CN106465725A - A kind of bactericidal composition containing fluoxastrobin and simeconazoles and its application - Google Patents
A kind of bactericidal composition containing fluoxastrobin and simeconazoles and its application Download PDFInfo
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- CN106465725A CN106465725A CN201610756411.2A CN201610756411A CN106465725A CN 106465725 A CN106465725 A CN 106465725A CN 201610756411 A CN201610756411 A CN 201610756411A CN 106465725 A CN106465725 A CN 106465725A
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- simeconazoles
- fluoxastrobin
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N55/00—Biocides, pest repellants or attractants, or plant growth regulators, containing organic compounds containing elements other than carbon, hydrogen, halogen, oxygen, nitrogen and sulfur
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/72—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms
- A01N43/88—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with nitrogen atoms and oxygen or sulfur atoms as ring hetero atoms six-membered rings with three ring hetero atoms
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- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
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Abstract
The invention discloses a kind of bactericidal composition containing fluoxastrobin and simeconazoles and its application., with fluoxastrobin and simeconazoles as principle active component, the weight of wherein fluoxastrobin and simeconazoles is than for 1～70 for this bactericidal composition：1～50.This bactericidal composition can be applicable to prevent and treat Cereal, fruit tree, vegetable disease, has higher synergistic function, overcomes and delayed the Drug resistance of pathogenic bacteria, and sterilization speed is fast, lasting period length, reduce application cost, and prevention effect is substantially better than its single dose and uses.The present invention can be used for the fungal disease prevented and treated on crops it is particularly possible to be used for the fungal disease such as control rust, glume blight, net blotch, powdery mildew, downy mildew, scab, damping-off, banded sclerotial blight, and effect is better than single dose and uses.
Description
Technical field
The present invention relates to a kind of bactericidal composition and application thereof, especially a kind of with fluoxastrobin and simeconazoles for mainly living
The bactericidal composition of property composition and its application.
Background technology
Fluoxastrobin (Fluoxastrobin), molecular formula：C21H16ClFN4O5, chemical name：{ 2- [6- (2- chlorobenzene oxygen
Base) -5-FU -4- base oxygen] phenyl } (5,6- dihydros-Isosorbide-5-Nitrae, 2- diazine -3- base) ketone O- methyloxime, structural formula：
Fluoxastrobin has the bactericidal activity of wide spectrum, to nearly all Mycophytes (Ascomycetes, Basidiomycetess, Oomycete
And Fungi Imperfecti) the tens of kinds of diseases such as disease such as rust, clever blessing disease, net blotch, powdery mildew, downy mildew all have good activity.
Simeconazoles (simeconazole), molecular formula：C14H20FN3OSi, chemical name：(RS) -2- (4- fluorophenyl) -1-
(1H-1,2,4-1 tri- -1- bases) -3- trimethyl silicon substrate propane -2- alcohol, chemical structural formula：
Simeconazoles Main Function mechanism is sterol demethylation inhibitors, destroys and stop the cell membrane important composition of pathogenic bacteria
The biosynthesiss of composition ergosterol, lead to cell membrane can not be formed, and make pathogenic bacteria dead.Due to having good absorbability,
There are in plant body the osmosiss of brilliance, therefore can promptly be absorbed by plants, and internally conduct；There is good protection
And therapeutic activity.Disease caused by multiple ascomycetess, basidiomycetes and Fungi Imperfecti can effectively be prevented and treated, especially to all kinds of powdery mildews, black
Star disease, rust, damping-off, banded sclerotial blight etc. have excellent preventive effect.
The difficulty of prevention and cure of phytopathogen is increasing at present, on the one hand, with the change of pattern of farming, melon fruits and vegetables etc.
Industrial crops cultivated area progressively expands, and disease occurrence degree, generation quantity all increase, and in preventing and treating, difficulty increases；Separately
On the one hand, the resistance of pathogen rises under lasting medicament selection pressure year by year, and the prevention effect of single dose is had a greatly reduced quality, plant
Disease control is faced with significant challenge.
Content of the invention
The purpose of the present invention is to provide a kind of applied widely, low cost, effect good fluorine-containing for above-mentioned technical problem
Fluoxastrobin and the plant bactericidal composition of simeconazoles.
It is a still further object of the present invention to provide this bactericidal composition causes answering on fungal disease in preventing and treating plant epiphyte
With especially in mycosises such as control rust, glume blight, net blotch, powdery mildew, downy mildew, scab, damping-off, banded sclerotial blights
In evil purposes.
The purpose of the present invention is realized by following measures：
A kind of bactericidal composition containing fluoxastrobin and simeconazoles, said composition is with fluoxastrobin and simeconazoles for mainly having
Effect composition, wherein fluoxastrobin and simeconazoles weight ratio is for 1～70：1～50.Wherein in bactericidal composition, active ingredient is with potentiation
Effective dose is present in compositionss.
In the present invention, the fluoxastrobin in bactericidal composition and simeconazoles can be in weight ratios 1～70：In the range of 1～50
Arbitrarily adjust, the such as weight of the two ratio is for 5～50：10～50,5～40：10～30,1～5：1～20,1～2：0.5～15,
1：1～10,1：1～9 etc..In another kind of scheme, fluoxastrobin and simeconazoles can select following weight than in any one
Plant or multiple：1:50、1:49、1:48、1:47、1:46、1:45、1:44、1:43、1:42、1:41、1:40、1:39、1:38、1:
37、1:36、1:35、1:34、1:33、1:32、1:31、1:30、1:29、1:28、1:27、1:26、1:25、1:24、1:23、1:
22、1:21、1:20、1:19、1:18、1:17、1:16、1:15、1:14、1:13、1:12、1:11、1:10、1:9、1:8、1:7、1:
6、1:5、1:4、1:3、1:2、1:1、2:1、3:1、4:1、5:1、6:1、7:1、8:1、9:1、10:1、11:1、12:1、13:1、14:
1、15:1、16:1、17:1、18:1、19:1、20:1、21:1、22:1、23:1、24:1、25:1、26:1、27:1、28:1、29:1、
30:1、31:1、32:1、33:1、34:1、35:1、36:1、37:1、38:1、39:1、40:1、41:1、42:1、43:1、44:1、
45:1、46:1、47:1、48:1、49:1、50:1、51:1、52:1、53:1、54:1、55:1、56:1、57:1、58:1、59:1、
60:1、61:1、62:1、63:1、64:1、65:1、66:1、67:1、68:1、69:1、70:1、2:3、2:5、3:4、3:5、3:2、4:
3、5:2、5:3 etc..
In the compositions of the present invention, the percentage by weight accounting for compositionss both fluoxastrobin and simeconazoles is 1～95%, excellent
Select 2～80%, further preferred 10～40%.
Described bactericidal composition, wherein with fluoxastrobin and simeconazoles as principle active component, is helped with known pesticide
Agent and/or excipient are configured to any one dosage form allow on pesticide.Known to these, auxiliary agent, excipient include but is not limited to
Dispersant, diffusant, defoamer, wetting agent, disintegrating agent etc., can adopt calcium dodecyl benzene sulfonate, alkylphenol-polyethenoxy
Ether, Ben-zylphenol Polyoxyethyl Ether, phenethyl phenol polyethenoxy ether, fatty alcohol-polyoxyethylene ether and its similar products, fatty amine gather
Oxygen vinyl Ether, fatty acid ethylene oxide addition product, polyoxyethylene polyoxy propylene block compound, castor oil polyoxyethylene ether, nonyl
Base phenol polyethenoxy ether, TWEEN Series, fatty alcohol-polyoxyethylene ether, Polyethylene Glycol series, Sulfonateses, carboxylate, sulfate,
One of phosphate, phosphite, lignosulfonates, xanthan gum, phenol formaldehyde condensate, ammonium salt, quaternary etc. or many
Individual combination, excipient includes Ketohexamethylene, dimethylbenzene, various solvent naphtha, water, antifreezing agent (as propylene glycol), deionized water etc..More than
Auxiliary agent, excipient and other adjuvant can be alone or be used in combination.
Described bactericidal composition, its dosage form is that cream, wettable powder, suspending agent, aqueous emulsion, microemulsion or moisture dissipate
Granule.
This bactericidal composition can be applicable to prevent and treat resistance plant fungal disease aspect, particularly preventing and treating Cereal, fruit tree, vegetable
The application of dish crop pest aspect.
The present composition scope of application increases it is adaptable to preventing and treating Cereal, fruit tree, the disease of vegetable, particularly prevents and treats
Rust, glume blight, net blotch, powdery mildew, downy mildew, scab, damping-off, banded sclerotial blight.Bactericidal composition of the present invention is to ascus
Bacterium, basidiomycetes, Fungi Imperfecti fungal disease have good prevention effect；And suppress insect or funguses to unitary agent (the phonetic bacterium of fluorine
Ester and simeconazoles are arbitrary) drug-fast generation.
Application on preparation preventing and treating refractory fungal for the bactericidal composition of the present invention, especially in control rust, glume blight, net
Pinta, powdery mildew, downy mildew, scab, damping-off, the application of banded sclerotial blight class fungal disease all have significant effect.Above-mentioned kill
Bacteria composition can produce higher synergistic function, and the consumption of the amount ratio independent reactive compound of this mixture is significantly
Reduce, that is, the activity of mixture is more than the activity of independent component.
Compared with prior art beneficial effects of the present invention：(1) compared with single dose, said composition antagonism fungal disease has
Substantially synergistic function, overcomes and has delayed Drug resistance, and expanding prevention is composed hence it is evident that improve prevention effect；(2) reduce preventing and treating
Recruitment, drug cost；(3) pesticide that is alternative conventional and being also easy to produce resistance；(4) compared with single dose, produce and use cost fall
Low；(5) suppress the drug-fast generation of funguses, its effect uses apparently higher than its single dose.
Specific embodiment
The invention will be further described with reference to embodiments, and in embodiment, the preparation method of dosage form is routine side
Method, " % " of the present invention is mass percent.
Indoor biometricses are tested：
Adopt mycelial growth rate method indoors, measure different agents to wheat powdery mildew bacterial strain (Erysiphe
Graminis D.c.f.sp.tritici E.Marchal) EC50Value, using co-toxicity coefficient computational methods, calculates mixture
Co-toxicity coefficient (CTC), determines the building performance of mixture, circular is as follows：
With in mixture, a certain single dose (generally selects EC as standard agent50Junior), calculated：
Single dose toxicity index=standard agent EC50/ certain single dose EC50×100
The toxicity index of the toxicity index of theoretical toxicity index=A single dose × A single dose proportion+B single dose in mixture
× B single dose proportion in mixture
The EC of actual measurement toxicity index=standard single dose50The EC of value/mixture50Value × 100
Co-toxicity coefficient=actual measurement toxicity index/theoretical toxicity index × 100
Co-toxicity coefficient is classified：When CTC is more than 120, mixture has synergetic, and it is antagonism that CTC is less than when 80, and CTC exists
It is summation action between 80-120.
Table 1：The indoor biometricses result to wheat powdery mildew bacterial strain for the fluoxastrobin+simeconazoles different ratio
| Medicament | Virulence regression equation | EC50(mg/L) | Co-toxicity coefficient |
| Fluoxastrobin (A) | Y=2.54X+3.33 | 4.552 | - |
| Simeconazoles (B) | Y=1.60X+3.86 | 5.169 | - |
| A:B=70:1 | Y=1.28X+4.15 | 4.647 | 111.42 |
| A:B=10:1 | Y=2.45X+3.80 | 3.082 | 169.54 |
| A:B=1:1 | Y=2.41X+3.14 | 5.894 | 242.26 |
| A:B=1:3 | Y=1.92X+3.09 | 9.835 | 159.15 |
| A:B=1:6 | Y=2.15X+3.03 | 8.244 | 198.02 |
| A:B=1:10 | Y=1.88X+3.36 | 7.495 | 222.45 |
| A:B=1:20 | Y=3.11X+3.57 | 2.891 | 201.75 |
| A:B=1:70 | Y=2.45X+3.30 | 4.932 | 118.79 |
Field control effectiveness test：
The pesticidal preparations preventing and treating wheat powdery mildew test being obtained with following embodiments.
1st, test process：This test medicine consumption sets three concentration for the treatment of, comparison medicine respectively according to the difference of each composition
Agent is pesticide single dose 10% fluoxastrobin EC and 20% simeconazoles WP and blank clean water experiment respectively.
2nd, each plot area of test method is 66.7m2, it is repeated 3 times；Investigation drug effect side after investigating before dispenser and preventing and treating
Method is：In test process area, (every takes 5M to 5 points of randomization2), carry out the state of an illness according to national field test relevant criterion
Classification, calculates preventive effect.
3rd, result of the test see table：
Shown by indoor biometricses and field efficacy result, fluoxastrobin and simeconazoles compositionss have significantly collaborative increasing
Effect acts on, and the prevention effect of compositionss is excellent, and prevention effect is all better than single dose kind, has using value in agricultural application.
Two kinds of reactive compounds can be processed into any one dosage form of permission, illustrates two kinds with specific embodiment below
The preparation that effective ingredient is processed into, but the preparation that can process of this two kinds of active components be not limited only to set forth below.
Embodiment 1：
By fluoxastrobin 5g, simeconazoles 10g, detergent LS (to methoxyl group fatty acid amido benzene sulfonic acid sodium salt) 2g, diffusant
NNO (sodium methylene bis-naphthalene sulfonate) 4g, white carbon 5g, Kaolin adds to 100g mixture and carries out comminution by gas stream, is obtained and effectively becomes
Weight percentage is divided to be 15% fluoxastrobin-simeconazoles wettable powder.
Embodiment 2：
By fluoxastrobin 3g, simeconazoles 12g, sodium lauryl sulphate 3g, dispersing agent NNO 4g, white carbon 5g, Kaolin adds
Carry out comminution by gas stream to 100g mixture, prepared effective ingredient weight percentage is 15% fluoxastrobin-simeconazoles wettability
Powder.
Embodiment 3：
By fluoxastrobin 2g, simeconazoles 14g, sodium lauryl sulphate 3g, dispersing agent NNO 4g, white carbon 5g, Kaolin adds
Carry out comminution by gas stream to 100g mixture, prepared effective ingredient weight percentage is 16% fluoxastrobin-simeconazoles wettability
Powder.
Embodiment 4：
Weigh 5g fluoxastrobin, 50g simeconazoles, phenethyl phenol polyethenoxy ether phosphate ester 3g, agriculture breast 33#2g, alkyl phenol
Polyoxyethylene ether 1g, 150# solvent naphtha 13g, adds water to 100g.The method that above raw material is routinely prepared aqueous emulsion puts into mixed
Close the mixing of kettle high speed, making effective Ingredients Weight percentage composition is 55% fluoxastrobin-simeconazoles aqueous emulsion.
Embodiment 5：
Weigh 2g fluoxastrobin, 30g simeconazoles, calcium dodecyl benzene sulfonate 6g, phenethyl phenol polyethenoxy ether phosphate ester
3g, agriculture breast 33#2g, alkylphenol polyoxyethylene 1g, isopropanol 10g, add water to 100g.Above raw material is routinely prepared microemulsion
The method of agent puts in mixing kettle and mixes, and making effective Ingredients Weight percentage composition is 32% fluoxastrobin-simeconazoles microemulsion
Agent.
Embodiment 6：
Weigh 1g fluoxastrobin, 5g simeconazoles, phenethyl phenol polyethenoxy ether phosphate ester 3g, agriculture breast 33#2g, alkyl phenol gather
Oxygen vinyl Ether 1g, 150# solvent naphtha 13g, adds water to 100g.The method that above raw material is routinely prepared aqueous emulsion puts into mixing
Kettle high speed mixes, and making effective Ingredients Weight percentage composition is 6% fluoxastrobin-simeconazoles aqueous emulsion.
Embodiment 7：
Weigh 50g fluoxastrobin, 20g simeconazoles, calcium dodecyl benzene sulfonate 5g, phenethyl phenol polyethenoxy ether 2g, castor
Oleum Sesami polyoxyethylene ether 2g, 150# solvent naphtha is to 100g.The method that above raw material is routinely prepared cream puts in mixing kettle
Mixing, making effective Ingredients Weight percentage composition is 70% fluoxastrobin-simeconazoles cream.
Embodiment 8：
Weigh 2g fluoxastrobin, 40g simeconazoles, calcium dodecyl benzene sulfonate 8g, phenethyl phenol polyethenoxy ether 5g, 150#
Solvent naphtha is to 100g.The method that above raw material is routinely prepared cream puts in mixing kettle and mixes, and makes effective Ingredients Weight
Percentage composition is 42% fluoxastrobin-simeconazoles cream.
Embodiment 9：
Weigh 5g fluoxastrobin, 20g simeconazoles, calcium dodecyl benzene sulfonate 6g, phenethyl phenol polyethenoxy ether phosphate ester
3g, agriculture breast 33#2g, alkylphenol polyoxyethylene 1g, isopropanol 10g, add water to 100g.Above raw material is routinely prepared microemulsion
The method of agent puts in mixing kettle and mixes, and making effective Ingredients Weight percentage composition is 25% fluoxastrobin-simeconazoles microemulsion
Agent.
Embodiment 10：
Weigh 5g fluoxastrobin, 0.5g simeconazoles, calcium dodecyl benzene sulfonate 6g, phenethyl phenol polyethenoxy ether 7g,
150# solvent naphtha is to 100g.The method that above raw material is routinely prepared cream puts in mixing kettle and mixes, and makes effective ingredient
Weight percentage is 5.5% fluoxastrobin-simeconazoles cream.
Embodiment 11：
Weigh 5g fluoxastrobin, 30g simeconazoles, calcium dodecyl benzene sulfonate 4g, phenethyl phenol polyethenoxy ether 4g, 150#
Solvent naphtha is to 100g.The method that above raw material is routinely prepared cream puts in mixing kettle and mixes, and makes effective Ingredients Weight
Percentage composition is 35% fluoxastrobin-simeconazoles cream.
Embodiment 12：
Weigh 10g fluoxastrobin, 10g simeconazoles, lignin 2g, polyoxyethylene poly-oxygen propylene aether and its sulfate 4g, yellow
Virgin rubber 0.15g, ethylene glycol 5g, silica ethane 0.10g, aluminium-magnesium silicate 0.5g, complement to 100g with water, in the presence of sand mill
Making effective Ingredients Weight percentage composition is 20% fluoxastrobin-fluosilicic azole suspending agent.
Embodiment 13：
Weigh 30g fluoxastrobin, 12g simeconazoles, lignin 2g, polyoxyethylene poly-oxygen propylene aether and its sulfate 4g, yellow
Virgin rubber 0.15g, ethylene glycol 5g, silica ethane 0.10g, aluminium-magnesium silicate 0.5g, complement to 100g with water, in the presence of sand mill
Making effective Ingredients Weight percentage composition is 42% fluoxastrobin-fluosilicic azole suspending agent.
Embodiment 14：
Weigh 2g fluoxastrobin, 5g simeconazoles, wooden sodium sulfonate 8g, sodium lauryl sulphate 2g, ammonium sulfate 5g, polyethylene
Alcohol 5g, Borax 2g, white carbon 3g, kieselguhr complement to 100g, and above raw material is formed with imitating into by water dispersible granular agent method
Weight percentage is divided to be 7% fluoxastrobin-simeconazoles water dispersion granule.
Embodiment 15：
Weigh 4g fluoxastrobin, 13g simeconazoles, wooden sodium sulfonate 8g, sodium lauryl sulphate 2g, ammonium sulfate 5g, poly- second
Enol 5g, Borax 2g, kieselguhr 28g complements to 100g, and above raw material is formed with imitating composition weight by water dispersible granular agent method
Amount percentage composition is 17% fluoxastrobin-simeconazoles water dispersion granule.
Embodiment 16：
Weigh 5g fluoxastrobin, 15g simeconazoles, lignin 2g, polyoxyethylene poly-oxygen propylene aether and its sulfate 4g, xanthan
Glue 0.15g, ethylene glycol 5g, silica ethane 0.10g, aluminium-magnesium silicate 0.5g, complement to 100g with water, make in the presence of sand mill
One-tenth effective ingredient weight percentage is 20% fluoxastrobin-fluosilicic azole suspending agent.
Claims (10)
1. a kind of bactericidal composition containing fluoxastrobin and simeconazoles is it is characterised in that said composition is with fluoxastrobin and simeconazoles
For principle active component, the weight of wherein fluoxastrobin and simeconazoles is than for 1～70：1～50.
2. bactericidal composition according to claim 1 is it is characterised in that the weight of described fluoxastrobin and simeconazoles is than for 1
～5：1～20.
3. bactericidal composition according to claim 1 is it is characterised in that the weight of described fluoxastrobin and simeconazoles is than for 1
～2：0.5～15.
4. the bactericidal composition according to claim 1 or 3 is it is characterised in that the weight ratio of described fluoxastrobin and simeconazoles
For 1：1～10.
5. bactericidal composition according to claim 1 is it is characterised in that both described fluoxastrobin and simeconazoles account for combination
The percentage by weight of thing is 2～80%.
6. bactericidal composition according to claim 5 is it is characterised in that both described fluoxastrobin and simeconazoles account for combination
The percentage by weight of thing is 10～40%.
7. bactericidal composition according to claim 1 is it is characterised in that said composition is based on fluoxastrobin and simeconazoles
Want effective ingredient, be configured to any one dosage form of permission on pesticide with insecticides adjuvant and/or excipient.
8. bactericidal composition according to claim 7 it is characterised in that described dosage form be cream, suspending agent, aqueous emulsion, can
WP, microemulsion or water dispersion granule.
9. the bactericidal composition containing fluoxastrobin and simeconazoles described in claim 1 is on preventing and treating resistance plant fungal disease
Application.
10. the bactericidal composition containing fluoxastrobin and simeconazoles described in claim 1 control rust, glume blight, net blotch,
Application on powdery mildew, downy mildew, scab, damping-off or banded sclerotial blight class fungal disease.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060014738A1 (en) * | 2002-06-24 | 2006-01-19 | Ulrike Wachendorff-Neumann | Fungicidal combination of active substances |
| CN101039578A (en) * | 2004-10-12 | 2007-09-19 | 拜尔农作物科学股份公司 | Fungicidal active ingredient combinations containing fluoxastrobin |
| CN102715173A (en) * | 2012-06-28 | 2012-10-10 | 杭州宇龙化工有限公司 | Bactericidal composition containing phenylate diazole and fluoxastrobin and application of bactericidal composition |
| CN102763656A (en) * | 2012-07-13 | 2012-11-07 | 王学权 | Fungicide containing tebuconazole |
-
2016
- 2016-08-29 CN CN201610756411.2A patent/CN106465725A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060014738A1 (en) * | 2002-06-24 | 2006-01-19 | Ulrike Wachendorff-Neumann | Fungicidal combination of active substances |
| CN101039578A (en) * | 2004-10-12 | 2007-09-19 | 拜尔农作物科学股份公司 | Fungicidal active ingredient combinations containing fluoxastrobin |
| CN102715173A (en) * | 2012-06-28 | 2012-10-10 | 杭州宇龙化工有限公司 | Bactericidal composition containing phenylate diazole and fluoxastrobin and application of bactericidal composition |
| CN102763656A (en) * | 2012-07-13 | 2012-11-07 | 王学权 | Fungicide containing tebuconazole |
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Application publication date: 20170301 |