CN106852329A - A kind of all your compound methods with Quizalotop-ethyl microemulsion - Google Patents
A kind of all your compound methods with Quizalotop-ethyl microemulsion Download PDFInfo
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- CN106852329A CN106852329A CN201510892935.XA CN201510892935A CN106852329A CN 106852329 A CN106852329 A CN 106852329A CN 201510892935 A CN201510892935 A CN 201510892935A CN 106852329 A CN106852329 A CN 106852329A
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- China
- Prior art keywords
- quizalotop
- ethyl
- stirring
- acetone
- sulfonic acid
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
- A01N37/22—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
- A01N43/60—1,4-Diazines; Hydrogenated 1,4-diazines
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- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Dispersion Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of all your compound methods with Quizalotop-ethyl microemulsion, the product belongs to herbicide field；With all that 12-13%, Quizalotop-ethyl 6-7%, acetone 16%, methyl naphthalene sulfonic acid sodium 3%, water 62%, by blending finished product under given conditions, the advantage of the production method is the present invention：Using common apparatus, process is simple, reaction condition be gentle, pollution-free waste discharge；All you and Quizalotop-ethyl compounding have synergistic effect, after above-mentioned two kinds of herbicides and auxiliary material compounding, the effect is significant of anti-weeding is higher than alone all you or Quizalotop-ethyl, herbicidal effect is greatly enhanced, and can be used to preventing and kill off that the broad leaved weeds such as lamb's-quarters, amaranth, knotweed and barnyard grass, green bristlegrass, wild oat etc. be annual, perennial grassy weed.
Description
Technical field
The invention belongs to herbicide field, more particularly to a kind of all your compound methods with Quizalotop-ethyl microemulsion.
Background technology
All you are amide-type selective herbicide, and sterling is colourless liquid, and odorless can be partially soluble in water when more than 20 DEG C, to people and animals' low toxicity.All you are main is absorbed by young shoot, conduction upwards, suppress the growth of young shoot and root, the protein synthesis of the main sprout inhibition seed of mechanism of action, secondly suppress choline and penetrate into phosphatide, interference lecithin is formed, and because the ability that grassy weed young shoot absorbs all thats is stronger than broad leaved weed, thus the medicine prevents and kill off the effect of grassy weed far better than broad leaved weed.All your missible oil is brown color liquid, emulsifiability is good, can mutually be mixed with many herbicides, it is used in dry crop more, such as vegetables, orchard, nursery, the broad leaved weeds such as annual gramineous weed and three-coloured amaranth, purslane such as eleusine indica, lady's-grass, green bristlegrass, cotton grass and cyperus iria, chufa, 20-50 days lasting period in soil can effectively be prevented and kill off.For flaxen homogeneously crystallized, its mechanism of action is absorbed by weeds cauline leaf to Quizalotop-ethyl outward appearance, the Bidirectional Conduction up and down in plant, is accumulated in top and intercalary meristematic, suppresses cell fatty acid synthesis, makes weeds necrosis.Quizalotop-ethyl is a kind of new stem and leaf treating agent in dry farmland of high selectivity, there is the selectivity of height between grassy weed and dicotyledonous crops, there are good preventive effect, work fast, efficacy stability to the grassy weed in broad leaf crop field, it is difficult to be influenceed by environmental conditions such as rainwater temperature and humidity, medicament can spread all over complete stool to annual grassy weeds in 24 hours, and young leaves turns yellow within 2-3 days, stops growing, cauline leaf is in downright bad shape within 4-7 days, and whole strain is withered in 10 days；By after medicine, medicament conducts rapidly perennial weeds to underground rhizome tissue, is allowed to lose power of regeneration；Quizalotop-ethyl is mainly used in the crop fields such as soybean, cotton, peanut, beet, tomato, wild cabbage, grape, prevents and kill off the annual and perennial grassy weed such as barnyard grass, lady's-grass, eleusine indica, amur foxtail, green bristlegrass, wild oat, Bermuda grass, reed, cogongrass.After above-mentioned two kinds of herbicides and auxiliary material compounding, the effect is significant of anti-weeding is higher than alone all you or Quizalotop-ethyl, herbicidal effect is greatly enhanced, and can be used to preventing and kill off that the broad leaved weeds such as lamb's-quarters, amaranth, knotweed and barnyard grass, green bristlegrass, wild oat etc. be annual, perennial grassy weed.
The content of the invention
Present invention mainly solves problem be to provide a kind of compound method of all you and Quizalotop-ethyl microemulsion, produce the raw material that the product uses is by weight ratio：All your 12-13%, Quizalotop-ethyl 6-7%, acetone 16%, methyl naphthalene sulfonic acid sodium 3%, water 62%.
The technical solution adopted by the present invention is：
（1）First the acetone of formula ratio is added in the first agitator tank, stirring is started under normal temperature, Quizalotop-ethyl, the methyl naphthalene sulfonic acid sodium of formula ratio, stirring reaction 0.2-0.3 hours are added while stirring；
（2）First the water of formula ratio is added in high-speed stirred tank, stirring is started under normal temperature, the rotating speed of agitator is 30-40 revs/min, and all thats of formula ratio are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 210-220 revs/min, the mixture of acetone, Quizalotop-ethyl, methyl naphthalene sulfonic acid sodium is slowly added into high-speed stirred tank, finished product is obtained after stirring reaction 0.5-0.6 hours.
Further technical scheme of the invention is：
Described all your purity is that the purity of 80%, Quizalotop-ethyl is 70%.
Step（1）, step（2）Described normal temperature is 0-38 DEG C.
The beneficial effects of the invention are as follows：There is provided a kind of all your compound methods with Quizalotop-ethyl microemulsion, the advantage of the production method is：Process is simple, environmental pollution is small, the reaction time is short, reaction condition is gentle, all you and Quizalotop-ethyl compounding have synergistic effect, after above-mentioned two kinds of herbicides and auxiliary material compounding, the effect is significant of anti-weeding is higher than alone all you or Quizalotop-ethyl, herbicidal effect is greatly enhanced, and can be used to preventing and kill off that the broad leaved weeds such as lamb's-quarters, amaranth, knotweed and barnyard grass, green bristlegrass, wild oat etc. be annual, perennial grassy weed.
Specific embodiment
Embodiment 1：
The acetone that total amount is 16% first being accounted in the first agitator tank to add, stirring being started under normal temperature, addition while stirring accounts for the Quizalotop-ethyl that total amount is 7%, accounts for the methyl naphthalene sulfonic acid sodium that total amount is 3%, stirring reaction 0.2 hour；The water that total amount is 62% first being accounted in high-speed stirred tank to add, stirring being started under normal temperature, the rotating speed of agitator is 40 revs/min, all thats for accounting for that total amount is 12% are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 210 revs/min, the mixture of acetone, Quizalotop-ethyl, methyl naphthalene sulfonic acid sodium is slowly added into high-speed stirred tank, stirring reaction obtains finished product after 0.6 hour.
Embodiment 2：
The acetone that total amount is 16% first being accounted in the first agitator tank to add, stirring being started under normal temperature, addition while stirring accounts for the Quizalotop-ethyl that total amount is 6.5%, accounts for the methyl naphthalene sulfonic acid sodium that total amount is 3%, stirring reaction 0.25 hour；The water that total amount is 62% first being accounted in high-speed stirred tank to add, stirring being started under normal temperature, the rotating speed of agitator is 35 revs/min, all thats for accounting for that total amount is 12.5% are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 215 revs/min, the mixture of acetone, Quizalotop-ethyl, methyl naphthalene sulfonic acid sodium is slowly added into high-speed stirred tank, stirring reaction obtains finished product after 0.55 hour.
Embodiment 3：
The acetone that total amount is 16% first being accounted in the first agitator tank to add, stirring being started under normal temperature, addition while stirring accounts for the Quizalotop-ethyl that total amount is 6%, accounts for the methyl naphthalene sulfonic acid sodium that total amount is 3%, stirring reaction 0.3 hour；The water that total amount is 62% first being accounted in high-speed stirred tank to add, stirring being started under normal temperature, the rotating speed of agitator is 30 revs/min, all thats for accounting for that total amount is 13% are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 220 revs/min, the mixture of acetone, Quizalotop-ethyl, methyl naphthalene sulfonic acid sodium is slowly added into high-speed stirred tank, stirring reaction obtains finished product after 0.5 hour.
Claims (3)
1. a kind of compound method of all you and Quizalotop-ethyl microemulsion, the weight proportion using raw material is：All your 12-13%, Quizalotop-ethyl 6-7%, acetone 16%, methyl naphthalene sulfonic acid sodium 3%, water 62%；It is characterized in that：
（1）First the acetone of formula ratio is added in the first agitator tank, stirring is started under normal temperature, Quizalotop-ethyl, the methyl naphthalene sulfonic acid sodium of formula ratio, stirring reaction 0.2-0.3 hours are added while stirring；
（2）First the water of formula ratio is added in high-speed stirred tank, stirring is started under normal temperature, the rotating speed of agitator is 30-40 revs/min, and all thats of formula ratio are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 210-220 revs/min, the mixture of acetone, Quizalotop-ethyl, methyl naphthalene sulfonic acid sodium is slowly added into high-speed stirred tank, finished product is obtained after stirring reaction 0.5-0.6 hours.
2. the compound method of as claimed in claim 1 a kind of all you and Quizalotop-ethyl microemulsion, it is characterised in that：Described all your purity is that the purity of 80%, Quizalotop-ethyl is 70%.
3. the compound method of as claimed in claim 1 a kind of all you and Quizalotop-ethyl microemulsion, it is characterised in that：Step（1）, step（2）Described normal temperature is 0-38 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510892935.XA CN106852329A (en) | 2015-12-08 | 2015-12-08 | A kind of all your compound methods with Quizalotop-ethyl microemulsion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510892935.XA CN106852329A (en) | 2015-12-08 | 2015-12-08 | A kind of all your compound methods with Quizalotop-ethyl microemulsion |
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| Publication Number | Publication Date |
|---|---|
| CN106852329A true CN106852329A (en) | 2017-06-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510892935.XA Pending CN106852329A (en) | 2015-12-08 | 2015-12-08 | A kind of all your compound methods with Quizalotop-ethyl microemulsion |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108902142A (en) * | 2018-08-08 | 2018-11-30 | 许昌市建安区昌盛日化实业有限公司 | A kind of Herbicidal combinations and nursery hedgerow herbicides special |
| CN110352974A (en) * | 2019-08-28 | 2019-10-22 | 沈阳农业大学 | Early stage herbicidal ative composition and herbicide after one seedling |
-
2015
- 2015-12-08 CN CN201510892935.XA patent/CN106852329A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108902142A (en) * | 2018-08-08 | 2018-11-30 | 许昌市建安区昌盛日化实业有限公司 | A kind of Herbicidal combinations and nursery hedgerow herbicides special |
| CN110352974A (en) * | 2019-08-28 | 2019-10-22 | 沈阳农业大学 | Early stage herbicidal ative composition and herbicide after one seedling |
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| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170616 |
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| WD01 | Invention patent application deemed withdrawn after publication |