CN106544139A - A kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss - Google Patents
A kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss Download PDFInfo
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- CN106544139A CN106544139A CN201610966139.0A CN201610966139A CN106544139A CN 106544139 A CN106544139 A CN 106544139A CN 201610966139 A CN201610966139 A CN 201610966139A CN 106544139 A CN106544139 A CN 106544139A
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/085—Phosphorus oxides, acids or salts
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/022—Ethene
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- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/024—Propene
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- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/16—Paraffin waxes; Petrolatum, e.g. slack wax
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/281—Esters of (cyclo)aliphatic monocarboxylic acids
- C10M2207/2815—Esters of (cyclo)aliphatic monocarboxylic acids used as base material
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/08—Halogenated waxes
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/08—Amides
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- C—CHEMISTRY; METALLURGY
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/024—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/06—Thio-acids; Thiocyanates; Derivatives thereof
- C10M2219/062—Thio-acids; Thiocyanates; Derivatives thereof having carbon-to-sulfur double bonds
- C10M2219/066—Thiocarbamic type compounds
- C10M2219/068—Thiocarbamate metal salts
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/09—Heterocyclic compounds containing no sulfur, selenium or tellurium compounds in the ring
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/049—Phosphite
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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Abstract
The invention discloses a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss, are combined as composite foundation oil using the metallocene polyalphaolefin base of mass ratio 50% and 50% Esters oil butyl stearate, coordinate various compound additives.Including:Antioxidant, metal deactivator, oiliness improver, friction improver, extreme pressure agent, antiwear additive, antirust agent, oxidation and corrosion inhibitor, viscosifier, filler etc..The characteristics of compositionss of the present invention have good cooling, lubricity, diffusibility, cleaning, rust-preventing characteristic, antioxygen anti-corrosive properties, reduction galled spotss and adhesiveness.
Description
Technical field
A kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss of the present invention belong to metal working lubricant field.
Background technology
Tungsten alloy is the alloy for adding other elements composition with tungsten as base.In a metal, the fusing point highest of tungsten, elevated temperature strength
It is all good with creep-resistant property and heat conduction, conductive and electron emission capability, than great, except being largely used to manufacture hard alloy and work
Outside alloy addition, tungsten and its alloy are widely used in electronics, electric light source industry, are also used in the departments such as space flight, casting, weapon
Make rocket nozzle, die casting, armor-piercing bullet core, contact, heater and heat screen etc..
Rotary pressure technology originates from ancient times pottery, is that one kind combines forging, extruding, draw piece, bending, looping mill rolling, transverse rolling
With few advanced technologies without machining of the process characteristic such as edging.Generally by metal letter base, plate blank or prefabricated blank tail
Hold out against on spinning machine mould, plug and blank rotation are driven by main shaft;Material is squeezed in by spinning wheel from blank side simultaneously
On the core of rotation, material is made to produce the continuous plastic deformation of pointwise, so as to obtain the hollow rotary body zero of various shape of generatrix
Part.According to the blank thickness situation of change during rotary pressing processing, spinning process is divided into two kinds of conventional spinning and shear spinning,
That is conventional spinning and shear spinning.
The referred to as general rotation of conventional spinning.During general rotation, the thickness of blank is held essentially constant, and shaping relies primarily on blank edge
The contraction of circumference and along radial direction it is indeformable realizing with length.Which is mainly characterized by forming process, substantially can be seen
Go out the change of blank external diameter.The basic mode of conventional spinning has:Draw spinning (drawing rotation), necking in spindown (contracting rotation) and expanding bulging
Three kinds of (expanding rotation) etc..
Tungsten alloy temperature rotary pressing processing technology lubricant requires there is good thermal oxidation stability, antifriction extreme-pressure anti-wear, adhesion
Property, low volatility, enough film strengths and thickness, with big lower pressure and vibration produced by overcoming during warm rotary pressing processing
And because the strength of materials is high, poor ductility, deformation are difficult, mould infringement is big, and precision is difficult to ensure that, processes the severe technology of operating mode
Problem.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of with good cooling, lubricity, diffusibility, cleaning
Property, rust-preventing characteristic, antioxygen anti-corrosive properties and adhesiveness, the tungsten alloy temperature rotary pressing processing technology lubricant for reducing galled spotss combines
Thing.
The present invention solves above-mentioned technical problem by following technical solution:
A kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss, using the metallocene poly alpha olefin base of mass ratio 50%
Plinth oil and 50% Esters oil butyl stearate it is compound coordinate various compound additives as composite foundation oil, its respective quality
Percent into being grouped into:
Component | Mass percentage content |
Base oil | Surplus |
Antioxidant | 0.05~0.3% |
Metal deactivator | 0.05~0.3% |
Oiliness improver | 4~6% |
Friction improver | 1~2% |
Extreme pressure agent | 3~5% |
Antiwear additive | 5~7% |
Antirust agent | 0.06~0.3% |
Oxidation and corrosion inhibitor | 0.5~1.2% |
Viscosifier | 2~6% |
Filler | 3~5% |
The mass percent summation of above each component is 100%.
Antioxidant is that the sulfenyl phenolate T504 of the butyl octyl diphenylamines T557 and 50% using mass ratio 50% is combined.
Metal deactivator is using benzotriazole derivant T551.Oiliness improver is sulfuration cottonseed oil T404.
Friction improver is sulfur cupric phosphate T461.Extreme pressure agent is acid dibutyl phosphite T304.
Antiwear additive is chlorination stone sodium T502.
Antirust agent be the 2-mercaptobenzimidazole of mass ratio 50% and 50% N- oleoyl propylhomoserin octadecylammonium salt T711 it is multiple
Close.
Oxidation and corrosion inhibitor is dialkyl dithio amino tungsten.Viscosifier are ethylene-propylene copolymer T613A.
Filler is No. 85 microwaxes.
It is an advantage of the current invention that:
The present invention compositionss have good cooling, lubricity (extreme-pressure anti-wear load), diffusibility, cleaning,
Rust-preventing characteristic, antioxygen anti-corrosive properties, reduce galled spotss;There are good thermal oxidation stability, antifriction extreme-pressure anti-wear, adhesiveness and low wave
Send out property, have enough film strengths and thickness, with big lower pressure produced by overcoming during warm rotary pressing processing and vibration and
Because the strength of materials is high, poor ductility, deformation are difficult, and mould infringement is big, and precision is difficult to ensure that, process the severe technology of operating mode and ask
Topic.
Specific embodiment
Embodiment 1:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
Embodiment 2:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
Embodiment 3:
Following each component is pressed the mediation of row mass percent to form:
Above each component mass percentage content summation is 100%.
The key technical indexes of 3 product of embodiment
Project | Index |
100 DEG C of kinematic viscosity/(mm2﹒ s-1) | 24.5 |
Flash-point/DEG C | 271 |
Condensation point/DEG C | -26 |
Viscosity index (VI) | 146 |
82 DEG C of (40-37-3)/min of demulsification number | 10 |
Corrosion (copper sheet, 100 DEG C, 3h)/level | 1 |
Tetra-ball machine test, Pb/N | 1058 |
Sintering load, PD/N | 7810 |
Terraced nurse is agreed, N | 338 |
Moisture, % | Vestige |
Mechanical admixture, % | Nothing |
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % | 6.6 |
The key technical indexes of 2 product of embodiment
Project | Index |
100 DEG C of kinematic viscosity/(mm2﹒ s-1) | 24.1 |
Flash-point/DEG C | 266 |
Condensation point/DEG C | -28 |
Viscosity index (VI) | 162 |
82 DEG C of (40-37-3)/min of demulsification number | 11 |
Corrosion (copper sheet, 100 DEG C, 3h)/level | 1 |
Tetra-ball machine test, Pb/N | 1065 |
Sintering load, PD/N | 7836 |
Terraced nurse is agreed, N | 341 |
Moisture, % | Vestige |
Mechanical admixture, % | Nothing |
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % | 6.1 |
The key technical indexes of 1 product of embodiment
Project | Index |
100 DEG C of kinematic viscosity/(mm2﹒ s-1) | 24.9 |
Flash-point/DEG C | 274 |
Condensation point/DEG C | -26 |
Viscosity index (VI) | 154 |
82 DEG C of (40-37-3)/min of demulsification number | 9 |
Corrosion (copper sheet, 100 DEG C, 3h)/level | 1 |
Tetra-ball machine test, Pb/N | 1032 |
Sintering load, PD/N | 7785 |
Terraced nurse is agreed, N | 331 |
Moisture, % | Vestige |
Mechanical admixture, % | Nothing |
Evaporation loss (Noack methods, 250 DEG C, 1h) (m), % | 6.8 |
Claims (10)
1. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss, it is characterised in that:Using the metallocene of mass ratio 50%
Poly alpha olefin base oil and 50% Esters oil butyl stearate it is compound coordinate various compound additives as composite foundation oil,
Its each mass percent into being grouped into:
The mass percent summation of above each component is 100%.
2. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that antioxidant
It is that the sulfenyl phenolate T504 of butyl octyl diphenylamines T557 and 50% using mass ratio 50% is combined.
3. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that metal subtracts
Agent living is benzotriazole derivant T551.
4. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that oiliness improver
It is sulfuration cottonseed oil T404.
5. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that rub and change
It is sulfur cupric phosphate T461 to enter agent.
6. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that extreme pressure agent
It is acid dibutyl phosphite T304.
7. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that antiwear additive
It is chlorinated paraffin T502.
8. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that antirust agent
It is that the 2-mercaptobenzimidazole of mass ratio 50% and 50% N- oleoyl propylhomoserin octadecylammonium salt T711 are combined.
9. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that antioxygen is anti-
Rotten agent is dialkyl dithio amino tungsten.
10. a kind of tungsten alloy temperature rotary pressing processing technology lubricant compositionss as claimed in claim 1, it is characterised in that viscosifier
It is ethylene-propylene copolymer T613A;Filler is No. 85 microwaxes.
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Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103525526A (en) * | 2013-10-21 | 2014-01-22 | 广西大学 | Lubricant of tail gas recovery compressor |
CN104450070A (en) * | 2014-11-17 | 2015-03-25 | 广西大学 | Warm forging lubricant composition of tungsten and tungsten alloy |
CN105602679A (en) * | 2015-11-23 | 2016-05-25 | 广西大学 | Castor oil-based lubricant composition for circulatory system of ash-free paper machine |
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- 2016-11-04 CN CN201610966139.0A patent/CN106544139A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103525526A (en) * | 2013-10-21 | 2014-01-22 | 广西大学 | Lubricant of tail gas recovery compressor |
CN104450070A (en) * | 2014-11-17 | 2015-03-25 | 广西大学 | Warm forging lubricant composition of tungsten and tungsten alloy |
CN105602679A (en) * | 2015-11-23 | 2016-05-25 | 广西大学 | Castor oil-based lubricant composition for circulatory system of ash-free paper machine |
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