CN106561647A - Corythucha ciliate adult dispelling agent - Google Patents
Corythucha ciliate adult dispelling agent Download PDFInfo
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- CN106561647A CN106561647A CN201610972466.7A CN201610972466A CN106561647A CN 106561647 A CN106561647 A CN 106561647A CN 201610972466 A CN201610972466 A CN 201610972466A CN 106561647 A CN106561647 A CN 106561647A
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- trans
- caryophyllene
- liquid paraffin
- adult
- solution
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N27/00—Biocides, pest repellants or attractants, or plant growth regulators containing hydrocarbons
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- Life Sciences & Earth Sciences (AREA)
- Dentistry (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Agronomy & Crop Science (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention discloses a corythucha ciliate adult dispelling agent, in which trans-beta-caryophyllene is a functional component. The trans-beta-caryophyllene can be processed in the form of a trans-beta-caryophyllene liquid paraffin solution, and preferably, the concentration of the liquid paraffin solution is 0.01 [mu]g/[mu]l, 0.1 [mu]g/[mu]l and 1 [mu]g/[mu]l. The corythucha ciliate adult dispelling agent is prepared from existing chemical products, wherein the components are stable and the dispelling agent is simple in preparation method. The dispelling agent has significant dispelling effect on corythucha ciliate adults and may be applied in prevention and treatment of the corythucha ciliate. The dispelling agent can prevent damages caused by the corythucha ciliate. The components are industrial raw materials, so that the dispelling agent is simple in preparation method, has low cost, is safe to human and animals, is free of environment pollution and has wide application prospect.
Description
Technical field
The present invention relates to a kind of insect repellent, and in particular to one kind is used to prevent and treat corythucha ciliate
The repellant of (Corythucha ciliata) adult.
Background technology
Corythucha ciliate Corythucha ciliata (Say), belongs to Semiptera (Hemiptera), Tingidae
(Tingidae), square wing lace bug belongs to (Corythucha).Original is distributed in North America Middle Eastern, subsequently in succession incoming Europe,
The ground such as Asia, with extremely strong diffusivity.Corythucha ciliate can directly endanger plane plant, moreover it is possible to propagate outstanding bell
Wooden leaf spoting bacteria (Gnomonia platani) and Ceratocystis fimbriata bacterium (Geratocystis fimbriata) coordinated damage, can
Trees are caused to fall leaves in advance, growth interruption, tree vigo(u)r be weak or even death.The worm from 2006 Wuhan find first invasion after,
Spread throughout the country rapidly, at present in China Hunan, Hubei, Shanghai, Zhejiang, Jiangsu, Shandong, Henan, Chongqing, Guizhou and north
There is harm on the ground such as capital.The State Administration of Forestry 2006 lists China's forestry danger harmful organism list, 2007 and handle in the worm
The worm is published as poor risk Harmful.
At present, for the preventing and treating of plane tree square chi lace bug depends on insecticide, including tree crown spraying, trunk injection and
The methods such as trunk spraying.But, it is relatively costly using insecticide.Plane tree is widely used in urban afforestation in China, and the worm is main
Occur in city and residential quarter, therefore can also dirt be caused to environment for insecticide constitutes harm using meeting to human health
Dye, and the stinkbug has generated drug resistance to phosphoric acid ester insecticide.Therefore, exploitation is sustainable, eco-friendly prevents and treats skill
Art becomes the task of top priority.
Pest damage is controlled using the infochemical of insecticide itself, not only prevention effect is good, and environmentally friendly, because
This becomes one of important means of pests control in sustainable agriculture.The present invention is based on this premise, it is intended to find a kind of safe nothing
Corythucha ciliate adult repellent agent that is harmful, with low cost, being easy to popularization.
The content of the invention
It is an object of the invention to provide a kind of stably the good corythucha ciliate adult of release, prevention effect can walk quickly and keep away
Agent.
A kind of corythucha ciliate adult repellent agent, including solvent and functional component, the functional component be trans-β-
Caryophyllene.
The solvent is liquid paraffin.
The concentration of the trans-β-caryophyllene is 0.01 μ g/ μ L-1 μ g/ μ L.
The repellent agent is the trans-β-caryophyllene solution of 0.01 μ g/ μ L, 0.1 μ g/ μ L and 1 μ g/ μ L.
Corythucha ciliate is prepared into repellent agent using following methods, prepare first the trans-β-caryophyllene of 1 μ g/ μ L/
Liquid paraffin solution, vibration makes its mix homogeneously, then trans-β-caryophyllene/liquid paraffin solution is used successively into liquid paraffin
It is diluted to the trans-β-caryophyllene solution of desired concn.
Described trans-β-caryophyllene is bought from Sigma-Aldrich.
Application of the trans-β-caryophyllene as repellent agent functional component in corythucha ciliate is prevented and treated.
The present invention early stage corythucha ciliate alarm pheromones research on the basis of, find one kind can effectively walk quickly and keep away it is outstanding
Compound trans-β-the caryophyllene of Suzuki side wing lace bug adult, the compound is the raw material of industry, and preparation method is simple, and price is low
It is honest and clean, and to person poultry safety, it is free from environmental pollution, have broad application prospects.
Description of the drawings
Trans-the β of Fig. 1-caryophyllene walks quickly and keeps away effect to corythucha ciliate adult.
Specific embodiment
Following examples are that the present invention is further illustrated, rather than limitation of the present invention.
Embodiment 1：
Agents useful for same concentration is：
1) trans-β-caryophyllene solution of 1 μ g/ μ L, solvent needed for dilution is liquid paraffin.
2) trans-β-caryophyllene solution of 0.1 μ g/ μ L, solvent needed for dilution is liquid paraffin.
3) trans-β-caryophyllene solution of 0.01 μ g/ μ L, solvent needed for dilution is liquid paraffin.
4) trans-β-caryophyllene solution of 0.001 μ g/ μ L, solvent needed for dilution is liquid paraffin.
The compound method of above-mentioned solution：Trans-β-caryophyllene/liquid paraffin the solution of 1 μ g/ μ L is prepared first, and vibration makes
Its mix homogeneously, is then diluted to the anti-of desired concn with liquid paraffin successively by trans-β-caryophyllene/liquid paraffin solution
Formula-β-caryophyllene solution, so as to make the corythucha ciliate adult repellant of the present invention.
1. the two-arm and length of straight pipe of Y-shaped olfactometer is 10 centimetres, a diameter of 1.5 centimetres.Air flow rate is by stream
Gauge is controlled at 250 milliliters per minute.The corythucha ciliate adult for just sprouting wings is for the experiment.
2. 10 μ l are taken every time with pipettor to be added on filter paper block, compareed with liquid paraffin, be placed on Y-shaped olfactometer two
End, accesses every time a cephalont, accesses from the mouth of pipe, observes 10 minutes, records result.If do not made a choice, nothing is recorded as
Reaction.
3. 10 cephalonts are often done, is overturned and is exchanged Y-shaped pipe left and right directions, to exclude impact of the environment to experimental result.Often survey
After trying 20 cephalonts, cleaned with acetone, then with steeped ethanol absorbent cotton wipe olfactometer inwall, with distilled water flushing after,
Dry in baking oven.
4. entirely determine and carry out in behavior case, temperature control is at 26 DEG C.Repetition 5-7 time is tested, every time 10 cephalont.As a result
Such as Fig. 1.
As seen from Figure 1,1 μ g/ μ L, 0.1 μ g/ μ L and the trans-β-caryophyllene of 0.01 μ g/ μ L can effectively to plane tree
Square wing lace bug adult is walked quickly and kept away, and with higher rate is walked quickly and kept away, and is advantageously implemented the bionomic control of corythucha ciliate.Thus
Show, the corythucha ciliate adult repellent agent of the present invention has good effect.
Embodiment 2：
Agents useful for same concentration is：
1) trans-β-caryophyllene solution of 1 μ g/ μ L, solvent needed for dilution is liquid paraffin.
2) trans-β-caryophyllene solution of 0.1 μ g/ μ L, solvent needed for dilution is liquid paraffin.
3) trans-β-caryophyllene solution of 0.01 μ g/ μ L, solvent needed for dilution is liquid paraffin.
4) trans-β-caryophyllene solution of 0.001 μ g/ μ L, solvent needed for dilution is liquid paraffin.
The compound method of above-mentioned solution：Trans-β-caryophyllene/liquid paraffin the solution of 1 μ g/ μ L is prepared first, and vibration makes
Its mix homogeneously, is then diluted to the anti-of desired concn with liquid paraffin successively by trans-β-caryophyllene/liquid paraffin solution
Formula-β-caryophyllene solution, so as to make the corythucha ciliate adult repellant of the present invention.Trans-β-caryophyllene is liquid
Preparation, is directly diluted to above-mentioned each strength solution with liquid paraffin.
If 1. field acquisition dry tablet has the blade of a large amount of adults.
2. on blade with liquid-transfering gun gently plus 1 μ g/ μ L the μ L of trans-β-caryophyllene solution 1, every 2min record one
Secondary, 4min when altogether calculates the mobility of adult to weigh the effect of walking quickly and keeping away of trans-β-caryophyllene, concrete outcome such as table 1：
3. 1 μ g/ μ L, 0.1 μ g/ μ L, 0.01 μ g/ μ L and the trans-β-caryophyllene pair of 0.001 μ g/ μ L are carried out as stated above
Adult walks quickly and keeps away the experiment of effect.
4. above-mentioned experiment is using liquid paraffin solution as control, and experiment process method is identical.
Table 1：Trans-β-caryophyllene walks quickly and keeps away effect to corythucha ciliate adult
As can be seen from Table 1,1 μ g/ μ L, 0.1 μ g/ μ L, the trans-β-caryophyllene of 0.01 μ g/ μ L are to corythucha ciliate
Adult walks quickly and keeps away effect substantially, it is indicated above that the corythucha ciliate adult repellent agent of the present invention has good effect.
Claims (8)
1. a kind of corythucha ciliate adult repellent agent, including solvent and functional component, the functional component is trans-β-stone
Bamboo alkene.
2. repellent agent according to claim 1, the solvent is liquid paraffin.
3. repellent agent according to claim 2, the concentration of the trans-β-caryophyllene is 0.01 μ g/ μ L-1 μ g/ μ L.
4. repellent agent according to claim 3, the repellent agent be 0.01 μ g/ μ L, 0.1 μ g/ μ L and 1 μ g/ μ L it is trans-
The liquid paraffin solution of β-caryophyllene.
5. the compound method of corythucha ciliate adult repellent agent according to claim 1, prepares first 1 μ g/ μ L's
Trans-β-caryophyllene/liquid paraffin solution, vibration makes its mix homogeneously, then by trans-β-caryophyllene/liquid paraffin solution
Trans-β-caryophyllene the solution of desired concn is diluted to liquid paraffin successively, so as to make plane tree side's wing net of the present invention
Stinkbug adult repellant.
6. application of the trans-β-caryophyllene as repellent agent functional component in corythucha ciliate is prevented and treated.
7. application according to claim 6, the trans-β-caryophyllene is dissolved in solvent liquid paraffin and forms solution.
8. application according to claim 7, the concentration of the trans-β-caryophyllene is 0.1mg/mL-1mg/mL.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610972466.7A CN106561647B (en) | 2016-11-01 | 2016-11-01 | A kind of corythucha ciliate adult repellant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610972466.7A CN106561647B (en) | 2016-11-01 | 2016-11-01 | A kind of corythucha ciliate adult repellant |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106561647A true CN106561647A (en) | 2017-04-19 |
| CN106561647B CN106561647B (en) | 2018-10-12 |
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| CN201610972466.7A Active CN106561647B (en) | 2016-11-01 | 2016-11-01 | A kind of corythucha ciliate adult repellant |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102084860A (en) * | 2011-03-15 | 2011-06-08 | 浙江农林大学 | Bisexual adult attractant for colorado potato beetles |
| CN103651305A (en) * | 2013-12-22 | 2014-03-26 | 中国计量学院 | Method for trapping empoasca vitis gothe by means of tea plantation weed rosemary smell |
| CN103931581A (en) * | 2014-03-01 | 2014-07-23 | 中国计量学院 | Method for trapping and killing empoasca vitis by using mint volatile matter |
| CN104094928A (en) * | 2014-07-31 | 2014-10-15 | 福建省农业科学院植物保护研究所 | Mango deporaus marginatus pascoe attractant and preparation method thereof |
| CN104782594A (en) * | 2015-02-03 | 2015-07-22 | 中国农业科学院植物保护研究所 | Composite attractant luring female and male moths of chilo suppressalis simultaneously and application of composite attractant |
-
2016
- 2016-11-01 CN CN201610972466.7A patent/CN106561647B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102084860A (en) * | 2011-03-15 | 2011-06-08 | 浙江农林大学 | Bisexual adult attractant for colorado potato beetles |
| CN103651305A (en) * | 2013-12-22 | 2014-03-26 | 中国计量学院 | Method for trapping empoasca vitis gothe by means of tea plantation weed rosemary smell |
| CN103931581A (en) * | 2014-03-01 | 2014-07-23 | 中国计量学院 | Method for trapping and killing empoasca vitis by using mint volatile matter |
| CN104094928A (en) * | 2014-07-31 | 2014-10-15 | 福建省农业科学院植物保护研究所 | Mango deporaus marginatus pascoe attractant and preparation method thereof |
| CN104782594A (en) * | 2015-02-03 | 2015-07-22 | 中国农业科学院植物保护研究所 | Composite attractant luring female and male moths of chilo suppressalis simultaneously and application of composite attractant |
Non-Patent Citations (1)
| Title |
|---|
| 徐延熙等: "被害马尾松(Pinus massoniana)针叶挥发性物质的提取、鉴定及蚕饰腹寄蝇(Blepharipa zebina)的电生理活性", 《生态学报》 * |
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| CN106561647B (en) | 2018-10-12 |
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Effective date of registration: 20211125 Address after: 300457 east of Fengshan Road, south of Caiyun East Street, west of Zhongshan Road and north of Changhong East Street, modern industrial park, Tianjin Economic and Technological Development Zone, Binhai New Area, Tianjin Patentee after: Zhongnong Fengmao Plant Protection Machinery Co.,Ltd. Address before: 11 Shuguang Huayuan Middle Road, Haidian District, Beijing 100097 Patentee before: BEIJING ACADEMY OF AGRICULTURE AND FORESTRY SCIENCES |
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