CN106565322A - Chelating plant source insect-damage-resistant leaf fertilizer and preparation method thereof - Google Patents
Chelating plant source insect-damage-resistant leaf fertilizer and preparation method thereof Download PDFInfo
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- CN106565322A CN106565322A CN201610952701.4A CN201610952701A CN106565322A CN 106565322 A CN106565322 A CN 106565322A CN 201610952701 A CN201610952701 A CN 201610952701A CN 106565322 A CN106565322 A CN 106565322A
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- plant source
- insect
- foliage fertilizer
- water
- damage
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Classifications
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D5/00—Fertilisers containing magnesium
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
Abstract
The invention discloses a chelating plant source insect-damage-resistant leaf fertilizer and a preparation method thereof. The chelating plant source insect-damage-resistant leaf fertilizer is prepared from the following raw materials in parts by weight: plant source fresh materials, ethyl acetate, ethyl alcohol, sodium selenite, calcium magnesium phosphate fertilizers, humic acid powder, phenylalanine, magnesium sulfate, zinc chloride, ferrous sulfate, chalcanthite, edible fungi residue, glauconite powder, moss soil, blue algae, boric acid and a proper amount of water. The moss soil containing rich moss cells and the blue algae on the surface of the water layer of Chaohu are used as raw materials; crushing treatment is performed by using an ultrasonic crushing instrument, so that algae cells and moss cells are broken to release contents; the contents are rich in various plant growth hormone and accelerants; in addition, the ingredients are natural ingredients and are favorable for the crop growth; through the chelation of boracic acid and humic acid, the added inorganic mineral elements can also be easily adsorbed and utilized; the natural plant source wax ingredients are used as insect-resistance substance; no hazard is remained; and the chelating plant source insect-damage-resistant leaf fertilizer is healthier.
Description
Technical field
The invention belongs to the Technology field of fertilizer, and in particular to a kind of Chelating state plant source insect pest foliage fertilizer and
Its preparation method.
Background technology
Plant waxiness is having for element of the first species's complexity that plant is formed to adapt to external environment in growth and development process
The general name of machine mixture, is covered in exposed aerial plant tissue, including the bolt matter substrate of underground, calluss and flower
Powder etc., plays a part of to protect plant.Its main component has aliphatic compound, cyclic compound, phytosterin compound etc.,
With aliphatic compound, including long-chain fatty acid, aldehyde, primary and secondary alcohol etc. are modal components.The thing of plant surface waxiness
Physical chemistry characteristic can resist various biological with abiotic infringement, and these infringements include fungal disease, plant-feed insect, too
Positive ray, solidification point etc..
The arena that plant surface waxiness or plant, plant-feed insect and its Predator and host marking interact, its
It is plant and phytophagous elder brother that distinctive chemical composition and morphological feature give one of its distinctive ecological function, these functions
The medium of the interphase interaction of worm.The physical arrangement and quantity of plant surface waxiness can affect the attachment and shifting of plant-feed insect
It is dynamic.Surface waxiness can pass through the predation for affecting the hostile phytophagous insect in day, so as to the behavior of remote-effects phytophagous insect.Surface
Waxiness extract and single wax component can stimulate or suppress plant-feed insect spawning, activity and take food.Alkane, wax
The aliphatic compounds such as ester, free alkyl alcohol and acid are the main components of surface waxiness, select host plant in plant-feed insect
In, aliphatic compound plays particularly important effect；Aromatic compound also affects selection of the insecticide to host plant.
Plant-feed insect is less to be taken food on the few phenotypic crop of smooth waxiness, on the few phenotypic crop of smooth waxiness, surface
The quantity of waxiness is few, and chemical constituent and morphological feature are also different.Surface waxiness can pass through to affect the hostile phytophagous insect in day
Predation, so as to the behavior of remote-effects phytophagous insect.The adhesive ability of the multipair natural enemy of surface waxiness has detrimental effect, such as may be used
Reduce the predations of the natural enemy insect to plant-feed insect such as Chrysopa, the considerable ladybug of anchor speckle, minute pirate bugs.
The wax coat on blade top layer is into these waxinesss are protecting blade by high light spoke by hydrophobic compound group
Penetrate, the infringement of insect and microorganism serves very crucial effect, but the using effect which results in foliage fertilizer is not good, one
The characteristics of aspect foliage fertilizer will overcome surface hydrophobicity, stops in the effective time of blade face in foliage fertilizer, is extremely difficult to good effect
Really, and foliage fertilizer is substantially into blade, have experiment to prove that the thin blade of waxiness absorbs by way of free diffusing
Nutrient is more preferable.
The content of the invention
The present invention seeks to improve adhesive force of the foliage fertilizer on crop leaf surface, absorbability and the life of foliage fertilizer are improved
Thing insect resistance capacity, invention develop a kind of foliage fertilizer that with the addition of plant leaf blade top layer waxiness, realize particular by following methods
's：
A kind of Chelating state plant source insect pest foliage fertilizer, it is characterised in that be made up of the raw material of following weight portion：The fresh material of plant source
20 ~ 30, ethyl acetate 15 ~ 20, ethanol 6 ~ 12, sodium selenite 1 ~ 4, calcium magnesium phosphate 15 ~ 25, humic acid powder 4 ~ 8, Phenylalanine 15
~ 25, magnesium sulfate 10 ~ 18, zinc chloride 10 ~ 15, ferrous sulfate 6 ~ 10, copper sulphate pentahydrate 10 ~ 15, edible fungi residues 20 ~ 30, lichen soil
50 ~ 80, cyanophyceae 80 ~ 120, boric acid 8 ~ 15 and appropriate water；
The fresh material of described plant source is with weight（Part）Following raw material for unit is mixed：Eucalyptus leaveses 10 ~ 15, Fructus Rubi 7 ~
10th, lucerne place 15 ~ 20, Folium Populi Davidianae 4 ~ 8, cercis leaf 1 ~ 4, wheat leaf 6 ~ 10, Folium Crataegi 2 ~ 5, leaf of Semen Maydis 3 ~ 7.
A kind of preparation method of Chelating state plant source insect pest foliage fertilizer, it is characterised in that including following step：
（1）In the fresh material of plant source being added after ethanol dilution 50 ~ 60%, homogenate will be ground to form, be subsequently adding ethyl acetate, water-bath 55 ~
Under the conditions of 70 DEG C extract 2.0 ~ 2.5h, after the completion of sucking filtration obtain filtrate, then at 70 ~ 80 DEG C of rotated evaporimeter concentrate lixiviating solution extremely
40~60%；
（2）Mixed edible bacteria residue, lichen soil and cyanophyceae, add the water of 6 ~ 10 times of its weight portions, and high shear agitation is equal to solution
Even, then ultrasound wave carries out break process to cell and obtains serosity, and supernatant is obtained after centrifugation；
（3）, in reactor, after adding the water of 30 ~ 50% its total amount, hyperbaric heating is stirred to melting for mixing humic acid powder and boric acid
State, then mixes magnesium sulfate, zinc chloride, ferrous sulfate and other following residual componentss being not directed to and adds, be incubated 70 ~ 90 DEG C
30 ~ 40min of stirring is chelated, after the completion of be watered 100 ~ 150 times of dilution foliage fertilizer；
（4）Phenylalanine is mixed（1）Gained lixiviating solution and（2）The supernatant, add to（3）Mixing foliage fertilizer in, stir
Mix mixing.
Compositing characteristic and its pest-resistant principle of the invention according to waxiness in background technology, the basic point of departure of preparation are to utilize
Plant waxiness extract is raw material, prepares the additive of foliage fertilizer, crop is protected using natural insect resistace active component,
This measure can reduce the pesticide residues of crop, improve crop quality, can improve substantially extraction step through years of researches
Suddenly：（1）It is to choose containing abundant waxiness and the plant leaf blade with insect pest characteristic, eucalyptus leaveses have to diamond-back moth significantly walks quickly and keeps away
Effect, the surface waxiness of Herba Medicaginiss then has good protective effect to variegation aphid, in the surface waxiness of Fructus Rubi containing Squalene,
The good insect repelling components such as plant sterol, tocopherol and vanillin, the also Cortex Populi dividianae with the effect of above effect same
Leaf, cercis, Folium Crataegi, wheat leaf, leaf of Semen Maydis etc.；（2）Using certain density ethyl acetate aqueous solution as extractant, then
Defibrination is carried out to the blade rich in waxiness, is mixed after ethyl acetate extractant is added, 60 DEG C of extractions of water-bath, this process is not only
Blade face top layer wax component can be extracted, while the volatility lipid in blade can be extracted, is equally had and is walked quickly and kept away evil well
The effect of worm, after the completion of high speed centrifugation remove blade residue, by gained filtrate by Rotary Evaporators heating concentration.
By in the plant leaf blade lixiviating solution that above method is obtained containing the volatile aromatic fat and surface lipophilic in blade
Property compound wax component, and all there are obvious boiling characteristics, after being sprayed to blade, insect had and walks quickly and keeps away work well
With, by the use of being slightly soluble in the ethyl acetate of water as extractant, can with the problem of the neutralizing plant extract poorly water-soluble of a part,
Remaining ethyl acetate after the completion of extraction, its characteristic for being slightly soluble in water serve the work of bridge well as a kind of intermediate
With, add to the water miscible foliage fertilizer of water-wet side connection after foliage fertilizer, and the wax component that the connection of lipophilic end is extracted, and according to
Similar compatibility principle, waxiness and the waxiness perfect adaptation of blade surface, promote foliage fertilizer to adsorb in blade surface, improve foliage fertilizer
Utilization rate.
Beneficial effects of the present invention：Invention is using the lichen soil containing abundant mossy cell and the cyanophyceae of water of Chaohu Lake layer surface
As raw material, break process being carried out using Ultrasonic Cell Disruptor, making frustule and mossy cell rupture release content, content is rich
Containing various auxins and accelerator, and natural component, be conducive to the growth of crop, through boric acid and the chela of humic acid
Close, the inorganic mineral element of addition is also easier to be absorbed and used, using natural plant source wax component as pest-resistant material,
Non-hazardous are remained, more healthy.
Specific embodiment
Embodiment 1：
A kind of Chelating state plant source insect pest foliage fertilizer, it is characterised in that by following weight portion（Kg）Raw material make：Plant source
Fresh material 26, ethyl acetate 16, ethanol 8, sodium selenite 2, calcium magnesium phosphate 18, humic acid powder 6, Phenylalanine 20, magnesium sulfate 14, chlorine
Change zinc 12, ferrous sulfate 9, copper sulphate pentahydrate 12, edible fungi residues 25, lichen soil 60, cyanophyceae 100, boric acid 10 and appropriate water；
The fresh material of described plant source is with weight（Kg）Following raw material for unit is mixed：Eucalyptus leaveses 12, Fructus Rubi 8, lucerne
Place 18, Folium Populi Davidianae 6, cercis leaf 3, wheat leaf 7, Folium Crataegi 3, leaf of Semen Maydis 5.
A kind of preparation method of Chelating state plant source insect pest foliage fertilizer, it is characterised in that including following step：
（1）In the fresh material of plant source being added after ethanol dilution 50 ~ 60%, homogenate will be ground to form, be subsequently adding ethyl acetate, water-bath 55 ~
Under the conditions of 70 DEG C extract 2.0 ~ 2.5h, after the completion of sucking filtration obtain filtrate, then at 70 ~ 80 DEG C of rotated evaporimeter concentrate lixiviating solution extremely
40~60%；
（2）Mixed edible bacteria residue, lichen soil and cyanophyceae, add the water of 6 ~ 10 times of its weight portions, and high shear agitation is equal to solution
Even, then ultrasound wave carries out break process to cell and obtains serosity, and supernatant is obtained after centrifugation；
（3）, in reactor, after adding the water of 30 ~ 50% its total amount, hyperbaric heating is stirred to melting for mixing humic acid powder and boric acid
State, then mixes magnesium sulfate, zinc chloride, ferrous sulfate and other following residual componentss being not directed to and adds, be incubated 70 ~ 90 DEG C
30 ~ 40min of stirring is chelated, after the completion of be watered 100 ~ 150 times of dilution foliage fertilizer；
（4）Phenylalanine is mixed（1）Gained lixiviating solution and（2）The supernatant, add to（3）Mixing foliage fertilizer in, stir
Mix mixing.
By the present invention foliage fertilizer be used for Fructus Lycopersici esculenti planting experiment, by invention foliage fertilizer by per mu of 150 ~ 200Kg amount
Uniformly it is sprayed on the blade of Fructus Lycopersici esculenti, as a result relative to conventional common foliage fertilizer, the assimilation effect of foliage fertilizer of the present invention is more preferable,
The incidence rate of pest and disease damage is reduced, and the yield of Fructus Lycopersici esculenti has been lifted.
Claims (2)
1. a kind of Chelating state plant source insect pest foliage fertilizer, it is characterised in that be made up of the raw material of following weight portion：Plant source is fresh
Material 20 ~ 30, ethyl acetate 15 ~ 20, ethanol 6 ~ 12, sodium selenite 1 ~ 4, calcium magnesium phosphate 15 ~ 25, humic acid powder 4 ~ 8, Phenylalanine
15 ~ 25, magnesium sulfate 10 ~ 18, zinc chloride 10 ~ 15, ferrous sulfate 6 ~ 10, copper sulphate pentahydrate 10 ~ 15, edible fungi residues 20 ~ 30, lichen
Soil 50 ~ 80, cyanophyceae 80 ~ 120, boric acid 8 ~ 15 and appropriate water；
The fresh material of described plant source is with weight（Part）Following raw material for unit is mixed：Eucalyptus leaveses 10 ~ 15, Fructus Rubi 7 ~
10th, lucerne place 15 ~ 20, Folium Populi Davidianae 4 ~ 8, cercis leaf 1 ~ 4, wheat leaf 6 ~ 10, Folium Crataegi 2 ~ 5, leaf of Semen Maydis 3 ~ 7.
2. a kind of preparation method of Chelating state plant source insect pest foliage fertilizer according to claim 1, it is characterised in that include
Following step：
（1）In the fresh material of plant source being added after ethanol dilution 50 ~ 60%, homogenate will be ground to form, be subsequently adding ethyl acetate, water-bath 55 ~
Under the conditions of 70 DEG C extract 2.0 ~ 2.5h, after the completion of sucking filtration obtain filtrate, then at 70 ~ 80 DEG C of rotated evaporimeter concentrate lixiviating solution extremely
40~60%；
（2）Mixed edible bacteria residue, lichen soil and cyanophyceae, add the water of 6 ~ 10 times of its weight portions, and high shear agitation is equal to solution
Even, then ultrasound wave carries out break process to cell and obtains serosity, and supernatant is obtained after centrifugation；
（3）, in reactor, after adding the water of 30 ~ 50% its total amount, hyperbaric heating is stirred to melting for mixing humic acid powder and boric acid
State, then mixes magnesium sulfate, zinc chloride, ferrous sulfate and other following residual componentss being not directed to and adds, be incubated 70 ~ 90 DEG C
30 ~ 40min of stirring is chelated, after the completion of be watered 100 ~ 150 times of dilution foliage fertilizer；
（4）Phenylalanine is mixed（1）Gained lixiviating solution and（2）The supernatant, add to（3）Mixing foliage fertilizer in, stir
Mix mixing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610952701.4A CN106565322A (en) | 2016-11-03 | 2016-11-03 | Chelating plant source insect-damage-resistant leaf fertilizer and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610952701.4A CN106565322A (en) | 2016-11-03 | 2016-11-03 | Chelating plant source insect-damage-resistant leaf fertilizer and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106565322A true CN106565322A (en) | 2017-04-19 |
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| CN201610952701.4A Pending CN106565322A (en) | 2016-11-03 | 2016-11-03 | Chelating plant source insect-damage-resistant leaf fertilizer and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101103733A (en) * | 2006-01-20 | 2008-01-16 | 杨长举 | Calamus plant insecticide |
| CN101172903A (en) * | 2007-10-26 | 2008-05-07 | 山东省农业科学院土壤肥料研究所 | Plant source disease-resistant foliage fertilizer and method for producing the same |
| CN104478574A (en) * | 2014-12-01 | 2015-04-01 | 宁夏共享生物化工有限公司 | Method for preparing fertilizer containing humic acid concentrated chelating trace elements |
| CN105777385A (en) * | 2016-04-18 | 2016-07-20 | 合肥市农泰农业科技有限公司 | Nutrition spray with lasting pest resisting effect and preparation method thereof |
| CN105884543A (en) * | 2016-06-24 | 2016-08-24 | 安徽省安庆市金太阳生物科技有限责任公司 | Pest-resistant fertilizer additive and preparation method thereof |
| CN105967897A (en) * | 2016-06-22 | 2016-09-28 | 望江乐和生态农业有限公司 | Effect promoting agent for improving foliar fertilizer effect and preparation method of effect promoting agent |
-
2016
- 2016-11-03 CN CN201610952701.4A patent/CN106565322A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101103733A (en) * | 2006-01-20 | 2008-01-16 | 杨长举 | Calamus plant insecticide |
| CN101172903A (en) * | 2007-10-26 | 2008-05-07 | 山东省农业科学院土壤肥料研究所 | Plant source disease-resistant foliage fertilizer and method for producing the same |
| CN104478574A (en) * | 2014-12-01 | 2015-04-01 | 宁夏共享生物化工有限公司 | Method for preparing fertilizer containing humic acid concentrated chelating trace elements |
| CN105777385A (en) * | 2016-04-18 | 2016-07-20 | 合肥市农泰农业科技有限公司 | Nutrition spray with lasting pest resisting effect and preparation method thereof |
| CN105967897A (en) * | 2016-06-22 | 2016-09-28 | 望江乐和生态农业有限公司 | Effect promoting agent for improving foliar fertilizer effect and preparation method of effect promoting agent |
| CN105884543A (en) * | 2016-06-24 | 2016-08-24 | 安徽省安庆市金太阳生物科技有限责任公司 | Pest-resistant fertilizer additive and preparation method thereof |
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Application publication date: 20170419 |