CN106435591A - Metal product polishing liquid and preparation method thereof - Google Patents
Metal product polishing liquid and preparation method thereof Download PDFInfo
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- CN106435591A CN106435591A CN201610977259.0A CN201610977259A CN106435591A CN 106435591 A CN106435591 A CN 106435591A CN 201610977259 A CN201610977259 A CN 201610977259A CN 106435591 A CN106435591 A CN 106435591A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
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Abstract
The invention discloses metal product polishing liquid. The polishing liquid is prepared from, by weight, 20-30 parts of citric acid, 50-100 parts of glacial acetic acid, 2-10 parts of 2-ethylimidazole, 5-12 parts of salicylic acid, 10-20 parts of glycolic acid, 8-15 parts of 1H-benzotriazole, 20-80 parts of polyethylene glycol 8000, 100-150 parts of tetrahydrofurfuryl alcohol, 50-150 parts of ethyl alcohol, 80-100 parts of butyl acetate, 5-12 parts of oleic alcohol polyoxyethylene ether, 5-12 parts of ethylenediamine, 4-6 parts of nano-silicon dioxide, 3-9 parts of nano-zinc oxide and 30-80 parts of auxiliaries. The metal product polishing liquid contains the auxiliaries, the auxiliaries contain rice bran and mango skin, an oxide layer on the surface of a metal product can be effectively removed by means of extraction, tea seed powder can remove blots on the surface of the metal product, effective substances in a polishing agent can easily make direct contact with the oxide layer on the surface of the metal product, the efficiency is improved when the polishing agent removes the oxide layer, and after being modified through iron powder, latex powder and natural resin can form a layer of compact protective film on the surface layer of the metal product after being polished.
Description
Technical field
The present invention relates to field of surface technology, and in particular to a kind of metallic article polishing fluid and preparation method thereof.
Background technology
Polishing refer to using machinery, chemistry or electrochemistry effect, make workpiece surface roughness reduce, with obtain light,
The processing method of flat surface.Using flexible polishing instrument and abrasive grain or other polishing mediums, surface of the work is carried out
Modification processing.Wherein chemical polishing is to eliminate mill by chemical reagent to the selective dissolution effect in the uneven region of sample surfaces
Trace, a kind of method of etch leveling.The operation principle of chemical polishing；Test button surface respectively constitutes the electrochemical potentials of phase not
Same, many micro- potentials are defined, and uneven dissolution can be produced in chemical solution.In course of dissolution, sample face top layer can produce
Layer oxide film, specimen surface projection is thin due to mucosa, and the dissolving expansion rate of metal is slower, the surface light after polishing
Sliding, but it is formed with little fluctuating waveform, it is impossible to reach very good requirement.Using microscope under low and medium amplification
During observation, this little fluctuating typically within the vertical distinguishing ability of object lens, still it is observed that very clearly organizing.Chemistry is thrown
The advantage of light：Chemical polishing appts are simple, can process the part of shape matching complexity.Impact polishing effect wherein in chemical polishing
Fruit maximum is polishing fluid, and polishing fluid is typically made up of mineral acid strong acid at this stage, with stronger corrosivity.
Content of the invention
It is an object of the invention to the problems referred to above are directed to, a kind of high-efficiency environment friendly metallic article polishing fluid is provided.
The present invention provide technical scheme be：
A kind of metallic article polishing fluid, the polishing fluid is made up of following weight portion material：Citric acid 20-30 part, ice vinegar
Sour 50-100 part, 2- ethyl imidazol(e) 2-10 part, salicylic acid 5-12 part, glycolic 10-20 part, phenylpropyl alcohol triazole 8-15 part, poly- second
Glycol 800020-80 part, tetrahydrofurfuryl alcohol 100-150 part, ethanol 50-150 part, butyl acetate 80-100 part, oleic alcohol polyoxyethylene
Ether 5-12 part, ethylenediamine 5-12 part, nano silicon 4-6 part, nano zine oxide 3-9 part, auxiliary agent 30-80 part；The auxiliary agent
It is made up of following weight portion material：Testa oryzae 50-100 part, mangrove bark 100-200 part, camellia oleosa seed powder 80-120 part, green tea powder 50-90
Part, Fructus Maydiss 30-50 part, latex powder 50-80 part, iron powder 5-20 part, natural resin 30-60 part, Sorbitol 10-25 part,
Olive oil 20-30 part, Oleum Cocois 50-100 part, Oleum Terebinthinae 100-200 part, water 200-400 part, ethanol 200-400 part；Described help
Agent is made up of following methods：Testa oryzae, Fructus Maydiss, mangrove bark are crushed grinds, after mixing, ball milling 1-2 hour, filters
To extracting solution A and filtering residue, ethanol after filtering residue is mixed, is added with camellia oleosa seed powder, green tea powder, reflux, extract, 1-2 time, after filtering merging
Extracting solution B is concentrated under reduced pressure to give, after latex powder, natural resin, iron powder are mixed with Oleum Terebinthinae, placement is subzero 20 DEG C, and 10-24 is little
Shi Hou, rises again after taking-up to 25 DEG C, carries out dispersion 1-2 hour at a high speed using dispersion machine and obtains extracting solution C, by extracting solution A, B, C
Mix homogeneously with Sorbitol, olive oil, Oleum Cocois carry out again 1-2 hour high speed dispersion after, filtered using double-layer leaching net
To the auxiliary agent.
Preferably, the polishing fluid is made up of following weight portion material：25 parts of citric acid, 90 parts of glacial acetic acid, 2- ethyl
8 parts of imidazoles, 10 parts of salicylic acid, 15 parts of glycolic, 12 parts of phenylpropyl alcohol triazole, 65 parts of Macrogol 8000,130 parts of tetrahydrofurfuryl alcohol,
140 parts of ethanol, 90 parts of butyl acetate, 10 parts of oleic alcohol polyoxyethylene ether, 10 parts of ethylenediamine, 5 parts of nano silicon, nano oxidized
6 parts of zinc, 70 parts of auxiliary agent.
Preferably, the nano silicon, the particle diameter of nano zine oxide are 50-100 nanometer.
Preferably, the auxiliary agent is made up of following weight portion material：80 parts of Testa oryzae, 120 parts of mangrove bark, camellia oleosa seed powder 90
Part, 65 parts of green tea powder, 45 parts of Fructus Maydiss, 75 parts of latex powder, 15 parts of iron powder, 50 parts of natural resin, 20 parts of Sorbitol, Fructus Canarii albi
25 parts of oil, 85 parts of Oleum Cocois, 180 parts of Oleum Terebinthinae, 380 parts of water, 350 parts of ethanol.
The present invention also provides a kind of preparation method of described metallic article polishing fluid, the preparation method of the polishing fluid：
Comprise the following steps：
1., citric acid, glacial acetic acid, glycolic, salicylic acid are mixed with tetrahydrofurfuryl alcohol, stirs and obtain to wherein solid dissolving
Liquid a；
2., by butyl acetate, ethanol, Macrogol 8000 be heated to 60 DEG C stirring 0.5 hour molten to Macrogol 8000
Solution, solution is cooled to room temperature and obtains liquid b；
3., after liquid a and liquid b mix homogeneously, nano silicon, nano zine oxide, three nitrogen of phenylpropyl alcohol will be sequentially added
Azoles, 2- ethyl imidazol(e), are disperseed using emulsion dispersion machine, and each material jitter time is 0.5-1 hour, to obtain mixed emulsion
d；
4., ethylenediamine, oleic alcohol polyoxyethylene ether, auxiliary agent are added to mixed emulsion d, after stirring, are put into ball mill
Ball milling is carried out, Ball-milling Time is 3-6 hour, to obtain final product the polishing fluid.
Preferably, the rate of dispersion of step 3. middle emulsion dispersion is 15000rmp, and temperature keeps during scattered
At 40-50 DEG C.
Preferably, step 4. in be additionally included in ball milling after, filtered, filtered using the filter screen of 1-10 micron.
The present invention can be using spraying friction, or the mode that soaks carries out being polished metallic article.
Beneficial effects of the present invention are as follows：
The present invention contains auxiliary agent without harmful substances such as strong acid and strong bases in the present invention, contain Testa oryzae, Fructus Mangifera Indicae wherein in auxiliary agent
Skin can effectively remove the oxide layer of surface of metal product by extracting, and camellia oleosa seed powder can remove surface of metal product pollution, be conducive to
Active substance in polishing agent and surface of metal product oxide layer directly contact, improve the efficiency that polishing agent removes removing oxide layer, breast
Rubber powder, natural resin can form one layer fine and close protection on its top layer in metallic article by iron powder is modified after polishing
Film, the metallic article that can allow after polishing is difficult oxidized corrosion, green containing abundant unsaturated fatty acid collaboration in Fructus Maydiss
Tea polyphenols in tea powder play stronger antioxidation.
Specific embodiment
With reference to specific embodiment, the present invention is described in further detail, to make those skilled in the art's reference say
Bright book word can be implemented according to this.
Embodiment 1：
A kind of metallic article polishing fluid, the polishing fluid is made up of following weight portion material：20 parts of citric acid, glacial acetic acid 50
Part, 2 parts of 2- ethyl imidazol(e), 5 parts of salicylic acid, 10 parts of glycolic, 8 parts of phenylpropyl alcohol triazole, 20 parts of Macrogol 8000, tetrahydrofurfuryl alcohol
100 parts, 50 parts of ethanol, 80 parts of butyl acetate, 5 parts of oleic alcohol polyoxyethylene ether, 5 parts of ethylenediamine, nano silicon 4 part, nanometer
3 parts of zinc oxide, 30 parts of auxiliary agent；The auxiliary agent is made up of following weight portion material：50 parts of Testa oryzae, 100 parts of mangrove bark, camellia oleosa seed powder 80
Part, 50 parts of green tea powder, 30 parts of Fructus Maydiss, 50 parts of latex powder, 5 parts of iron powder, 30 parts of natural resin, 10 parts of Sorbitol, Fructus Canarii albi
20 parts of oil, 50 parts of Oleum Cocois, 100 parts of Oleum Terebinthinae, 200 parts of water, 200 parts of ethanol；The auxiliary agent is made up of following methods：By rice
Bran, Fructus Maydiss, mangrove bark crush grinds, after mixing, ball milling 1 hour, and extracting solution A and filtering residue is filtrated to get, by filtering residue
Addition ethanol after mixing with camellia oleosa seed powder, green tea powder, reflux, extract, 1 time, filters after merging and is concentrated under reduced pressure to give extracting solution B, by breast
After rubber powder, natural resin, iron powder are mixed with Oleum Terebinthinae, placement is subzero 20 DEG C, after 10 hours, is risen again to 25 DEG C after taking-up, adopts
Dispersion machine carries out dispersion at a high speed and obtains extracting solution C in 1 hour, and extracting solution A, B, C are mixed with Sorbitol, olive oil, Oleum Cocois
After the uniform high speed dispersion for carrying out 1 hour again, the auxiliary agent is filtrated to get using double-layer leaching net.
The present invention also provides a kind of preparation method of described metallic article polishing fluid, the preparation method of the polishing fluid：
Comprise the following steps：
1., citric acid, glacial acetic acid, glycolic, salicylic acid are mixed with tetrahydrofurfuryl alcohol, stirs and obtain to wherein solid dissolving
Liquid a；
2., by butyl acetate, ethanol, Macrogol 8000 be heated to 60 DEG C stirring 0.5 hour molten to Macrogol 8000
Solution, solution is cooled to room temperature and obtains liquid b；
3., after liquid a and liquid b mix homogeneously, nano silicon, nano zine oxide, three nitrogen of phenylpropyl alcohol will be sequentially added
Azoles, 2- ethyl imidazol(e), are disperseed using emulsion dispersion machine, and each material jitter time is 0.5 hour, to obtain mixed emulsion d；
4., ethylenediamine, oleic alcohol polyoxyethylene ether, auxiliary agent are added to mixed emulsion d, after stirring, are put into ball mill
Ball milling is carried out, Ball-milling Time is 3 hours, to obtain final product the polishing fluid.
Embodiment 2
A kind of metallic article polishing fluid, the polishing fluid is made up of following weight portion material：30 parts of citric acid, glacial acetic acid
100 parts, 10 parts of 2- ethyl imidazol(e), 12 parts of salicylic acid, 20 parts of glycolic, 15 parts of phenylpropyl alcohol triazole, 80 parts of Macrogol 8000, four
150 parts of hydrogen furfuryl alcohol, 150 parts of ethanol, 100 parts of butyl acetate, 12 parts of oleic alcohol polyoxyethylene ether, 12 parts of ethylenediamine, nanometer titanium dioxide
6 parts of silicon, 9 parts of nano zine oxide, 80 parts of auxiliary agent；The auxiliary agent is made up of following weight portion material：100 parts of Testa oryzae, mangrove bark 200
Part, 120 parts of camellia oleosa seed powder, 90 parts of green tea powder, 50 parts of Fructus Maydiss, 80 parts of latex powder, 20 parts of iron powder, 60 parts of natural resin, Pyrusussuriensiss
25 parts of sugar alcohol, 30 parts of olive oil, 100 parts of Oleum Cocois, 200 parts of Oleum Terebinthinae, 400 parts of water, 400 parts of ethanol；The auxiliary agent is by following
Method is made：Testa oryzae, Fructus Maydiss, mangrove bark are crushed grinds, after mixing, ball milling 1-2 hour, it is filtrated to get extracting solution
A and filtering residue, addition ethanol after filtering residue is mixed with camellia oleosa seed powder, green tea powder, reflux, extract, 2 times, filters concentrating under reduced pressure after merging and obtains
To extracting solution B, after latex powder, natural resin, iron powder are mixed with Oleum Terebinthinae, placement is subzero 20 DEG C, after 24 hours, returns after taking-up
Temperature is carried out dispersion at a high speed using dispersion machine and obtains extracting solution C in 2 hours, by extracting solution A, B, C and Sorbitol, Fructus Canarii albi to 25 DEG C
After oil, Oleum Cocois mix homogeneously carry out the high speed dispersion of 2 hours again, the auxiliary agent is filtrated to get using double-layer leaching net；Described receive
Rice silicon dioxide, the particle diameter of nano zine oxide are 50-100 nanometer.
The preparation method of described metallic article polishing fluid, the preparation method of the polishing fluid：Comprise the following steps：
1., citric acid, glacial acetic acid, glycolic, salicylic acid are mixed with tetrahydrofurfuryl alcohol, stirs and obtain to wherein solid dissolving
Liquid a；
2., by butyl acetate, ethanol, Macrogol 8000 be heated to 60 DEG C stirring 0.5 hour molten to Macrogol 8000
Solution, solution is cooled to room temperature and obtains liquid b；
3., after liquid a and liquid b mix homogeneously, nano silicon, nano zine oxide, three nitrogen of phenylpropyl alcohol will be sequentially added
Azoles, 2- ethyl imidazol(e), are disperseed using emulsion dispersion machine, and each material jitter time is 1 hour, to obtain mixed emulsion d, breast
Change scattered rate of dispersion for 15000rmp, temperature is maintained at 40 DEG C during scattered；
4., ethylenediamine, oleic alcohol polyoxyethylene ether, auxiliary agent are added to mixed emulsion d, after stirring, are put into ball mill
Ball milling is carried out, and Ball-milling Time is 3 hours, to be filtered, filtration is carried out using the filter screen of 1-10 micron and obtain final product the polishing fluid.
Embodiment 3
A kind of metallic article polishing fluid, the polishing fluid is made up of following weight portion material：25 parts of citric acid, glacial acetic acid 90
Part, 8 parts of 2- ethyl imidazol(e), 10 parts of salicylic acid, 15 parts of glycolic, 12 parts of phenylpropyl alcohol triazole, 65 parts of Macrogol 8000, tetrahydrochysene bran
130 parts of alcohol, 140 parts of ethanol, 90 parts of butyl acetate, 10 parts of oleic alcohol polyoxyethylene ether, 10 parts of ethylenediamine, 5 parts of nano silicon,
6 parts of nano zine oxide, 70 parts of auxiliary agent；The auxiliary agent is made up of following weight portion material：80 parts of Testa oryzae, 120 parts of mangrove bark, camellia oleosa seed
90 parts of powder, 65 parts of green tea powder, 45 parts of Fructus Maydiss, 75 parts of latex powder, 15 parts of iron powder, 50 parts of natural resin, 20 parts of Sorbitol,
25 parts of olive oil, 85 parts of Oleum Cocois, 180 parts of Oleum Terebinthinae, 380 parts of water, 350 parts of ethanol；The auxiliary agent is made up of following methods：Will
Testa oryzae, Fructus Maydiss, mangrove bark crush grinds, after mixing, ball milling 1-2 hour, and extracting solution A and filtering residue is filtrated to get, will
Filtering residue mix with camellia oleosa seed powder, green tea powder after add ethanol, reflux, extract, 1-2 time, filter merging after be concentrated under reduced pressure to give extracting solution
B, after latex powder, natural resin, iron powder are mixed with Oleum Terebinthinae, placement is subzero 20 DEG C, after 20 hours, is risen again to 25 after taking-up
DEG C, dispersion at a high speed is carried out using dispersion machine and obtains extracting solution C within 1 hour, by extracting solution A, B, C and Sorbitol, olive oil, Cortex cocois radiciss
After oily mix homogeneously carries out the high speed dispersion of 2 hours again, the auxiliary agent is filtrated to get using double-layer leaching net；The nanometer titanium dioxide
Silicon, the particle diameter of nano zine oxide are 50-100 nanometer.
The preparation method of described metallic article polishing fluid, the preparation method of the polishing fluid：Comprise the following steps：
1., citric acid, glacial acetic acid, glycolic, salicylic acid are mixed with tetrahydrofurfuryl alcohol, stirs and obtain to wherein solid dissolving
Liquid a；
2., by butyl acetate, ethanol, Macrogol 8000 be heated to 60 DEG C stirring 0.5 hour molten to Macrogol 8000
Solution, solution is cooled to room temperature and obtains liquid b；
3., after liquid a and liquid b mix homogeneously, nano silicon, nano zine oxide, three nitrogen of phenylpropyl alcohol will be sequentially added
Azoles, 2- ethyl imidazol(e), are disperseed using emulsion dispersion machine, and each material jitter time is 0.5 hour, to obtain mixed emulsion d,
The rate of dispersion of emulsion dispersion is 15000rmp, and temperature is maintained at 50 DEG C during scattered；
4., ethylenediamine, oleic alcohol polyoxyethylene ether, auxiliary agent are added to mixed emulsion d, after stirring, are put into ball mill
Ball milling is carried out, and Ball-milling Time is 6 hours, to be filtered, filtration is carried out using the filter screen of 1-10 micron and obtain final product the polishing fluid.
Although embodiment of the present invention is disclosed as above, but its be not restricted in description and embodiment listed
With, it can be applied to various suitable the field of the invention completely, for those skilled in the art, can be easily
Other modification is realized, therefore under the general concept for being limited without departing substantially from claim and equivalency range, the present invention is not limited
In specific details and shown here as the embodiment with description.
Claims (7)
1. a kind of metallic article polishing fluid, it is characterised in that the polishing fluid is made up of following weight portion material：Citric acid 20-
30 parts, glacial acetic acid 50-100 part, 2- ethyl imidazol(e) 2-10 part, salicylic acid 5-12 part, glycolic 10-20 part, phenylpropyl alcohol triazole 8-
15 parts, Macrogol 8000 20-80 part, tetrahydrofurfuryl alcohol 100-150 part, ethanol 50-150 part, butyl acetate 80-100 part, oleyl alcohol
Polyoxyethylene ether 5-12 part, ethylenediamine 5-12 part, nano silicon 4-6 part, nano zine oxide 3-9 part, auxiliary agent 30-80 part；
The auxiliary agent is made up of following weight portion material：Testa oryzae 50-100 part, mangrove bark 100-200 part, camellia oleosa seed powder 80-120 part, green tea
Powder 50-90 part, Fructus Maydiss 30-50 part, latex powder 50-80 part, iron powder 5-20 part, natural resin 30-60 part, Sorbitol
10-25 part, olive oil 20-30 part, Oleum Cocois 50-100 part, Oleum Terebinthinae 100-200 part, water 200-400 part, ethanol 200-400
Part；The auxiliary agent is made up of following methods：Testa oryzae, Fructus Maydiss, mangrove bark are crushed grinds, after mixing, ball milling 1-2 is little
When, extracting solution A and filtering residue is filtrated to get, after filtering residue is mixed with camellia oleosa seed powder, green tea powder, adds ethanol, reflux, extract, 1-2 time, mistake
Filter is concentrated under reduced pressure to give extracting solution B after merging, and after latex powder, natural resin, iron powder are mixed with Oleum Terebinthinae, places subzero 20
DEG C, after 10-24 hour, rise again after taking-up to 25 DEG C, dispersion 1-2 hour at a high speed is carried out using dispersion machine extracting solution C is obtained, will carry
Take after liquid A, B, C mixed homogeneously with Sorbitol, olive oil, Oleum Cocois and carry out the high speed dispersion of 1-2 hour again, using double-deck filter
Net filtration obtains the auxiliary agent.
2. metallic article polishing fluid as claimed in claim 1, it is characterised in that the polishing fluid is by following weight portion material system
Become：25 parts of citric acid, 90 parts of glacial acetic acid, 8 parts of 2- ethyl imidazol(e), 10 parts of salicylic acid, 15 parts of glycolic, 12 parts of phenylpropyl alcohol triazole,
65 parts of Macrogol 8000,130 parts of tetrahydrofurfuryl alcohol, 140 parts of ethanol, 90 parts of butyl acetate, 10 parts of oleic alcohol polyoxyethylene ether, second two
10 parts of amine, 5 parts of nano silicon, 6 parts of nano zine oxide, 70 parts of auxiliary agent.
3. metallic article polishing fluid as claimed in claim 1, it is characterised in that the nano silicon, nano zine oxide
Particle diameter be 50-100 nanometer.
4. metallic article polishing fluid as claimed in claim 1, it is characterised in that the auxiliary agent is by following weight portion material system
Become：80 parts of Testa oryzae, 120 parts of mangrove bark, 90 parts of camellia oleosa seed powder, 65 parts of green tea powder, 45 parts of Fructus Maydiss, 75 parts of latex powder, iron powder 15
Part, 50 parts of natural resin, 20 parts of Sorbitol, 25 parts of olive oil, 85 parts of Oleum Cocois, 180 parts of Oleum Terebinthinae, 380 parts of water, ethanol
350 parts.
5. the preparation method of the metallic article polishing fluid as described in arbitrary in claim 1-4, it is characterised in that the polishing fluid
Preparation method：Comprise the following steps：
1., citric acid, glacial acetic acid, glycolic, salicylic acid are mixed with tetrahydrofurfuryl alcohol, stirs to wherein solid dissolving and obtain liquid
a；
2., butyl acetate, ethanol, Macrogol 8000 are heated to 60 DEG C of stirrings to dissolve to Macrogol 8000 for 0.5 hour, will
Solution is cooled to room temperature and obtains liquid b；
3., after liquid a and liquid b mix homogeneously, nano silicon, nano zine oxide, phenylpropyl alcohol triazole, 2- will be sequentially added
Ethyl imidazol(e), is disperseed using emulsion dispersion machine, and each material jitter time is 0.5-1 hour, to obtain mixed emulsion d；
4., ethylenediamine, oleic alcohol polyoxyethylene ether, auxiliary agent are added to mixed emulsion d, after stirring, being put into ball mill is carried out
Ball milling, Ball-milling Time is 3-6 hour, to obtain final product the polishing fluid.
6. the preparation method of metallic article polishing fluid as claimed in claim 5, it is characterised in that step 3. middle emulsion dispersion
Rate of dispersion is 15000rmp, and temperature is maintained at 40-50 DEG C during scattered.
7. the preparation method of metallic article polishing fluid as claimed in claim 5, it is characterised in that step 4. in be additionally included in ball
After mill, filtered, filtered using the filter screen of 1-10 micron.
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| CN201610977259.0A CN106435591A (en) | 2016-11-04 | 2016-11-04 | Metal product polishing liquid and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610977259.0A CN106435591A (en) | 2016-11-04 | 2016-11-04 | Metal product polishing liquid and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107164763A (en) * | 2017-05-14 | 2017-09-15 | 常州市奥普泰克光电科技有限公司 | A kind of preparation method of metal polish |
| CN107326372A (en) * | 2017-06-17 | 2017-11-07 | 常州市玉宇化工有限公司 | A kind of preparation method of wax removing agent |
| CN109401632A (en) * | 2018-11-20 | 2019-03-01 | 吴江市格瑞福金属制品有限公司 | A kind of environment-friendly type polishing fluid and preparation method thereof for casting |
| CN111718656A (en) * | 2019-03-22 | 2020-09-29 | 福吉米株式会社 | Polishing composition and polishing method |
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| CN101747843A (en) * | 2008-12-19 | 2010-06-23 | 安集微电子（上海）有限公司 | Chemical-mechanical polishing solution |
| CN102758205A (en) * | 2012-07-13 | 2012-10-31 | 东莞市东辉贸易有限公司 | Aluminum alloy polishing solution and preparing method thereof |
| CN102953063A (en) * | 2012-11-20 | 2013-03-06 | 无锡常安通用金属制品有限公司 | Metal polishing solution |
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| CN101037571A (en) * | 2007-04-25 | 2007-09-19 | 上海三瑞化学有限公司 | Low-luster polishing agent combination and preparation method thereof |
| CN101747843A (en) * | 2008-12-19 | 2010-06-23 | 安集微电子（上海）有限公司 | Chemical-mechanical polishing solution |
| CN102758205A (en) * | 2012-07-13 | 2012-10-31 | 东莞市东辉贸易有限公司 | Aluminum alloy polishing solution and preparing method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107164763A (en) * | 2017-05-14 | 2017-09-15 | 常州市奥普泰克光电科技有限公司 | A kind of preparation method of metal polish |
| CN107326372A (en) * | 2017-06-17 | 2017-11-07 | 常州市玉宇化工有限公司 | A kind of preparation method of wax removing agent |
| CN107326372B (en) * | 2017-06-17 | 2019-12-03 | 苏州元联科技创业园管理有限公司 | A kind of preparation method of wax removing agent |
| CN109401632A (en) * | 2018-11-20 | 2019-03-01 | 吴江市格瑞福金属制品有限公司 | A kind of environment-friendly type polishing fluid and preparation method thereof for casting |
| CN111718656A (en) * | 2019-03-22 | 2020-09-29 | 福吉米株式会社 | Polishing composition and polishing method |
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