CN106511939A - 一种羔羊用中药组合物的制备方法 - Google Patents
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Abstract
本发明公开了一种羔羊用中药组合物的制备方法,包括:将吐温80、环氧氯丙烷、液体石蜡混合均匀得到第一预制料;向明胶磷酸盐缓冲溶液中加入1‑乙基‑(3‑二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌,冷冻干燥,加入纳米二氧化硅微球、水,升温搅拌,再加入戊二醛继续搅拌,室温静置,冷冻干燥得到第二预制料;将淀粉、第二预制料、水混合搅拌,降至室温,加入氢氧化钠搅拌,继续加入环氧氯丙烷和第一预制料,搅拌,过滤,洗涤得到第三预制料;将黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子等粉碎,过筛,加入水浸泡,加热蒸煮,再加入贝壳粉、伊蒙粘土、羟乙基纤维素搅拌,加入第三预制料搅拌,造粒得到羔羊用中药组合物。
Description
技术领域
本发明涉及羔羊技术领域,尤其涉及一种羔羊用中药组合物的制备方法。
背景技术
反刍动物就是有反刍现象的动物,比如羊,因为植物的纤维是比较难消化的。反刍动物采食一般比较匆忙,特别是粗饲料,大部分未经充分咀嚼就吞咽进入瘤胃,羔羊采食了大量容易发酵的饲料,在瘤胃内微生物的作用下异常发酵,迅速产生大量的气体,致使瘤胃急剧膨胀,隔与胸腔器官受到压迫,呼吸与血液循环障碍,发生窒息现象的一种疾病。羔羊由于免疫力差,瘤胃发育不成熟,上述状况易导致羔羊病死率较高,亟待解决。
发明内容
基于背景技术存在的技术问题,本发明提出了一种羔羊用中药组合物的制备方法,所得中药组合物具有消食下气、开胃宽敞的功效,可用于羔羊胃鼓气的预防与治疗,增强羔羊自身免疫力及抗病力,有效降低羔羊病死率。
本发明提出的一种羔羊用中药组合物的制备方法,包括如下步骤:
S1、将吐温80、环氧氯丙烷、液体石蜡混合均匀得到第一预制料;
S2、向明胶磷酸盐缓冲溶液中加入1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌,冷冻干燥,加入纳米二氧化硅微球、水,升温搅拌,再加入戊二醛继续搅拌,室温静置,冷冻干燥得到第二预制料;
S3、将淀粉、第二预制料、水混合搅拌,降至室温,加入氢氧化钠搅拌,继续加入环氧氯丙烷和第一预制料,搅拌,过滤,洗涤得到第三预制料;
S4、将黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实粉碎,过筛,加入水浸泡,加热蒸煮,再加入贝壳粉、伊蒙粘土、羟乙基纤维素搅拌,加入第三预制料搅拌,造粒得到羔羊用中药组合物。
优选地,S1中,吐温80、环氧氯丙烷、液体石蜡的重量比为2-4:5-10:50-100。
优选地,S2中,向明胶磷酸盐缓冲溶液中加入1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌2-4h,冷冻干燥,加入纳米二氧化硅微球、水,升温至65-75℃搅拌20-40min,再加入戊二醛继续搅拌20-40min,室温静置20-40min,冷冻干燥得到第二预制料。
优选地,S2中,明胶磷酸盐缓冲溶液的质量浓度为0.4-0.8wt%,其pH值为6-6.4。
优选地,S2中,明胶磷酸盐缓冲溶液、1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐、纳米二氧化硅微球、水、戊二醛的重量比为2-6:1-2:1-5:40-60:0.5-1。
优选地,S3中,将淀粉、第二预制料、水混合搅拌20-40min,搅拌温度为70-80℃,降至室温,加入氢氧化钠搅拌5-10min,继续加入环氧氯丙烷和第一预制料,搅拌2-6min,搅拌速度为500-900r/min,过滤,洗涤得到第三预制料。
优选地,S3中,第一预制料、第二预制料、淀粉、氢氧化钠、环氧氯丙烷和水的重量比为5-15:1-4:5-10:1-3:1-4:50-100。
优选地,S4中,黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实、贝壳粉、伊蒙粘土、羟乙基纤维素、第三预制料的重量比为15-35:5-15:2-10:2-8:1-6:2-8:15-20:5-15:1-6:1-5:1-6:2-6:1-4:1-6:2-8:5-12:15-25:5-10:5-15:2-6:1-4:5-12:2-7。
优选地,S4中,将黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实粉碎,过60目筛,加入10倍重量的水浸泡,加热蒸煮至含水量为20-40wt%,再加入贝壳粉、伊蒙粘土、羟乙基纤维素搅拌15-35min,加入第三预制料搅拌40-80min,造粒得到羔羊用中药组合物。
本发明采用黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实经过一定方式处理后与贝壳粉、伊蒙粘土、羟乙基纤维素协同作用,所得中药组合物具有消食下气、开胃宽敞的功效,可用于羔羊胃鼓气的预防与治疗,增强羔羊自身免疫力及抗病力,有效降低羔羊病死率。其中第二预制料不仅多孔,而且吸水性强,持水性优良,在一定条件下结合在淀粉上形成凝胶状物质,吸附能力强,而贝壳粉、伊蒙粘土内金属离子游离后,部分可与羟乙基纤维素交联成凝胶,与第三预制料配合作用,使本发明吸水性强,持水性优良,包覆在预处理中药组分外层,便于本发明在羔羊瘤胃中吸水浸泡,增加本发明利用率,成本低,见效快,维持时间长,稳定性好。
具体实施方式
下面,通过具体实施例对本发明的技术方案进行详细说明。
实施例1
本发明提出的一种羔羊用中药组合物的制备方法,包括如下步骤:
S1、将吐温80、环氧氯丙烷、液体石蜡混合均匀得到第一预制料;
S2、向明胶磷酸盐缓冲溶液中加入1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌,冷冻干燥,加入纳米二氧化硅微球、水,升温搅拌,再加入戊二醛继续搅拌,室温静置,冷冻干燥得到第二预制料;
S3、将淀粉、第二预制料、水混合搅拌,降至室温,加入氢氧化钠搅拌,继续加入环氧氯丙烷和第一预制料,搅拌,过滤,洗涤得到第三预制料;
S4、将黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实粉碎,过筛,加入水浸泡,加热蒸煮,再加入贝壳粉、伊蒙粘土、羟乙基纤维素搅拌,加入第三预制料搅拌,造粒得到羔羊用中药组合物。
实施例2
本发明提出的一种羔羊用中药组合物的制备方法,包括如下步骤:
S1、将吐温80、环氧氯丙烷、液体石蜡混合均匀得到第一预制料;
S2、向明胶磷酸盐缓冲溶液中加入1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌3.5h,冷冻干燥,加入纳米二氧化硅微球、水,升温至68℃搅拌35min,再加入戊二醛继续搅拌25min,室温静置35min,冷冻干燥得到第二预制料;
S3、将淀粉、第二预制料、水混合搅拌25min,搅拌温度为78℃,降至室温,加入氢氧化钠搅拌6min,继续加入环氧氯丙烷和第一预制料,搅拌5min,搅拌速度为600r/min,过滤,洗涤得到第三预制料;
S4、将黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实粉碎,过60目筛,加入10倍重量的水浸泡,加热蒸煮至含水量为35wt%,再加入贝壳粉、伊蒙粘土、羟乙基纤维素搅拌20min,加入第三预制料搅拌70min,造粒得到羔羊用中药组合物。
实施例3
本发明提出的一种羔羊用中药组合物的制备方法,包括如下步骤:
S1、将吐温80、环氧氯丙烷、液体石蜡混合均匀得到第一预制料;
S2、向明胶磷酸盐缓冲溶液中加入1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌2.5h,冷冻干燥,加入纳米二氧化硅微球、水,升温至72℃搅拌25min,再加入戊二醛继续搅拌35min,室温静置25min,冷冻干燥得到第二预制料;
S3、将淀粉、第二预制料、水混合搅拌35min,搅拌温度为72℃,降至室温,加入氢氧化钠搅拌8min,继续加入环氧氯丙烷和第一预制料,搅拌3min,搅拌速度为800r/min,过滤,洗涤得到第三预制料;
S4、将黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实粉碎,过60目筛,加入10倍重量的水浸泡,加热蒸煮至含水量为25wt%,再加入贝壳粉、伊蒙粘土、羟乙基纤维素搅拌30min,加入第三预制料搅拌50min,造粒得到羔羊用中药组合物。
实施例4
本发明提出的一种羔羊用中药组合物的制备方法,包括如下步骤:
S1、按重量份将2份吐温80、10份环氧氯丙烷、50份液体石蜡混合均匀得到第一预制料;
S2、按重量份向6份pH值为6-6.4、质量浓度为0.4wt%的明胶磷酸盐缓冲溶液中加入2份1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌2h,冷冻干燥,加入5份纳米二氧化硅微球、40份水,升温至75℃搅拌20min,再加入1份戊二醛继续搅拌20min,室温静置40min,冷冻干燥得到第二预制料;
S3、按重量份将5份淀粉、4份第二预制料、50份水混合搅拌40min,搅拌温度为70℃,降至室温,加入3份氢氧化钠搅拌5min,继续加入4份环氧氯丙烷和5份第一预制料,搅拌6min,搅拌速度为500r/min,过滤,洗涤得到第三预制料;
S4、按重量份将35份黄芩、5份龙葵、10份生姜、2份石榴皮、6份赤芍、2份辣椒、20份藿香、5份山楂、6份麦芽、1份莱菔子、6份大黄、2份玄明粉、4份槟榔、1份苍术、8份陈皮、5份厚朴、25份甘草、5份木香、15份枳实粉碎,过60目筛,加入10倍重量的水浸泡2天,加热蒸煮至含水量为40wt%,再加入2份贝壳粉、4份伊蒙粘土、5份羟乙基纤维素搅拌35min,加入2份第三预制料搅拌80min,造粒得到羔羊用中药组合物。
实施例5
本发明提出的一种羔羊用中药组合物的制备方法,包括如下步骤:
S1、按重量份将4份吐温80、5份环氧氯丙烷、100份液体石蜡混合均匀得到第一预制料;
S2、按重量份向2份pH值为6-6.4、质量浓度为0.8wt%的明胶磷酸盐缓冲溶液中加入1份1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌4h,冷冻干燥,加入1份纳米二氧化硅微球、60份水,升温至65℃搅拌40min,再加入0.5份戊二醛继续搅拌40min,室温静置20min,冷冻干燥得到第二预制料;
S3、按重量份将10份淀粉、1份第二预制料、100份水混合搅拌20min,搅拌温度为80℃,降至室温,加入1份氢氧化钠搅拌10min,继续加入1份环氧氯丙烷和15份第一预制料,搅拌2min,搅拌速度为900r/min,过滤,洗涤得到第三预制料;
S4、按重量份将15份黄芩、15份龙葵、2份生姜、8份石榴皮、1份赤芍、8份辣椒、15份藿香、15份山楂、1份麦芽、5份莱菔子、1份大黄、6份玄明粉、1份槟榔、6份苍术、2份陈皮、12份厚朴、15份甘草、10份木香、5份枳实粉碎,过60目筛,加入10倍重量的水浸泡6天,加热蒸煮至含水量为20wt%,再加入6份贝壳粉、1份伊蒙粘土、12份羟乙基纤维素搅拌15min,加入7份第三预制料搅拌40min,造粒得到羔羊用中药组合物。
以上所述,仅为本发明较佳的具体实施方式,但本发明的保护范围并不局限于此,任何熟悉本技术领域的技术人员在本发明揭露的技术范围内,根据本发明的技术方案及其发明构思加以等同替换或改变,都应涵盖在本发明的保护范围之内。
Claims (9)
1.一种羔羊用中药组合物的制备方法,其特征在于,包括如下步骤:
S1、将吐温80、环氧氯丙烷、液体石蜡混合均匀得到第一预制料;
S2、向明胶磷酸盐缓冲溶液中加入1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌,冷冻干燥,加入纳米二氧化硅微球、水,升温搅拌,再加入戊二醛继续搅拌,室温静置,冷冻干燥得到第二预制料;
S3、将淀粉、第二预制料、水混合搅拌,降至室温,加入氢氧化钠搅拌,继续加入环氧氯丙烷和第一预制料,搅拌,过滤,洗涤得到第三预制料;
S4、将黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实粉碎,过筛,加入水浸泡,加热蒸煮,再加入贝壳粉、伊蒙粘土、羟乙基纤维素搅拌,加入第三预制料搅拌,造粒得到羔羊用中药组合物。
2.根据权利要求1所述羔羊用中药组合物的制备方法,其特征在于,S1中,吐温80、环氧氯丙烷、液体石蜡的重量比为2-4:5-10:50-100。
3.根据权利要求1或2所述羔羊用中药组合物的制备方法,其特征在于,S2中,向明胶磷酸盐缓冲溶液中加入1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐搅拌2-4h,冷冻干燥,加入纳米二氧化硅微球、水,升温至65-75℃搅拌20-40min,再加入戊二醛继续搅拌20-40min,室温静置20-40min,冷冻干燥得到第二预制料。
4.根据权利要求1-3任一项所述羔羊用中药组合物的制备方法,其特征在于,S2中,明胶磷酸盐缓冲溶液的质量浓度为0.4-0.8wt%,其pH值为6-6.4。
5.根据权利要求1-4任一项所述羔羊用中药组合物的制备方法,其特征在于,S2中,明胶磷酸盐缓冲溶液、1-乙基-(3-二甲基氨基丙基)碳酰二亚胺盐酸盐、纳米二氧化硅微球、水、戊二醛的重量比为2-6:1-2:1-5:40-60:0.5-1。
6.根据权利要求1-5任一项所述羔羊用中药组合物的制备方法,其特征在于,S3中,将淀粉、第二预制料、水混合搅拌20-40min,搅拌温度为70-80℃,降至室温,加入氢氧化钠搅拌5-10min,继续加入环氧氯丙烷和第一预制料,搅拌2-6min,搅拌速度为500-900r/min,过滤,洗涤得到第三预制料。
7.根据权利要求1-6任一项所述羔羊用中药组合物的制备方法,其特征在于,S3中,第一预制料、第二预制料、淀粉、氢氧化钠、环氧氯丙烷和水的重量比为5-15:1-4:5-10:1-3:1-4:50-100。
8.根据权利要求1-7任一项所述羔羊用中药组合物的制备方法,其特征在于,S4中,黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实、贝壳粉、伊蒙粘土、羟乙基纤维素、第三预制料的重量比为15-35:5-15:2-10:2-8:1-6:2-8:15-20:5-15:1-6:1-5:1-6:2-6:1-4:1-6:2-8:5-12:15-25:5-10:5-15:2-6:1-4:5-12:2-7。
9.根据权利要求1-8任一项所述羔羊用中药组合物的制备方法,其特征在于,S4中,将黄芩、龙葵、生姜、石榴皮、赤芍、辣椒、藿香、山楂、麦芽、莱菔子、大黄、玄明粉、槟榔、苍术、陈皮、厚朴、甘草、木香、枳实粉碎,过60目筛,加入10倍重量的水浸泡,加热蒸煮至含水量为20-40wt%,再加入贝壳粉、伊蒙粘土、羟乙基纤维素搅拌15-35min,加入第三预制料搅拌40-80min,造粒得到羔羊用中药组合物。
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