CN106525815A - 一种燃油样品拉曼光谱测试方法 - Google Patents
一种燃油样品拉曼光谱测试方法 Download PDFInfo
- Publication number
- CN106525815A CN106525815A CN201610991655.9A CN201610991655A CN106525815A CN 106525815 A CN106525815 A CN 106525815A CN 201610991655 A CN201610991655 A CN 201610991655A CN 106525815 A CN106525815 A CN 106525815A
- Authority
- CN
- China
- Prior art keywords
- oil sample
- fuel oil
- carbon material
- graphitized carbon
- test method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000001237 Raman spectrum Methods 0.000 title claims abstract description 60
- 239000000295 fuel oil Substances 0.000 title claims abstract description 44
- 238000000034 method Methods 0.000 title claims abstract description 34
- 239000003921 oil Substances 0.000 claims abstract description 51
- 238000001914 filtration Methods 0.000 claims abstract description 45
- 239000003575 carbonaceous material Substances 0.000 claims abstract description 42
- 238000012360 testing method Methods 0.000 claims abstract description 30
- 239000002245 particle Substances 0.000 claims abstract description 10
- 238000010998 test method Methods 0.000 claims description 23
- 229910052799 carbon Inorganic materials 0.000 claims description 22
- 150000001721 carbon Chemical group 0.000 claims description 15
- 229920000742 Cotton Polymers 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 10
- 229910052756 noble gas Inorganic materials 0.000 claims description 9
- 150000002835 noble gases Chemical class 0.000 claims description 9
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 6
- 230000007613 environmental effect Effects 0.000 claims description 6
- 239000006229 carbon black Substances 0.000 claims description 5
- 229910052786 argon Inorganic materials 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000004744 fabric Substances 0.000 claims description 2
- 239000011521 glass Substances 0.000 claims description 2
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 238000005087 graphitization Methods 0.000 claims 1
- 238000001179 sorption measurement Methods 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 3
- 125000005575 polycyclic aromatic hydrocarbon group Chemical group 0.000 abstract description 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 4
- 238000009396 hybridization Methods 0.000 abstract 2
- 150000004945 aromatic hydrocarbons Chemical class 0.000 abstract 1
- 238000001228 spectrum Methods 0.000 description 26
- 239000000463 material Substances 0.000 description 13
- 238000001069 Raman spectroscopy Methods 0.000 description 12
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 9
- 241000894007 species Species 0.000 description 5
- 230000003595 spectral effect Effects 0.000 description 5
- 238000001514 detection method Methods 0.000 description 4
- 239000002283 diesel fuel Substances 0.000 description 4
- 239000003502 gasoline Substances 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 125000003118 aryl group Chemical group 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 239000000446 fuel Substances 0.000 description 3
- 238000012545 processing Methods 0.000 description 3
- 238000004611 spectroscopical analysis Methods 0.000 description 3
- 239000004215 Carbon black (E152) Substances 0.000 description 2
- 230000003064 anti-oxidating effect Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 229930195733 hydrocarbon Natural products 0.000 description 2
- 150000002430 hydrocarbons Chemical class 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 241000872198 Serjania polyphylla Species 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 125000004429 atom Chemical group 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 238000002189 fluorescence spectrum Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000003209 petroleum derivative Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/62—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light
- G01N21/63—Systems in which the material investigated is excited whereby it emits light or causes a change in wavelength of the incident light optically excited
- G01N21/65—Raman scattering
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/34—Purifying; Cleaning
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Engineering & Computer Science (AREA)
- Biomedical Technology (AREA)
- Molecular Biology (AREA)
- Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610991655.9A CN106525815B (zh) | 2016-11-10 | 2016-11-10 | 一种燃油样品拉曼光谱测试方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610991655.9A CN106525815B (zh) | 2016-11-10 | 2016-11-10 | 一种燃油样品拉曼光谱测试方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106525815A true CN106525815A (zh) | 2017-03-22 |
CN106525815B CN106525815B (zh) | 2019-04-05 |
Family
ID=58351101
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610991655.9A Active CN106525815B (zh) | 2016-11-10 | 2016-11-10 | 一种燃油样品拉曼光谱测试方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106525815B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109459424A (zh) * | 2018-12-06 | 2019-03-12 | 浙江大学 | 一种柴油拉曼光谱荧光消除方法 |
CN110836885A (zh) * | 2019-12-19 | 2020-02-25 | 西安石油大学 | 一种基于拉曼光谱结合随机森林算法的汽油掺假鉴别分析方法 |
CN112782146A (zh) * | 2019-11-11 | 2021-05-11 | 中国石油天然气股份有限公司 | 一种基于拉曼光谱的汽油烯烃含量分析方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0989638A (ja) * | 1995-09-22 | 1997-04-04 | Hitachi Cable Ltd | 残留加工油量の測定方法 |
CN101323794A (zh) * | 2008-07-28 | 2008-12-17 | 华东理工大学 | 一种球形活性炭燃料油吸附脱硫剂及其制备方法 |
CN101403696A (zh) * | 2008-10-21 | 2009-04-08 | 浙江大学 | 一种基于拉曼光谱的测量汽油烯烃含量的方法 |
CN202398223U (zh) * | 2011-08-17 | 2012-08-29 | 金涌 | 石墨化碳纤维过滤介质 |
CN103645171A (zh) * | 2013-12-03 | 2014-03-19 | 深圳市疾病预防控制中心 | 一种基于拉曼光谱法检测地沟油的方法 |
CN105136682A (zh) * | 2015-07-06 | 2015-12-09 | 天津工业大学 | 一种燃油中芳烃含量快速、准确测定的新方法 |
-
2016
- 2016-11-10 CN CN201610991655.9A patent/CN106525815B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0989638A (ja) * | 1995-09-22 | 1997-04-04 | Hitachi Cable Ltd | 残留加工油量の測定方法 |
CN101323794A (zh) * | 2008-07-28 | 2008-12-17 | 华东理工大学 | 一种球形活性炭燃料油吸附脱硫剂及其制备方法 |
CN101403696A (zh) * | 2008-10-21 | 2009-04-08 | 浙江大学 | 一种基于拉曼光谱的测量汽油烯烃含量的方法 |
CN202398223U (zh) * | 2011-08-17 | 2012-08-29 | 金涌 | 石墨化碳纤维过滤介质 |
CN103645171A (zh) * | 2013-12-03 | 2014-03-19 | 深圳市疾病预防控制中心 | 一种基于拉曼光谱法检测地沟油的方法 |
CN105136682A (zh) * | 2015-07-06 | 2015-12-09 | 天津工业大学 | 一种燃油中芳烃含量快速、准确测定的新方法 |
Non-Patent Citations (4)
Title |
---|
O. A. MASLOVA ET AL.: "Determination of crystallite size in polished graphitized carbon by Raman spectroscopy", 《PHYSICAL REVIEW B》 * |
娄婷婷等: "激光拉曼指纹图谱鉴别石油产品初探", 《光谱学与光谱分析》 * |
张健等: "生物柴油/柴油颗粒的拉曼光谱分析", 《光谱学与光谱分析》 * |
田高友: "拉曼光谱技术在石油化工领域应用进展", 《现代科学仪器》 * |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109459424A (zh) * | 2018-12-06 | 2019-03-12 | 浙江大学 | 一种柴油拉曼光谱荧光消除方法 |
CN109459424B (zh) * | 2018-12-06 | 2020-04-03 | 浙江大学 | 一种柴油拉曼光谱荧光消除方法 |
CN112782146A (zh) * | 2019-11-11 | 2021-05-11 | 中国石油天然气股份有限公司 | 一种基于拉曼光谱的汽油烯烃含量分析方法 |
CN112782146B (zh) * | 2019-11-11 | 2022-11-04 | 中国石油天然气股份有限公司 | 一种基于拉曼光谱的汽油烯烃含量分析方法 |
CN110836885A (zh) * | 2019-12-19 | 2020-02-25 | 西安石油大学 | 一种基于拉曼光谱结合随机森林算法的汽油掺假鉴别分析方法 |
Also Published As
Publication number | Publication date |
---|---|
CN106525815B (zh) | 2019-04-05 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN106525815A (zh) | 一种燃油样品拉曼光谱测试方法 | |
CN109557071B (zh) | 一种危险液体混合物的拉曼光谱定性定量识别方法 | |
CN1614391A (zh) | 中草药真伪及质量鉴别的快速无损分析方法 | |
CN102435575A (zh) | 一种检测近红外二维相关光谱的方法 | |
CN107271426A (zh) | 一种用激光诱导击穿光谱检测重金属污水的预处理方法 | |
CN106365159B (zh) | 一种银纳米粒-碳纳米管嵌入的氧化石墨烯复合薄膜、及其制备方法和应用 | |
CN109459424B (zh) | 一种柴油拉曼光谱荧光消除方法 | |
CN110836881B (zh) | 石墨相氮化碳/金纳米粒子比色荧光检测抗生素的方法 | |
CN101738339B (zh) | 一种用于调合汽油的近红外成套预处理装置 | |
CN103592225A (zh) | 土壤红外光声光谱快速测定仪及其土壤理化性质测定方法 | |
CN115326985A (zh) | 一种蜈蚣配方颗粒特征图谱及其构建方法和应用 | |
Liu et al. | Surface functional groups and graphitization degree of soot in the sooting history of methane premixed flame | |
CN108693134A (zh) | 基于太赫兹时域光谱仪的鉴别手性药物的方法 | |
CN106769890A (zh) | 一种基于石墨烯增敏的光纤甲烷传感器及制备方法 | |
Carver et al. | Spectroscopic studies of explosives: 1—detection of nitro compounds on silica gel and carbon by non‐resonant Raman spectroscopy | |
Zhou et al. | Rapid Analysis of Fruit Acids by Laser-Engraved Free-Standing Terahertz Metamaterials | |
WO2020113723A1 (zh) | 用于对手性化合物进行检测的基底材料 | |
CN207832528U (zh) | 一种车载气体检测仪用采样探头 | |
Lv et al. | Differentiation of inks used for seals by confocal Raman microscopy and Fourier transform infrared microscopy | |
CN105445220A (zh) | 一种旋光异构体的简易鉴别方法 | |
Hemmings | Raman spectroscopy of fibres | |
CN104568546B (zh) | 一种制备大气颗粒物空白样品的方法 | |
CN110907427B (zh) | 一种氨基酸辅助的sers活性试纸的制备方法 | |
CN109959632B (zh) | 一种用近红外光谱技术检测水分子状态的方法 | |
RU2248571C1 (ru) | Способ экспресс-идентификации бензинов |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20231109 Address after: 401331 No.20, North 1st Road, Chenjiaqiao University Town, Shapingba District, Chongqing Patentee after: PLA Army Service College Address before: 401331 No.20, North 1st Road, Chenjiaqiao University Town, Shapingba District, Chongqing Patentee before: PLA Army Service College Patentee before: BEIJING KAISHENG RUICHENG TECHNOLOGY CO.,LTD. Effective date of registration: 20231109 Address after: 401331 No.20, North 1st Road, Chenjiaqiao University Town, Shapingba District, Chongqing Patentee after: PLA Army Service College Patentee after: BEIJING KAISHENG RUICHENG TECHNOLOGY CO.,LTD. Address before: 401311 College of Logistics Engineering, University Town, Shapingba District, Chongqing Patentee before: Logistical Engineering University of PLA Patentee before: BEIJING KAISHENG RUICHENG TECHNOLOGY CO.,LTD. |
|
TR01 | Transfer of patent right | ||
CB03 | Change of inventor or designer information |
Inventor after: Guan Liang Inventor after: Wang Liguang Inventor after: Li Sheng Inventor after: Gong Yingzhong Inventor after: Yu Xingchen Inventor before: Guan Liang Inventor before: Wang Liguang Inventor before: Li Sheng Inventor before: Gong Yingzhong Inventor before: Yu Xingchen Inventor before: Ji Nan |
|
CB03 | Change of inventor or designer information | ||
CI03 | Correction of invention patent |
Correction item: Inventor Correct: Guan Liang|Wang Liguang|Gong Yingzhong|Yu Xingchen False: Guan Liang|Wang Liguang|Li Sheng|Gong Yingzhong|Yu Xingchen Number: 48-02 Volume: 39 |
|
CI03 | Correction of invention patent |