CN106852330A - A kind of all your compound methods with atrazine microemulsion - Google Patents
A kind of all your compound methods with atrazine microemulsion Download PDFInfo
- Publication number
- CN106852330A CN106852330A CN201510892448.3A CN201510892448A CN106852330A CN 106852330 A CN106852330 A CN 106852330A CN 201510892448 A CN201510892448 A CN 201510892448A CN 106852330 A CN106852330 A CN 106852330A
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- CN
- China
- Prior art keywords
- atrazine
- stirring
- added
- weeds
- ethanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
- A01N37/22—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof the nitrogen atom being directly attached to an aromatic ring system, e.g. anilides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/66—1,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms
- A01N43/68—1,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms with two or three nitrogen atoms directly attached to ring carbon atoms
- A01N43/70—Diamino—1,3,5—triazines with only one oxygen, sulfur or halogen atom or only one cyano, thiocyano (—SCN), cyanato (—OCN) or azido (—N3) group directly attached to a ring carbon atom
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Toxicology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of all your compound methods with atrazine microemulsion, the product belongs to herbicide field；The present invention is raw material with that 12-13%, atrazine 5-6%, ethanol 16%, Negel 5%, water 61%, and by blending finished product under given conditions, the advantage of the production method is：Using common apparatus, process is simple, reaction condition be gentle, pollution-free waste discharge；All you and atrazines have synergistic effect, will all after you and two kinds of herbicides of atrazine and auxiliary material compounding, and higher than alone all you or atrazine, the effect of management of weeds is greatly enhanced the effect is significant of management of weeds, and the kind of management of weeds is greatly increased.
Description
Technical field
The invention belongs to herbicide field, more particularly to a kind of all your compound methods with atrazine microemulsion.
Background technology
All you are amide-type selective herbicide, and sterling is colourless liquid, and odorless can be partially soluble in water when more than 20 DEG C, to people and animals' low toxicity.All you are main is absorbed by young shoot, conduction upwards, suppress the growth of young shoot and root, the protein synthesis of the main sprout inhibition seed of mechanism of action, secondly suppress choline and penetrate into phosphatide, interference lecithin is formed, and because the ability that grassy weed young shoot absorbs all thats is stronger than broad leaved weed, thus the medicine prevents and kill off the effect of grassy weed far better than broad leaved weed.All your missible oil is brown color liquid, emulsifiability is good, can mutually be mixed with many herbicides, it is used in dry crop more, such as vegetables, orchard, nursery, the broad leaved weeds such as annual gramineous weed and three-coloured amaranth, purslane such as eleusine indica, lady's-grass, green bristlegrass, cotton grass and cyperus iria, chufa, 20-50 days lasting period in soil can effectively be prevented and kill off.Atrazine is mainly absorbed by plant root and conducted upwards, suppress the photosynthesis of weeds, make its withered, it is characterized in interior and inhales selective before seedling, after seedling closing herbicide, based on root absorption, cauline leaf absorbs little, and its herbicide controlling spectrum is wider, various annual gramineaes and broad leaved weed can be prevented and kill off, it is adaptable to which the dry crop such as corn, sorghum, sugarcane, fruit tree, nursery, forest land is prevented and kill off
Lady's-grass, barnyard grass, green bristlegrass, nutgrass flatsedge, amur foxtail, knotweed, lamb's-quarters, Cruciferae, pulse family weeds, especially there is preferable selectivity to corn, also have certain inhibitory action to some perennial weeds.After inciting somebody to action all thats and two kinds of herbicides of atrazine and auxiliary material compounding, higher than alone all that or atrazine, the effect of management of weeds is greatly enhanced the effect is significant of management of weeds, and the kind of management of weeds is greatly increased.
The content of the invention
Present invention mainly solves problem be to provide a kind of compound method of all you and atrazine microemulsion, produce the raw material that the product uses is by weight ratio：All your 12-13%, atrazine 5-6%, ethanol 16%, Negel 5%, water 61%.
The technical solution adopted by the present invention is：
（1）First the ethanol of formula ratio is added in the first agitator tank, stirring is started under normal temperature, atrazine, the base sodium naphthalene sulfonate of formula ratio, stirring reaction 0.4-0.5 hours are added while stirring；
（2）First the water of formula ratio is added in high-speed stirred tank, stirring is started under normal temperature, the rotating speed of agitator is 30-40 revs/min, and all thats of formula ratio are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 210-220 revs/min, the mixture of ethanol, atrazine, base sodium naphthalene sulfonate is slowly added into high-speed stirred tank, finished product is obtained after stirring reaction 0.7-0.8 hours.
Further technical scheme of the invention is：
Described all your purity is that the purity of 80%, atrazine is 75%.
Step（1）, step（2）Described normal temperature is 0-38 DEG C.
The beneficial effects of the invention are as follows：There is provided a kind of all your compound methods with atrazine microemulsion, the advantage of the production method is：Process is simple, environmental pollution is small, the reaction time is short, reaction condition is gentle, all you and atrazine have synergistic effect, after inciting somebody to action all thats and two kinds of herbicides of atrazine and auxiliary material compounding, the effect is significant of management of weeds is higher than alone all you or atrazine, the effect of management of weeds is greatly enhanced, and the kind of management of weeds is greatly increased.
Specific embodiment
Embodiment 1：
The ethanol that total amount 16% will be first accounted in the first agitator tank is added, and stirring is started under normal temperature, is added while stirring and is accounted for the atrazine of total amount 6%, accounts for the base sodium naphthalene sulfonate of total amount 5%, stirring reaction 0.4 hour；The water that total amount 61% will be first accounted in high-speed stirred tank is added, and stirring is started under normal temperature, and the rotating speed of agitator is 30 revs/min, and all thats for accounting for total amount 12% are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 210 revs/min, the mixture of ethanol, atrazine, base sodium naphthalene sulfonate is slowly added into high-speed stirred tank, stirring reaction obtains finished product after 0.7 hour.
Embodiment 2：
The ethanol that total amount 16% will be first accounted in the first agitator tank is added, and stirring is started under normal temperature, is added while stirring and is accounted for the atrazine of total amount 5.5%, accounts for the base sodium naphthalene sulfonate of total amount 5%, stirring reaction 0.45 hour；The water that total amount 61% will be first accounted in high-speed stirred tank is added, and stirring is started under normal temperature, and the rotating speed of agitator is 35 revs/min, and all thats for accounting for total amount 12.5% are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 215 revs/min, the mixture of ethanol, atrazine, base sodium naphthalene sulfonate is slowly added into high-speed stirred tank, stirring reaction obtains finished product after 0.75 hour.
Embodiment 3：
The ethanol that total amount 16% will be first accounted in the first agitator tank is added, and stirring is started under normal temperature, is added while stirring and is accounted for the atrazine of total amount 5%, accounts for the base sodium naphthalene sulfonate of total amount 5%, stirring reaction 0.5 hour；The water that total amount 61% will be first accounted in high-speed stirred tank is added, and stirring is started under normal temperature, and the rotating speed of agitator is 40 revs/min, and all thats for accounting for total amount 13% are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 220 revs/min, the mixture of ethanol, atrazine, base sodium naphthalene sulfonate is slowly added into high-speed stirred tank, stirring reaction obtains finished product after 0.8 hour.
Claims (3)
1. a kind of compound method of all you and atrazine microemulsion, the weight proportion using raw material is：All your 12-13%, atrazine 5-6%, ethanol 16%, Negel 5%, water 61%；It is characterized in that：
（1）First the ethanol of formula ratio is added in the first agitator tank, stirring is started under normal temperature, atrazine, the base sodium naphthalene sulfonate of formula ratio, stirring reaction 0.4-0.5 hours are added while stirring；
（2）First the water of formula ratio is added in high-speed stirred tank, stirring is started under normal temperature, the rotating speed of agitator is 30-40 revs/min, and all thats of formula ratio are added while stirring；The rotating speed of agitator in fast agitator tank is heightened for 210-220 revs/min, the mixture of ethanol, atrazine, base sodium naphthalene sulfonate is slowly added into high-speed stirred tank, finished product is obtained after stirring reaction 0.7-0.8 hours.
2. the compound method of as claimed in claim 1 a kind of all you and atrazine microemulsion, it is characterised in that：Described all your purity is that the purity of 80%, atrazine is 75%.
3. the compound method of as claimed in claim 1 a kind of all you and atrazine microemulsion, it is characterised in that：Step（1）, step（2）Described normal temperature is 0-38 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510892448.3A CN106852330A (en) | 2015-12-08 | 2015-12-08 | A kind of all your compound methods with atrazine microemulsion |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510892448.3A CN106852330A (en) | 2015-12-08 | 2015-12-08 | A kind of all your compound methods with atrazine microemulsion |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106852330A true CN106852330A (en) | 2017-06-16 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510892448.3A Pending CN106852330A (en) | 2015-12-08 | 2015-12-08 | A kind of all your compound methods with atrazine microemulsion |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106852330A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108124886A (en) * | 2017-12-23 | 2018-06-08 | 山东滨农科技有限公司 | A kind of herbicidal composition containing isopropyl methoxalamine |
-
2015
- 2015-12-08 CN CN201510892448.3A patent/CN106852330A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108124886A (en) * | 2017-12-23 | 2018-06-08 | 山东滨农科技有限公司 | A kind of herbicidal composition containing isopropyl methoxalamine |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170616 |
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| WD01 | Invention patent application deemed withdrawn after publication |