CN107164763A - A kind of preparation method of metal polish - Google Patents
A kind of preparation method of metal polish Download PDFInfo
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- CN107164763A CN107164763A CN201710337165.1A CN201710337165A CN107164763A CN 107164763 A CN107164763 A CN 107164763A CN 201710337165 A CN201710337165 A CN 201710337165A CN 107164763 A CN107164763 A CN 107164763A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
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Abstract
The invention discloses a kind of preparation method of metal polish, belong to field of metal surface treatment technology.The present invention is raw material first with hawthorn and ethanol solution, it is made after concentrate with petroleum ether etc. through stratification, chlorogenic acid concentrate is made in revolving, self-control sol solutionses and ammonium hydrogen carbonate etc. are centrifuged again, collect after lower sediment washing is dried and mill, obtain and mix scattered after titanic oxide hollow microballoon with chlorogenic acid concentrate, ball milling sieves after revolving again, with sodium salicylate solution etc. mix deaeration after modified titanium dioxide powder modified light stream is made and become liquid, finally again with atoleine, the ultrasonic disperses such as ethylene glycol and standing and defoaming processing, metal polish can be obtained, polishing agent stability of the present invention is good, brightness coverage capability is strong, the feature of environmental protection is good, preferable polishing effect can be played to various complicated metallic articles, and the antirust ability of metallic article can be improved, extend the holding time of metallic article, have broad application prospects.
Description
Technical field
The invention discloses a kind of preparation method of metal polish, belong to field of metal surface treatment technology.
Background technology
The processing method means of Treatment of Metal Surface are varied, such as plating, electrophoresis, chemical treatment, surface polishing.And
Metallic article in use, due to oxidation, the moist or contact reason such as chemical substance and corrosive gas in air, is caused
Surface of metal product corrosion, adheres to foul greasy dirt situation, in order to increase surface of metal product finish, it is often necessary to metal system
Product carry out surface polishing.
Polishing agent is often added during polishing, to improve the brightness of metallic element, and metal surface is cleaned.
Polishing is a kind of burnishing action.Polishing agent " tears " scalping, below one layer keep its mobility within moment, and solidifying
Gu before, and because the effect of surface tension is smoothened, also has and think that polishing is a kind of face surface tension effect, polished
Cheng Zhong, the heat produced for friction can make surface softening melting, so not being simple mechanical grinding.The metal in polishing
Superficial layer is melted, but because substrate metal has high thermal conductivity, superficial layer is promptly frozen into amorphous state again, in solidification
Before, it is smoothened due to surface tension and the effect of the frictional force of polishing agent.
Existing metal polish kind is many, but the solution of most formulations is unstable, and brightness coverage capability is poor, especially multiple
Miscellaneous part or product, exists and returns fast, the halfway phenomenon of cleaning of becoming rusty.In addition, existing chemical polishing agent primary raw material is strong
Acid or phosphate, in polishing process, can produce corrosive gas, certain pollution, unfavorable operation people are caused to working environment
Member's is healthy.It would therefore be highly desirable to develop that a kind of stability is good, brightness coverage capability strong and cleaning effect thoroughly medal polish
Agent product.
The content of the invention
Present invention mainly solves technical problem：Not good, the brightness coverage capability for existing metal polish stability
Difference, there is provided a kind of preparation method of metal polish for the defect undesirable to the cleaning effect of complicated metallic article.
In order to solve the above-mentioned technical problem, the technical solution adopted in the present invention is：
（1）3~5kg hawthorn are taken, are dried and ball milling, 50 mesh sieves is crossed, obtains hawthorn fruit, in mass ratio 1:10, by hawthorn fruit with
Mass fraction mixes for 70% ethanol solution, is filtered to get filtrate after ultrasonic extraction, filtrate rotary evaporation is obtained into concentrate；
（2）In mass ratio 1:5, concentrate is mixed with petroleum ether and is placed in separatory funnel, stratification simultaneously collects subnatant
Body, then by volume 1:5, lower floor's liquid is mixed with ethyl acetate and is placed in separatory funnel, stratification collects subnatant
Phase, by subnatant rotary evaporation, obtains chlorogenic acid concentrate；
（3）450~500mL deionized waters, 100~150mL absolute ethyl alcohols and the stirring of 15~20mL butyl titanates are weighed respectively
Mixing, ultrasonic disperse obtains sol solutionses, in mass ratio 1：1：10, sol solutionses, ammonium hydrogen carbonate are mixed with absolute ethyl alcohol, centrifuged
And collect lower sediment, washing, dry, titanic oxide hollow microballoon of milling to obtain；
（4）In mass ratio 1:5, titanic oxide hollow microballoon is mixed with chlorogenic acid concentrate, ultrasonic disperse obtains mixed dispersion liquid,
Rotary evaporated to dryness obtains dried object and ball milling, crosses 200 mesh sieves, obtains modified titanium dioxide powder, count by weight, weigh respectively
45~50 parts of 0.1mol/L sodium hydroxide solutions, 10~15 parts of modified titanium dioxide powders and 45~50 parts of mass fractions are 0.1%
Sodium salicylate solution stirring mixing, standing and defoaming is prepared into modified light stream and becomes liquid；
（5）Count by weight, 40~50 parts of modified light streams are weighed respectively and become liquid, 10~15 parts of atoleines, 1~2 part of emulsification
Agent OP-10,1~2 part of ethylene glycol, 0.5~1.0 part of dimethyl silicone polymer stirring mixing and ultrasonic disperse, standing and defoaming, you can
It is prepared into a kind of metal polish.
Step（1）Described ultrasonic extraction conditions are the ultrasonic extraction under 200~300W.
Step（2）Described rotating evaporation temperature is 45~50 DEG C.
The beneficial effects of the invention are as follows：
（1）The present invention prepares modified photocatalytic rheology liquid by salicylic acid solution and titanium dioxide granule, and becoming liquid by light stream answers
The vermiculate glues of part formation, and photosensitive material titanium dioxide combination embedded in system, form the intelligent worm of light sensitivity
Shape micelle volume, the material stability formed by its compounding is strong, effectively improves polishing fluid stability；
（2）The present invention becomes liquid by preparing light stream, chlorogenic acid is loaded into the hollow titanium dioxide surface of photochemical catalyst, in polishing fluid
During use, the photochemical catalyst loaded through chlorogenic acid becomes liquid synergy with light stream, during routine use, through ultraviolet light
Catalysis and solidification so that polishing agent after use, in polished metal surface formation diaphragm and can cover metal level, this
Outside, the brightness coverage capability of metal polish is strong, and cleaning is thorough, can effectively delay metal to return rust speed, to fine metal system
Product also have preferable polishing effect, and ensure that the performance of the finish of metal surface.
Embodiment
3~5kg hawthorn are chosen first, by hawthorn vacuum freeze drying and ball milling, are crossed 50 mesh sieves, hawthorn fruit are obtained, by matter
Amount compares 1:10, be that 70% ethanol solution is mixed by hawthorn fruit and mass fraction, under 200~300W ultrasonic extraction 45~
60min, is treated after the completion of ultrasonic extraction, filters to get filtrate, and filtrate is evaporated into filtrate original volume as rotation at 75~80 DEG C
1/5, concentrate is prepared into, then in mass ratio 1:5, concentrate is mixed with petroleum ether and is placed in separatory funnel, stands and divides
Layer simultaneously collects lower floor's liquid, then by volume 1:5, lower floor's liquid is mixed with ethyl acetate and is placed in separatory funnel, is stood
Lower floor's liquid phase is collected in layering, and lower floor's liquid phase is placed in into rotation at 45~50 DEG C is evaporated to the 1/3 of lower floor's liquid phase original volume, is prepared into
Chlorogenic acid concentrate, weighs 450~500mL deionized waters, 100~150mL absolute ethyl alcohols and the fourth of 15~20mL metatitanic acids four respectively
Ester is placed in beaker, and mixing is stirred at room temperature and is placed in 10~15min of ultrasonic disperse under 200~300W, treats that ultrasonic disperse is complete
Cheng Hou, obtains sol solutionses, then in mass ratio 1：1：10, sol solutionses, ammonium hydrogen carbonate are mixed with absolute ethyl alcohol and is placed in reactor,
At 65~70 DEG C after 3~5h of insulation reaction, 10~15min is centrifuged under 2500~3000r/min, lower sediment is collected
And be washed with deionized 3~5 times, the precipitation after washing is placed at 75~80 DEG C and dries 10~12h, mills and is prepared into dioxy
Change titanium tiny balloon, in mass ratio 1:5, titanic oxide hollow microballoon is mixed with chlorogenic acid concentrate, surpassed under 200~300W
Sound disperses after 10~15min, obtains mixed dispersion liquid and is placed in rotary evaporated to dryness at 75~80 DEG C, obtains dried object and ball milling, mistake
200 mesh sieves, are prepared into modified titanium dioxide powder, then count by weight, and it is 0.1mol/L that 45~50 parts of concentration are weighed respectively
Sodium hydroxide solution, 10~15 parts of modified titanium dioxide powders and 45~50 parts of mass fractions be that 0.1% sodium salicylate solution is put
In beaker, magnetic agitation is mixed after 10~12h under 1000~1200r/min, and 20~24h of standing and defoaming is prepared into modification
Light stream becomes liquid, finally counts by weight, and 40~50 parts of modified light streams are weighed respectively and become liquid, 10~15 parts of atoleines, 1~2
Part emulsifier op-10,1~2 part of ethylene glycol, 0.5~1.0 part of dimethyl silicone polymer are placed in three-necked flask, in 200~300W
After 10~15min of lower ultrasonic disperse, 3~5h of standing and defoaming, you can be prepared into a kind of metal polish.
Example 1
3kg hawthorn are chosen first, by hawthorn vacuum freeze drying and ball milling, are crossed 50 mesh sieves, are obtained hawthorn fruit, in mass ratio 1:
10, it is that 70% ethanol solution is mixed by hawthorn fruit and mass fraction, the ultrasonic extraction 45min under 200W treats that ultrasonic extraction is completed
Afterwards, filter to get filtrate, filtrate is evaporated to the 1/5 of filtrate original volume as rotation at 75 DEG C, concentrate is prepared into, then by matter
Amount compares 1:5, concentrate is mixed with petroleum ether and is placed in separatory funnel, stratification simultaneously collects lower floor's liquid, then by volume
Than 1:5, lower floor's liquid is mixed with ethyl acetate and is placed in separatory funnel, stratification collects lower floor's liquid phase, by subnatant
Mutually it is placed in rotation at 45 DEG C and is evaporated to the 1/3 of lower floor's liquid phase original volume, be prepared into chlorogenic acid concentrate, 450mL is weighed respectively and is gone
Ionized water, 100mL absolute ethyl alcohols and 15mL butyl titanates are placed in beaker, and mixing is stirred at room temperature and is placed in surpassing under 200W
Sound disperses 10min, treats after the completion of ultrasonic disperse, obtains sol solutionses, then in mass ratio 1：1：10, by sol solutionses, ammonium hydrogen carbonate and nothing
Water-ethanol mixing is placed in reactor, and at 65 DEG C after insulation reaction 3h, 10min is centrifuged under 2500r/min, is collected
Lower sediment is simultaneously washed with deionized 3 times, and the precipitation after washing is placed at 75 DEG C and dries 10h, mills and is prepared into titanium dioxide
Titanium tiny balloon, in mass ratio 1:5, titanic oxide hollow microballoon is mixed with chlorogenic acid concentrate, the ultrasonic disperse under 250W
After 10min, obtain mixed dispersion liquid and be placed in rotary evaporated to dryness at 75 DEG C, obtain dried object and ball milling, cross 200 mesh sieves, be prepared into
Modified titanium dioxide powder, then count by weight, weigh respectively 45 parts of concentration for 0.1mol/L sodium hydroxide solution, 10 parts
Modified titanium dioxide powder and 45 parts of mass fractions are that 0.1% sodium salicylate solution is placed in beaker, the magnetic force under 1000r/min
After stirring mixing 10h, standing and defoaming 20h is prepared into modified light stream and becomes liquid, finally counts by weight, and weighing 40 parts respectively changes
Property light stream become liquid, 10 parts of atoleines, 1 part of emulsifier op-10,1 part of ethylene glycol, 0.5 part of dimethyl silicone polymer and be placed in three mouthfuls
In flask, under 200W after ultrasonic disperse 10min, standing and defoaming 3h, you can be prepared into a kind of metal polish.
First in mass ratio 1:40, metal polish produced by the present invention is mixed with temperature for 15 DEG C of water stirring
2min, obtains polishing fluid, then puts into polished metal substrate in polishing fluid, is standing and soak for taking out after 3min, then will immersion
Metal substrate afterwards is transferred in baking oven, and 10min is dried under the conditions of temperature is 70 DEG C, is finally taken out metal substrate natural cooling and is
Can.After testing, metal polish polishing effect produced by the present invention is good, and brightness coverage capability is strong, can make the metal system after polishing
Product surface smoothness is up to 10 grades, while polishing agent of the present invention has preferably cleaning anti-rust action, with using traditional polishing agent
Metallic article is compared, and 8 days, and this hair are extended using antirust time limit of the metallic article of polishing agent of the present invention under exposed environments
Preferably, under normal temperature sealed environment, the pot-life is up to 16 months bright polishing agent stability.
Example 2
4kg hawthorn are chosen first, by hawthorn vacuum freeze drying and ball milling, are crossed 50 mesh sieves, are obtained hawthorn fruit, in mass ratio 1:
10, it is that 70% ethanol solution is mixed by hawthorn fruit and mass fraction, the ultrasonic extraction 53min under 250W treats that ultrasonic extraction is completed
Afterwards, filter to get filtrate, filtrate is evaporated to the 1/5 of filtrate original volume as rotation at 78 DEG C, concentrate is prepared into, then by matter
Amount compares 1:5, concentrate is mixed with petroleum ether and is placed in separatory funnel, stratification simultaneously collects lower floor's liquid, then by volume
Than 1:5, lower floor's liquid is mixed with ethyl acetate and is placed in separatory funnel, stratification collects lower floor's liquid phase, by subnatant
Mutually it is placed in rotation at 48 DEG C and is evaporated to the 1/3 of lower floor's liquid phase original volume, be prepared into chlorogenic acid concentrate, 475mL is weighed respectively and is gone
Ionized water, 125mL absolute ethyl alcohols and 18mL butyl titanates are placed in beaker, and mixing is stirred at room temperature and is placed in surpassing under 250W
Sound disperses 13min, treats after the completion of ultrasonic disperse, obtains sol solutionses, then in mass ratio 1：1：10, by sol solutionses, ammonium hydrogen carbonate and nothing
Water-ethanol mixing is placed in reactor, and at 69 DEG C after insulation reaction 4h, 13min is centrifuged under 2750r/min, is collected
Lower sediment is simultaneously washed with deionized 4 times, and the precipitation after washing is placed at 78 DEG C and dries 11h, mills and is prepared into titanium dioxide
Titanium tiny balloon, in mass ratio 1:5, titanic oxide hollow microballoon is mixed with chlorogenic acid concentrate, the ultrasonic disperse under 250W
After 13min, obtain mixed dispersion liquid and be placed in rotary evaporated to dryness at 78 DEG C, obtain dried object and ball milling, cross 200 mesh sieves, be prepared into
Modified titanium dioxide powder, then count by weight, weigh respectively 48 parts of concentration for 0.1mol/L sodium hydroxide solution, 13 parts
Modified titanium dioxide powder and 48 parts of mass fractions are that 0.1% sodium salicylate solution is placed in beaker, the magnetic force under 1100r/min
After stirring mixing 11h, standing and defoaming 22h is prepared into modified light stream and becomes liquid, finally counts by weight, and weighing 45 parts respectively changes
Property light stream become liquid, 13 parts of atoleines, 1 part of emulsifier op-10,1 part of ethylene glycol, 0.8 part of dimethyl silicone polymer and be placed in three mouthfuls
In flask, under 250W after ultrasonic disperse 13min, standing and defoaming 4h, you can be prepared into a kind of metal polish.
First in mass ratio 1:50, metal polish produced by the present invention is mixed with temperature for 25 DEG C of water stirring
2min, obtains polishing fluid, then puts into polished metal substrate in polishing fluid, is standing and soak for taking out after 4min, then will immersion
Metal substrate afterwards is transferred in baking oven, and 13min is dried under the conditions of temperature is 75 DEG C, is finally taken out metal substrate natural cooling and is
Can.After testing, metal polish polishing effect produced by the present invention is good, and brightness coverage capability is strong, can make the metal system after polishing
Product surface smoothness is up to 10 grades, while polishing agent of the present invention has preferably cleaning anti-rust action, with using traditional polishing agent
Metallic article is compared, and is extended 11 days using antirust time limit of the metallic article of polishing agent of the present invention under exposed environments, and this
Preferably, under normal temperature sealed environment, the pot-life is up to 17 months invention polishing agent stability.
Example 3
5kg hawthorn are chosen first, by hawthorn vacuum freeze drying and ball milling, are crossed 50 mesh sieves, are obtained hawthorn fruit, in mass ratio 1:
10, it is that 70% ethanol solution is mixed by hawthorn fruit and mass fraction, the ultrasonic extraction 60min under 300W treats that ultrasonic extraction is completed
Afterwards, filter to get filtrate, filtrate is evaporated to the 1/5 of filtrate original volume as rotation at 80 DEG C, concentrate is prepared into, then by matter
Amount compares 1:5, concentrate is mixed with petroleum ether and is placed in separatory funnel, stratification simultaneously collects lower floor's liquid, then by volume
Than 1:5, lower floor's liquid is mixed with ethyl acetate and is placed in separatory funnel, stratification collects lower floor's liquid phase, by subnatant
Mutually it is placed in rotation at 50 DEG C and is evaporated to the 1/3 of lower floor's liquid phase original volume, be prepared into chlorogenic acid concentrate, 500mL is weighed respectively and is gone
Ionized water, 150mL absolute ethyl alcohols and 20mL butyl titanates are placed in beaker, and mixing is stirred at room temperature and is placed in surpassing under 300W
Sound disperses 15min, treats after the completion of ultrasonic disperse, obtains sol solutionses, then in mass ratio 1：1：10, by sol solutionses, ammonium hydrogen carbonate and nothing
Water-ethanol mixing is placed in reactor, and at 70 DEG C after insulation reaction 5h, 15min is centrifuged under 3000r/min, is collected
Lower sediment is simultaneously washed with deionized 5 times, and the precipitation after washing is placed at 80 DEG C and dries 12h, mills and is prepared into titanium dioxide
Titanium tiny balloon, in mass ratio 1:5, titanic oxide hollow microballoon is mixed with chlorogenic acid concentrate, the ultrasonic disperse under 300W
After 15min, obtain mixed dispersion liquid and be placed in rotary evaporated to dryness at 80 DEG C, obtain dried object and ball milling, cross 200 mesh sieves, be prepared into
Modified titanium dioxide powder, then count by weight, weigh respectively 50 parts of concentration for 0.1mol/L sodium hydroxide solution, 15 parts
Modified titanium dioxide powder and 50 parts of mass fractions are that 0.1% sodium salicylate solution is placed in beaker, the magnetic force under 1200r/min
After stirring mixing 12h, standing and defoaming 24h is prepared into modified light stream and becomes liquid, finally counts by weight, and weighing 50 parts respectively changes
Property light stream become liquid, 15 parts of atoleines, 2 parts of emulsifier op-10s, 2 parts of ethylene glycol, 1.0 parts of dimethyl silicone polymers and be placed in three mouthfuls
In flask, under 300W after ultrasonic disperse 15min, standing and defoaming 5h, you can be prepared into a kind of metal polish.
First in mass ratio 1:60, metal polish produced by the present invention is mixed with temperature for 35 DEG C of water stirring
3min, obtains polishing fluid, then puts into polished metal substrate in polishing fluid, is standing and soak for taking out after 5min, then will immersion
Metal substrate afterwards is transferred in baking oven, and 15min is dried under the conditions of temperature is 80 DEG C, is finally taken out metal substrate natural cooling and is
Can.After testing, metal polish polishing effect produced by the present invention is good, and brightness coverage capability is strong, can make the metal system after polishing
Product surface smoothness is up to 11 grades, while polishing agent of the present invention has preferably cleaning anti-rust action, with using traditional polishing agent
Metallic article is compared, and is extended 15 days using antirust time limit of the metallic article of polishing agent of the present invention under exposed environments, and this
Preferably, under normal temperature sealed environment, the pot-life is up to 18 months invention polishing agent stability.
Claims (3)
1. a kind of preparation method of metal polish, it is characterised in that specifically preparation process is：
（1）3~5kg hawthorn are taken, are dried and ball milling, 50 mesh sieves is crossed, obtains hawthorn fruit, in mass ratio 1:10, by hawthorn fruit with
Mass fraction mixes for 70% ethanol solution, is filtered to get filtrate after ultrasonic extraction, filtrate rotary evaporation is obtained into concentrate；
（2）In mass ratio 1:5, concentrate is mixed with petroleum ether and is placed in separatory funnel, stratification simultaneously collects subnatant
Body, then by volume 1:5, lower floor's liquid is mixed with ethyl acetate and is placed in separatory funnel, stratification collects subnatant
Phase, by lower floor's liquid phase rotary evaporation, obtains chlorogenic acid concentrate；
（3）450~500mL deionized waters, 100~150mL absolute ethyl alcohols and the stirring of 15~20mL butyl titanates are weighed respectively
Mixing, ultrasonic disperse obtains sol solutionses, in mass ratio 1：1：10, sol solutionses, ammonium hydrogen carbonate are mixed with absolute ethyl alcohol, centrifuged
And collect lower sediment, washing, dry, titanic oxide hollow microballoon of milling to obtain；
（4）In mass ratio 1:5, titanic oxide hollow microballoon is mixed with chlorogenic acid concentrate, ultrasonic disperse obtains mixed dispersion liquid,
Rotary evaporated to dryness obtains dried object and ball milling, crosses 200 mesh sieves, obtains modified titanium dioxide powder, count by weight, weigh respectively
45~50 parts of 0.1mol/L sodium hydroxide solutions, 10~15 parts of modified titanium dioxide powders and 45~50 parts of mass fractions are 0.1%
Sodium salicylate solution stirring mixing, standing and defoaming is prepared into modified light stream and becomes liquid；
（5）Count by weight, 40~50 parts of modified light streams are weighed respectively and become liquid, 10~15 parts of atoleines, 1~2 part of emulsification
Agent OP-10,1~2 part of ethylene glycol, 0.5~1.0 part of dimethyl silicone polymer stirring mixing and ultrasonic disperse, standing and defoaming, you can
It is prepared into a kind of metal polish.
2. a kind of preparation method of metal polish according to claim 1, it is characterised in that：Step（1）Described is super
Sound extraction conditions are the ultrasonic extraction under 200~300W.
3. a kind of preparation method of metal polish according to claim 1, it is characterised in that：Step（2）Described rotation
Turn evaporating temperature for 45~50 DEG C.
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| CN201710337165.1A CN107164763A (en) | 2017-05-14 | 2017-05-14 | A kind of preparation method of metal polish |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107541730A (en) * | 2017-09-25 | 2018-01-05 | 常州市宇科不绣钢有限公司 | A kind of preparation method of liquid metals polishing agent |
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| CN106435591A (en) * | 2016-11-04 | 2017-02-22 | 广西钱隆投资管理有限公司 | Metal product polishing liquid and preparation method thereof |
| CN106567080A (en) * | 2016-11-10 | 2017-04-19 | 仇颖莹 | Method for preparing metal polishing agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103757636A (en) * | 2014-01-07 | 2014-04-30 | 华南理工大学 | Chemical polishing solution and alloy surface polishing treatment method |
| CN104328434A (en) * | 2014-09-22 | 2015-02-04 | 马鞍山市申马机械制造有限公司 | Mirror roller polishing agent and preparation method thereof |
| CN104888698A (en) * | 2015-05-21 | 2015-09-09 | 安徽凤凰滤清器股份有限公司 | Adsorbent capable of adsorbing gasoline steam |
| CN105349999A (en) * | 2015-11-19 | 2016-02-24 | 苏州捷德瑞精密机械有限公司 | Environment-friendly polishing solution and preparation method thereof |
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| CN107541730A (en) * | 2017-09-25 | 2018-01-05 | 常州市宇科不绣钢有限公司 | A kind of preparation method of liquid metals polishing agent |
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Application publication date: 20170915 |