CN1064214C - Method for preparing plant bactericide using traditional Chinese medincinal herbs - Google Patents
Method for preparing plant bactericide using traditional Chinese medincinal herbs Download PDFInfo
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- CN1064214C CN1064214C CN96115719A CN96115719A CN1064214C CN 1064214 C CN1064214 C CN 1064214C CN 96115719 A CN96115719 A CN 96115719A CN 96115719 A CN96115719 A CN 96115719A CN 1064214 C CN1064214 C CN 1064214C
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- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 27
- 239000003899 bactericide agent Substances 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title abstract description 4
- 235000008216 herbs Nutrition 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 13
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000007787 solid Substances 0.000 claims abstract description 9
- 241000411851 herbal medicine Species 0.000 claims abstract description 8
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 7
- 240000001851 Artemisia dracunculus Species 0.000 claims abstract description 6
- 241000050051 Chelone glabra Species 0.000 claims abstract description 6
- 239000000292 calcium oxide Substances 0.000 claims abstract description 6
- 235000012255 calcium oxide Nutrition 0.000 claims abstract description 6
- 239000003814 drug Substances 0.000 claims description 12
- 238000002360 preparation method Methods 0.000 claims description 8
- 230000000855 fungicidal effect Effects 0.000 claims description 7
- 239000000417 fungicide Substances 0.000 claims description 7
- 239000000706 filtrate Substances 0.000 claims description 6
- 235000013305 food Nutrition 0.000 claims description 6
- 235000003092 Artemisia dracunculus Nutrition 0.000 claims description 5
- 240000001579 Cirsium arvense Species 0.000 claims description 5
- 235000005918 Cirsium arvense Nutrition 0.000 claims description 5
- 240000000774 Cunila origanoides Species 0.000 claims description 5
- 235000018274 Cunila origanoides Nutrition 0.000 claims description 5
- 235000014866 Dictamnus albus Nutrition 0.000 claims description 5
- 241000132171 Phryma leptostachya Species 0.000 claims description 5
- 230000000740 bleeding effect Effects 0.000 claims description 5
- 239000003755 preservative agent Substances 0.000 claims description 5
- 230000002335 preservative effect Effects 0.000 claims description 5
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 5
- 239000004299 sodium benzoate Substances 0.000 claims description 5
- 235000010234 sodium benzoate Nutrition 0.000 claims description 5
- 235000013399 edible fruits Nutrition 0.000 abstract description 8
- 241000196324 Embryophyta Species 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 3
- 238000002791 soaking Methods 0.000 abstract description 3
- 241000223600 Alternaria Species 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract 4
- MFYSUUPKMDJYPF-UHFFFAOYSA-N 2-[(4-methyl-2-nitrophenyl)diazenyl]-3-oxo-n-phenylbutanamide Chemical compound C=1C=CC=CC=1NC(=O)C(C(=O)C)N=NC1=CC=C(C)C=C1[N+]([O-])=O MFYSUUPKMDJYPF-UHFFFAOYSA-N 0.000 abstract 1
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 abstract 1
- 235000003097 Artemisia absinthium Nutrition 0.000 abstract 1
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 abstract 1
- 235000003261 Artemisia vulgaris Nutrition 0.000 abstract 1
- 241000212948 Cnidium Species 0.000 abstract 1
- 244000018716 Impatiens biflora Species 0.000 abstract 1
- 235000015912 Impatiens biflora Nutrition 0.000 abstract 1
- 206010029400 Nicotinic acid deficiency Diseases 0.000 abstract 1
- 208000002141 Pellagra Diseases 0.000 abstract 1
- 241000601242 Rotaria Species 0.000 abstract 1
- 241000219784 Sophora Species 0.000 abstract 1
- 235000005155 Tanacetum balsamita Nutrition 0.000 abstract 1
- 241000234299 Zingiberaceae Species 0.000 abstract 1
- 239000004599 antimicrobial Substances 0.000 abstract 1
- 239000001138 artemisia absinthium Substances 0.000 abstract 1
- 230000000149 penetrating effect Effects 0.000 abstract 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 abstract 1
- 241000234314 Zingiber Species 0.000 description 6
- 235000006886 Zingiber officinale Nutrition 0.000 description 6
- 235000008397 ginger Nutrition 0.000 description 6
- 206010043866 Tinea capitis Diseases 0.000 description 5
- 230000035613 defoliation Effects 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 239000007921 spray Substances 0.000 description 5
- 208000009189 tinea favosa Diseases 0.000 description 5
- 241001645362 Valsa Species 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 239000004115 Sodium Silicate Substances 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- 229940079593 drug Drugs 0.000 description 3
- 230000000857 drug effect Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 3
- 229910052911 sodium silicate Inorganic materials 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- GAMFEMAXLMWCRG-UHFFFAOYSA-N bis(dimethylcarbamothioylsulfanyl)arsanyl n,n-dimethylcarbamodithioate Chemical compound CN(C)C(=S)S[As](SC(=S)N(C)C)SC(=S)N(C)C GAMFEMAXLMWCRG-UHFFFAOYSA-N 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 231100000241 scar Toxicity 0.000 description 2
- 235000014347 soups Nutrition 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 1
- 244000291564 Allium cepa Species 0.000 description 1
- 235000002732 Allium cepa var. cepa Nutrition 0.000 description 1
- 239000005739 Bordeaux mixture Substances 0.000 description 1
- 206010020649 Hyperkeratosis Diseases 0.000 description 1
- 239000005802 Mancozeb Substances 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- FROZIYRKKUFAOC-UHFFFAOYSA-N amobam Chemical compound N.N.SC(=S)NCCNC(S)=S FROZIYRKKUFAOC-UHFFFAOYSA-N 0.000 description 1
- 244000052616 bacterial pathogen Species 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- 239000010871 livestock manure Substances 0.000 description 1
- 230000003641 microbiacidal effect Effects 0.000 description 1
- 229940124561 microbicide Drugs 0.000 description 1
- 239000002855 microbicide agent Substances 0.000 description 1
- 239000002420 orchard Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a method for preparing plant bactericide by Chinese herbal medicines, which comprises: proportionally mixing lightyellow sophora root, baical skullcap root and dictamni cortex, crushing, adding to water in certain proportion, soaking at the temperature of 50 to 65 DEG C, and then filtering; crushing argy wormwood leaf, common cephalanoplos herb, common cnidium fruit and garden balsam stem, adding to the water in certain proportion, soaking at the temperature of 75 to 85 DEG C, and then filtering; proportionally mixing the two filtering solutions, and then adding a few penetrating agents and antiseptic agents to obtain liquid bactericide; adding a little quicklime to the two filtering residues to obtain solid bactericide, wherein the liquid bactericide has specially good effects on fruit tree rot and alternaria leaf spot, and the solid bactericide has unexpectedly preventing and treating effects on pellagra of root tuber plants in the ginger family.
Description
The present invention relates to a kind of preparation method of bactericide, particularly a kind of method for preparing bactericide with Chinese herbal medicine.
Due to the polyphyly germs such as plant rot, spot defoliation, bark favus, very heavy to the harm of plant.Especially fruit tree, the easiest trouble rot, spot defoliation, thereby cause the underproduction, even total crop failure, bring heavy losses to the orchard worker.If existing drug main chemicals asomate and iodine solution etc., the former toxicity is seriously polluted greatly, and the high control efficiency of latter's medicine cost is undesirable.CN1072065A discloses a kind of " preventing and treating microbicide compositions of apple valsa canker and preparation method thereof ", the composition that is characterized in a kind of green onion, ginger liquid and liquid sodium silicate is made bactericide, wherein liquid sodium silicate (being commonly called as sodium silicate) alkalescence is extremely strong, is used for not meeting on the fruit tree production requirement of pollution-free food.Other has a CN1040126A document to disclose " a kind of production method of preventing and treating the Chinese herbal and crude drugs preparations of apple valsa canker " to propose to use the herbal control apple valsa canker, and complicated cost is higher but it is filled a prescription, and only effective to apple valsa canker.
The objective of the invention is to overcome the shortcoming of prior art, a kind of preparation method that can prevent and treat the Chinese herbal medicine bactericide of plant rot, spot defoliation, bark favus is provided.
The preparation method of Chinese herbal medicine bactericide of the present invention is as follows, below is weight portion:
(1) kuh-seng 100-80 part, root of large-flowered skullcap 50-40 part, dittany bark 50-40 part is pulverized, and adds in 1600-3000 part water, and 50-65 ℃ was soaked 40-50 hour, filtered;
(2) tarragon 100-80 part, field thistle 25-20 part, frutus cnidii 25-20 part, lopseed 50-40 part is pulverized, and adds in 1600-2400 part water, and 75-85 ℃ was soaked 20-30 hour, filtered;
(3) with the filtrate in above-mentioned 1 and 2 by weight (1-2): ratio (1-2) is mixed, the preservative food that the alumen of medicament gross weight 1-2% was made bleeding agent, 0.5-1% after adding mixed respectively again mixes and is liquid fungicide with Sodium Benzoate or limewash;
(4) filter residue in above-mentioned 1 and 2 is added the quicklime of its gross weight 1-2%, mixing is solid bactericide.
Liquid fungicide of the present invention can effectively be prevented and treated fruit tree putrefaction disease and spot defoliation, and solid bactericide has good control efficiency to rot and the bark favus of ginger class root piece plant, and indoor antibacterial test and field experiment show that efficient is 100%.Production process of the present invention is pollution-free, no gurry, and all raw material all is used appropriately, and the simple cost of technology is low, and can make full use of the Chinese herbal medicine resource of China's abundant.
Bactericide using method of the present invention is as follows: fruit tree putrefaction disease, with 50 times of liquid fungicide soup dilutions, smear fruit tree sufferer place; The fruit tree spot defoliation is with 50 times of soup dilutions, spraying; Ginger rot and bark favus impose on Tanaka with solid bactericide by 20 kilograms every mu.
Bactericide of the present invention is as follows with existing similar agricultural chemicals effect contrast:
Table one. prevent and treat the contrast of apple canker drug effect
The processing project | Test strain number | With concentration (doubly) | Sick scar number before handling | Handle the sick scar number of back major criminal | Efficient (%) | Callus mean breadth (mm) |
Bactericide of the present invention | 30 | 500 | 99 | 4 | 95 | 15 |
40% asomate | 30 | 50 | 120 | 12 | 90 | 3 |
843 rehabilitation agents | 30 | Former medicine | 100 | 50 | 50 | 9 |
Blank | 10 | The spray clear water | 40 | 35 | 5 | 2 |
Table two. the contrast of control alternaria leaf spot of apple drug effect
The processing project | Spray medicine multiple | Spray medicine strain number | The investigation number of blade | The sick number of sheets | Efficient (%) |
Bactericide of the present invention | 1500 | 15 | 600 | 12 | 98 |
Mancozeb | 500 | 15 | 600 | 48 | 92 |
Tuzet | 500 | 15 | 600 | 30 | 95 |
Blank | The spray clear water | 15 | 600 | 303 | 49.5 |
Table three. the contrast of control ginger bark favus drug effect
The processing project | Contents processing | Test mu number (mu) | The investigation total block data | Morbidity ginger piece number | The incidence of disease (%) |
Bactericide of the present invention | With base manure mix at 2: 1000 and execute | 0.5 | 1500 | 0 | 0 |
50% ambam | 1000 times of liquid sprayings spray in 7 days/time 3 times | 0.5 | 1500 | 215 | 13 |
1: 1: 100 bordeaux mixture | Ginger piece seed soaking 20 minutes | 0.5 | 1500 | 300 | 20 |
Blank | Not medication | 0.5 | 1500 | 420 | 28 |
Embodiment 1.
(1) kuh-seng is 100 parts, 50 parts of the roots of large-flowered skullcap, and 50 parts of dittany barks are pulverized, and add in 2000 parts of water, and 60 ℃ were soaked 48 hours, filtered;
(2) tarragon is 100 parts, 25 parts of field thistles, and 25 parts of frutus cnidiis, 50 parts of lopseeds are pulverized, and add in 2000 parts of water, and 80 ℃ were soaked 24 hours, filtered;
(3) filtrate in above-mentioned 1 and 2 is mixed by weight 1: 1 ratio, add respectively again that the alumen that mixes back medicament gross weight 1.5% is made bleeding agent, 0.5% food is made preservative with Sodium Benzoate, mix and be liquid fungicide;
(4) filter residue in above-mentioned 1 and 2 is added the quicklime of its gross weight 1%, mixing is solid bactericide.
Embodiment 2.
(1) kuh-seng is 80 parts, 40 parts of the roots of large-flowered skullcap, and 40 parts of dittany barks are pulverized, and add in 1600 parts of water, and 64 ℃ were soaked 40 hours, filtered;
(2) tarragon is 80 parts, 20 parts of field thistles, and 20 parts of frutus cnidiis, 40 parts of lopseeds are pulverized, and add in 1600 parts of water, and 85 ℃ were soaked 20 hours, filtered;
(3) filtrate in above-mentioned 1 and 2 is mixed by weight 1: 1.2 ratio, add the alumen that mixes back medicament gross weight 1.2% more respectively and make bleeding agent, 0.6% preservative food Sodium Benzoate, mix and be liquid fungicide;
(4) filter residue in above-mentioned 1 and 2 is added the quicklime of its gross weight 1.5%, mixing is solid bactericide.
Embodiment 3. is as described in the embodiment 1, and different is to add 3000 parts in water in (1), adds 2400 parts in water in (2), and two kinds of filtrate ratios are 1.5: 1 in (3).
Claims (2)
1. the preparation method of a Chinese herbal medicine bactericide is characterized in that, comprises the steps, below is weight portion:
(1) kuh-seng 100-80 part, root of large-flowered skullcap 50-40 part, dittany bark 50-40 part is pulverized, and adds in 1600-3000 part water, and 50-65 ℃ was soaked 40-50 hour, filtered;
(2) tarragon 100-80 part, field thistle 25-20 part, frutus cnidii 25-20 part, lopseed 50-40 part is pulverized, and adds in 1600-2400 part water, and 75-85 ℃ was soaked 20-30 hour, filtered;
(3) with the filtrate in above-mentioned (1) and (2) by weight (1-2): ratio (1-2) is mixed, the preservative food that the alumen of medicament gross weight 1-2% was made bleeding agent, 0.5-1% after adding mixed respectively again mixes and is liquid fungicide with Sodium Benzoate or limewash;
(4) filter residue in above-mentioned (1) and (2) is added the quicklime of its gross weight 1-2%, mixing is solid bactericide.
2. the preparation method of Chinese herbal medicine bactericide as claimed in claim 1 is characterized in that, described step is as follows, below is weight portion:
(1) kuh-seng is 100 parts, 50 parts of the roots of large-flowered skullcap, and 50 parts of dittany barks are pulverized, and add in 2000 parts of water, and 60 ℃ were soaked 48 hours, filtered;
(2) tarragon is 100 parts, 25 parts of field thistles, and 25 parts of frutus cnidiis, 50 parts of lopseeds are pulverized, and add in 2000 parts of water, and 80 ℃ were soaked 24 hours, filtered;
(3) filtrate in above-mentioned (1) and (2) is mixed by weight 1: 1 ratio, add the alumen that mixes back medicament gross weight 1.5% more respectively and make bleeding agent, 0.5% preservative food Sodium Benzoate, mix and be liquid fungicide;
(4) filter residue in above-mentioned (1) and (2) is added the quicklime of its gross weight 1%, mixing is solid bactericide.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN96115719A CN1064214C (en) | 1996-04-05 | 1996-04-05 | Method for preparing plant bactericide using traditional Chinese medincinal herbs |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN96115719A CN1064214C (en) | 1996-04-05 | 1996-04-05 | Method for preparing plant bactericide using traditional Chinese medincinal herbs |
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CN1142897A CN1142897A (en) | 1997-02-19 |
CN1064214C true CN1064214C (en) | 2001-04-11 |
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CN96115719A Expired - Fee Related CN1064214C (en) | 1996-04-05 | 1996-04-05 | Method for preparing plant bactericide using traditional Chinese medincinal herbs |
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Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102217661B (en) * | 2011-04-28 | 2013-09-04 | 刘荣常 | Botanical bactericide and preparation method and application thereof |
CN102870833A (en) * | 2012-10-15 | 2013-01-16 | 青岛青大海魁生物技术有限公司 | Chinese medicinal herb marine polypeptide chelate fungicide and preparation method |
CN103250534B (en) * | 2013-04-22 | 2015-03-25 | 范惠明 | Silybum marianum high-yield cultivation method |
CN103875722B (en) * | 2014-03-14 | 2016-04-13 | 内蒙古帅旗生物科技股份有限公司 | Chinese herbal medicine merges the botanical fungicide extracted |
CN104814114A (en) * | 2015-05-29 | 2015-08-05 | 黄琳 | Fresh-keeping method of prawn |
CN105123784A (en) * | 2015-09-18 | 2015-12-09 | 昆明线敌生物科技有限公司 | Traditional Chinese medicine preparation for preventing and treating ginger bacterial wilt and preparation method of traditional Chinese medicine preparation |
CN106342925A (en) * | 2016-08-24 | 2017-01-25 | 蒋丽红 | Biological pesticide specially used for eggplants, and preparation method of biological pesticide |
CN107251922A (en) * | 2017-07-31 | 2017-10-17 | 张其明 | A kind of Chinese medicine composition, its preparation method and application for suppressing apple cultivation class germ |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1037441A (en) * | 1988-05-10 | 1989-11-29 | 靳学文 | With Chinese medicine is the farming fruit medicine manufacture method of raw material |
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1996
- 1996-04-05 CN CN96115719A patent/CN1064214C/en not_active Expired - Fee Related
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1037441A (en) * | 1988-05-10 | 1989-11-29 | 靳学文 | With Chinese medicine is the farming fruit medicine manufacture method of raw material |
Non-Patent Citations (1)
Title |
---|
中药大辞典第一版 1986.6.1 江苏新医学院,上海科技出版社 * |
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