CN106472930A - A kind of Millettia speciosa champ health care beverage - Google Patents
A kind of Millettia speciosa champ health care beverage Download PDFInfo
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- CN106472930A CN106472930A CN201610902825.1A CN201610902825A CN106472930A CN 106472930 A CN106472930 A CN 106472930A CN 201610902825 A CN201610902825 A CN 201610902825A CN 106472930 A CN106472930 A CN 106472930A
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- millettia speciosa
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- health care
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- 238000011049 filling Methods 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000001530 fumaric acid Substances 0.000 description 1
- 235000020510 functional beverage Nutrition 0.000 description 1
- 238000003304 gavage Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 125000000623 heterocyclic group Chemical group 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 238000011081 inoculation Methods 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000002398 materia medica Substances 0.000 description 1
- FRSVXKSGQILUAB-UHFFFAOYSA-N millettiasaponin A Natural products OC1C(O)C(O)C(C)OC1OC1C(OC2C(OC(C(O)C2O)C(O)=O)OC2C(C3C(C4C(C5(CCC6(C)C(OC(C)=O)CC(C)(CC6C5=CC4)C(O)=O)C)(C)CC3)(C)CC2)(C)CO)OC(CO)C(O)C1O FRSVXKSGQILUAB-UHFFFAOYSA-N 0.000 description 1
- 201000008383 nephritis Diseases 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 235000020823 overnutrition Nutrition 0.000 description 1
- 238000009928 pasteurization Methods 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 208000008423 pleurisy Diseases 0.000 description 1
- -1 polypropylene pyrroles Polymers 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 208000008128 pulmonary tuberculosis Diseases 0.000 description 1
- 230000010349 pulsation Effects 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 230000002040 relaxant effect Effects 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 210000002435 tendon Anatomy 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
- 230000003867 tiredness Effects 0.000 description 1
- 208000016255 tiredness Diseases 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 1
- 230000008736 traumatic injury Effects 0.000 description 1
- 239000011800 void material Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/38—Other non-alcoholic beverages
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- A61K36/185—Magnoliopsida (dicotyledons)
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/486—Millettia
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Abstract
The invention discloses a kind of Millettia speciosa champ health care beverage, including following raw material：Millettia Speciosa, black tea, Flos Caryophylli, Folium Nelumbinis, Radix Puerariae, Flos Lonicerae, Flos Sophorae, preserved plum vinegar, ginkgetin, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont EEA2112AC compatilizer, food grade antioxidant 264, xanthan gum, epoxidized soybean oil fatty acid, lemon yellow pigment, nisin, selenium element, manganese element, cobalt element, proline, isoleucine, serine, threonine, Vitamin E, vitamin B1, vitamin C, aspartyl-phenylalanine methyl ester, sucrose, dihydro jasmone, ethyl is fragrant, carvone, methyl-furfuryl fumarate, 51 guanosine monophosphate disodium, guanyl potassium.The Millettia speciosa champ health care beverage of the present invention is nutritious, and sour-sweet tasty and refreshing, tea perfume is strong, is a kind of new Chinese medicine Millettia speciosa champ health care beverage；The Millettia speciosa champ health care beverage drinking the present invention has functions that implication of dispelling, and has remarkable effect to treatment or mitigation implication symptom.
Description
Technical field
The invention belongs to technical field of beverage processing is and in particular to a kind of Millettia speciosa champ health care beverage.
Background technology
Millettia Speciosa is the drying of pulse family Millettia plant beautiful millettia Millettia speciosa Champ.
Root, is commonly called as Tianniudali.Taste is micro- sweet, and main component contains alkaloid, coumarin and saccharide.Hainan Quan Dao is distributed.Guangxi, wide
The provinces and regions such as east, Fujian are also distributed.Initially《The SHENGCAO property of medicine is standby will》Record：" strengthening bone and muscle, relieving heat toxin are managed internal injury, are controlled traumatic injury, leaching
Wine nourishing kidney.", Guangzhou army《Conventional Chinese herbal medicine handbook》：" relaxing muscles and tendons and activating QI and blood in the collateral, qi-restoratives lung moistening.Control lumbago and skelalgia, rheumatic arthralgia, Chronic Liver
Scorching, pulmonary tuberculosis.”、《Guangxi book on Chinese herbal medicine a collection of selected materials》：" QI invigorating lung moistening.Control body void after being ill, cough due to deficiency of the lung, rheumatic arthralgia, lumbago and skelalgia.”、
《National Chinese herbal medicine compilation》：" control chronic bronchitiss, seminal emission, leucorrhea ",《Guangxi ethnic drug short course》：" control cough, nephritis, wind
Wet, anemia.”、《Fujian medicine will》：" expelling wind and removing dampness controls pleuritis." Millettia Speciosa is used as medicine with rhizome, whole year can adopt, and clean and cut
Piece, dry or cook dry standby.Mel is perfect natural health agent and enamel, and this viewpoint is by long history institute
Confirm.《Compendium of Materia Medica》Record：The work(that Mel is used as medicine has five, heat clearing away, invigorating middle warmer, removing toxic substances, profit bath, pain relieving.
Modern study shows, Millettia Speciosa root such as pterocarpan containing alkaloid：(-)-3-hydroxy-9-methoxypterocarpan (medicarpin) and saponin
Class：Millettiasaponin A, B (Uchiyama T, et al.Heterocycles, 2003,60：655).Root decoct or
Ethanol extraction gavages, to due to ammonia spraying draw the mice coughing have obvious antitussive action (Xu Honghua writes. Chinese herbal medicine
Coloured picture handbook (one). Guangzhou：Guangdong Science Press, 2003：22).Millettia Speciosa polysaccharide is that Millettia Speciosa adjusts immune work(
One of main active of energy.Have dual regulation (Zheng Yuansheng, etc. Guangdong to mice T lymphopoiesis
Pharmaceutical college's journal, 2008,24：58).The raw material that the 70's began to build kidney ball, building-up body capsule etc. as strong waist is used for middle one-tenth
The production of medicine, extensively applies in Guangdong and Guangxi Provinces area.Additionally, domestic conventional Millettia Speciosa among the people is as stewed stocks.
Functional drinkss, are the favorites of beverage market in recent years." red cattle " before more than ten years outshines others, to 2002-
" pulsation " in 2003, and beverage production enterprise afterwards is nearly all in production functional drinkss.Current commercial type
Functional beverage such as fire-toxin releasing herb tea " Wang Laoji " etc..But both at home and abroad there is not yet Millettia Speciosa health beverage about having implication effect of dispelling
The document of material aspect or patent report.
Abundant with growth in the living standard and material, people's dietetic level has very big improvement, people eat more
It is better to come, also more and more greasy, and a lot of people have different degrees of overnutrition and obesity；So not only very unsightly,
And be possible to grow a series of diseases, impact people's is healthy, thus now increasing people start except
Carry out positive sports, participate in outside exercising with oxygen, also focus on diet, take in some and can go oil removal, improve internal ring
Border, the Foods or drinkses of nutrient health, due to above reason, beverage industry development is maked rapid progress, wide in variety colorful, especially
The beverage with health care more becomes new lover, and tea vinegar drink is also just arisen at the historic moment.
Tea vinegar not only sour-sweet delicious food, tea perfume is strong, special mouthfeel, suits the taste of both old and young, and nutritious, containing multiple to people
The beneficial composition of body, such as catechin can eliminate the free radical in human body, are a kind of protective agents of natural pigment, can suppress cholesterol
Increase, vessel softening；Tea polyphenols have the effect of defying age, antioxidation, antibacterial and diseases prevention；Tea vinegar has Fructus Alpiniae Oxyphyllae of refreshing oneself, promotes the production of body fluid
Quench the thirst, diuresis removing toxic substances, the effect of allaying tiredness.
But tea vinegar drink kind is actually rare in the market, and exist production the tea vinegar drink cycle long, produce
The problems such as product storage time is short.As patent of invention " chrysanthemum tea vinegar beverage（The patent No.：ZL201210267461.6) " disclose one
Plant chrysanthemum tea vinegar beverage and preparation method thereof, the method needs to inoculate acetic acid bacteria fermentation 30-40 days in inoculation fermentation step, leads
Cause long the production cycle；Additionally, adopting vacuum filling, sealing in fill step, vacuum is 0.04-0.05Mpa, fill temperature
Degree controls at 60-75 DEG C, and due to fill, the vacuum of sealing and temperature, low to result in product storage time short.And for example invent specially
A kind of sharp " tea vinegar drink and preparation method thereof（The patent No.：ZL201210162462.4) " disclose the sugary tea juice liquid of gained
In, sealing and fermenting 22-25 days at 25-28 DEG C, then filtered, after pasteurization, obtained final product tea vinegar drink, this producer
Method there is also the problem of long the production cycle.Therefore, how to solve long the production cycle, the problems such as product storage time is short, become
The direction studied from now on.
For many years, China's tea industry is rapidly developed, but still there is Summer-autumn tea tree fresh leaf serious waste of resources etc.
Outstanding problem, in the urgent need to increasing the exploitation of tea resource, and the Development and Production of tea vinegar drink, tea resource not only can be solved
The problem wasting, and have also been enlarged the output value chain of tea resource, therefore, tea vinegar drink DEVELOPMENT PROSPECT is wide.
Content of the invention
The technical problem to be solved in the present invention is to provide a kind of Millettia speciosa champ health care beverage, to solve to produce cattle in prior art
Teabag drink long the production cycle energetically, storage time is short, the problems such as mouthfeel is not good enough.The Millettia speciosa champ health care beverage nutrition of the present invention is rich
Richness, sour-sweet tasty and refreshing, tea perfume is strong, is a kind of new Chinese medicine Millettia speciosa champ health care beverage；Drink the Millettia Speciosa health beverage of the present invention
Material has functions that implication of dispelling, and has remarkable effect to treatment or mitigation implication symptom.
In order to solve above technical problem, the present invention employs the following technical solutions：
A kind of Millettia speciosa champ health care beverage, in units of weight portion, including following raw material：Millettia Speciosa 152-210 part, black tea 71-100
Part, Flos Caryophylli 7-10 part, Folium Nelumbinis 9-14 part, Radix Puerariae 6-12 part, Flos Lonicerae 7-10 part, Flos Sophorae 5-7 part, preserved plum vinegar 5-9 part, Gingko yellow
Ketone 2.4-4.2 part, polyvinyl pyrilodone 0.7-1.1 part, hydroxypropyl methyl cellulose potassium 0.4-0.7 part, agar 0.5-0.8
Part, Dupont EEA2112AC compatilizer 0.7-1.2 part, food grade antioxidant 264 0.6-0.9 part, xanthan gum 0.5-1.2
Part, epoxidized soybean oil fatty acid 0.3-0.6 part, lemon yellow pigment 0.3-0.5 part, nisin 0.5-0.8 part, selenium element
0.2-0.3 part, manganese element 0.2-0.3 part, cobalt element 0.1-0.2 part, proline 0.3-0.5 part, isoleucine 0.2-0.4 part,
Serine 0.2-0.3 part, threonine 0.2-0.4 part, Vitamin E 0.2-0.3 part, vitamin B1 0.2-0.3 part, vitamin C
0.2-0.4 part, aspartyl-phenylalanine methyl ester 0.03-0.05 part, sucrose 1.5-2.5 part, dihydro jasmone 0.03-0.06
Part, ethyl perfume 0.02-0.04 part, carvone 0.04-0.06 part, methyl-furfuryl fumarate 0.5-0.9 part, 51- guanosine monophosphate disodium
0.2-0.3 part, guanyl potassium 0.1-0.2 part；
The preparation method of described Millettia speciosa champ health care beverage, comprises the following steps：
S1：The preparation of Millettia Speciosa juice, comprises the following steps；
S11：The Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 150-200 mesh sieve, prepared Millettia Speciosa minces；
S12：It is 1 in mass ratio that the Millettia Speciosa that step S11 is obtained minces with water:The ratio mixing of 3-7 loads extraction pot, in pressure
Power is under 4-6MPa, uses 4-6 layer filtered through gauze, prepared filtrate A after decocting in water 0.3-0.6h；
S13：The filtrate A rotating speed that step S12 is obtained is the centrifuge of 4000-5000r/min, in vacuum is
Sucking filtration roguing under 0.076-0.085MPa, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps：
S21：Black tea is dried to water content≤8.5% pulverizing, crosses 100-140 mesh sieve, with the second for 75%-84% for the mass fraction
Alcohol-water solution is 1 in mass ratio:12-14 mixes, and is 150-180W in microwave power, and temperature extracts 18- at being 44-48 DEG C
30min, filters, and concentrates, prepared tea polyphenols crude extract A；
S22：The tea polyphenols crude extract A that step S21 is obtained is added in the KCl solution that concentration is 17%-19%, and pH regulator is extremely
5.8-6.2, removes impurity, using aperture for 0.01-0.03 μm of filter membrane in temperature under centrifugal rotational speed is for 4000-5000r/min
For filtering to the solution after centrifugation at 32-35 DEG C, prepared liquor B；
S23：By step S22 be obtained liquor B with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3：Flos Caryophylli, Folium Nelumbinis, Radix Puerariae, Flos Lonicerae, Flos Sophorae are separately dried the co-grinding to water content≤7.5%, add water,
Solid-liquid ratio is 1:13-15（W/V）, microwave power is 180-220W, and Extracting temperature is 90-95 DEG C, and extraction time is 1.3-1.7h,
Then filtering residue, prepared medicinal liquid；
S4：By medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step S1, step S2, step S3, preserved plum vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont EEA2112AC compatilizer, food stage
After antioxidant 264, xanthan gum, epoxidized soybean oil fatty acid, 1300-1500 part water mix, it is 155-174W in microwave power, temperature
Spend for 62-66 DEG C, speed of agitator is to stir 0.4-0.8h under 200-400r/min, and uniform mixed liquor A is obtained；
The preparation method of described ginkgetin comprises the following steps：
S41：Dry Folium Ginkgo is pulverized and is crossed 100-120 mesh sieve, prepared Ginkgo Leaf；
S42：The Ginkgo Leaf that step S41 is obtained is extracted using 45-65 DEG C of water, and in extraction, microwave power is 150-
200W, solid-to-liquid ratio is 1:12-15（W/V）, extraction time is 0.5-1h, extracts 2-3 time, and filtration, merging filtrate after extraction are obtained
Mixing lixiviating solution；
S43：The mixing lixiviating solution concentrate drying that step S42 is obtained, is obtained extraction cream, is used in extraction 6.5-6.8 times of body of cream
The water of long-pending 48-56 DEG C is dissolved, and carries out extraction 2-3 time using anhydrous ethyl acetate solvent, continues to use anhydrous ethyl acetate
Carry out multiple crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.5-5.8（W/V）, prepared crystal crude product；
S44：By the prepared crystal crude product of step S43 through supercritical CO2Extraction, the condition of extraction：Extraction kettle pressure is 14-
20MPa, extraction temperature is 46-48 DEG C, and extraction time is 25-35min, prepared ginkgetin；
S5：To step S4 be obtained uniform mixed liquor A in add lemon yellow pigment, nisin, selenium element, manganese element,
Cobalt element, proline, isoleucine, serine, threonine, Vitamin E, vitamin B1, vitamin C, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, sucrose, dihydro jasmone, ethyl perfume, carvone, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
Microwave power is 138-152W, and temperature is 48-55 DEG C, and speed of agitator is to stir 0.4-0.6h under 300-500r/min, is obtained all
Even mixed liquid B；
S6：The uniform mixed liquor that step S5 is obtained is 134-136 DEG C in temperature, and pressure is the 2-4s that sterilizes under 210-230KPa,
Uniform mixed liquor C is obtained；
S7：The uniform mixed liquor C that step S6 is obtained is 0.089-0.093MPa in vacuum, and temperature is carried out at being 88-92 DEG C
Fill, sealing, are then cooled to room temperature, prepared Millettia speciosa champ health care beverage.
Preferably, microwave power described in step S3 is 220W, and Extracting temperature is 92 DEG C, and extraction time is 1.4h.
Preferably, microwave power described in step S4 is 174W, and temperature is 66 DEG C, and speed of agitator is to stir under 400r/min
0.4h.
Preferably, microwave power described in step S5 is 152W, and temperature is 54 DEG C, and speed of agitator is to stir under 4000r/min
Mix 0.4h.
Preferably, temperature described in step S6 is 136 DEG C, and pressure is the 2s that sterilizes under 230KPa.
Preferably, vacuum described in step S6 is 0.093MPa, and temperature carries out fill, sealing at being 92 DEG C.
The invention has the advantages that：
（1）The Millettia speciosa champ health care beverage of the present invention is nutritious, and sour-sweet tasty and refreshing, tea perfume is strong, is that a kind of new Chinese medicine cattle is big
Force health-care beverage；
（2）The Millettia speciosa champ health care beverage drinking the present invention has functions that implication of dispelling, and treatment or mitigation implication symptom are had significantly
Effect；
（3）The Millettia speciosa champ health care beverage of the present invention is with short production cycle, and shelf life of products is long；
（4）The present invention is compared with prior art：Fill, sealing, using higher temperature and vacuum, more can extend product storage
Time；
（5）The Millettia speciosa champ health care beverage constitutive material source of the present invention is easy to get, preparation method uncomplicated it is easy to popularization and application.
Specific embodiment
For ease of more fully understanding the present invention, it is illustrated by following examples, these embodiments belong to the present invention's
Protection domain, but do not limit the scope of the invention.
In an embodiment, described Millettia speciosa champ health care beverage, in units of weight portion, including following raw material：Millettia Speciosa 152-
210 parts, black tea 71-100 part, Flos Caryophylli 7-10 part, Folium Nelumbinis 9-14 part, Radix Puerariae 6-12 part, Flos Lonicerae 7-10 part, Flos Sophorae 5-7 part, prunus mume (sieb.) sieb.et zucc.
Sub- vinegar 5-9 part, ginkgetin 2.4-4.2 part, polyvinyl pyrilodone 0.7-1.1 part, hydroxypropyl methyl cellulose potassium 0.4-0.7
Part, agar 0.5-0.8 part, Dupont EEA2112AC compatilizer 0.7-1.2 part, food grade antioxidant 264 0.6-0.9 part,
Xanthan gum 0.5-1.2 part, epoxidized soybean oil fatty acid 0.3-0.6 part, lemon yellow pigment 0.3-0.5 part, nisin
0.5-0.8 part, selenium element 0.2-0.3 part, manganese element 0.2-0.3 part, cobalt element 0.1-0.2 part, proline 0.3-0.5 part, different
Leucine 0.2-0.4 part, serine 0.2-0.3 part, threonine 0.2-0.4 part, Vitamin E 0.2-0.3 part, vitamin B1
0.2-0.3 part, vitamin C 0.2-0.4 part, aspartyl-phenylalanine methyl ester 0.03-0.05 part, sucrose 1.5-2.5 part, two
Hydrogen jasmone 0.03-0.06 part, ethyl perfume 0.02-0.04 part, carvone 0.04-0.06 part, methyl-furfuryl fumarate 0.5-0.9
Part, 51- guanosine monophosphate disodium 0.2-0.3 part, guanyl potassium 0.1-0.2 part；
The preparation method of described Millettia speciosa champ health care beverage, comprises the following steps：
S1：The preparation of Millettia Speciosa juice, comprises the following steps；
S11：The Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 150-200 mesh sieve, prepared Millettia Speciosa minces；
S12：It is 1 in mass ratio that the Millettia Speciosa that step S11 is obtained minces with water:The ratio mixing of 3-7 loads extraction pot, in pressure
Power is under 4-6MPa, uses 4-6 layer filtered through gauze, prepared filtrate A after decocting in water 0.3-0.6h；
S13：The filtrate A rotating speed that step S12 is obtained is the centrifuge of 4000-5000r/min, in vacuum is
Sucking filtration roguing under 0.076-0.085MPa, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps：
S21：Black tea is dried to water content≤8.5% pulverizing, crosses 100-140 mesh sieve, with the second for 75%-84% for the mass fraction
Alcohol-water solution is 1 in mass ratio:12-14 mixes, and is 150-180W in microwave power, and temperature extracts 18- at being 44-48 DEG C
30min, filters, and concentrates, prepared tea polyphenols crude extract A；
S22：The tea polyphenols crude extract A that step S21 is obtained is added in the KCl solution that concentration is 17%-19%, and pH regulator is extremely
5.8-6.2, removes impurity, using aperture for 0.01-0.03 μm of filter membrane in temperature under centrifugal rotational speed is for 4000-5000r/min
For filtering to the solution after centrifugation at 32-35 DEG C, prepared liquor B；
S23：By step S22 be obtained liquor B with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3：Flos Caryophylli, Folium Nelumbinis, Radix Puerariae, Flos Lonicerae, Flos Sophorae are separately dried the co-grinding to water content≤7.5%, add water,
Solid-liquid ratio is 1:13-15（W/V）, microwave power is 180-220W, and Extracting temperature is 90-95 DEG C, and extraction time is 1.3-1.7h,
Then filtering residue, prepared medicinal liquid；
S4：By medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step S1, step S2, step S3, preserved plum vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont EEA2112AC compatilizer, food stage
After antioxidant 264, xanthan gum, epoxidized soybean oil fatty acid, 1300-1500 part water mix, it is 155-174W in microwave power, temperature
Spend for 62-66 DEG C, speed of agitator is to stir 0.4-0.8h under 200-400r/min, and uniform mixed liquor A is obtained；
The preparation method of described ginkgetin comprises the following steps：
S41：Dry Folium Ginkgo is pulverized and is crossed 100-120 mesh sieve, prepared Ginkgo Leaf；
S42：The Ginkgo Leaf that step S41 is obtained is extracted using 45-65 DEG C of water, and in extraction, microwave power is 150-
200W, solid-to-liquid ratio is 1:12-15（W/V）, extraction time is 0.5-1h, extracts 2-3 time, and filtration, merging filtrate after extraction are obtained
Mixing lixiviating solution；
S43：The mixing lixiviating solution concentrate drying that step S42 is obtained, is obtained extraction cream, is used in extraction 6.5-6.8 times of body of cream
The water of long-pending 48-56 DEG C is dissolved, and carries out extraction 2-3 time using anhydrous ethyl acetate solvent, continues to use anhydrous ethyl acetate
Carry out multiple crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.5-5.8（W/V）, prepared crystal crude product；
S44：By the prepared crystal crude product of step S43 through supercritical CO2Extraction, the condition of extraction：Extraction kettle pressure is 14-
20MPa, extraction temperature is 46-48 DEG C, and extraction time is 25-35min, prepared ginkgetin；
S5：To step S4 be obtained uniform mixed liquor A in add lemon yellow pigment, nisin, selenium element, manganese element,
Cobalt element, proline, isoleucine, serine, threonine, Vitamin E, vitamin B1, vitamin C, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, sucrose, dihydro jasmone, ethyl perfume, carvone, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
Microwave power is 138-152W, and temperature is 48-55 DEG C, and speed of agitator is to stir 0.4-0.6h under 300-500r/min, is obtained all
Even mixed liquid B；
S6：The uniform mixed liquor that step S5 is obtained is 134-136 DEG C in temperature, and pressure is the 2-4s that sterilizes under 210-230KPa,
Uniform mixed liquor C is obtained；
S7：The uniform mixed liquor C that step S6 is obtained is 0.089-0.093MPa in vacuum, and temperature is carried out at being 88-92 DEG C
Fill, sealing, are then cooled to room temperature, prepared Millettia speciosa champ health care beverage.
It is illustrated below by more specifically embodiment.
Embodiment 1
A kind of Millettia speciosa champ health care beverage, in units of weight portion, including following raw material：185 parts of Millettia Speciosa, 90 parts of black tea, Flos Caryophylli 8
Part, 12 parts of Folium Nelumbinis, 10 parts of Radix Puerariae, 9 parts of Flos Lonicerae, 6 parts of Flos Sophorae, 8 parts of preserved plum vinegar, 3.5 parts of ginkgetin, polyvinyl pyrilodone
1 part, 0.6 part of hydroxypropyl methyl cellulose potassium, 0.7 part of agar, 1 part of Dupont EEA2112AC compatilizer, food grade antioxidant
264 0.8 parts, 0.9 part of xanthan gum, 0.5 part of epoxidized soybean oil fatty acid, 0.4 part of lemon yellow pigment, nisin 0.7
Part, 0.2 part of selenium element, 0.2 part of manganese element, 0.1 part of cobalt element, 0.4 part of proline, 0.3 part of isoleucine, 0.2 part of serine,
0.3 part of threonine, 0.2 part of Vitamin E, 0.2 part of vitamin B1,0.3 part of vitamin C, aspartyl-phenylalanine methyl ester
0.04 part, 2 parts of sucrose, 0.05 part of dihydro jasmone, fragrant 0.03 part of ethyl, 0.05 part of carvone, methyl-furfuryl fumarate 0.8
Part, 0.2 part of 51- guanosine monophosphate disodium, 0.1 part of guanyl potassium；
The preparation method of described Millettia speciosa champ health care beverage, comprises the following steps：
S1：The preparation of Millettia Speciosa juice, comprises the following steps；
S11：The Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 180 mesh sieve, prepared Millettia Speciosa minces；
S12：It is 1 in mass ratio that the Millettia Speciosa that step S11 is obtained minces with water:5 ratio mixing loads extraction pot, in pressure
For under 5MPa, with 5 layers of filtered through gauze after decocting in water 0.5h, prepared filtrate A；
S13：The filtrate A rotating speed that step S12 is obtained is the centrifuge of 4500r/min, is 0.082MPa in vacuum
Lower sucking filtration roguing, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps：
S21：Black tea is dried to water content≤8.5% pulverizing, crosses 130 mesh sieves, the ethanol water being 82% with mass fraction
It is 1 in mass ratio:13 mixing, are 170W in microwave power, and temperature extracts 25min at being 46 DEG C, filters, and concentrates, and prepared tea is many
Phenol crude extract A；
S22：The tea polyphenols crude extract A that step S21 is obtained is added in the KCl solution that concentration is 18%, pH regulator to 6,
Centrifugal rotational speed is to remove impurity under 4500r/min, using aperture be 0.02 μm of filter membrane temperature be at 34 DEG C to centrifugation after molten
Liquid is filtered, prepared liquor B；
S23：By step S22 be obtained liquor B with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3：Flos Caryophylli, Folium Nelumbinis, Radix Puerariae, Flos Lonicerae, Flos Sophorae are separately dried the co-grinding to water content≤7.5%, add water,
Solid-liquid ratio is 1:15（W/V）, microwave power is 200W, and Extracting temperature is 93 DEG C, and extraction time is 1.4h, and then filtering residue is obtained
Medicinal liquid；
S4：By medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step S1, step S2, step S3, preserved plum vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont EEA2112AC compatilizer, food stage
After antioxidant 264, xanthan gum, epoxidized soybean oil fatty acid, 1200 parts of water mix, it is 165W in microwave power, temperature is 64 DEG C,
Speed of agitator is to stir 0.6h under 300r/min, and uniform mixed liquor A is obtained；
The preparation method of described ginkgetin comprises the following steps：
S41：Dry Folium Ginkgo is pulverized and is crossed 100 mesh sieve, prepared Ginkgo Leaf；
S42：The Ginkgo Leaf that step S41 is obtained is extracted using 55 DEG C of water, and in extraction, microwave power is 180W, Gu
Liquor ratio is 1:14（W/V）, extraction time is 0.8h, extracts 2 times, and filtration, merging filtrate after extraction are obtained mixing lixiviating solution；
S43：The mixing lixiviating solution concentrate drying that step S42 is obtained, is obtained extraction cream, is used in extraction 6.6 times of volumes of cream
52 DEG C of water is dissolved, and carries out extracting 2 times using anhydrous ethyl acetate solvent, continuation is repeatedly tied with anhydrous ethyl acetate
Brilliant process, in crystallization process, solid-to-liquid ratio is 1:5.6（W/V）, prepared crystal crude product；
S44：By the prepared crystal crude product of step S43 through supercritical CO2Extraction, the condition of extraction：Extraction kettle pressure is
18MPa, extraction temperature is 47 DEG C, and extraction time is 30min, prepared ginkgetin；
S5：To step S4 be obtained uniform mixed liquor A in add lemon yellow pigment, nisin, selenium element, manganese element,
Cobalt element, proline, isoleucine, serine, threonine, Vitamin E, vitamin B1, vitamin C, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, sucrose, dihydro jasmone, ethyl perfume, carvone, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
Microwave power is 145W, and temperature is 52 DEG C, and speed of agitator is to stir 0.5h under 400r/min, and uniform mixed liquid B is obtained；
S6：The uniform mixed liquor that step S5 is obtained is 135 DEG C in temperature, and pressure is the 3s that sterilizes under 230KPa, is obtained and uniformly mixes
Close liquid C；
S7：The uniform mixed liquor C that step S6 is obtained is 0.092MPa in vacuum, and temperature carries out fill, sealing at being 90 DEG C,
It is then cooled to room temperature, prepared Millettia speciosa champ health care beverage.
Embodiment 2
A kind of Millettia speciosa champ health care beverage, in units of weight portion, including following raw material：152 parts of Millettia Speciosa, 71 parts of black tea, Flos Caryophylli 7
Part, 9 parts of Folium Nelumbinis, 6 parts of Radix Puerariae, 7 parts of Flos Lonicerae, 5 parts of Flos Sophorae, 5 parts of preserved plum vinegar, 2.4 parts of ginkgetin, polyvinyl pyrilodone
0.7 part, 0.4 part of hydroxypropyl methyl cellulose potassium, 0.5 part of agar, 0.7 part of Dupont EEA2112AC compatilizer, food stage resist
264 0.6 parts of oxygen agent, 0.5 part of xanthan gum, 0.3 part of epoxidized soybean oil fatty acid, 0.3 part of lemon yellow pigment, nisin
0.5 part, 0.2 part of selenium element, 0.2 part of manganese element, 0.1 part of cobalt element, 0.3 part of proline, 0.2 part of isoleucine, serine 0.2
Part, 0.2 part of threonine, 0.2 part of Vitamin E, 0.2 part of vitamin B1,0.2 part of vitamin C, aspartyl-phenyl alanine first
Fragrant 0.02 part of 0.03 part of ester, 1.5 parts of sucrose, 0.03 part of dihydro jasmone, ethyl, 0.04 part of carvone, methyl-furfuryl fumarate
0.5 part, 0.2 part of 51- guanosine monophosphate disodium, 0.1 part of guanyl potassium；
The preparation method of described Millettia speciosa champ health care beverage, comprises the following steps：
S1：The preparation of Millettia Speciosa juice, comprises the following steps；
S11：The Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 150 mesh sieve, prepared Millettia Speciosa minces；
S12：It is 1 in mass ratio that the Millettia Speciosa that step S11 is obtained minces with water:3 ratio mixing loads extraction pot, in pressure
For under 4MPa, with 4 layers of filtered through gauze after decocting in water 0.6h, prepared filtrate A；
S13：The filtrate A rotating speed that step S12 is obtained is the centrifuge of 4000r/min, is 0.076MPa in vacuum
Lower sucking filtration roguing, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps：
S21：By black tea dry to water content be 8.2% after pulverize, cross 100 mesh sieves, the ethanol water being 75% with mass fraction
It is 1 in mass ratio:12 mixing, are 150W in microwave power, and temperature extracts 30min at being 44 DEG C, filters, and concentrates, and prepared tea is many
Phenol crude extract A；
S22：The tea polyphenols crude extract A that step S21 is obtained is added in the KCl solution that concentration is 17%, pH regulator to 5.8,
Remove impurity under centrifugal rotational speed is for 4000r/min, using aperture be 0.01 μm of filter membrane temperature be at 32 DEG C to centrifugation after
Solution is filtered, prepared liquor B；
S23：By step S22 be obtained liquor B with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3：Flos Caryophylli, Folium Nelumbinis, Radix Puerariae, Flos Lonicerae, Flos Sophorae are separately dried the co-grinding to water content≤7.5%, add water,
Solid-liquid ratio is 1:13（W/V）, microwave power is 180W, and Extracting temperature is 90 DEG C, and extraction time is 1.7h, and then filtering residue is obtained
Medicinal liquid；
S4：By medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step S1, step S2, step S3, preserved plum vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont EEA2112AC compatilizer, food stage
After antioxidant 264, xanthan gum, epoxidized soybean oil fatty acid, 1300 parts of water mix, it is 155W in microwave power, temperature is 62 DEG C,
Speed of agitator is to stir 0.8h under 200r/min, and uniform mixed liquor A is obtained；
The preparation method of described ginkgetin comprises the following steps：
S41：Dry Folium Ginkgo is pulverized and is crossed 100 mesh sieve, prepared Ginkgo Leaf；
S42：The Ginkgo Leaf that step S41 is obtained is extracted using 45 DEG C of water, and in extraction, microwave power is 150W, Gu
Liquor ratio is 1:12（W/V）, extraction time is 1h, extracts 2 times, and filtration, merging filtrate after extraction are obtained mixing lixiviating solution；
S43：The mixing lixiviating solution concentrate drying that step S42 is obtained, is obtained extraction cream, is used in extraction 6.5 times of volumes of cream
48 DEG C of water is dissolved, and carries out extracting 2 times using anhydrous ethyl acetate solvent, continuation is repeatedly tied with anhydrous ethyl acetate
Brilliant process, in crystallization process, solid-to-liquid ratio is 1:5.5（W/V）, prepared crystal crude product；
S44：By the prepared crystal crude product of step S43 through supercritical CO2Extraction, the condition of extraction：Extraction kettle pressure is
14MPa, extraction temperature is 46 DEG C, and extraction time is 35min, prepared ginkgetin；
S5：To step S4 be obtained uniform mixed liquor A in add lemon yellow pigment, nisin, selenium element, manganese element,
Cobalt element, proline, isoleucine, serine, threonine, Vitamin E, vitamin B1, vitamin C, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, sucrose, dihydro jasmone, ethyl perfume, carvone, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
Microwave power is 138W, and temperature is 48 DEG C, and speed of agitator is to stir 0.6h under 300r/min, and uniform mixed liquid B is obtained；
S6：The uniform mixed liquor that step S5 is obtained is 134 DEG C in temperature, and pressure is the 4s that sterilizes under 210KPa, is obtained and uniformly mixes
Close liquid C；
S7：The uniform mixed liquor C that step S6 is obtained is 0.089MPa in vacuum, and temperature carries out fill, sealing at being 88 DEG C,
It is then cooled to room temperature, prepared Millettia speciosa champ health care beverage.
Embodiment 3
A kind of Millettia speciosa champ health care beverage, in units of weight portion, including following raw material：210 parts of Millettia Speciosa, 100 parts of black tea, Flos Caryophylli
10 parts, 14 parts of Folium Nelumbinis, 12 parts of Radix Puerariae, 10 parts of Flos Lonicerae, 7 parts of Flos Sophorae, 9 parts of preserved plum vinegar, 4.2 parts of ginkgetin, polypropylene pyrroles
1.1 parts of alkanone, 0.7 part of hydroxypropyl methyl cellulose potassium, 0.8 part of agar, 1.2 parts of Dupont EEA2112AC compatilizer, food
0.9 part of antioxidant 264 of level, 1.2 parts of xanthan gum, 0.6 part of epoxidized soybean oil fatty acid, 0.5 part of lemon yellow pigment, nisin
0.8 part of rhzomorph, 0.3 part of selenium element, 0.3 part of manganese element, 0.2 part of cobalt element, 0.5 part of proline, isoleucine 0.4 part, thread ammonia
0.3 part of acid, 0.4 part of threonine, 0.3 part of Vitamin E, 0.3 part of vitamin B1,0.4 part of vitamin C, aspartoyl phenylpropyl alcohol ammonia
Fragrant 0.04 part of 0.05 part of sour methyl ester, 2.5 parts of sucrose, 0.06 part of dihydro jasmone, ethyl, 0.06 part of carvone, fumaric acid furfuryl alcohol
0.9 part of methyl ester, 0.3 part of 51- guanosine monophosphate disodium, 0.2 part of guanyl potassium；
The preparation method of described Millettia speciosa champ health care beverage, comprises the following steps：
S1：The preparation of Millettia Speciosa juice, comprises the following steps；
S11：The Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 200 mesh sieve, prepared Millettia Speciosa minces；
S12：It is 1 in mass ratio that the Millettia Speciosa that step S11 is obtained minces with water:7 ratio mixing loads extraction pot, in pressure
Power is under 6MPa, with 6 layers of filtered through gauze after decocting in water 0.3h, prepared filtrate A；
S13：The filtrate A rotating speed that step S12 is obtained is the centrifuge of 5000r/min, is 0.085MPa in vacuum
Lower sucking filtration roguing, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps：
S21：Black tea is dried to water content≤8.5% pulverizing, crosses 140 mesh sieves, with the ethanol water for 75%-84% for the mass fraction
Solution is 1 in mass ratio:14 mixing, are 180W in microwave power, and temperature extracts 18min at being 48 DEG C, filters, and concentrates, and is obtained
Tea polyphenols crude extract A；
S22：The tea polyphenols crude extract A that step S21 is obtained is added in the KCl solution that concentration is 19%, pH regulator to 6.2,
Remove impurity under centrifugal rotational speed is for 5000r/min, using aperture be 0.03 μm of filter membrane temperature be at 35 DEG C to centrifugation after
Solution is filtered, prepared liquor B；
S23：By step S22 be obtained liquor B with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3：Flos Caryophylli, Folium Nelumbinis, Radix Puerariae, Flos Lonicerae, Flos Sophorae are separately dried the co-grinding to water content≤7.5%, add water,
Solid-liquid ratio is 1:15（W/V）, microwave power is 220W, and Extracting temperature is 95 DEG C, and extraction time is 1.3h, and then filtering residue is obtained
Medicinal liquid；
S4：By medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step S1, step S2, step S3, preserved plum vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont EEA2112AC compatilizer, food stage
After antioxidant 264, xanthan gum, epoxidized soybean oil fatty acid, 1500 parts of water mix, it is 174W in microwave power, temperature is 66 DEG C,
Speed of agitator is to stir 0.4h under 400r/min, and uniform mixed liquor A is obtained；
The preparation method of described ginkgetin comprises the following steps：
S41：Dry Folium Ginkgo is pulverized and is crossed 120 mesh sieve, prepared Ginkgo Leaf；
S42：The Ginkgo Leaf that step S41 is obtained is extracted using 65 DEG C of water, and in extraction, microwave power is 200W, Gu
Liquor ratio is 1:15（W/V）, extraction time is 0.5h, extracts 3 times, and filtration, merging filtrate after extraction are obtained mixing lixiviating solution；
S43：The mixing lixiviating solution concentrate drying that step S42 is obtained, is obtained extraction cream, is used in extraction 6.8 times of volumes of cream
56 DEG C of water is dissolved, and carries out extracting 3 times using anhydrous ethyl acetate solvent, continuation is repeatedly tied with anhydrous ethyl acetate
Brilliant process, in crystallization process, solid-to-liquid ratio is 1:5.8（W/V）, prepared crystal crude product；
S44：By the prepared crystal crude product of step S43 through supercritical CO2Extraction, the condition of extraction：Extraction kettle pressure is
20MPa, extraction temperature is 48 DEG C, and extraction time is 25min, prepared ginkgetin；
S5：To step S4 be obtained uniform mixed liquor A in add lemon yellow pigment, nisin, selenium element, manganese element,
Cobalt element, proline, isoleucine, serine, threonine, Vitamin E, vitamin B1, vitamin C, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, sucrose, dihydro jasmone, ethyl perfume, carvone, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
Microwave power is 152W, and temperature is 55 DEG C, and speed of agitator is to stir 0.4h under 500r/min, and uniform mixed liquid B is obtained；
S6：The uniform mixed liquor that step S5 is obtained is 136 DEG C in temperature, and pressure is the 2s that sterilizes under 230KPa, is obtained and uniformly mixes
Close liquid C；
S7：The uniform mixed liquor C that step S6 is obtained is 0.093MPa in vacuum, and temperature carries out fill, sealing at being 92 DEG C,
It is then cooled to room temperature, prepared Millettia speciosa champ health care beverage.
Millettia speciosa champ health care beverage obtained by embodiment 1-3 is carried out with organoleptic quality, physical and chemical quality, preparation time mensure,
Result is as shown in table 1,2,3.
The organoleptic quality of table 1 Millettia speciosa champ health care beverage
As shown in Table 1, limpid, golden yellow bright on the Millettia speciosa champ health care beverage color and luster that the present invention is obtained；Mouthfeel tea flavour is substantially, sour-sweet
Tasty and refreshing；Heavy flavour of vinegar fragrance on fragrance, has tea perfume.
The physical and chemical quality of table 2 Millettia speciosa champ health care beverage
As shown in Table 2, the Millettia speciosa champ health care beverage acetic acid content that the present invention is obtained is 11.63-12.38g/L, and polyphenol content is
1.39-1.64g/L, pH value is 6.4-6.67.
The preparation time of table 3 Millettia speciosa champ health care beverage
As shown in Table 3, the preparation time of the Millettia speciosa champ health care beverage that the present invention is obtained is more shorter than the preparation time of prior art, from
And shorten the production cycle, reduces cost.
The Millettia speciosa champ health care beverage of the present invention is dispelled implication effect test
Choose 100 people with implication symptom, wherein male 48 people, female 52 people.Drink the Millettia speciosa champ health care beverage 3 of the present invention daily
Cup, every glass of 250mL, obtain result of the test after 5 days as shown in table 4.
Table 4 is dispelled implication effect test result
As shown in Table 4, the Millettia speciosa champ health care beverage of the present invention being capable of effectively treatment or mitigation implication symptom.
Above content it cannot be assumed that the present invention be embodied as be confined to these explanations, the affiliated technology neck for the present invention
For the those of ordinary skill in domain, without departing from the inventive concept of the premise, some simple deduction or replace can also be made,
The scope of patent protection that the present invention is determined all should be considered as belonging to by the claims submitted to.
Claims (6)
1. a kind of Millettia speciosa champ health care beverage is it is characterised in that in units of weight portion, including following raw material：Millettia Speciosa 152-210
Part, black tea 71-100 part, Flos Caryophylli 7-10 part, Folium Nelumbinis 9-14 part, Radix Puerariae 6-12 part, Flos Lonicerae 7-10 part, Flos Sophorae 5-7 part, Fructus Armeniacae Mume
Vinegar 5-9 part, ginkgetin 2.4-4.2 part, polyvinyl pyrilodone 0.7-1.1 part, hydroxypropyl methyl cellulose potassium 0.4-0.7
Part, agar 0.5-0.8 part, Dupont EEA2112AC compatilizer 0.7-1.2 part, food grade antioxidant 264 0.6-0.9 part,
Xanthan gum 0.5-1.2 part, epoxidized soybean oil fatty acid 0.3-0.6 part, lemon yellow pigment 0.3-0.5 part, nisin
0.5-0.8 part, selenium element 0.2-0.3 part, manganese element 0.2-0.3 part, cobalt element 0.1-0.2 part, proline 0.3-0.5 part, different
Leucine 0.2-0.4 part, serine 0.2-0.3 part, threonine 0.2-0.4 part, Vitamin E 0.2-0.3 part, vitamin B1
0.2-0.3 part, vitamin C 0.2-0.4 part, aspartyl-phenylalanine methyl ester 0.03-0.05 part, sucrose 1.5-2.5 part, two
Hydrogen jasmone 0.03-0.06 part, ethyl perfume 0.02-0.04 part, carvone 0.04-0.06 part, methyl-furfuryl fumarate 0.5-0.9
Part, 51- guanosine monophosphate disodium 0.2-0.3 part, guanyl potassium 0.1-0.2 part；
The preparation method of described Millettia speciosa champ health care beverage, comprises the following steps：
S1：The preparation of Millettia Speciosa juice, comprises the following steps；
S11：The Millettia Speciosa cleaning strand grinding machine is crushed, is filtered with 150-200 mesh sieve, prepared Millettia Speciosa minces；
S12：It is 1 in mass ratio that the Millettia Speciosa that step S11 is obtained minces with water:The ratio mixing of 3-7 loads extraction pot, in pressure
Power is under 4-6MPa, uses 4-6 layer filtered through gauze, prepared filtrate A after decocting in water 0.3-0.6h；
S13：The filtrate A rotating speed that step S12 is obtained is the centrifuge of 4000-5000r/min, in vacuum is
Sucking filtration roguing under 0.076-0.085MPa, prepared Millettia Speciosa juice；
S2, the preparation of tea polyphenols, comprise the following steps：
S21：Black tea is dried to water content≤8.5% pulverizing, crosses 100-140 mesh sieve, with the second for 75%-84% for the mass fraction
Alcohol-water solution is 1 in mass ratio:12-14 mixes, and is 150-180W in microwave power, and temperature extracts 18- at being 44-48 DEG C
30min, filters, and concentrates, prepared tea polyphenols crude extract A；
S22：The tea polyphenols crude extract A that step S21 is obtained is added in the KCl solution that concentration is 17%-19%, and pH regulator is extremely
5.8-6.2, removes impurity, using aperture for 0.01-0.03 μm of filter membrane in temperature under centrifugal rotational speed is for 4000-5000r/min
For filtering to the solution after centrifugation at 32-35 DEG C, prepared liquor B；
S23：By step S22 be obtained liquor B with butyl ether extract, freezing, be dried after be obtained tea polyphenols；
S3：Flos Caryophylli, Folium Nelumbinis, Radix Puerariae, Flos Lonicerae, Flos Sophorae are separately dried the co-grinding to water content≤7.5%, add water,
Solid-liquid ratio is 1:13-15（W/V）, microwave power is 180-220W, and Extracting temperature is 90-95 DEG C, and extraction time is 1.3-1.7h,
Then filtering residue, prepared medicinal liquid；
S4：By medicinal liquid prepared to tea polyphenols prepared to the prepared Millettia Speciosa juice of step S1, step S2, step S3, preserved plum vinegar, silver
Flavone, polyvinyl pyrilodone, hydroxypropyl methyl cellulose potassium, agar, Dupont EEA2112AC compatilizer, food stage
After antioxidant 264, xanthan gum, epoxidized soybean oil fatty acid, 1300-1500 part water mix, it is 155-174W in microwave power, temperature
Spend for 62-66 DEG C, speed of agitator is to stir 0.4-0.8h under 200-400r/min, and uniform mixed liquor A is obtained；
The preparation method of described ginkgetin comprises the following steps：
S41：Dry Folium Ginkgo is pulverized and is crossed 100-120 mesh sieve, prepared Ginkgo Leaf；
S42：The Ginkgo Leaf that step S41 is obtained is extracted using 45-65 DEG C of water, and in extraction, microwave power is 150-
200W, solid-to-liquid ratio is 1:12-15（W/V）, extraction time is 0.5-1h, extracts 2-3 time, and filtration, merging filtrate after extraction are obtained
Mixing lixiviating solution；
S43：The mixing lixiviating solution concentrate drying that step S42 is obtained, is obtained extraction cream, is used in extraction 6.5-6.8 times of body of cream
The water of long-pending 48-56 DEG C is dissolved, and carries out extraction 2-3 time using anhydrous ethyl acetate solvent, continues to use anhydrous ethyl acetate
Carry out multiple crystallization treatment, in crystallization process, solid-to-liquid ratio is 1:5.5-5.8（W/V）, prepared crystal crude product；
S44：By the prepared crystal crude product of step S43 through supercritical CO2Extraction, the condition of extraction：Extraction kettle pressure is 14-
20MPa, extraction temperature is 46-48 DEG C, and extraction time is 25-35min, prepared ginkgetin；
S5：To step S4 be obtained uniform mixed liquor A in add lemon yellow pigment, nisin, selenium element, manganese element,
Cobalt element, proline, isoleucine, serine, threonine, Vitamin E, vitamin B1, vitamin C, aspartoyl phenylpropyl alcohol ammonia
Sour methyl ester, sucrose, dihydro jasmone, ethyl perfume, carvone, methyl-furfuryl fumarate, 51- guanosine monophosphate disodium, guanyl potassium,
Microwave power is 138-152W, and temperature is 48-55 DEG C, and speed of agitator is to stir 0.4-0.6h under 300-500r/min, is obtained all
Even mixed liquid B；
S6：The uniform mixed liquor that step S5 is obtained is 134-136 DEG C in temperature, and pressure is the 2-4s that sterilizes under 210-230KPa,
Uniform mixed liquor C is obtained；
S7：The uniform mixed liquor C that step S6 is obtained is 0.089-0.093MPa in vacuum, and temperature is carried out at being 88-92 DEG C
Fill, sealing, are then cooled to room temperature, prepared Millettia speciosa champ health care beverage.
2. Millettia speciosa champ health care beverage according to claim 1 is it is characterised in that microwave power described in step S3 is
220W, Extracting temperature is 92 DEG C, and extraction time is 1.4h.
3. Millettia speciosa champ health care beverage according to claim 2 is it is characterised in that microwave power described in step S4 is
174W, temperature is 66 DEG C, and speed of agitator is to stir 0.4h under 400r/min.
4. Millettia speciosa champ health care beverage according to claim 3 is it is characterised in that microwave power described in step S5 is
152W, temperature is 54 DEG C, and speed of agitator is to stir 0.4h under 4000r/min.
5. Millettia speciosa champ health care beverage according to claim 1, it is characterised in that temperature described in step S6 is 136 DEG C, is pressed
Power is the 2s that sterilizes under 230KPa.
6. Millettia speciosa champ health care beverage according to claim 1 is it is characterised in that vacuum described in step S6 is
0.093MPa, temperature carries out fill, sealing at being 92 DEG C.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108338272A (en) * | 2018-01-30 | 2018-07-31 | 广西东兰县隘洞拉社通达种养专业合作社 | A kind of sow feed and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101611909A (en) * | 2009-05-05 | 2009-12-30 | 潘泰安 | Full nutrient Chinese wolfberry health-care fruit juice and production method thereof |
| CN105767396A (en) * | 2016-05-12 | 2016-07-20 | 广西科技大学鹿山学院 | Lipid-lowering ginkgo seed tea |
-
2016
- 2016-10-17 CN CN201610902825.1A patent/CN106472930A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101611909A (en) * | 2009-05-05 | 2009-12-30 | 潘泰安 | Full nutrient Chinese wolfberry health-care fruit juice and production method thereof |
| CN105767396A (en) * | 2016-05-12 | 2016-07-20 | 广西科技大学鹿山学院 | Lipid-lowering ginkgo seed tea |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108338272A (en) * | 2018-01-30 | 2018-07-31 | 广西东兰县隘洞拉社通达种养专业合作社 | A kind of sow feed and preparation method thereof |
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