CN106520308A - Lubricant composite for permalloy cold forging processing technology - Google Patents
Lubricant composite for permalloy cold forging processing technology Download PDFInfo
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- CN106520308A CN106520308A CN201610962500.2A CN201610962500A CN106520308A CN 106520308 A CN106520308 A CN 106520308A CN 201610962500 A CN201610962500 A CN 201610962500A CN 106520308 A CN106520308 A CN 106520308A
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/048—Mixtures of base-materials and additives the additives being a mixture of compounds of unknown or incompletely defined constitution, non-macromolecular and macromolecular compounds
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/06—Well-defined aromatic compounds
- C10M2203/065—Well-defined aromatic compounds used as base material
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/022—Ethene
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
- C10M2205/024—Propene
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
- C10M2205/18—Natural waxes, e.g. ceresin, ozocerite, bees wax, carnauba; Degras
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/08—Halogenated waxes
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
- C10M2215/064—Di- and triaryl amines
- C10M2215/065—Phenyl-Naphthyl amines
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/022—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of hydrocarbons, e.g. olefines
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/024—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/08—Thiols; Sulfides; Polysulfides; Mercaptals
- C10M2219/082—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms
- C10M2219/087—Thiols; Sulfides; Polysulfides; Mercaptals containing sulfur atoms bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Derivatives thereof, e.g. sulfurised phenols
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
- C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
- C10M2223/04—Phosphate esters
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2227/00—Organic non-macromolecular compounds containing atoms of elements not provided for in groups C10M2203/00, C10M2207/00, C10M2211/00, C10M2215/00, C10M2219/00 or C10M2223/00 as ingredients in lubricant compositions
- C10M2227/06—Organic compounds derived from inorganic acids or metal salts
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/04—Siloxanes with specific structure
- C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2290/00—Mixtures of base materials or thickeners or additives
- C10M2290/04—Synthetic base oils
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/04—Detergent property or dispersant property
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/244—Metal working of specific metals
Abstract
The invention discloses a lubricant composite for a permalloy cold forging processing technology. According to the lubricant composite, an MVI90BS base oil with the mass ratio of five sixths and alkyl naphthalene with the mass ratio of one sixth are compounded to serve as a base oil, and a variety of composite additives are added. The composite additives comprise an antioxidant, a metal deactivator, an oiliness agent, a friction modifier, an extreme pressure agent, an antiwear agent, an anti-foaming agent, an antirust agent, a tackifier and the like. The composite is excellent in lubricating property, good in diffusion property and leanability, great in oil film thickness and strength, good in cooling property and scuffing and scratching resistance, high in surface smoothness and long in corrosionproof period.
Description
Technical field
A kind of permalloy Cold Forging technology lubricant composition of the present invention belongs to metal working lubricant field.
Background technology
Permalloy refers to iron-nickel alloy, the wide range of its nickel content, between 35%-90%.The maximum of permalloy
Feature is with very high low-intensity magnetic field permeability.Their saturation induction density is typically between 0.6--1.0T.Permalloy
It is a kind of iron-nickel alloy for having higher magnetic conductivity under compared with low-intensity magnetic field, dilval of the nickel content more than 30%, in room temperature
Shi Douwei single-phase face-centered cubic (γ) structure, but the phase structure near 30%Ni is very unstable, therefore the iron nickel of practicality
Magnetically soft alloy, nickel content is all more than 36%.Iron-nickel alloy near nickeliferous 75% (atomic fraction), the meeting in this single-phase alloy
Generation Ni3Fe long-range orders change, at this moment the lattice constant and physical property of alloy, and such as resistivity and magnetic etc. can all occur to become
Change.Therefore, impact of the ordering transition to performance is considered.Generally in Ni3The additional elements such as a small amount of Mo or Cu are added in Fe alloys,
To suppress the generation of long-range order.
Cold forging refers to the various bulk formings that below the recrystallization temperature of metal is carried out.Cold forging is to material recrystallization temperature
Following processing and forming, is the forging carried out below recovery temperature.The forging that being accustomed to not heated blank in production is carried out claims
For cold forging.Cold forging surface quality is good, and dimensional accuracy is high, can replace some machinings.Cold forging can make metal strengthening, improve zero
The intensity of part.Cold-forging technique is a kind of precision plastic forming technology, with the unrivaled advantage of machining, the such as machine of product
Tool performance is good, productivity ratio is high and stock utilization is high, is particularly suitable for producing in enormous quantities, and can be used as the system of final products
Method is made, is had a wide range of applications in the industry such as transport facility Aero-Space and machine tool industry.
The content of the invention
The technical problem to be solved in the present invention is to provide that a kind of greasy property is excellent, diffusivity is good, cleaning is good, oil
Film thickness and intensity are big, cooling is good, anti scuffing and scratch are good, surface smoothness is high, the permalloy of anticorrosive cycle length
Cold Forging technology lubricant composition.
The present invention solves above-mentioned technical problem by following technical solution:
A kind of permalloy Cold Forging technology lubricant composition, the MVI90BS using mass ratio 5/6ths are basic
Oil and 1/6th alkylnaphthalenes it is compound based on oil, coordinate various compound additives, the composition of its respective mass percent
Composition:
The mass percent summation of above each component is 100%.
Antioxidant is that the N- phenyl-alpha-naphthylamines T531 of the sulfenyl phenolate T504 and 50% of mass ratio 50% is combined;
Metal deactivator is benzotriazole derivative T551.
Oiliness improver is sulfurized olefin cotton oil T405A;Friction improver is phosphate T451.
Extreme pressure agent is boronation phosphamidon ester T3011;Antiwear additive is chlorinated paraffin T301.
Anti-foaming agent is ethyl silicon oil;Antirust agent be the barium mahogany sulfonate of mass ratio 50% and 50% lanolin be combined.
Tackifier are ethylene-propylene copolymer T613A.
Remarkable advantage of the present invention is:The composition greasy property of the present invention is excellent, extreme-pressure anti-wear large carrying capacity, diffusion
Property it is good, cleaning is good, and oil film thickness and intensity are big, and cooling is good, and anti scuffing and scratch are good, and surface smoothness is high, resists
Abrasion cycle is long.
Specific embodiment
Embodiment 1:
Following each component is pressed the mediation of row mass percent to form:
Component | Mass percentage content |
The MVI90BS base oils of mass ratio 5/6ths and 1/6th alkylnaphthalene are compound | Surplus |
The sulfenyl phenolate (T504) of mass ratio 50% and 50% N- phenyl-alpha-naphthylamines (T531) are compound | 0.15% |
Benzotriazole derivative (T551) | 0.1% |
Sulfurized olefin cotton oil (T405A) | 4.5% |
Phosphate (T451) | 2.55% |
Boronation phosphamidon ester (T3011) | 3.5% |
Chlorinated paraffin (T301) | 4.5% |
Ethyl silicon oil | 20ppm |
The barium mahogany sulfonate of mass ratio 50% and 50% lanolin are compound | 0.4% |
Ethylene-propylene copolymer (T613A) | 2.1% |
Above each component mass percentage content summation is 100%.
Embodiment 2:
Following each component is pressed the mediation of row mass percent to form:
Component | Mass percentage content |
The MVI90BS base oils of mass ratio 5/6ths and 1/6th alkylnaphthalene are compound | Surplus |
The sulfenyl phenolate (T504) of mass ratio 50% and 50% N- phenyl-alpha-naphthylamines (T531) are compound | 0.05% |
Benzotriazole derivative (T551) | 0.25% |
Sulfurized olefin cotton oil (T405A) | 6.5% |
Phosphate (T451) | 3.75% |
Boronation phosphamidon ester (T3011) | 4.75% |
Chlorinated paraffin (T301) | 6.9% |
Ethyl silicon oil | 20ppm |
The barium mahogany sulfonate of mass ratio 50% and 50% lanolin are compound | 0.3% |
Ethylene-propylene copolymer (T613A) | 2.1% |
Above each component mass percentage content summation is 100%.
Embodiment 3:
Following each component is pressed the mediation of row mass percent to form:
Component | Mass percentage content |
The MVI90BS base oils of mass ratio 5/6ths and 1/6th alkylnaphthalene are compound | Surplus |
The sulfenyl phenolate (T504) of mass ratio 50% and 50% N- phenyl-alpha-naphthylamines (T531) are compound | 0.1% |
Benzotriazole derivative (T551) | 0.25% |
Sulfurized olefin cotton oil (T405A) | 6.5% |
Phosphate (T451) | 3.55% |
Boronation phosphamidon ester (T3011) | 4.6% |
Chlorinated paraffin (T301) | 6.75% |
Ethyl silicon oil | 25ppm |
The barium mahogany sulfonate of mass ratio 50% and 50% lanolin are compound | 0.15% |
Ethylene-propylene copolymer (T613A) | 5.1% |
Above each component mass percentage content summation is 100%.
The key technical indexes of 1 product of embodiment:
The key technical indexes of 2 product of embodiment:
The key technical indexes of 3 product of embodiment:
Claims (6)
1. a kind of permalloy Cold Forging technology lubricant composition, it is characterised in that:Using mass ratio 5/6ths
MVI90BS base oils and 1/6th alkylnaphthalene it is compound based on oil, coordinate various compound additives, its respective quality hundred
Fraction into being grouped into:
The mass percent summation of above each component is 100%.
2. a kind of permalloy Cold Forging technology lubricant composition as claimed in claim 1, it is characterised in that antioxidant
Be mass ratio 50% sulfenyl phenolate T504 and 50% N- phenyl-alpha-naphthylamines T531 be combined;Metal deactivator is that benzotriazole spreads out
Biological T551.
3. a kind of permalloy Cold Forging technology lubricant composition as claimed in claim 1, it is characterised in that oiliness improver
It is sulfurized olefin cotton oil T405A;Friction improver is phosphate T451.
4. a kind of permalloy Cold Forging technology lubricant composition as claimed in claim 1, it is characterised in that extreme pressure agent
It is boronation phosphamidon ester T3011;Antiwear additive is chlorinated paraffin T301.
5. a kind of permalloy Cold Forging technology lubricant composition as claimed in claim 1, it is characterised in that anti-foaming agent
It is ethyl silicon oil;Antirust agent be the barium mahogany sulfonate of mass ratio 50% and 50% lanolin be combined.
6. a kind of permalloy Cold Forging technology lubricant composition as claimed in claim 1, it is characterised in that tackifier
It is ethylene-propylene copolymer T613A.
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王先会: "《工业润滑油生产与应用》", 30 November 2011, 中国石化出版社 * |
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