds ethanol extraction for preparing adds water, microwave extraction 3-7 minute, moringa seeds is obtained Tea extract;Wherein, the power of microwave is 0.5-1.5KW, is extracted 1-3 time, prepares moringa seeds water extract;
3) with beta-schardinger dextrin-(β-CD) as inclusion material, it is with the mass ratio of moringa seeds ethanol extraction according to beta-schardinger dextrin- 1:1-1:3, ultrasound wave (power is 100-500W) ultrasound 40-90 minutes, afterwards cold preservation or freezing 60-240 minutes are adopted, take out Filter, with absolute ethanol washing 2-3 time, precipitation drying, obtains final product moringa seeds tea bag compound;
4) moringa seeds water extract and moringa seeds tea bag compound are mixed, and adds diluent and binding agent, by extruding The mode of molding, prepares moringa seeds tea.
Wherein, diluent is that mass ratio is 1:1-4:1 ethyl cellulose and the mixture of Microcrystalline Cellulose;Binding agent is Mass-volume concentration is the ethyl cellulose ethanol solution of 3-5%;The quality consumption of diluent is the 2-5 of moringa seeds water extract Times;The quality consumption of binding agent is the 1%-10% of diluent, moringa seeds water extract and moringa seeds tea bag compound quality total amount.
Wherein, (1) microwave extraction is that the new technique that a kind of latest development of extraction yield is got up is improved using microwave energy.It Principle be in microwave field, absorb microwave ability difference cause some of some regions or extraction system of base matter Component is heated by selectivity, so that take material by leather separate from matrix or system, enters people to dielectric constant is less, microwave In the extractant of absorbability relative mistake;Microwave extraction has that equipment is simple, applied widely, extraction efficiency is high, favorable reproducibility, It is time-consuming, save reagent, pollute it is little the features such as.Compared with traditional alcohol reflux and decocting cooking method, the method is being protected While holding higher extraction ratio, the time used by extraction process is substantially reduced, and significantly reduce impurity in extracting solution Content.
(2) inclusion technique is a special kind of skill to form clathrate, being widely used in pharmaceuticss.Clathrate is a kind of point Son is embedded in the void structure of another kind of molecule and obtained molecular complex by bag, and the formation of clathrate is depended primarily on and divided The structure of son and enclosed molecule, its stability dependency is in the power of the intermolecular Van der Waals force of host and guest;Because β-CD have circular hollow hole Cave, and have outer hydrophilic, the hydrophobic special construction in ring of ring, so bag can be formed with many materials, particularly fat-soluble medicine Compound so that the water solublity increase of clathrate, while also masking the special odor of some materials.So, in moringa seeds tea Inclusion technique is adopted in preparation process, increases the cumulative release amount of the flavones ingredient in moringa seeds, while covering moringa seeds Abnormal smells from the patient.
(3) slow release of medicine is to be combined pharmaceutically active molecule with macromolecule carrier after (or compound, encapsulation), and throwing is applied to life In vivo by control modes such as diffusion, infiltrations, pharmaceutically active molecule is discharged again thing activity with appropriate concentration and persistent period Come, so as to reach the purpose for giving full play to curative effect of medication.The characteristics of medicament slow release is by the effective control to drug medical dosage System, can reduce the toxic and side effects of medicine, reduce Drug resistance, improve the stability and effective rate of utilization of medicine.Due to macromolecule The research of Thermosensitive Material Used for Controlled Releasing of Medicine so that the slow release method of medicine is developed rapidly.In the preparation process of moringa seeds tea, select Macromolecular material enables flavones ingredient and polysaccharide in moringa seeds tea slowly to discharge, to reach " tea " as slow-release material Effect.
Embodiment 1
A kind of preparation method of moringa seeds tea, comprises the following steps:
1) it is 1 according to mass volume ratio:Moringa seeds addition volumetric concentration is 5 points of microwave extraction in 65% ethanol by 10 Clock, wherein, the power of microwave is 1.0KW, is extracted 1 time, prepares moringa seeds ethanol extraction;
2) by step 1) the moringa seeds ethanol extraction for preparing adds water, microwave extraction 5 minutes that moringa seeds tea is obtained Water extract;Wherein, the power of microwave is 1.0KW, is extracted 1 time, prepares moringa seeds water extract;
3) with beta-schardinger dextrin-(β-CD) as inclusion material, it is with the mass ratio of moringa seeds ethanol extraction according to beta-schardinger dextrin- 1:2, adopt ultrasound wave (power is 300W) ultrasound 65 minutes, cold preservation afterwards or freezing 150 minutes, sucking filtration is washed with dehydrated alcohol Wash 2-3 time, precipitate drying, obtain final product moringa seeds tea bag compound;
4) moringa seeds water extract and moringa seeds tea bag compound are mixed, and adds diluent and binding agent, by extruding The mode of molding, prepares moringa seeds tea.Wherein, diluent is that mass ratio is 2.5:1 ethyl cellulose and Microcrystalline Cellulose Mixture;Binding agent is ethyl cellulose ethanol solution that mass-volume concentration is 4%;The quality consumption of diluent is moringa seeds 3.5 times of water extract;The quality consumption of binding agent is that diluent, moringa seeds water extract and moringa seeds tea bag compound quality are total The 5% of amount.
Embodiment 2
A kind of preparation method of moringa seeds tea, comprises the following steps:
1) it is 1 according to mass volume ratio:Moringa seeds addition volumetric concentration is 3 points of microwave extraction in 80% ethanol by 8 Clock, wherein, the power of microwave is 1.5KW, is extracted 1 time, prepares moringa seeds ethanol extraction;
2) by step 1) the moringa seeds ethanol extraction for preparing adds water, microwave extraction 3 minutes that moringa seeds tea is obtained Water extract;Wherein, the power of microwave is 1.5KW, is extracted 1 time, prepares moringa seeds water extract;
3) with beta-schardinger dextrin-(β-CD) as inclusion material, it is with the mass ratio of moringa seeds ethanol extraction according to beta-schardinger dextrin- 1:1, adopt ultrasound wave (power is 500W) ultrasound 40 minutes, cold preservation afterwards or freezing 240 minutes, sucking filtration is washed with dehydrated alcohol Wash 2 times, precipitate drying, obtain final product moringa seeds tea bag compound;
4) moringa seeds water extract and moringa seeds tea bag compound are mixed, and adds diluent and binding agent, by extruding The mode of molding, prepares moringa seeds tea.Wherein, diluent is that mass ratio is 1:1 ethyl cellulose and Microcrystalline Cellulose it is mixed Compound;Binding agent is ethyl cellulose ethanol solution that mass-volume concentration is 3%;The quality consumption of diluent is moringa seeds water 5 times of extract;The quality consumption of binding agent is diluent, moringa seeds water extract and moringa seeds tea bag compound quality total amount 1%.
Embodiment 3
A kind of preparation method of moringa seeds tea, comprises the following steps:
1) it is 1 according to mass volume ratio:Moringa seeds addition volumetric concentration is 7 points of microwave extraction in 50% ethanol by 12 Clock, wherein, the power of microwave is 0.5KW, is extracted 3 times, prepares moringa seeds ethanol extraction;
2) by step 1) the moringa seeds ethanol extraction for preparing adds water, microwave extraction 7 minutes that moringa seeds tea is obtained Water extract;Wherein, the power of microwave is 0.5KW, is extracted 3 times, prepares moringa seeds water extract;
3) with beta-schardinger dextrin-(β-CD) as inclusion material, it is with the mass ratio of moringa seeds ethanol extraction according to beta-schardinger dextrin- 1:3, adopt ultrasound wave (power is 100W) ultrasound 90 minutes, cold preservation afterwards or freezing 60 minutes, sucking filtration uses absolute ethanol washing 3 times, drying is precipitated, obtain final product moringa seeds tea bag compound;
4) moringa seeds water extract and moringa seeds tea bag compound are mixed, and adds diluent and binding agent, by extruding The mode of molding, prepares moringa seeds tea.Wherein, diluent is that mass ratio is 4:1 ethyl cellulose and Microcrystalline Cellulose it is mixed Compound;Binding agent is ethyl cellulose ethanol solution that mass-volume concentration is 5%;The quality consumption of diluent is moringa seeds water 2 times of extract;The quality consumption of binding agent is diluent, moringa seeds water extract and moringa seeds tea bag compound quality total amount 10%.
Comparative example 1
Moringa seeds are crushed, with starch slurry as binding agent, by extrusion molding, moringa seeds tea granule is prepared into.
The technique effect of the present invention is illustrated with reference to specific experimental data:
First, microwave extraction technological feasibility checking:
According to step 1 in embodiment 1) and step 2) prepare moringa seeds ethanol extraction and moringa seeds water extract;Repeat 4 It is secondary;Experimental result see the table below 1:
The microwave extraction technological feasibility of table 1 is verified
From table 1 it follows that the practical process of microwave extraction moringa seeds, and process stabilizing, favorable reproducibility.
2nd, moringa seeds tea is prepared using this method and traditional method
The moringa seeds tea of preparation is compared with moringa seeds tea obtained in traditional preparation methods, mainly from soup look, abnormal smells from the patient, Polysaccharide dissolution rate and Cumulative release amount, flavonoid dissolution rate and cumulative release amount etc. are compared, and prepared by this method peppery Wooden seed tea, by weighing two plant teas equivalent to identical moringa seeds, adds same amount of boiling water with traditional moringa seeds tea, soaks respectively Bubble four times, every time bubble 10 minutes, determine respectively the flavone and polysaccharide in each tea, then four tea are merged, and see its color, taste Its taste, and calculate the cumulative release amount of flavone and polysaccharide.Its result see the table below 2:
The moringa seeds tea quality preservation that embodiment 1-3 of table 2 is prepared with comparative example 1
From Table 2, it can be seen that moringa seeds tea is extracted, after inclusion, the dissolution of flavone is substantially increased, while polysaccharide Dissolution is also improved;And the amount and abnormal smells from the patient of oils and fatss in moringa seeds tea are reduced, soup look is also brighter.Therefore, prepared by the present invention Method not only improves the flavones content in moringa seeds tea, also makes soup look, the abnormal smells from the patient of moringa seeds tea more preferably.
Described above illustrates and describes some preferred embodiments of invention, but as previously mentioned, it should be understood that invention is not Form disclosed herein is confined to, the exclusion to other embodiment is not to be taken as, and can be used for various other combinations, modification And environment, and can be carried out by the technology or knowledge of above-mentioned teaching or association area in invention contemplated scope described herein Change.And change that those skilled in the art are carried out and change be without departing from the spirit and scope of invention, then all should be in the appended power of invention In the protection domain that profit is required.

Claims (7)

1. a kind of preparation method of moringa seeds tea, it is characterised in that comprise the following steps:
1) moringa seeds are added in ethanol, microwave extraction prepares moringa seeds ethanol extraction;
2) moringa seeds after is extracted ethanol add water, microwave extraction that moringa seeds tea extract is obtained;
3) with beta-schardinger dextrin-to include material, moringa seeds ethanol extraction is mixed with beta-schardinger dextrin-, using supersound process, afterwards Cold preservation or freezing, sucking filtration, with absolute ethanol washing 2-3 time, precipitates drying, obtains final product moringa seeds tea bag compound;
4) moringa seeds water extract and moringa seeds tea bag compound are mixed, and adds diluent and binding agent, by extrusion molding Mode, prepare moringa seeds tea.
2. the preparation method of moringa seeds tea according to claim 1, it is characterised in that the step 1) in moringa seeds with The mass ratio of water is 1:8-1:12, the volumetric concentration of ethanol is 50%-80%.
3. the preparation method of moringa seeds tea according to claim 1, it is characterised in that the step 1) and step 2) in The microwave extraction time is 3-7 minutes, and microwave extraction power is 0.5-1.5KW, and microwave extraction number of times is 1-3 time.
4. the preparation method of moringa seeds tea according to claim 1, it is characterised in that the step 3) in beta-schardinger dextrin- It is 1 with the mass ratio of Moringa seed extract:1-1:3.
5. the preparation method of moringa seeds tea according to claim 1, it is characterised in that the step 3) in ultrasound wave when Between be 40-90 minutes, ultrasonic power is 100-500W;Cold preservation or cooling time are 60-240 minutes.
6. the preparation method of moringa seeds tea according to claim 1, it is characterised in that the step 4) in diluent be Mass ratio is 1:1-4:1 ethyl cellulose and the mixture of Microcrystalline Cellulose;Binding agent is that mass-volume concentration is 3-5%'s Ethyl cellulose ethanol solution;The quality consumption of diluent is 2-5 times of moringa seeds water extract;The quality consumption of binding agent is The 1%-10% of diluent, moringa seeds water extract and moringa seeds tea bag compound quality total amount.
7. the moringa seeds tea that a kind of preparation method by described in any claim in claim 1-6 is prepared.
CN201710012029.5A 2017-01-09 2017-01-09 Moringa seed tea and preparation method thereof Pending CN106666005A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107348489A (en) * 2017-07-27 2017-11-17 贵阳学院 Moringa superfine powder, tablet, the preparation method of chewable tablets
CN108771074A (en) * 2018-05-17 2018-11-09 广西柳州市桑辰科技有限公司 A kind of production method of moringa seeds solid beverage

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CN103828965A (en) * 2014-02-28 2014-06-04 徐星航 Compound black tea granules and preparation method thereof
CN103931823A (en) * 2013-01-22 2014-07-23 青岛市市立医院 Pomegranate leaf granular tea and preparation method thereof
CN105594924A (en) * 2015-12-18 2016-05-25 信宜市四海永丰现代种养场 Natural moringa tea preparation method

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WO2006085710A1 (en) * 2005-02-11 2006-08-17 Amorepacific Corporation Method of preparing the granular green tea powder
CN103931823A (en) * 2013-01-22 2014-07-23 青岛市市立医院 Pomegranate leaf granular tea and preparation method thereof
CN103168887A (en) * 2013-03-25 2013-06-26 无锡爱迪信光电科技有限公司 Method for preparing maca tea bag
CN103828965A (en) * 2014-02-28 2014-06-04 徐星航 Compound black tea granules and preparation method thereof
CN105594924A (en) * 2015-12-18 2016-05-25 信宜市四海永丰现代种养场 Natural moringa tea preparation method

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107348489A (en) * 2017-07-27 2017-11-17 贵阳学院 Moringa superfine powder, tablet, the preparation method of chewable tablets
CN108771074A (en) * 2018-05-17 2018-11-09 广西柳州市桑辰科技有限公司 A kind of production method of moringa seeds solid beverage
CN108771074B (en) * 2018-05-17 2021-08-31 广西贺州市桑辰科技有限公司 Preparation method of moringa seed solid beverage

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