CN106634617A - Preparation method of high-stability polishing agent - Google Patents
Preparation method of high-stability polishing agent Download PDFInfo
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- CN106634617A CN106634617A CN201610990466.XA CN201610990466A CN106634617A CN 106634617 A CN106634617 A CN 106634617A CN 201610990466 A CN201610990466 A CN 201610990466A CN 106634617 A CN106634617 A CN 106634617A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
The invention relates to a preparation method of a high-stability polishing agent, belonging to the technical field of polishing agent preparation. The method comprises the following steps: heating fresh beeswax and a potassium hydroxide ethanol solution under reflux, dropwisely adding a calcium chloride solution into the mixed reflux solution, heating, carrying out vacuum filtration, drying, extracting with acetone, and collecting the beeswax extract, wherein the combination degree and stability of the polishing agent components are enhanced; and mixing propanol, ethyl orthosilicate and the like with isopropanol, and collecting the silicon-doping aluminum oxide powder. Since the silicon-doped aluminum oxide powder has higher specific area and higher stability, the beeswax extract permeates into the pores of the silicon-doped aluminum oxide powder in the compounding process of the silicon-doped aluminum oxide powder and beeswax extract, thereby inhibiting the dispersity of the composite polishing agent, enhancing the structural stability of the polishing agent, and effectively overcoming the defect of stratification after long-time standing. The high-stability polishing agent has favorable polishing effect, and can be widely used in the fields of vehicles, house appliances and the like.
Description
Technical field
The present invention relates to a kind of preparation method of high stability polisher, belongs to polisher preparing technical field.
Background technology
Polisher is for vehicle（Automobile, motorcycle, bicycle etc.）And housed device（Such as refrigerator, washing machine, various families
Electrical appliance and furniture, floor etc.）Paint film and electrodeposited coating surface decontamination, glazing and protection a kind of milky or transparence it is molten
Liquid.
For a long time, people have been used up traditional wiping method and carry out cleaning and polishing to body surface, i.e., first to needing
The body surface to be wiped carries out clear water and rinses, and uses cloth to wipe with and wipes, and is then waxed in its surface with wax polish, throws Jing after Exposure to Sunlight
Light, the whole operation that wipes need to be carried out one by one.The method not only consumes substantial amounts of clear water, and increases the labour intensity of people.Wipe
Bright dose of appearance then changes the traditional wiping method of people.Due to polisher collection cleaning agent, glazing agent, antirust agent, antistatic
Agent makes the operations such as cleaning once complete in one, alleviates the labour intensity of people, has saved physical resources, adapts to modernization
The needs of life.With the improvement of people's living standards, people increase the demand of polisher increasingly, are greatly promoted wiping
The research and development of bright dose of project.
At present polisher is usually creamy product, is mainly made up of solvent, emulsifying agent, brightener, grinding agent etc., such product
The maximum shortcoming of product is that stability is bad, is long placed in easily layering, simultaneously because brightener, grinding agent raw material select inappropriate, it is past
It is not good enough toward brightness effect, so preparing, a kind of stability is strong, wipe the good polisher of polishing effect particularly important.
The content of the invention
The technical problem to be solved：It is bad for traditional polisher stability, it is long placed in easily layering, and light
The problem of bright less effective, there is provided a kind of by extracting to beeswax, collects its emulsification wax, then with silicon doped aluminium
Powder is combined the method for preparing polisher, and the present invention is first heated to reflux fresh beeswax and potassium hydroxide-ethanol solution
Afterwards, calcium chloride solution, heated, suction filtration and drying are added dropwise in mixing phegma, then with acetone extraction, are collected beeswax and is extracted
Thing, strengthens conjugation and stability between each polisher component, after then mixing with isopropanol with materials such as propyl alcohol, tetraethyl orthosilicates
Calcining, collects silicon doped aluminium powder, because silicon doped aluminium powder has higher specific surface area and stronger stablizes
Performance, is being carried out in recombination process with above-mentioned beeswax extract, and beeswax extract is infiltrated in doped aluminium powder hole, suppression
The dispersiveness of the compound polisher of system, improves polisher structural stability can, and it is long placed in the defect of layering to effectively solving, polishes effect
It is good, can be widely applied to the fields such as vehicle and housed device.
To solve above-mentioned technical problem, the technical solution used in the present invention is：
（1）In mass ratio 1:10, fresh beeswax is mixed with the stirring of the potassium hydroxide-ethanol solution of mass fraction 5%, at 80～90 DEG C
25～30min of lower heating water bath, continues thereafter with and is heated to backflow, insulation 1～2h of backflow, and after the completion of waiting to flow back, collecting to mix
Phegma, in mass ratio 1:5, the calcium chloride solution of mass fraction 5% is dropped in mixing phegma, it is incubated at 75～80 DEG C
1～2h of heating, subsequently stops heating and standing being cooled to room temperature, and suction filtration simultaneously collects filter cake, and vacuum freeze drying is collected dry
Filter cake；
（2）In mass ratio 1:8, the dry cake of above-mentioned preparation is mixed with acetone stirring, the heating water bath 45 at 45～50 DEG C
～60min, subsequently stands and is cooled to room temperature, and suction filtration simultaneously collects filtrate, filtrate rotated at 95～100 DEG C and is evaporated to original volume
1/10, be prepared into beeswax extract concentrate, it is standby；
（3）Count by weight, 15～20 parts of propyl alcohol, 3～5 parts of tetraethyl orthosilicates, 2～3 parts of ethene-vinyl acetates are weighed respectively
Copolymer, 20～25 parts of absolute ethyl alcohols and 1～2 part of sulfuric acid of mass concentration 98% are placed in beaker, and stirring mixing juxtaposition is at room temperature
10～12h of ageing, is prepared into mixed liquor；
（4）In mass ratio 1:3, aluminium isopropoxide is mixed with the mixed liquor stirring of above-mentioned preparation, then under 800～1000r/min
Stirring 6～8h of mixing, subsequently still aging 20～24h, collects to obtain aqueous precursor gel liquid, aqueous precursor gel liquid is placed in into 150～
25～30min is dried in 200 DEG C of Muffle furnaces, subsequently 800～1000 DEG C is warming up to by 10 DEG C/min, after insulation 1～2h of calcining, is stopped
Only heat, standing is cooled to room temperature, collect dry particle and milled 120 mesh sieve, obtain silicon doped aluminium powder；
（5）Count by weight, silicon doped aluminium powder, 10～15 parts of steps of 45～50 parts of above-mentioned preparations are weighed respectively
（2）The beeswax of preparation extracts concentrate, 1～2 part of oleic acid, 2～3 parts of paraffin oils, 1～2 part of polyacrylamide and 1～2 part of second two
Alcohol is placed in dispersion tank, 1～2h of polishing dispersion under 1500～2000r/min, and the mesh sieve of subsequent mistake 200 simultaneously collects filtrate, in room
Still aging 6～8h under temperature, you can be prepared into a kind of high stability polisher.
The application process of the present invention：High stability polisher prepared by the present invention is sprayed in furniture surface spot, is treated
After furniture surface moistening, 3～5min is stood, and wiped back and forth 2～3 times with scouring pad, finally dried with dry wipe.Jing is examined
Survey, compared with traditional polisher, high stability polisher wiping effect prepared by the present invention is good, wipes caudacoria laying dust amount and is less than
4mg/cm2, furniture surface light is as new, and service life extends 4～5 months, product use and preserve during without lamination,
Good stability.
Compared with additive method, Advantageous Effects are the present invention：
（1）Compared with traditional polisher, service life extends 4～5 months to high stability polisher prepared by the present invention, is difficult
Layering, good stability；
（2）High stability polisher wiping effect prepared by the present invention is good, by wiping thing surface-brightening as newly, wiped caudacoria laying dust amount
Less than 4mg/cm2。
Specific embodiment
First in mass ratio 1:10, fresh beeswax is mixed with the stirring of the potassium hydroxide-ethanol solution of mass fraction 5%, 80
25～30min of heating water bath at～90 DEG C, continues thereafter with and is heated to backflow, insulation 1～2h of backflow, after the completion of waiting to flow back, collects
Must mix phegma, in mass ratio 1:5, the calcium chloride solution of mass fraction 5% is dropped in mixing phegma, at 75～80 DEG C
1～2h of lower Heat preservation, subsequently stops heating and standing being cooled to room temperature, and suction filtration simultaneously collects filter cake, and vacuum freeze drying is collected
Obtain dry cake；In mass ratio 1:8, the dry cake of above-mentioned preparation is mixed with acetone stirring, the water-bath at 45～50 DEG C adds
45～60min of heat, subsequently stands and is cooled to room temperature, and suction filtration simultaneously collects filtrate, filtrate rotated at 95～100 DEG C and is evaporated to original
The 1/10 of volume, is prepared into beeswax and extracts concentrate, standby；Then count by weight, weigh respectively 15～20 parts of propyl alcohol, 3
～5 parts of tetraethyl orthosilicates, 2～3 parts of ethylene-vinyl acetate copolymers, 20～25 parts of absolute ethyl alcohols and 1～2 part of mass concentration 98%
Sulfuric acid is placed in beaker, and stirring mixing juxtaposition is aged at room temperature 10～12h, is prepared into mixed liquor；In mass ratio 1:3, will be different
Aluminium propoxide mixes with the mixed liquor stirring of above-mentioned preparation, then 6～8h of stirring mixing under 800～1000r/min, subsequently stands old
Change 20～24h, collect to obtain aqueous precursor gel liquid, by aqueous precursor gel liquid be placed in 150～200 DEG C of Muffle furnaces be dried 25～
30min, is subsequently warming up to 800～1000 DEG C by 10 DEG C/min, after insulation 1～2h of calcining, stops heating, and standing is cooled to room
Temperature, collects dry particle and milled 120 mesh sieve, obtains silicon doped aluminium powder；Finally count by weight, 45 are weighed respectively
The silicon doped aluminium powder of～50 parts of above-mentioned preparations, the beeswax of 10～15 parts of preparations extract concentrate, 1～2 part of oleic acid, 2～3
Part paraffin oil, 1～2 part of polyacrylamide and 1～2 part of ethylene glycol are placed in dispersion tank, the polishing point under 1500～2000r/min
1～2h is dissipated, the mesh sieve of subsequent mistake 200 simultaneously collects filtrate, at room temperature still aging 6～8h, you can be prepared into a kind of high stability
Polisher.
Example 1
First in mass ratio 1:10, fresh beeswax is mixed with the stirring of the potassium hydroxide-ethanol solution of mass fraction 5%, at 90 DEG C
Heating water bath 30min, continues thereafter with and is heated to backflow, insulation backflow 2h, and after the completion of waiting to flow back, collecting must mix phegma, press
Mass ratio 1:5, the calcium chloride solution of mass fraction 5% is dropped in mixing phegma, Heat preservation 2h, subsequently stops at 80 DEG C
Only heat and stand and be cooled to room temperature, suction filtration simultaneously collects filter cake, and vacuum freeze drying collects to obtain dry cake；In mass ratio 1:8,
The dry cake of above-mentioned preparation is mixed with acetone stirring, the heating water bath 60min at 50 DEG C, subsequently stands and be cooled to room temperature,
Suction filtration simultaneously collects filtrate, filtrate is rotated at 100 DEG C and is evaporated to the 1/10 of original volume, is prepared into beeswax and extracts concentrate, standby
With；Then count by weight, weigh respectively 20 parts of propyl alcohol, 5 parts of tetraethyl orthosilicates, 3 parts of ethylene-vinyl acetate copolymers, 25
Part absolute ethyl alcohol and 2 parts of sulfuric acid of mass concentration 98% are placed in beaker, and stirring mixing juxtaposition is aged at room temperature 12h, is prepared into mixed
Close liquid；In mass ratio 1:3, aluminium isopropoxide is mixed with the mixed liquor stirring of above-mentioned preparation, then the stirring mixing under 1000r/min
8h, subsequently still aging 24h, collects to obtain aqueous precursor gel liquid, aqueous precursor gel liquid is placed in 200 DEG C of Muffle furnaces and is dried
30min, is subsequently warming up to 1000 DEG C by 10 DEG C/min, after insulation calcining 2h, stops heating, and standing is cooled to room temperature, collects dry
Dry particle and milled 120 mesh sieve, obtain silicon doped aluminium powder；Finally count by weight, 50 parts of above-mentioned systems are weighed respectively
Standby silicon doped aluminium powder, 15 parts of beeswaxs extraction concentrate, 2 parts of oleic acid, 3 parts of paraffin oils, 2 parts of polyacrylamides for preparing
It is placed in dispersion tank with 2 parts of ethylene glycol, the polishing dispersion 2h under 2000r/min, the mesh sieve of subsequent mistake 200 simultaneously collects filtrate, in room
Still aging 8h under temperature, you can be prepared into a kind of high stability polisher.
High stability polisher prepared by the present invention is sprayed in furniture surface spot, it is quiet after furniture surface moistening
5min is put, and is wiped back and forth 3 times with scouring pad, finally dried with dry wipe.After testing, compared with traditional polisher,
High stability polisher wiping effect prepared by the present invention is good, wipes caudacoria laying dust amount for 3.8mg/cm2, furniture surface light is such as
Newly, and service life extend 5 months, there is not lamination, good stability.
Example 2
First in mass ratio 1:10, fresh beeswax is mixed with the stirring of the potassium hydroxide-ethanol solution of mass fraction 5%, at 80 DEG C
Heating water bath 25min, continues thereafter with and is heated to backflow, insulation backflow 1h, and after the completion of waiting to flow back, collecting must mix phegma, press
Mass ratio 1:5, the calcium chloride solution of mass fraction 5% is dropped in mixing phegma, Heat preservation 1h, subsequently stops at 75 DEG C
Only heat and stand and be cooled to room temperature, suction filtration simultaneously collects filter cake, and vacuum freeze drying collects to obtain dry cake；In mass ratio 1:8,
The dry cake of above-mentioned preparation is mixed with acetone stirring, the heating water bath 45min at 45 DEG C, subsequently stands and be cooled to room temperature,
Suction filtration simultaneously collects filtrate, filtrate is rotated at 95 DEG C and is evaporated to the 1/10 of original volume, is prepared into beeswax and extracts concentrate, standby
With；Then count by weight, weigh respectively 15 parts of propyl alcohol, 3 parts of tetraethyl orthosilicates, 2 parts of ethylene-vinyl acetate copolymers, 20
Part absolute ethyl alcohol and 1 part of sulfuric acid of mass concentration 98% are placed in beaker, and stirring mixing juxtaposition is aged at room temperature 10h, is prepared into mixed
Close liquid；In mass ratio 1:3, aluminium isopropoxide is mixed with the mixed liquor stirring of above-mentioned preparation, then the stirring mixing under 800r/min
6h, subsequently still aging 20h, collects to obtain aqueous precursor gel liquid, aqueous precursor gel liquid is placed in 150 DEG C of Muffle furnaces and is dried
25min, is subsequently warming up to 800 DEG C by 10 DEG C/min, after insulation calcining 1h, stops heating, and standing is cooled to room temperature, collects drying
Particle and milled 120 mesh sieve, obtain silicon doped aluminium powder；Finally count by weight, 45 parts of above-mentioned preparations are weighed respectively
Silicon doped aluminium powder, 10 parts preparation beeswax extract concentrates, 1 part of oleic acid, 2 parts of paraffin oils, 1 part of polyacrylamide and
1 part of ethylene glycol is placed in dispersion tank, the polishing dispersion 1h under 1500r/min, and the mesh sieve of subsequent mistake 200 simultaneously collects filtrate, in room temperature
Under still aging 6h, you can be prepared into a kind of high stability polisher.
High stability polisher prepared by the present invention is sprayed in furniture surface spot, it is quiet after furniture surface moistening
3min is put, and is wiped back and forth 2 times with scouring pad, finally dried with dry wipe.After testing, compared with traditional polisher,
High stability polisher wiping effect prepared by the present invention is good, wipes caudacoria laying dust amount less than 3.8mg/cm2, furniture surface light
It is such as new, and service life extends 4 months, lamination, good stability does not occur.
Example 3
First in mass ratio 1:10, fresh beeswax is mixed with the stirring of the potassium hydroxide-ethanol solution of mass fraction 5%, at 85 DEG C
Heating water bath 27min, continues thereafter with and is heated to backflow, insulation backflow 1h, and after the completion of waiting to flow back, collecting must mix phegma, press
Mass ratio 1:5, the calcium chloride solution of mass fraction 5% is dropped in mixing phegma, Heat preservation 1h, subsequently stops at 77 DEG C
Only heat and stand and be cooled to room temperature, suction filtration simultaneously collects filter cake, and vacuum freeze drying collects to obtain dry cake；In mass ratio 1:8,
The dry cake of above-mentioned preparation is mixed with acetone stirring, the heating water bath 50min at 47 DEG C, subsequently stands and be cooled to room temperature,
Suction filtration simultaneously collects filtrate, filtrate is rotated at 98 DEG C and is evaporated to the 1/10 of original volume, is prepared into beeswax and extracts concentrate, standby
With；Then count by weight, weigh respectively 17 parts of propyl alcohol, 4 parts of tetraethyl orthosilicates, 2 parts of ethylene-vinyl acetate copolymers, 22
Part absolute ethyl alcohol and 1 part of sulfuric acid of mass concentration 98% are placed in beaker, and stirring mixing juxtaposition is aged at room temperature 11h, is prepared into mixed
Close liquid；In mass ratio 1:3, aluminium isopropoxide is mixed with the mixed liquor stirring of above-mentioned preparation, then the stirring mixing under 900r/min
7h, subsequently still aging 22h, collects to obtain aqueous precursor gel liquid, aqueous precursor gel liquid is placed in 170 DEG C of Muffle furnaces and is dried
27min, is subsequently warming up to 900 DEG C by 10 DEG C/min, after insulation calcining 1h, stops heating, and standing is cooled to room temperature, collects drying
Particle and milled 120 mesh sieve, obtain silicon doped aluminium powder；Finally count by weight, 47 parts of above-mentioned preparations are weighed respectively
Silicon doped aluminium powder, 12 parts preparation beeswax extract concentrates, 1 part of oleic acid, 2 parts of paraffin oils, 2 parts of polyacrylamides and
1 part of ethylene glycol is placed in dispersion tank, the polishing dispersion 2h under 1700r/min, and the mesh sieve of subsequent mistake 200 simultaneously collects filtrate, in room temperature
Under still aging 7h, you can be prepared into a kind of high stability polisher.
High stability polisher prepared by the present invention is sprayed in furniture surface spot, it is quiet after furniture surface moistening
4min is put, and is wiped back and forth 2 times with scouring pad, finally dried with dry wipe.After testing, compared with traditional polisher,
High stability polisher wiping effect prepared by the present invention is good, wipes caudacoria laying dust amount for 3.6mg/cm2, furniture surface light is such as
Newly, and service life extend 5 months, there is not lamination, good stability.
Claims (1)
1. a kind of preparation method of high stability polisher, it is characterised in that concrete preparation process is：
（1）In mass ratio 1:10, fresh beeswax is mixed with the stirring of the potassium hydroxide-ethanol solution of mass fraction 5%, at 80～90 DEG C
25～30min of lower heating water bath, continues thereafter with and is heated to backflow, insulation 1～2h of backflow, and after the completion of waiting to flow back, collecting to mix
Phegma, in mass ratio 1:5, the calcium chloride solution of mass fraction 5% is dropped in mixing phegma, it is incubated at 75～80 DEG C
1～2h of heating, subsequently stops heating and standing being cooled to room temperature, and suction filtration simultaneously collects filter cake, and vacuum freeze drying is collected dry
Filter cake；
（2）In mass ratio 1:8, the dry cake of above-mentioned preparation is mixed with acetone stirring, the heating water bath 45 at 45～50 DEG C
～60min, subsequently stands and is cooled to room temperature, and suction filtration simultaneously collects filtrate, filtrate rotated at 95～100 DEG C and is evaporated to original volume
1/10, be prepared into beeswax extract concentrate, it is standby；
（3）Count by weight, 15～20 parts of propyl alcohol, 3～5 parts of tetraethyl orthosilicates, 2～3 parts of ethene-vinyl acetates are weighed respectively
Copolymer, 20～25 parts of absolute ethyl alcohols and 1～2 part of sulfuric acid of mass concentration 98% are placed in beaker, and stirring mixing juxtaposition is at room temperature
10～12h of ageing, is prepared into mixed liquor；
（4）In mass ratio 1:3, aluminium isopropoxide is mixed with the mixed liquor stirring of above-mentioned preparation, then under 800～1000r/min
Stirring 6～8h of mixing, subsequently still aging 20～24h, collects to obtain aqueous precursor gel liquid, aqueous precursor gel liquid is placed in into 150～
25～30min is dried in 200 DEG C of Muffle furnaces, subsequently 800～1000 DEG C is warming up to by 10 DEG C/min, after insulation 1～2h of calcining, is stopped
Only heat, standing is cooled to room temperature, collect dry particle and milled 120 mesh sieve, obtain silicon doped aluminium powder；
（5）Count by weight, silicon doped aluminium powder, 10～15 parts of steps of 45～50 parts of above-mentioned preparations are weighed respectively
（2）The beeswax of preparation extracts concentrate, 1～2 part of oleic acid, 2～3 parts of paraffin oils, 1～2 part of polyacrylamide and 1～2 part of second two
Alcohol is placed in dispersion tank, 1～2h of polishing dispersion under 1500～2000r/min, and the mesh sieve of subsequent mistake 200 simultaneously collects filtrate, in room
Still aging 6～8h under temperature, you can be prepared into a kind of high stability polisher.
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| CN201610990466.XA CN106634617B (en) | 2016-11-10 | 2016-11-10 | A kind of preparation method of high stability polisher |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104046245A (en) * | 2014-06-11 | 2014-09-17 | 泰安麦丰新材料科技有限公司 | Manufacturing method of silicon-aluminum composite polishing solution |
| CN104513616A (en) * | 2013-09-27 | 2015-04-15 | 青岛蓝农谷农产品研究开发有限公司 | Environment-friendly stable leather finishing wax |
| CN105951103A (en) * | 2016-05-27 | 2016-09-21 | 郑旭彬 | Polishing paste for metal rear cover of tablet computer and production technology thereof |
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2016
- 2016-11-10 CN CN201610990466.XA patent/CN106634617B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104513616A (en) * | 2013-09-27 | 2015-04-15 | 青岛蓝农谷农产品研究开发有限公司 | Environment-friendly stable leather finishing wax |
| CN104046245A (en) * | 2014-06-11 | 2014-09-17 | 泰安麦丰新材料科技有限公司 | Manufacturing method of silicon-aluminum composite polishing solution |
| CN105951103A (en) * | 2016-05-27 | 2016-09-21 | 郑旭彬 | Polishing paste for metal rear cover of tablet computer and production technology thereof |
Non-Patent Citations (2)
| Title |
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| 翁杰 等: "蜂蜡、糠蜡中三十烷醇的分离提纯及其特性", 《厦门大学学报》 * |
| 贾玉娜: "氧化铝纳米结构纤维的制备及性质", 《中国优秀硕士学位论文全文数据库工程科技I辑》 * |
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Effective date of registration: 20180705 Address after: 050000 the 3-206 shop of world garden 3-206, 46 Donggang Road, Yuhua District, Shijiazhuang, Hebei. Applicant after: Hebei morning morning environment Polytron Technologies Inc Address before: No. 1, Chengyang street, Xushui District, Baoding, Hebei Applicant before: Hebei Chenyang IndustrialL&trade Group Co., Ltd. |
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| GR01 | Patent grant | ||
| GR01 | Patent grant |