CN108112604A - A kind of all you and Quizalotop-ethyl microemulsion - Google Patents
A kind of all you and Quizalotop-ethyl microemulsion Download PDFInfo
- Publication number
- CN108112604A CN108112604A CN201611057950.3A CN201611057950A CN108112604A CN 108112604 A CN108112604 A CN 108112604A CN 201611057950 A CN201611057950 A CN 201611057950A CN 108112604 A CN108112604 A CN 108112604A
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- CN
- China
- Prior art keywords
- ethyl
- quizalotop
- sulfonic acid
- sodium salt
- acid sodium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
- A01N37/22—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/60—1,4-Diazines; Hydrogenated 1,4-diazines
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of all you and Quizalotop-ethyl microemulsion, the products to belong to herbicide field；Preparing the raw material that the product uses includes：All your 10 11%, Quizalotop-ethyl 5 6%, ethyl alcohol 15%, benzene sulfonic acid sodium salt 2%, water 67%, by blending finished product under given conditions, the advantages of production method, is：Using common apparatus, simple for process, reaction condition is mild, pollution-free waste discharge；All you and Quizalotop-ethyl compounding have synergistic effect, the significant effect of anti-weeding, which is higher than, is applied alone all you or Quizalotop-ethyl, herbicidal effect greatly enhances, and available for preventing and kill off, the broad leaved weeds such as lamb's-quarters, amaranth, knotweed and barnyard grass, green bristlegrass, wild oat etc. are annual, perennial grassy weed.
Description
Technical field
The invention belongs to herbicide field more particularly to a kind of all preparation methods of that and Quizalotop-ethyl microemulsion.
Background technology
All you are amides selective herbicide, and sterling is colourless liquid, is mainly absorbed by young shoot, are conducted upwards, suppression
Secondly the growth of young shoot and root processed, the protein synthesis of the main sprout inhibition seed of mechanism of action inhibit choline and penetrate into phosphatide, do
It disturbs lecithin to be formed, since the ability that grassy weed young shoot absorbs all thats is stronger than broad leaved weed, thus the medicine prevents and kill off grass family
The effect of weeds is far better than broad leaved weed.All your missible oil is brown color liquid, and emulsifiability is good, can be with many herbicide phases
It is mixed, it is used in dry crop, the 20-50 days lasting period in soil more.Quizalotop-ethyl appearance is flaxen homogeneously crystallized, acts on machine
System is absorbed by weeds cauline leaf, and the Bidirectional Conduction up and down in plant is accumulated in top and intercalary meristematic, inhibits thin
Born of the same parents' aliphatic acid synthesizes, and makes weeds downright bad, Quizalotop-ethyl is a kind of new stem and leaf treating agent in dry farmland of high selectivity, in grass family
There is the selectivity of height between weeds and dicotyledonous crops, there is good preventive effect, effect speed to the grassy weed in broad leaf crop field
Degree is fast, and efficacy stability is not easy to be influenced by environmental conditions such as rainwater temperature and humidity, and medicament is interior when 24 is small to annual grassy weeds
Complete stool can be spread all over, young leaves turns yellow within 2-3 days, stops growing, and 4-7 days cauline leafs are in downright bad shape, and whole strain is withered in 10 days；Perennial weeds
After by medicine, medicament conducts rapidly to underground rhizome tissue, is allowed to lose power of regeneration.Above-mentioned two kinds of herbicides and auxiliary material are compounded
Afterwards, the significant effect of anti-weeding is higher than being applied alone all you or Quizalotop-ethyl, herbicidal effects to greatly enhance, available for preventing and kill off lamb's-quarters, amaranth, knotweed
Wait that broad leaved weeds and barnyard grass, green bristlegrass, wild oat etc. are annual, perennial grassy weed.
The content of the invention
Present invention mainly solves the problem of be to provide a kind of all you and Quizalotop-ethyl microemulsion, prepare the original that the product uses
Material be by weight ratio：All that 10-11%, Quizalotop-ethyl 5-6%, ethyl alcohol 15%, benzene sulfonic acid sodium salt 2%, water 67%.
The technical solution adopted by the present invention is：
（1）First the ethyl alcohol of formula ratio is added in the first agitator tank, starts to stir under room temperature, adds in formula ratio while stirring
Quizalotop-ethyl, benzene sulfonic acid sodium salt, be stirred to react 0.2-0.3 it is small when；
（2）First the water of formula ratio is added in high-speed stirred tank, starts to stir under room temperature, the rotating speed of blender turns for 20-25/
Divide, add in all thats of formula ratio while stirring；The rotating speed of blender in fast agitator tank is heightened as 190-200 revs/min, slowly
The mixture of ethyl alcohol, Quizalotop-ethyl, benzene sulfonic acid sodium salt is added in into high-speed stirred tank, be stirred to react 0.3-0.4 it is small when after obtain finished product.
The present invention further technical solution be：
The purity of all thats is 80%, the purity of Quizalotop-ethyl is 75%.
Step（1）, step（2）The room temperature is 0-38 DEG C.
The beneficial effects of the invention are as follows：Provide a kind of all you and Quizalotop-ethyl microemulsion, the advantages of production method is：
It is simple for process, environmental pollution is small, the reaction time is short, reaction condition is mild, all you and Quizalotop-ethyl compoundings have synergistic effect, prevent and kill off
The significant effect of grass is higher than being applied alone all you or Quizalotop-ethyl, herbicidal effects to greatly enhance, available for preventing and kill off the broad-leaveds such as lamb's-quarters, amaranth, knotweed
Weeds and barnyard grass, green bristlegrass, wild oat etc. are annual, perennial grassy weed.
Specific embodiment
Embodiment 1：
First the ethyl alcohol that total amount is 15% is added in the first agitator tank, starts to stir under room temperature, it is 6% to add in total amount while stirring
Quizalotop-ethyl, total amount be 2% benzene sulfonic acid sodium salt, be stirred to react 0.2 it is small when；In high-speed stirred tank first by total amount be 67% water
It adds in, starts to stir under room temperature, the rotating speed of blender is 20-25 revs/min, adds in all thats that total amount is 10% while stirring；It heightens
The rotating speed of blender is 190 revs/min in fast agitator tank, is slowly added in the mixture of ethyl alcohol, Quizalotop-ethyl, benzene sulfonic acid sodium salt high
Fast agitator tank, be stirred to react 0.4 it is small when after obtain finished product.
Embodiment 2：
First the ethyl alcohol that total amount is 15% is added in the first agitator tank, starts to stir under room temperature, adding in total amount while stirring is
5.5% Quizalotop-ethyl, the benzene sulfonic acid sodium salt that total amount is 2%, be stirred to react 0.25 it is small when；It is by total amount first in high-speed stirred tank
67% water adds in, and starts to stir under room temperature, and the rotating speed of blender is 20-25 revs/min, and it is 10.5% to add in total amount while stirring
All thats；The rotating speed of blender in fast agitator tank is heightened as 195 revs/min, slowly by ethyl alcohol, Quizalotop-ethyl, benzene sulfonic acid sodium salt it is mixed
Close object add in high-speed stirred tank, be stirred to react 0.35 it is small when after obtain finished product.
Embodiment 3：
First the ethyl alcohol that total amount is 15% is added in the first agitator tank, starts to stir under room temperature, it is 5% to add in total amount while stirring
Quizalotop-ethyl, total amount be 2% benzene sulfonic acid sodium salt, be stirred to react 0.2-0.3 it is small when；In high-speed stirred tank first by total amount be 67%
Water add in, start to stir under room temperature, the rotating speed of blender is 20-25 revs/min, add in while stirring total amount be 11% all you；
The rotating speed of blender in fast agitator tank is heightened as 200 revs/min, slowly by ethyl alcohol, Quizalotop-ethyl, benzene sulfonic acid sodium salt mixture
Add in high-speed stirred tank, be stirred to react 0.3 it is small when after obtain finished product.
Claims (3)
1. a kind of all you and Quizalotop-ethyl microemulsion, are using the weight proportion of raw material：All your 10-11%, Quizalotop-ethyl 5-6%,
Ethyl alcohol 15%, benzene sulfonic acid sodium salt 2%, water 67%；It is characterized in that：
（1）First the ethyl alcohol of formula ratio is added in the first agitator tank, starts to stir under room temperature, adds in formula ratio while stirring
Quizalotop-ethyl, benzene sulfonic acid sodium salt, be stirred to react 0.2-0.3 it is small when；
（2）First the water of formula ratio is added in high-speed stirred tank, starts to stir under room temperature, the rotating speed of blender turns for 20-25/
Divide, add in all thats of formula ratio while stirring；The rotating speed of blender in fast agitator tank is heightened as 190-200 revs/min, slowly
The mixture of ethyl alcohol, Quizalotop-ethyl, benzene sulfonic acid sodium salt is added in into high-speed stirred tank, be stirred to react 0.3-0.4 it is small when after obtain finished product.
2. a kind of all you and Quizalotop-ethyl microemulsion as described in claim 1, it is characterised in that：Described all your purity is
80%th, the purity of Quizalotop-ethyl is 75%.
3. a kind of all you and Quizalotop-ethyl microemulsion as described in claim 1, it is characterised in that：Step（1）, step（2）Institute
The room temperature stated is 0-38 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611057950.3A CN108112604A (en) | 2016-11-27 | 2016-11-27 | A kind of all you and Quizalotop-ethyl microemulsion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611057950.3A CN108112604A (en) | 2016-11-27 | 2016-11-27 | A kind of all you and Quizalotop-ethyl microemulsion |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108112604A true CN108112604A (en) | 2018-06-05 |
Family
ID=62224755
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611057950.3A Pending CN108112604A (en) | 2016-11-27 | 2016-11-27 | A kind of all you and Quizalotop-ethyl microemulsion |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108112604A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110352974A (en) * | 2019-08-28 | 2019-10-22 | 沈阳农业大学 | Early stage herbicidal ative composition and herbicide after one seedling |
-
2016
- 2016-11-27 CN CN201611057950.3A patent/CN108112604A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110352974A (en) * | 2019-08-28 | 2019-10-22 | 沈阳农业大学 | Early stage herbicidal ative composition and herbicide after one seedling |
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| Date | Code | Title | Description |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180605 |
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| WD01 | Invention patent application deemed withdrawn after publication |