CN106634617B - A kind of preparation method of high stability polisher - Google Patents
A kind of preparation method of high stability polisher Download PDFInfo
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- CN106634617B CN106634617B CN201610990466.XA CN201610990466A CN106634617B CN 106634617 B CN106634617 B CN 106634617B CN 201610990466 A CN201610990466 A CN 201610990466A CN 106634617 B CN106634617 B CN 106634617B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/02—Polishing compositions containing abrasives or grinding agents
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
- Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
Abstract
The present invention relates to a kind of preparation methods of high stability polisher, belong to polisher preparing technical field.After fresh beeswax and potassium hydroxide-ethanol solution are heated to reflux by the present invention first, calcium chloride solution is added dropwise in mixing phegma, it is heated, it filters and dry, acetone extraction is used again, collect beeswax extract, enhance conjugation and stability between each polisher component, then with propyl alcohol, the substances such as ethyl orthosilicate are calcined after being mixed with isopropanol, collect silicon doped aluminium powder, since silicon doped aluminium powder has higher specific surface area and stronger stability, with above-mentioned beeswax extract carry out recombination process in, beeswax extract infiltrates into doped aluminium powder hole, inhibit the dispersibility of compound polisher, improve polisher structural stability can, it effectively solves it and is long placed in the defect of layering, it is good to polish effect, it can be widely applied to the fields such as vehicle and housed device.
Description
Technical field
The present invention relates to a kind of preparation methods of high stability polisher, belong to polisher preparing technical field.
Background technology
Polisher is to be used for vehicle（Automobile, motorcycle, bicycle etc.）And housed device（Such as refrigerator, washing machine, various families
Electrical appliance and furniture, floor etc.）Paint film and electroplated layer surface decontamination, glazing and protection a kind of milky or transparence it is molten
Liquid.
For a long time, people carry out cleaning and polishing using traditional wiping method to body surface always, i.e., first to needing
The body surface to be wiped carries out clear water and rinses, and uses cloth to wipe with and wipes, and is then waxed with wax polish, is thrown after solarization on the surface thereof
Light, the entire process that wipes need to carry out one by one.This method not only consumes a large amount of clear water, and increases the labor intensity of people.It wipes
Bright dose of appearance then changes the traditional wiping method of people.Due to polisher collection detergent, glazing agent, antirust agent, antistatic
Agent makes the processes such as cleaning once complete in one, alleviates the labor intensity of people, has saved physical resources, adapts to modernization
The needs of life.As the improvement of people's living standards, people increase the demand of polisher increasingly, it is greatly promoted wiping
The research and development of bright dose of project.
Polisher is usually creamy product at present, is mainly made of solvent, emulsifier, brightener, grinding agent etc., such production
Product are maximum the disadvantage is that stability is bad, are long placed in easy layering, simultaneously because the selection of brightener, grinding agent raw material is inappropriate, it is past
Not good enough toward brightness effect, so preparing, a kind of stability is strong, and the good polisher of wiping polishing effect is particularly important.
Invention content
The technical problems to be solved by the invention：It is bad for traditional polisher stability, it is long placed in easy layering, and light
The problem of bright less effective, provide a kind of by being extracted to beeswax, collect its and emulsify wax, then with silicon doped aluminium
Fresh beeswax is heated to reflux by the compound method for preparing polisher of powder, the present invention with potassium hydroxide-ethanol solution first
Afterwards, it is added dropwise calcium chloride solution in mixing phegma, it is heated, filter and dry, then acetone extraction is used, it collects beeswax and extracts
Object enhances conjugation and stability between each polisher component, after then being mixed with isopropanol with substances such as propyl alcohol, ethyl orthosilicates
Silicon doped aluminium powder is collected in calcining, since silicon doped aluminium powder has higher specific surface area and stronger stabilization
Performance, in carrying out recombination process with above-mentioned beeswax extract, beeswax extract infiltrates into doped aluminium powder hole, suppression
The dispersibility of compound polisher is made, polisher structural stability can is improved, effectively solves it and be long placed in the defect of layering, polish effect
It is good, it can be widely applied to the fields such as vehicle and housed device.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
（1）In mass ratio 1:10, fresh beeswax and 5% potassium hydroxide-ethanol solution of mass fraction are stirred, 80~
25~30min of heating water bath at 90 DEG C, continues thereafter with and is heated to flowing back, and heat preservation 1~2h of reflux is waited after the completion of flowing back, collected
Mixing phegma, in mass ratio 1:5,5% calcium chloride solution of mass fraction is added dropwise in mixing phegma, at 75~80 DEG C
1~2h of Heat preservation then stops heating and standing being cooled to room temperature, filters and collect filter cake, vacuum freeze drying is collected
Dry cake；
（2）In mass ratio 1:8, the dry cake of above-mentioned preparation is stirred with acetone, at 45~50 DEG C water-bath add
45~60min of heat then stands and is cooled to room temperature, filters and collect filtrate, filtrate is rotated at 95~100 DEG C and is evaporated to original
The 1/10 of volume is prepared into beeswax extraction concentrate, spare；
（3）It counts in parts by weight, weighs 15~20 parts of propyl alcohol, 3~5 parts of ethyl orthosilicates, 2~3 parts of ethyl vinyl acetates respectively
Ethylene copolymer, 20~25 parts of absolute ethyl alcohols and 1~2 part of 98% sulfuric acid of mass concentration are placed in beaker, are stirred and are placed in room
Temperature is lower to be aged 10~12h, is prepared into mixed liquor；
（4）In mass ratio 1:3, aluminium isopropoxide and the mixed liquor of above-mentioned preparation are stirred, then in 800~1000r/
It is stirred 6~8h under min, subsequent still aging 20~for 24 hours, aqueous precursor gel liquid is collected to obtain, aqueous precursor gel liquid is placed in
Dry 25~30min in 150~200 DEG C of Muffle furnaces is then warming up to 800~1000 DEG C, 1~2h of heat preservation calcining by 10 DEG C/min
Afterwards, stop heating, standing is cooled to room temperature, and collects dry particle and milled 120 mesh sieves, obtain silicon doped aluminium powder；
（5）It counts in parts by weight, respectively the silicon doped aluminium powder of 45~50 parts of above-mentioned preparations of weighing, 10~15 parts of steps
Suddenly（2）Beeswax extraction concentrate, 1~2 part of oleic acid, 2~3 parts of paraffin oils, 1~2 part of polyacrylamide and 1~2 part of second of preparation
Glycol is placed in dispersion tank, and 1~2h of polishing dispersion, 200 mesh of subsequent mistake sieve and collect filtrate at 1500~2000r/min,
Still aging 6~8h at room temperature, you can be prepared into a kind of high stability polisher.
The application process of the present invention：High stability polisher prepared by the present invention is sprayed in furniture surface spot, is waited for
After furniture surface moistening, 3~5min is stood, is used in combination scouring pad to wipe back and forth 2~3 times, is finally dried with dry wipe.Through inspection
It surveys, compared with traditional polisher, high stability polisher wiping effect prepared by the present invention is good, wipes caudacoria dust accumulation amount and is less than
4mg/cm2, furniture surface light is for example new, and service life extends 4~5 months, product use and preserve during without lamination,
Stability is good.
Compared with other methods, advantageous effects are the present invention：
（1）For high stability polisher prepared by the present invention compared with traditional polisher, service life extends 4~5 months,
It is not easy to be layered, stability is good；
（2）High stability polisher wiping effect prepared by the present invention is good, for example new by wiping object surface-brightening, wipes caudacoria product
Dust quantity is less than 4mg/cm2。
Specific implementation mode
First in mass ratio 1:10, fresh beeswax and 5% potassium hydroxide-ethanol solution of mass fraction are stirred, 80
25~30min of heating water bath at~90 DEG C, continues thereafter with and is heated to flowing back, and heat preservation 1~2h of reflux is waited after the completion of flowing back, collected
Phegma, in mass ratio 1 must be mixed:5,5% calcium chloride solution of mass fraction is added dropwise in mixing phegma, at 75~80 DEG C
1~2h of lower Heat preservation then stops heating and standing being cooled to room temperature, filters and collect filter cake, and vacuum freeze drying is collected
Obtain dry cake；In mass ratio 1:8, the dry cake of above-mentioned preparation is stirred with acetone, at 45~50 DEG C water-bath add
45~60min of heat then stands and is cooled to room temperature, filters and collect filtrate, filtrate is rotated at 95~100 DEG C and is evaporated to original
The 1/10 of volume is prepared into beeswax extraction concentrate, spare；Then it counts in parts by weight, weighs 15~20 parts of propyl alcohol, 3 respectively
~5 parts of ethyl orthosilicates, 2~3 parts of ethylene-vinyl acetate copolymers, 20~25 parts of absolute ethyl alcohols and 1~2 part of mass concentration 98%
Sulfuric acid is placed in beaker, is stirred juxtaposition and is aged 10~12h at room temperature, is prepared into mixed liquor；In mass ratio 1:3, it will be different
Aluminium propoxide and the mixed liquor of above-mentioned preparation are stirred, then 6~8h is stirred at 800~1000r/min, are then stood old
Change 20~for 24 hours, aqueous precursor gel liquid is collected to obtain, aqueous precursor gel liquid is placed in 150~200 DEG C of Muffle furnaces dry 25~
30min is then warming up to 800~1000 DEG C, after 1~2h is calcined in heat preservation by 10 DEG C/min, stops heating, and standing is cooled to room
Temperature, collects dry particle and milled 120 mesh sieves, and obtains silicon doped aluminium powder；It finally counts in parts by weight, weighs 45 respectively
The silicon doped aluminium powder of~50 parts of above-mentioned preparations, 10~15 parts of beeswaxs prepared extract concentrate, 1~2 part of oleic acid, 2~3
Part paraffin oil, 1~2 part of polyacrylamide and 1~2 part of ethylene glycol are placed in dispersion tank, the polishing point at 1500~2000r/min
1~2h is dissipated, 200 mesh of subsequent mistake sieves and collect filtrate, at room temperature still aging 6~8h, you can is prepared into a kind of high stability
Polisher.
Example 1
First in mass ratio 1:10, fresh beeswax and 5% potassium hydroxide-ethanol solution of mass fraction are stirred, 90
Heating water bath 30min at DEG C is continued thereafter with and is heated to flowing back, and heat preservation reflux 2h is waited after the completion of flowing back, and collects to obtain mixing reflux
Liquid, in mass ratio 1:5,5% calcium chloride solution of mass fraction is added dropwise in mixing phegma, the Heat preservation 2h at 80 DEG C, with
Stop heating and standing afterwards being cooled to room temperature, filters and collect filter cake, vacuum freeze drying collects to obtain dry cake；In mass ratio
1:8, the dry cake of above-mentioned preparation is stirred, the heating water bath 60min at 50 DEG C with acetone, then stands and be cooled to room
Temperature filters and collects filtrate, and filtrate is rotated at 100 DEG C and is evaporated to the 1/10 of original volume, is prepared into beeswax extraction concentrate,
It is spare；Then count in parts by weight, respectively weigh 20 parts of propyl alcohol, 5 parts of ethyl orthosilicates, 3 parts of ethylene-vinyl acetate copolymers,
25 parts of absolute ethyl alcohols and 2 parts of 98% sulfuric acid of mass concentration are placed in beaker, are stirred juxtaposition and are aged 12h at room temperature, are prepared into
Mixed liquor；In mass ratio 1:3, aluminium isopropoxide and the mixed liquor of above-mentioned preparation are stirred, then stir and mix at 1000r/min
8h is closed, it is then still aging to collect to obtain aqueous precursor gel liquid for 24 hours, aqueous precursor gel liquid is placed in 200 DEG C of Muffle furnaces dry
30min is then warming up to 1000 DEG C, after 2h is calcined in heat preservation by 10 DEG C/min, stops heating, and standing is cooled to room temperature, and collects dry
Dry particle and milled 120 mesh sieve, obtain silicon doped aluminium powder；It finally counts in parts by weight, weighs 50 parts of above-mentioned systems respectively
The beeswax of standby silicon doped aluminium powder, 15 parts of preparations extracts concentrate, 2 parts of oleic acid, 3 parts of paraffin oils, 2 parts of polyacrylamides
It is placed in dispersion tank with 2 parts of ethylene glycol, the polishing dispersion 2h at 2000r/min, 200 mesh of subsequent mistake sieves and collect filtrate, in room
Still aging 8h under temperature, you can be prepared into a kind of high stability polisher.
High stability polisher prepared by the present invention is sprayed in furniture surface spot, it is quiet after furniture surface moistening
5min is set, is used in combination scouring pad to wipe back and forth 3 times, is finally dried with dry wipe.After testing, compared with traditional polisher,
High stability polisher wiping effect prepared by the present invention is good, and it is 3.8mg/cm to wipe caudacoria dust accumulation amount2, furniture surface light is such as
Newly, and service life extends 5 months, does not occur lamination, stability is good.
Example 2
First in mass ratio 1:10, fresh beeswax and 5% potassium hydroxide-ethanol solution of mass fraction are stirred, 80
Heating water bath 25min at DEG C is continued thereafter with and is heated to flowing back, and heat preservation reflux 1h is waited after the completion of flowing back, and collects to obtain mixing reflux
Liquid, in mass ratio 1:5,5% calcium chloride solution of mass fraction is added dropwise in mixing phegma, the Heat preservation 1h at 75 DEG C, with
Stop heating and standing afterwards being cooled to room temperature, filters and collect filter cake, vacuum freeze drying collects to obtain dry cake；In mass ratio
1:8, the dry cake of above-mentioned preparation is stirred, the heating water bath 45min at 45 DEG C with acetone, then stands and be cooled to room
Temperature filters and collects filtrate, and filtrate is rotated at 95 DEG C and is evaporated to the 1/10 of original volume, is prepared into beeswax extraction concentrate,
It is spare；Then count in parts by weight, respectively weigh 15 parts of propyl alcohol, 3 parts of ethyl orthosilicates, 2 parts of ethylene-vinyl acetate copolymers,
20 parts of absolute ethyl alcohols and 1 part of 98% sulfuric acid of mass concentration are placed in beaker, are stirred juxtaposition and are aged 10h at room temperature, are prepared into
Mixed liquor；In mass ratio 1:3, aluminium isopropoxide and the mixed liquor of above-mentioned preparation are stirred, then stir and mix at 800r/min
6h is closed, subsequent still aging 20h collects to obtain aqueous precursor gel liquid, aqueous precursor gel liquid is placed in 150 DEG C of Muffle furnaces dry
25min is then warming up to 800 DEG C, after 1h is calcined in heat preservation by 10 DEG C/min, stops heating, and standing is cooled to room temperature, and collects drying
Particle and milled 120 mesh sieve, obtain silicon doped aluminium powder；It finally counts in parts by weight, weighs 45 parts of above-mentioned preparations respectively
Silicon doped aluminium powder, 10 parts preparation beeswaxs extraction concentrate, 1 part of oleic acid, 2 parts of paraffin oils, 1 part of polyacrylamide and
1 part of ethylene glycol is placed in dispersion tank, and the polishing dispersion 1h at 1500r/min, 200 mesh of subsequent mistake sieves and collect filtrate, in room temperature
Under still aging 6h, you can be prepared into a kind of high stability polisher.
High stability polisher prepared by the present invention is sprayed in furniture surface spot, it is quiet after furniture surface moistening
3min is set, is used in combination scouring pad to wipe back and forth 2 times, is finally dried with dry wipe.After testing, compared with traditional polisher,
High stability polisher wiping effect prepared by the present invention is good, wipes caudacoria dust accumulation amount and is less than 3.8mg/cm2, furniture surface light
As new, and service life extends 4 months, does not occur lamination, stability is good.
Example 3
First in mass ratio 1:10, fresh beeswax and 5% potassium hydroxide-ethanol solution of mass fraction are stirred, 85
Heating water bath 27min at DEG C is continued thereafter with and is heated to flowing back, and heat preservation reflux 1h is waited after the completion of flowing back, and collects to obtain mixing reflux
Liquid, in mass ratio 1:5,5% calcium chloride solution of mass fraction is added dropwise in mixing phegma, the Heat preservation 1h at 77 DEG C, with
Stop heating and standing afterwards being cooled to room temperature, filters and collect filter cake, vacuum freeze drying collects to obtain dry cake；In mass ratio
1:8, the dry cake of above-mentioned preparation is stirred, the heating water bath 50min at 47 DEG C with acetone, then stands and be cooled to room
Temperature filters and collects filtrate, and filtrate is rotated at 98 DEG C and is evaporated to the 1/10 of original volume, is prepared into beeswax extraction concentrate,
It is spare；Then count in parts by weight, respectively weigh 17 parts of propyl alcohol, 4 parts of ethyl orthosilicates, 2 parts of ethylene-vinyl acetate copolymers,
22 parts of absolute ethyl alcohols and 1 part of 98% sulfuric acid of mass concentration are placed in beaker, are stirred juxtaposition and are aged 11h at room temperature, are prepared into
Mixed liquor；In mass ratio 1:3, aluminium isopropoxide and the mixed liquor of above-mentioned preparation are stirred, then stir and mix at 900r/min
7h is closed, subsequent still aging 22h collects to obtain aqueous precursor gel liquid, aqueous precursor gel liquid is placed in 170 DEG C of Muffle furnaces dry
27min is then warming up to 900 DEG C, after 1h is calcined in heat preservation by 10 DEG C/min, stops heating, and standing is cooled to room temperature, and collects drying
Particle and milled 120 mesh sieve, obtain silicon doped aluminium powder；It finally counts in parts by weight, weighs 47 parts of above-mentioned preparations respectively
Silicon doped aluminium powder, 12 parts preparation beeswaxs extraction concentrate, 1 part of oleic acid, 2 parts of paraffin oils, 2 parts of polyacrylamides and
1 part of ethylene glycol is placed in dispersion tank, and the polishing dispersion 2h at 1700r/min, 200 mesh of subsequent mistake sieves and collect filtrate, in room temperature
Under still aging 7h, you can be prepared into a kind of high stability polisher.
High stability polisher prepared by the present invention is sprayed in furniture surface spot, it is quiet after furniture surface moistening
4min is set, is used in combination scouring pad to wipe back and forth 2 times, is finally dried with dry wipe.After testing, compared with traditional polisher,
High stability polisher wiping effect prepared by the present invention is good, and it is 3.6mg/cm to wipe caudacoria dust accumulation amount2, furniture surface light is such as
Newly, and service life extends 5 months, does not occur lamination, stability is good.
Claims (1)
1. a kind of preparation method of high stability polisher, it is characterised in that specifically preparation process is：
（1）In mass ratio 1:10, fresh beeswax and 5% potassium hydroxide-ethanol solution of mass fraction are stirred, at 80~90 DEG C
25~30min of lower heating water bath, continues thereafter with and is heated to flowing back, and heat preservation 1~2h of reflux waits after the completion of flowing back, collects to obtain mixing
Phegma, in mass ratio 1:5,5% calcium chloride solution of mass fraction is added dropwise in mixing phegma, is kept the temperature at 75~80 DEG C
1~2h is heated, then stops heating and standing being cooled to room temperature, filters and collect filter cake, vacuum freeze drying is collected dry
Filter cake；
（2）In mass ratio 1:8, the dry cake of above-mentioned preparation is stirred with acetone, the heating water bath 45 at 45~50 DEG C
~60min then stands and is cooled to room temperature, filters and collect filtrate, filtrate is rotated at 95~100 DEG C and is evaporated to original volume
1/10, be prepared into beeswax extraction concentrate, it is spare；
（3）It counts in parts by weight, weighs 15~20 parts of propyl alcohol, 3~5 parts of ethyl orthosilicates, 2~3 parts of ethene-vinyl acetates respectively
Copolymer, 20~25 parts of absolute ethyl alcohols and 1~2 part of 98% sulfuric acid of mass concentration are placed in beaker, are stirred juxtaposition at room temperature
It is aged 10~12h, is prepared into mixed liquor；
（4）In mass ratio 1:3, aluminium isopropoxide and the mixed liquor of above-mentioned preparation are stirred, then at 800~1000r/min
It is stirred 6~8h, then still aging 20~for 24 hours, collects to obtain aqueous precursor gel liquid, aqueous precursor gel liquid is placed in 150~
Dry 25~30min in 200 DEG C of Muffle furnaces, is then warming up to 800~1000 DEG C by 10 DEG C/min, after 1~2h is calcined in heat preservation, stops
It only heats, standing is cooled to room temperature, and collects dry particle and milled 120 mesh sieves, obtain silicon doped aluminium powder；
（5）It counts in parts by weight, respectively the silicon doped aluminium powder of 45~50 parts of above-mentioned preparations of weighing, 10~15 parts of steps
（2）Beeswax extraction concentrate, 1~2 part of oleic acid, 2~3 parts of paraffin oils, 1~2 part of polyacrylamide and 1~2 part of second two of preparation
Alcohol is placed in dispersion tank, and 1~2h of polishing dispersion at 1500~2000r/min, 200 mesh of subsequent mistake sieves and collect filtrate, in room
Still aging 6~8h under temperature, you can be prepared into a kind of high stability polisher.
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| CN201610990466.XA CN106634617B (en) | 2016-11-10 | 2016-11-10 | A kind of preparation method of high stability polisher |
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| CN104513616B (en) * | 2013-09-27 | 2018-07-10 | 青岛博研达工业技术研究所(普通合伙) | Leather finish wax is stablized in a kind of environmental protection |
| CN104046245B (en) * | 2014-06-11 | 2016-03-09 | 泰安麦丰新材料科技有限公司 | A kind of manufacture method of sial composite polishing liquid |
| CN105951103A (en) * | 2016-05-27 | 2016-09-21 | 郑旭彬 | Polishing paste for metal rear cover of tablet computer and production technology thereof |
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