CN106490164A - A kind of milk powder high protein effervescent tablet and preparation method thereof - Google Patents
A kind of milk powder high protein effervescent tablet and preparation method thereof Download PDFInfo
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- CN106490164A CN106490164A CN201610915747.9A CN201610915747A CN106490164A CN 106490164 A CN106490164 A CN 106490164A CN 201610915747 A CN201610915747 A CN 201610915747A CN 106490164 A CN106490164 A CN 106490164A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/18—Milk in dried and compressed or semi-solid form
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/1522—Inorganic additives, e.g. minerals, trace elements; Chlorination or fluoridation of milk; Organic salts or complexes of metals other than natrium or kalium; Calcium enrichment of milk
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/1528—Fatty acids; Mono- or diglycerides; Petroleum jelly; Paraffine; Phospholipids; Derivatives thereof
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Abstract
The invention provides a kind of milk powder high protein effervescent tablet and preparation method thereof, the preparation method is granulated using soda acid separate type disintegrant, after alkali source particle and acid source particle are well mixed, with mix lubricant compression molding.The preparation method of the present invention, on the premise of effervescent tablet protein content is improved, conspicuousness overcomes the glutinous punching that dairy products occur during being disintegrated, disintegration time length, the defect for being also easy to produce the Character instabilities such as foam；The shape with change effervescent tablet of novelty, simultaneously increase specific surface area to realize the stability after the disintegration of product, the disintegration time of milk powder effervescent tablet is effectively shortened, increased albumen system stability, it is to avoid foam and the glutinous generation for rushing phenomenon in disintegrating procedue；There is fast disintegration rate, dimensionally stable product to be suitable for various quick consumer groups, can meet the demand of industrialized production completely using milk powder effervescent tablet obtained in preparation method of the present invention.
Description
Technical field
The invention belongs to food technology field, and in particular to a kind of milk powder high protein effervescent tablet and preparation method thereof.
Background technology
Since 2016, with the continuous intensification that China's dairy products relevant policies guiding is lower and dairy industry internationalization affects, breast system
Conduct industry will enter overall transformation period, and domestic consumer is to dairy products such as acidified milk, preserving milk, normal temperature milk and baby milk powders
Demand gradually increase.Requirement of the consumer groups to dairy products is also gradually stepped up, from the abundant and comprehensive battalion of single pursuit dairy products
Support, be transitioned into the selection to milk supply security, technique health, different dairy products consumer groups progressively present different purchases
Demand.For example, with the quickening pace of modern life, increasing consumer pursues the quick and easy and dairy products of nutrition, because
This, developing the dairy products for different consumer groups has positive meaning.
The new milk powder effervescent tablet of exploitation, not only can meet pursuit of the consumer groups to nutrition, and there is carrying side
Just, the convenient significant advantage of Instant Drinks.Effervescent tablet using reacting after soda acid contact, with meet water fater disintegration, release rapid,
The characteristics of infiltration rate is fast in vivo, bioavilability is high.Effervescent tablet also has relatively broad application, such as tea in field of food
Effervescent tablet, fruits and vegetables effervescent tablet, vitamin effervescent tablet etc..The current country is less for cow's milk class and the research of protide effervescent tablet, and
For other sheep breast, horse breasts etc. have no which is used for the preparation of effervescent tablet.
The newborn class effervescent tablet for develop that a class proterties is stable, protein content is high, facilitating Instant Drinks is one weight of dairy industry research and development of new product
The branch for wanting.At present, the milk powder effervescent tablet for having scholar's research to develop, only illustrates to the dispensing of milk powder effervescent tablet, non-opposite
Produce preparation technology, product disintegration proterties and stability to be analyzed；There is a kind of nutrient effervescence milk piece of scholar's research, in milk piece
Add VC、CaCO3Deng nutrition fortifier, the nutritive value of milk piece is improve, entered in terms of milk piece disintegrative, dissolubility, mouthfeel three
Row evaluation, determines the addition of milk piece optimum formula milk powder 35%；There is the preparation of scholar's research prebiotics milk effervescent tablet
Technique, determines that the main body formula of effervescent tablet is that 42.8%, dry milk concentration is 25.0% etc. for prebiotics content, and the effervescent tablet is intended to
Exploitation has the product of probiotic effects；Also scholar develops milk calcium solid beverage, its product optimum formula is：Milk calcium powder
40%th, sour milk powder 15% etc., preferably, the milk powder effervescent tablet mainly strengthens the interpolation of calcium to every evaluation index.
Cow's milk is concentrated on to the selection of milk powder effervescent tablet main base at present, the report newborn to sheep breast, bactrian camel milk, horse is there are no
Road.And preparation, disintegration state and the product stability of effervescent tablet is not investigated in the research and development for having part effervescent tablet.Due in effervescent tablet
Disintegrating procedue can produce a large amount of CO2, when pH value of solution reaches 4.6 or so, easily cause the precipitation precipitation of Proteins In Aqueous Solutions, serious shadow
Ring the stability of product.In addition, CO2Generation be easily caused protein solution system and produce a large amount of foams, from product appearance, make
Obtain consumer to be difficult to receive.To sum up, above-mentioned effervescent tablet major problem is that glutinous phenomenon, disintegration time length, the system of rushing is unstable etc..
Content of the invention
The technical problem to be solved in the present invention is to provide a kind of method for preparing milk powder high protein effervescent tablet.The preparation method
On the premise of effervescent tablet protein content is improved, conspicuousness overcomes the glutinous punching that dairy products occur during being disintegrated, disintegration time length, easy
Produce the defect of the Character instabilities such as foam.The shape with change effervescent tablet of novelty, while increase specific surface area to realize
Stability after the disintegration of product, effectively shorten the disintegration time of milk powder effervescent tablet, it is to avoid foam and glutinous in disintegrating procedue
Rush the generation of phenomenon.There is fast disintegration rate using preparation method gained milk powder effervescent tablet of the present invention, shape of product is steady
Fixed, it is suitable for various quick consumer groups, the demand of industrialized production can be met completely.
The inventors discovered that, a large amount of protein present in disintegrative system easily cause glutinous punching and the albumen of disintegrating procedue
Sedimentation problem.On the premise of increasing percent protein, the disintegration time of effervescent tablet to be shortened, within the time as short as possible, reaches
Stabilising system to finished product.
For solving above-mentioned technical problem, the present invention is adopted the technical scheme that：A kind of preparation of milk powder high protein effervescent tablet
Method, the method are comprised the following steps：
(1) using the new sweet milk after skimmed milk powder or process as effervescent tablet main base；
(2) granulated after mixing skimmed milk powder, alkali source, embedding medium, emulsifying agent, filler, activating agent with adhesive,
Alkali source particle is obtained after drying；Granulated after acid source, pH adjusting agent are mixed with adhesive, acid source particle after drying, is obtained；
(3), after being well mixed alkali source particle and acid source particle, the tablet of arcuate serrated shape is pressed into mix lubricant.
Further, in step (1), main base includes the one kind in fresh milk, horse breast, bactrian camel milk, through degreasing, bar
The material obtained after family name's sterilization, drying of dusting, or the skimmed milk powder after directly taking through sterilizing and drying；Interpolation quality is 6-10
Part.
Further, in step (2), alkali source is sodium acid carbonate or the one kind in sodium carbonate, and interpolation quality is 1-3 parts, wraps
Agent is buried for maltodextrin, interpolation quality is 0.1-1 parts；Emulsifying agent is monoglyceride, and interpolation quality is 0.05-0.2 parts.
Further, in step (2), filler is milk protein powder, and interpolation quality is 1-3 parts.
Further, in step (2), mixing of the activating agent for sucrose fatty ester and polyglyceryl fatty acid ester, Sucrose Fatty Acid Ester
The mass ratio of fat acid esters and polyglyceryl fatty acid ester is 1-2：1-2；Interpolation quality is 0.1-0.5 parts.
Further, in step (2), adhesive is PVP, and interpolation quality is 1-2 parts.
Further, in step (2), acid source is citric acid, tartaric acid, the one kind in fumaric acid；Interpolation quality is 2-5
Part；PH adjusting agent is disodium hydrogen phosphate, and interpolation quality is 0.1-0.5 parts.
Further, in step (3), lubricant is polyethylene glycol PEG6000 or polyethylene glycol PEG4000；Add quality
For 0.5-1 parts.
Number described above is mass parts.
Further, in step (3), the thickness of tablet is 1-5mm, preferably 2mm；Tablet diameters are 50-100mm, compared with
Good for 80mm, tablet height is 5-15mm, preferably 10mm.The shape of the tablet can shorten the Effervescent tablet disintegration time, shorter
Time in reach albumen system stability.
On the basis of common sense in the field is met, above-mentioned each optimum condition can be combined, and obtain final product each preferable reality of the present invention
Example.
Agents useful for same of the present invention and raw material are commercially available.
Present invention also offers milk powder high protein effervescent tablet obtained in a kind of described preparation method.
Beneficial effects of the present invention are：Milk powder high protein effervescent tablet of the present invention is improving the premise of effervescent tablet protein content
Under, conspicuousness overcomes the glutinous punching that dairy products occur during being disintegrated, disintegration time length, is also easy to produce lacking for the Character instabilities such as foam
Fall into；Novelty with the shape for changing effervescent tablet, while increase specific surface area to realize the stability after the disintegration of product, effectively
The disintegration time of milk powder effervescent tablet is shortened, increased albumen system stability, it is to avoid foam and glutinous punching are existing in disintegrating procedue
The generation of elephant；There is fast disintegration rate using milk powder effervescent tablet obtained in preparation method of the present invention, dimensionally stable product,
It is suitable for various quick consumer groups, the demand of industrialized production can be met completely.
Description of the drawings
Fig. 1 is the structural representation of milk powder high protein effervescent tablet of the present invention.
Specific embodiment
Embodiment of the present invention is described in detail with reference to embodiment and Figure of description,
It will be appreciated by those skilled in the art that the following example is merely to illustrate the present invention, and it is not construed as limiting the present invention's
Scope.
Embodiment 1
A kind of preparation method of milk powder high protein effervescent tablet, comprises the following steps：
(1) by skimmed milk powder 8g, sodium acid carbonate 2g, milk protein powder 2g, monoglyceride 0.1g, sucrose fatty ester
After 0.1g, polyglyceryl fatty acid ester 0.1g, maltodextrin 0.5g are well mixed, granulate simultaneously in the presence of adhesive PVP 0.8g
It is dried, alkali grain is obtained；
(2) granulated after mixing citric acid 3g, disodium hydrogen phosphate 0.2g with adhesive PVP 0.8g, be obtained after drying
Acid source particle；
(3), after being well mixed alkali source particle and acid source particle, mix with 6000 1.5g of PC polyethyleneglycol and be pressed into arc
Jagged tablet, obtains milk powder high protein effervescent tablet.The thickness of the tablet is 2mm；A diameter of 80mm, is highly 10mm.
The tablet for obtaining is dissolved in 100ml water, after disintegration certain time, a stable protein solution system is formed.
Disintegration time is determined：The effervescent tablet 3 for taking preparation is respectively placed in 25 DEG C of distilled water, around tablet or fragment
When gas stops overflowing, tablet should be dissolved or dispersed in water, left the consumed time (T) of the particle without aggregation.
PH is determined：After Effervescent tablet disintegration is stable, the pH value for determining the protein solution system using pH meter.
Determining the protein quantity：With reference to the conventional method that kjeldahl determination determines protein content in food.It is steady that precision weighs disintegration
Sample 3.0g after fixed, is placed in kelvin bottle；Add anhydrous cupric sulfate and potassium sulfate (both ratios 1：, and and sample mix 10)
Uniformly；Add 12ml sulfuric acid and 3ml hydrogen peroxide；After 420 DEG C are heated to liquid in bright blue-green, continue heating 1.5h；
Remove Temperature fall after heating source.Sample is distilled, after distillation 5min, in receiving bottle, adds 3 to drip 0.1% methyl red second
Alcoholic solution and 0.5% bromocresol green ethanol solution equal-volume mixed liquor and 2% boric acid of 10ml.Fixed with normal hydrochloric acid drop immediately
Distillate, is titrated to solution and is changed into bois de rose from blue-green, and do reagent blank control simultaneously.
Wherein：V titration sample consumption normal hydrochloric acid liquid product ml
V0Titration is blank to consume normal hydrochloric acid liquid product ml
C concentration of hydrochloric acid mol/L
Quality g of m samples
0.014 grams per milliequivalent nitrogen
6.38 nitrogen are converted into the coefficient of milk protein
After measured, disintegration time T of above-mentioned effervescent tablet1For 32.5 ± 2.1s, the solution ph is 6.1 ± 0.2, A1Albumen
Content is to there are no to stick in 3.28 ± 0.43%, and disintegrating procedue to rush phenomenon.
Embodiment 2
A kind of preparation method of milk powder high protein effervescent tablet, comprises the following steps：
(1) by degreasing horse milk powder 10g, sodium acid carbonate 1g, milk protein powder 1g, monoglyceride 0.05g, sucrose fatty ester
After 0.05g, polyglyceryl fatty acid ester 0.05g, maltodextrin 1g are well mixed, granulate in the presence of adhesive PVP 1g and go forward side by side
Row drying, is obtained alkali grain；
(2) granulated after mixing citric acid 2g, disodium hydrogen phosphate 0.5g with adhesive PVP 1g, acid after drying, is obtained
Source particle；
(3), after being well mixed alkali source particle and acid source particle, mix with 6000 1.5g of PC polyethyleneglycol and be pressed into arc
Jagged tablet, obtains milk powder high protein effervescent tablet.The thickness of the tablet is 1mm；A diameter of 50mm, is highly 5mm.Should
Tablet is dissolved in 100ml water, after disintegration certain time, forms a stable protein solution system.
The detection method of disintegration time, pH value and determining the protein quantity method with reference to described in embodiment 1.After measured, institute
State Effervescent tablet disintegration time T2For 47.3 ± 3.5s, the solution ph is 5.9 ± 0.3, protein content A2For 2.47 ± 0.19%,
There is fewer parts appearance to stick in disintegrating procedue and rush phenomenon, agitated rear glutinous group's disappearance.
Embodiment 3
A kind of preparation method of milk powder high protein effervescent tablet is comprised the following steps：
(1) by degreasing camel milk powder 6g, sodium acid carbonate 3g, milk protein powder 3g, monoglyceride 0.2g, sucrose fatty ester
After 0.25g, polyglyceryl fatty acid ester 0.25g, maltodextrin 0.1g are well mixed, granulate in the presence of adhesive PVP 0.5g
And be dried, alkali grain is obtained；
(2) granulated after mixing tartaric acid 5g, disodium hydrogen phosphate 0.1g with adhesive PVP 0.5g, be obtained after drying
Acid source particle；
(3), after being well mixed alkali source particle and acid source particle, mix with 4000 1g of PC polyethyleneglycol and be pressed into arc saw
The tablet of dentation, obtains milk powder high protein effervescent tablet.The thickness of the tablet is 5mm；A diameter of 100mm, is highly 15mm.Should
Tablet is dissolved in 200ml water, after disintegration certain time, forms a stable protein solution system.
Disintegration time, pH value and determining the protein quantity method are with reference to the detection method described in embodiment 1.After measured,
The Effervescent tablet disintegration time T3For 30.9 ± 1.7s, the solution ph is 6.0 ± 0.8, protein content A3For 2.83 ±
0.49%, do not occur sticking in disintegrating procedue and rush phenomenon.
Embodiment 4
A kind of preparation method of milk powder high protein effervescent tablet, comprises the following steps：
(1) by skimmed milk powder 8g, sodium carbonate 2g, milk protein powder 1g, monoglyceride 0.1g, sucrose fatty ester 0.05g,
After polyglyceryl fatty acid ester 0.1g, maltodextrin 0.5g are well mixed, granulate in the presence of adhesive PVP 0.75g and carry out
Dry, alkali grain is obtained；
(2) granulated after mixing fumaric acid 3g, disodium hydrogen phosphate 0.2g with adhesive PVP 0.75g, made after drying
Obtain acid source particle；
(3), after being well mixed alkali source particle and acid source particle, mix with 6000 1.2g of PC polyethyleneglycol and be pressed into arc
Jagged tablet, obtains milk powder high protein effervescent tablet.The thickness of the tablet is 2mm；A diameter of 80mm, is highly 10mm.
The tablet for obtaining is dissolved in 200ml water, after disintegration certain time, that is, a stable protein solution system is formed.
The detection method of disintegration time, pH value and determining the protein quantity method with reference to described in embodiment 1.The effervescent tablet
Disintegration time T4For 42.5 ± 1.9s, the pH value of the solution is 6.1 ± 0.4, protein content A4For 3.04 ± 0.45%, it was disintegrated
Cheng Wei appearance is glutinous to rush phenomenon.
Comparative example
The preparation method of the milk powder high protein effervescent tablet of the present invention is comprised the following steps：
(1) extracting degreasing milk powder 8g, sodium acid carbonate 2g, milk protein 2g, monoglyceride 0.2g, sucrose fatty ester 0.2g,
After polyglyceryl fatty acid ester 0.2g, maltodextrin 0.5g are uniformly mixed, granulate under adhesive PVP effects and done
Dry, obtain final product alkali grain；
(2) take after citric acid 5g, disodium hydrogen phosphate 0.5g uniformly mixed, granulate under adhesive PVP effects and go forward side by side
Row drying, obtains final product acid particles；
(3) mode is disintegrated using soda acid separate type effervescence granular, takes dried soda acid particle, in poly- second after being well mixed
Under glycol PFG6000 effects, zigzag tablet, as milk powder high protein effervescent tablet is pressed into.The tablet thickness is 2mm；Tablet
A diameter of 90mm, tablet height are 10mm.The tablet is dissolved in 150mL water, after disintegration certain time, a stable egg is formed
White solution system.
Existing milk effervescent tablet granulation shape thicknesses are thicker, easily occur sticking in course of dissolution and rush phenomenon, and dissolve uneven
Even, and often through protein content is reduced in existing research, to solve the problems, such as albumen precipitation.And the product of invention,
On the premise of improving albumen, effectively solving is glutinous to rush phenomenon, and overcomes the technical barrier of albumen precipitation.
Existing two kinds of milk effervescent tablets are selected, is tested after being obtained according to the preparation method that has reported.Determine respectively and collapse
Solution time, pH value and protein content, assay method are shown in Table 1 with reference to the detection method described in embodiment 1, testing result.
Table 1
As shown in table 1, effervescent tablet of the invention can significantly improve protein content, effectively shorten disintegration time, make albumen
Solution system is maintained in the range of stable pH.Comparing with other products has obvious advantage.
Presently preferred embodiments of the present invention is the foregoing is only, not in order to limit the present invention, all in essence of the invention
Any modification, equivalent and simple modifications for being made in content etc., should be included within the scope of the present invention.
Claims (10)
1. a kind of preparation method of milk powder high protein effervescent tablet, it is characterised in that the method is comprised the following steps：
(1) using the new sweet milk after skimmed milk powder or process as effervescent tablet main base；
(2) granulated after mixing skimmed milk powder, alkali source, embedding medium, emulsifying agent, filler, activating agent with adhesive, dried
Alkali source particle is obtained afterwards；Granulated after acid source, pH adjusting agent are mixed with adhesive, acid source particle after drying, is obtained；
(3), after being well mixed alkali source particle and acid source particle, the tablet of arcuate serrated shape is pressed into mix lubricant.
2. preparation method according to claim 1, it is characterised in that in step (1), main base include fresh milk,
One kind in horse breast, bactrian camel milk, the material obtained after degreasing, pasteurize, drying of dusting, or directly take through sterilizing and drying
Skimmed milk powder afterwards；Interpolation quality is 6-10 parts.
3. preparation method according to claim 1, it is characterised in that in step (2), alkali source are sodium acid carbonate or sodium carbonate
In one kind, interpolation quality be 1-3 parts；Embedding medium is maltodextrin, and interpolation quality is 0.1-1 parts；Emulsifying agent is monoglyceride, adds
Plus quality is 0.05-0.2 parts.
4. preparation method according to claim 1, it is characterised in that in step (2), filler are milk protein powder, add
Plus quality is 1-3 parts.
5. preparation method according to claim 1, it is characterised in that in step (2), activating agent be sucrose fatty ester and
The mass ratio of the mixing of polyglyceryl fatty acid ester, sucrose fatty ester and polyglyceryl fatty acid ester is 1-2：1-2；Adding quality is
0.1-0.5 parts.
6. preparation method according to claim 1, it is characterised in that in step (2), adhesive is PVP, adds matter
Measure as 1-2 parts.
7. preparation method according to claim 1, it is characterised in that in step (2), acid source are citric acid, tartaric acid, richness
One kind in horse acid；Interpolation quality is 2-5 parts；PH adjusting agent is disodium hydrogen phosphate, and interpolation quality is 0.1-0.5 parts.
8. preparation method according to claim 1, it is characterised in that in step (3), lubricant is polyethylene glycol
PEG6000 or polyethylene glycol PEG4000；Interpolation quality is 0.5-1 parts.
9. preparation method according to claim 1, it is characterised in that in step (3), the thickness of tablet is 1-5mm, diameter
For 50-100mm, it is highly 5-15mm.
10. milk powder high protein effervescent tablet obtained in the preparation method described in a kind of any one of claim 1-9.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115812887A (en) * | 2022-11-28 | 2023-03-21 | 仙乐健康科技股份有限公司 | An effervescent composition for producing food with milk cover and its preparation method |
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| CN106490164B (en) | 2019-11-05 |
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