CN103725382B - The lubricant that Ni-based ultrafine powder material cold forging is made - Google Patents
The lubricant that Ni-based ultrafine powder material cold forging is made Download PDFInfo
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- CN103725382B CN103725382B CN201310702989.6A CN201310702989A CN103725382B CN 103725382 B CN103725382 B CN 103725382B CN 201310702989 A CN201310702989 A CN 201310702989A CN 103725382 B CN103725382 B CN 103725382B
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- Prior art keywords
- agent
- lubricant
- powder material
- ultrafine powder
- oil
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- 238000010273 cold forging Methods 0.000 title claims abstract description 12
- 239000000463 material Substances 0.000 title claims abstract description 12
- 239000000314 lubricant Substances 0.000 title claims abstract description 11
- 239000000843 powder Substances 0.000 title claims abstract description 10
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 15
- 239000003921 oil Substances 0.000 claims abstract description 11
- 239000010729 system oil Substances 0.000 claims abstract description 7
- 239000003112 inhibitor Substances 0.000 claims abstract description 5
- 230000003647 oxidation Effects 0.000 claims abstract description 5
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 5
- 238000005728 strengthening Methods 0.000 claims abstract description 5
- 239000002131 composite material Substances 0.000 claims abstract description 4
- 239000000654 additive Substances 0.000 claims abstract description 3
- 230000000996 additive effect Effects 0.000 claims abstract description 3
- NNPPMTNAJDCUHE-UHFFFAOYSA-N isobutane Chemical compound CC(C)C NNPPMTNAJDCUHE-UHFFFAOYSA-N 0.000 claims description 10
- 238000005987 sulfurization reaction Methods 0.000 claims description 10
- DMBHHRLKUKUOEG-UHFFFAOYSA-N N-phenyl aniline Natural products C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 claims description 8
- LVGKNOAMLMIIKO-UHFFFAOYSA-N Elaidinsaeure-aethylester Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC LVGKNOAMLMIIKO-UHFFFAOYSA-N 0.000 claims description 5
- 239000004166 Lanolin Substances 0.000 claims description 5
- LVGKNOAMLMIIKO-QXMHVHEDSA-N ethyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC LVGKNOAMLMIIKO-QXMHVHEDSA-N 0.000 claims description 5
- 229940093471 ethyl oleate Drugs 0.000 claims description 5
- XLXGCFTYXICXJF-UHFFFAOYSA-N ethylsilicon Chemical group CC[Si] XLXGCFTYXICXJF-UHFFFAOYSA-N 0.000 claims description 5
- 229940039717 lanolin Drugs 0.000 claims description 5
- 235000019388 lanolin Nutrition 0.000 claims description 5
- 150000003014 phosphoric acid esters Chemical class 0.000 claims description 5
- 210000000582 semen Anatomy 0.000 claims description 5
- 239000002199 base oil Substances 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 2
- -1 diphenylamine compound Chemical class 0.000 claims description 2
- 238000005242 forging Methods 0.000 abstract description 7
- 239000002184 metal Substances 0.000 abstract description 7
- 229910052751 metal Inorganic materials 0.000 abstract description 7
- 230000001464 adherent effect Effects 0.000 abstract description 3
- 238000001816 cooling Methods 0.000 abstract description 3
- 239000000203 mixture Substances 0.000 abstract description 3
- 231100000956 nontoxicity Toxicity 0.000 abstract description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N nickel Substances [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 21
- 229910052759 nickel Inorganic materials 0.000 description 7
- 238000000034 method Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 3
- 230000007797 corrosion Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910000851 Alloy steel Inorganic materials 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229910001361 White metal Inorganic materials 0.000 description 1
- QXZUUHYBWMWJHK-UHFFFAOYSA-N [Co].[Ni] Chemical compound [Co].[Ni] QXZUUHYBWMWJHK-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 238000009713 electroplating Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 230000001050 lubricating effect Effects 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000010969 white metal Substances 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
The lubricant that Ni-based ultrafine powder material cold forging of the present invention is made, adopts oil based on No. 46 total loss system oil, coordinates multiple composite additive, comprise oiliness improver, anti-wear agent, extreme pressure agent, oxidation inhibitor, kilfoam, friction improver, strengthening agent.The lubricant that Ni-based ultrafine powder material cold forging of the present invention is made, its lubricity is good, and cooling, cleansing power by force, can reduce the adherent phenomenon of course of processing forging; Increase oil film strength in distorted area simultaneously, reduce frictional coefficient; Composition is stable, to metal and mould corrosion-free, nontoxicity, has no irritating odor.
Description
Technical field
The invention belongs to the field of lubricant that non-ferrous metal forging processing and lubrication, particularly Ni-based ultrafine powder material cold forging are made.
Background technology
Nickel, silvery white metal, fusing point 1455 DEG C, boiling point 2730 DEG C, density is 8.902g/cm
3.Nickel has good physical strength and ductility, infusibility, and matter is hard, has magnetic and good plasticity-.The erosion resistance had, not oxidized in atmosphere, resistance to highly basic again.Nickel is the metal of a medium tenacity.Metallic nickel is mainly used in electroplating industry, the article of nickel plating are attractive in appearance, totally, not easily corrosion again.
Because nickel has good physical strength and ductility, infusibility is high temperature resistant, and there is very high chemical stability, the feature such as not to be oxidized in atmosphere, therefore be a kind of very important non-ferrous metal raw material, be used to manufacture stainless steel, High Nickel Steel and structural alloy steel, be widely used in the various military industrial manufacturing enterprises such as aircraft, radar, guided missile, tank, naval vessels, spaceship, reactor.In civilian industry, it is a large amount of for various machinery manufacturing industry that nickel often makes structure iron, duriron, high temperature steel etc.Nickel also can make beramic color and coating for protection against corrosion, and nickel cobalt (alloy) is a kind of permanent magnet material, is widely used in the fields such as electronic telecontrol, nuclear industry and ultrasonic technique.
Cold-forging technique is a kind of precision plastic forming technology, has the unrivaled advantage of machining, as goods good mechanical property, productivity is high and material use efficiency is high, be particularly suitable for produce in enormous quantities, can production cost be reduced, improve added value of product.Use cold-forging technique processing Ni-based ultrafine powder material, the most important thing is to solve its mould problem.Cold-forging technique requires high to mold performance, for extending the mold use life-span, must use suitable lubricant in forging process.The cold forging lubricant of Ni-based ultrafine powder material can form composite lubricating film between forging and mould, avoids the adhesion of forging and mould, and slows down the gouging abrasion of metal fluid, extends die life.
Summary of the invention
The technical problem to be solved in the present invention is to provide the lubricant that a kind of Ni-based ultrafine powder material cold forging is made, and the lubricity of this lubricant is good, and cooling, cleansing power by force, can reduce the adherent phenomenon of course of processing forging; Increase oil film strength in distorted area simultaneously, reduce frictional coefficient; Composition is stable; To metal and mould corrosion-free; Nontoxicity, has no irritating odor.
The present invention solves the problems of the technologies described above by following technical scheme: adopt oil based on No. 46 total loss system oil, coordinate multiple composite additive, its each component and mass percent are:
| Component | Content (mass percent) |
| Base oil | Surplus |
| Oiliness improver | 5.0%～12.0% |
| Anti-wear agent | 5.0%～8.0% |
| Extreme pressure agent | 3.0%～5.0% |
| Oxidation inhibitor | 0.8%～1.2% |
| Kilfoam | 0.005%～0.01% |
| Friction improver | 3.0%～5.0% |
| Strengthening agent | 3.0%～5.0% |
Base oil is No. 46 total loss system oil.
Oiliness improver is sulfuration Oleum Gossypii semen.
Anti-wear agent is clorafin 42.
Extreme pressure agent is boronation phosphoric acid ester.
Oxidation inhibitor is mass ratio 40% ~ 60%2,6-ditertbutylparacresol and 60% ~ 40% dialkyl diphenylamine compound.
Kilfoam is ethyl silicon oil.
Friction improver is mass ratio 40% ~ 60% ethyl oleate and 60% ~ 40% lanolin compound.
Strengthening agent is sulfuration Trimethylmethane.
The lubricant that Ni-based ultrafine powder material cold forging of the present invention is made, its lubricity is good, and cooling, cleansing power by force, can reduce the adherent phenomenon of course of processing forging; Increase oil film strength in distorted area simultaneously, reduce frictional coefficient; Composition is stable, to metal and mould corrosion-free, nontoxicity, has no irritating odor.
Embodiment
Embodiment 1:
Following component is in harmonious proportion by mass percentage and forms:
| Component | Content (mass percent) |
| No. 46 total loss system oil | 75.8% |
| Sulfuration Oleum Gossypii semen | 2.0% |
| Clorafin 42 | 7.0% |
| Boronation phosphoric acid ester | 5.0% |
| Mass ratio 40%2,6-ditertbutylparacresol and 60% dialkyl diphenylamine | 1.19% |
| Ethyl silicon oil | 0.01% |
| Mass ratio 40% ethyl oleate and 60% lanolin | 4.0% |
| Sulfuration Trimethylmethane | 5.0% |
Above component summation is 100%.
Embodiment 2:
Following component is in harmonious proportion by mass percentage and forms:
| Component | Content (mass percent) |
| No. 46 total loss system oil | 78.1% |
| Sulfuration Oleum Gossypii semen | 5.0% |
| Clorafin 42 | 6.0% |
| Boronation phosphoric acid ester | 3.0% |
| Mass ratio 60%2,6-ditertbutylparacresol and 40% dialkyl diphenylamine | 0.892% |
| Ethyl silicon oil | 0.008% |
| Mass ratio 60% ethyl oleate and 40% lanolin | 3.0% |
| Sulfuration Trimethylmethane | 4.0% |
Above component summation is 100%.
Embodiment 3:
Following component is in harmonious proportion by mass percentage and forms:
| Component | Content (mass percent) |
| No. 46 total loss system oil | 71.5% |
| Sulfuration Oleum Gossypii semen | 9.0% |
| Clorafin 42 | 6.5% |
| Boronation phosphoric acid ester | 4.0% |
| Mass ratio 50%2,6-ditertbutylparacresol and 50% dialkyl diphenylamine | 0.993% |
| Ethyl silicon oil | 0.007% |
| Mass ratio 50% ethyl oleate and 50% lanolin | 4.0% |
| Sulfuration Trimethylmethane | 4.0% |
Above component summation is 100%.
The main physical and chemical index of embodiment 2 product is:
| Project | Quality index |
| Moisture, % | Vestige |
| 40 DEG C of kinematic viscosity mm 2/s | 43.4 |
| Flash-point (opening) DEG C, | 180 |
| Mechanical impurity, % | Nothing |
| Last non seizure load (Pb), Kg | 103 |
| Pour point, DEG C, | -10 |
| Water soluble acid or alkali | Nothing |
| Corrosion test (copper sheet, 100 DEG C, 3h), level | 1 |
| Viscosity index, is not less than | 95 |
Claims (1)
1. the lubricant made of Ni-based ultrafine powder material cold forging, it is characterized in that oil based on employing No. 46 total loss system oil, coordinate multiple composite additive, its each component and mass percent are:
Wherein:
Oiliness improver is sulfuration Oleum Gossypii semen;
Anti-wear agent is clorafin 42;
Extreme pressure agent is boronation phosphoric acid ester;
Oxidation inhibitor is mass ratio 40% ~ 60%2,6-ditertbutylparacresol and 60% ~ 40% dialkyl diphenylamine compound;
Kilfoam is ethyl silicon oil;
Friction improver is mass ratio 40% ~ 60% ethyl oleate and 60% ~ 40% lanolin compound;
Strengthening agent is sulfuration Trimethylmethane.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310702989.6A CN103725382B (en) | 2013-12-18 | 2013-12-18 | The lubricant that Ni-based ultrafine powder material cold forging is made |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310702989.6A CN103725382B (en) | 2013-12-18 | 2013-12-18 | The lubricant that Ni-based ultrafine powder material cold forging is made |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103725382A CN103725382A (en) | 2014-04-16 |
| CN103725382B true CN103725382B (en) | 2015-10-07 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310702989.6A Expired - Fee Related CN103725382B (en) | 2013-12-18 | 2013-12-18 | The lubricant that Ni-based ultrafine powder material cold forging is made |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103725382B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104974838A (en) * | 2015-07-20 | 2015-10-14 | 广西大学 | Rotary cold-forging vanadium alloy lubricant composition |
| CN106635287A (en) * | 2016-09-21 | 2017-05-10 | 广西大学 | Red copper spinning process lubricant |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103421587A (en) * | 2013-08-26 | 2013-12-04 | 广西大学 | Magnesium and magnesium alloy sheet strip cold rolling lubricating agent |
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2013
- 2013-12-18 CN CN201310702989.6A patent/CN103725382B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103421587A (en) * | 2013-08-26 | 2013-12-04 | 广西大学 | Magnesium and magnesium alloy sheet strip cold rolling lubricating agent |
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| Publication number | Publication date |
|---|---|
| CN103725382A (en) | 2014-04-16 |
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|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20151007 |