CN106420472A - Multifunctional anti-wrinkle skincare product composition and preparation method thereof - Google Patents
Multifunctional anti-wrinkle skincare product composition and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
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Abstract
The invention discloses a multifunctional anti-wrinkle skincare product composition and a preparation method thereof. The anti-wrinkle skincare product composition comprises the following components by weight percent: 0.01-15% of a moisturizer, 0.5-10% of a silybum marianum extract, 1-5% of carnosine, 0.1-5.0% of a thickener, 0.01-1.0% of a chelating agent, 0.1-5.0% of an emulsifier, 1-10% of an additive and the balance of deionized water. The multifunctional anti-wrinkle skincare product composition provided by the invention can resist three aging-inducing major biochemical reactions (formation of free radicals, lipid peroxidation and formation of cross-linking protein) at the same time through scientific collocation of two components with different activities so as to have apparent glycation resistance, and can maintain skin's elasticity, enhance skin's compactness, reduce production of wrinkles and fine lines, and protect the skin from aging caused by oxidation.
Description
Technical field
The present invention relates to a kind of skin care compositions, belong to cosmetic technical field, more particularly to one kind contains anti-saccharification
The carnosine of anti-oxidation efficacy and have anti-oxidation efficacy plant component milk thistle berry extract anti-wrinkle composition, it can prolong
Slow saccharification course of reaction, prevents the aging that skin oxidative causes and the wrinkle producing.
Background technology
Skin is to cover in the maximum organ of human body surface, due to directly contacting with external environment, aoxidized, drying and
The stimulation of a variety of factor such as ultraviolet, therefore be highly susceptible to damage.Simultaneously can be internal because of age, diet and habits and customs etc.
The impact of factor, leads to the decline of skin function and hereditary abnormalization, so that skin is easily aging, produces wrinkle.
Skin is in the outermost of human body, is made up of epidermis, corium, hypodermis, and major function is that protection body is exempted from
Injured by unfavorable external environment, its meeting miopragia because of the impact of the many factors such as extraneous, hereditary, shown old and feeble disease
Shape, so, anti-aging cosmetics have become one of product of vast female consumer active demand.
The form of skin senescence is mainly naturally-aged (i.e. endogenous is old and feeble) and light aging (i.e. exogenous aging), natural
Aging is mainly caused by body inherent cause, is limited to systemic sites hence it is evident that being characterized as wrinkle and relaxing, and pigmentation etc.
Phenomenon.Skin anti-aging is earnestly paid close attention to by people always, and related Aging Mechanism and anti-aging approach are also always people's research
Focus.Skin senescence is a kind of complicated multifactorial process that multiple mechanism simultaneously participate in, for resisting that single mechanism produces
The material that declines can only solve the problems, such as a certain link of aging, just can develop efficient anti-aging from multi-angle at many levels and make up
Product.
Existing anti-aging cosmetics mainly pass through to remove excessive free radicals, defend ultraviolet, promote Skin Cell newly old
Metabolism, moisturizing and reparation skin barrier function, replenishing collagen and this five aspect of elastin laminin carry out anti-aging.However, it is existing
With the presence of the anti-ageing approach of anti-wrinkle product relatively single, effect is inconspicuous, product stability is poor the problems such as.
Content of the invention
It is an object of the invention to provide a kind of multi-functional crease-resistant composite skin care product, its by interpolation have anti-saccharification and
The carnosine of anti-oxidation efficacy and the plant component milk thistle berry extract with anti-oxidation efficacy, allow composition in the same time pair
Anti- three kinds main biochemical reaction (formation of free radical, lipid peroxidation, the formation of crosslinking protein) leading to aging, thus
Maintain the elasticity of skin by anti-saccharification, reduce wrinkle and microgroove, the degree of compacting of lifting skin, protection skin opposing is by aoxidizing
The aging causing.
Another object of the present invention is the preparation method providing above-mentioned crease-resistant composite skin care product.
The object of the invention to solve the technical problems employs the following technical solutions to realize.Propose according to the present invention
The multi-functional crease-resistant composite skin care product of one kind, by weight percentage, comprise following components：
The NMF of 0.01-15%；The milk thistle berry extract of 0.5-5%；The carnosine of 1-5%；The thickening of 0.5-2.5%
Agent；The chelating agent of 0.01-0.5%；The emulsifying agent of 0.1-5.0%；The additive of 1-16%；Deionized water surplus.
The multi-functional crease-resistant composite skin care product of the embodiment of the present invention, by weight percentage, comprises following components：
The NMF of 0.5-5%；The milk thistle berry extract of 0.5-4%；The carnosine of 1-4%；The thickening of 0.8-1.5%
Agent；The chelating agent of 0.01-0.1%；The emulsifying agent of 0.5-3.0%；The additive of 2-10%；Deionized water surplus.
The multi-functional crease-resistant composite skin care product of the embodiment of the present invention, described NMF is Sodium Hyaluronate, butanediol, ring
One or more of five dimethyl silicone polymers, pungent glycol.Described thickener is PAA/acryloyldimethyl taurine
One or more of sodium copolymer, xanthan gum, Carbomer, cellulose.Described chelating agent is EDTA-2Na.Described emulsifying agent is
Cetearyl glucoside, stearine, PEG-40 Span60, Phosphoric acid monohexadecyl ester potassium, C12-20
Alkyl glucoside, PEG-20 methyl sesquistearate, methyl sesquistearate, sorbitan sesquioleate,
One or more of C20-C22 alkyl phosphate.
Described additive is diethyl hexylcarbonate, marine algae extract, dried tremella extract, tea (CAMELLIA
SINENSIS) leaf extract, pomegranate (PUNICA GRANATUM) extract, bacopa monnieri (BACOPA MONNIERA) extract
One or more of thing, ubiquinone.
The multi-functional crease-resistant composite skin care product of the embodiment of the present invention, by weight percentage, comprises following A, B, C tri-
Component：
Described component A comprises：Sodium Hyaluronate 0.01%～0.15%, butanediol 1.0%～8.0%, cetearyl
Glucoside 0.5%～3.0%, marine algae extract 1.0%～8.0%, EDTA-2Na 0.01%～0.1%, balance of deionization
Water；
Described B component comprises：Ring five dimethyl silicone polymer 1.0%～5.0%, PAA/acryloyldimethyl ox
Sodium sulfonate copolymers 0.5%～1.5%, diethyl hexylcarbonate 1.0%～8.0%；
Described component C comprises：Pungent glycol 0.5%～1.0%, carnosine 1.0%～4.0%, milk thistle berry extract 0.5%
～4.0%.
In addition, above-mentioned multi-functional crease-resistant composite skin care product is to be prepared by following processing step：
1) deionized water is added in emulsification pot, then will soak in Sodium Hyaluronate butanediol, add in emulsification pot,
Open stirring, sequentially add other remaining component A, be warming up to 80 DEG C, be incubated 10 minutes, high speed homogenization 5 minutes；
2) raw material of B component is mixed, add in oil phase pot, and when being warming up to 75 DEG C, oil phase pot material is passed through
In vacuum suction emulsification pot, high speed homogenization 8 minutes, cooling；
3) component C is mixed, add emulsification pot, high speed homogenization 2 minutes when 50 DEG C；
4) cooling, filtering and discharging when being down to 38 DEG C are continued；
5) inspection is qualified, filling.
Compared with prior art, the multi-functional crease-resistant composite skin care product of the present invention, it is right to come by way of three kinds different
Anti-aging, slow down the formation of wrinkle.Clinical trial certificate, it has obvious wrinkle resistance, by increasing capacitance it is possible to increase the elasticity of skin, carries
Rise skin tightness, be especially suitable for being equipped with facial mask essence, the plain and all kinds of face of re-surface intensive wrinkle correct or eye anti-aging cosmetics.
In addition, the multi-functional crease-resistant composite skin care product of the present invention compacting, effect ratio of the aspect such as crease-resistant, smooth skin
Traditional anti-wrinkle product becomes apparent from, and has higher market popularization value.
Brief description
Fig. 1 is canthus skin elasticity test compares figure after continuous using 4 weeks.
Fig. 2 is the improvement situation column compares figure using skin after 28 days.
Specific embodiment
The problem existing for existing anti-wrinkle product, the present invention carries out section by using two kinds of compositions with different activities
Learn collocation so that this composition the same time resist three kinds lead to aging main biochemical reaction (formation of free radical,
Lipid peroxidation, the formation of crosslinking protein), thus having the effect of significantly anti-saccharification, the elasticity of skin can be maintained,
The degree of compacting of lifting skin, reduces the generation of wrinkle and microgroove, the aging that protection skin causes because of oxidation.
Saccharification reaction is a kind of slow natural phenomena, and it affects structure and the activity of albumen.In skin, this anti-
The protein (collagen and elastin laminin) in skin corium should be made stiff, thus leading to skin to follow the string and crossing early ageing
Always, thus producing wrinkle.
Saccharification reaction is reduced sugar produced reaction with protein free amino, and reaction generates irreversible crosslinking protein,
It is referred to as AGE.It can to protein produce negative impact, structure and the activity of protein can be destroyed, make its produce bad and
Irreversible change, it makes the protein being present in skin corium become stiff and easy fragmentation, also can affect protein and its
The interaction of its cell, thus allowing skin to follow the string and plumpness, produces wrinkle.
Oxidation reaction can promote saccharification to react, the MDA for example being produced by the peroxidatic reaction of lipid of induced by ultraviolet irradiation
(MDA), MDA accelerates saccharification reaction, and MDA is a kind of bioactive molecule that can accelerate saccharification reaction, and skin contacts ultraviolet
Line can produce substantial amounts of active oxygen (ROS), and active oxygen (ROS) can lead to the polybasic unsaturated fatty acid in lipid to decompose generation third
Dialdehyde, because it can be used as the index of oxidative pressure a bit.MDA passes through oxidation, changes the mode such as protein structure and function
Go to damage protein, thus leading to the generation of AGE.
Oxidative pressure factor, particularly lipid peroxidation can make the progress faster of saccharification reaction, the combination of the present invention
Thing can suppress the peroxidation of lipid, answers such that it is able to preventing and slowing down this harmful sending out.
Clinical research shows, anti-saccharification anti-wrinkle composition is proved, it can be obviously improved the degree of compacting of skin, smoothness and
Water moisture feeling；After one month, the wrinkle depth of temporal wrinkle decreases 27%, and forehead line depth decreases 24%.
Carnosine is a kind of two peptide material being present in human body, and it is well-known because having potent anti-saccharogenic activity.Carnosine presses down
System is acted on by the protein cross that reduced sugar and active aldehydes (as MDA) induce, and carnosine role in saccharification reaction is
With the glycan molecule of skin protein competition, protection collagenous fibres and EF.
Milk thistle (SILYBUM MARIANUM) berry extract, it is a kind of flowering plant of daisy section, and this is a kind of body
Interior antioxidant and free radical scavenger, such as glutathione and superoxide dismutase, also can catch simultaneously and neutralize free radical, it
The release of energy anti-lipid peroxidation effect, inflammation and histamine.
Combine accompanying drawing below by way of concrete preferred embodiment (table 1) the multi-functional crease-resistant composite skin care product of the present invention is made
Further describe, but the present invention is not limited in below example.Following percentage is all weight percentage.
The raw material components composition of table 1 embodiment 1-3 and reference examples
The preparation method of the multi-functional crease-resistant composite skin care product described in table 1, its step is as follows：
1) deionized water is added in emulsification pot, then will soak in Sodium Hyaluronate butanediol, add in emulsification pot,
Open stirring, sequentially add other remaining component A, be warming up to 80 DEG C, be incubated 10 minutes, 5 points of (3000 revs/min) homogeneous at a high speed
Clock.
2) raw material of B component is mixed, add in oil phase pot, and when being warming up to 75 DEG C, oil phase pot material is passed through
In vacuum suction emulsification pot, (3000 revs/min) homogeneous 8 minutes at a high speed.Cooling.
3) component C is mixed, add emulsification pot, (2000 revs/min) homogeneous 2 minutes at a high speed when 50 DEG C.
4) cooling, filtering and discharging when being down to 38 DEG C are continued.
5) inspection is qualified, filling.
Effete test embodiment
First, human body skin compacts efficacy test
Test sample：Embodiment.
Experimenter：30～40 years old age, women, 30 people.
Test position：Canthus.
Using method：Uniform application is in designated area.
Usage cycles：4 weeks.
Usage frequency：Daily 2 times.
Test parameter：1st, skin elasticity analyzer Cutometer MPA 580 is used for detecting skin elasticity index：
Conceptual design：0th day.
Research starts the last week, and target site stops using any a compact or old and feeble product；Cleaning target site by target
Position is exposed in the environment of constant temperature constant temperature, rests 20 minutes；Target site is carried out with the parametric measurement of skin elasticity index；Clap
According to；Distribution sample.
14th day,
Target site is exposed in the environment of constant temperature and humidity, rests 20 minutes；Skin elasticity index is carried out to target site
Parameter testing；Take pictures.
28th day,
Target site is exposed in the environment of constant temperature and humidity, rests 20 minutes；Skin elasticity index is carried out to target site
Parameter testing；Take pictures.
Data statistics：Data is counted using SPSS 13.0for Windows software kit, before the test after difference
Application pairing T detection is compared, and its significance is P<0.05.
Test result：Coefficient of skin elasticity；In Fig. 1, note：Skin elasticity ()；* represent compared with basic value have notable
Change (P<0.05).
As shown in figure 1, continuously using embodiment after 4 weeks, contrast basic value, canthus skin elasticity all has in test process
Conspicuousness is lifted.
2nd, skin is made to youthen (clinical trial)
Test sample：Embodiment 1, embodiment 2, embodiment 3, reference examples.
Volunteer's age：45～65 years old
Sex：Women.
Volunteer's number：25 people.
Method of testing：The inner forearm of female volunteers, respectively using embodiment and reference examples lotion, uses 2 times daily,
Persistently using 28 days；Respectively using skin elasticity tester, moisture of skin tester and PRIMOS system, to skin tightness,
Humidity and smooth sense are estimated.
Experimental result：After using product 28 days, using aspects such as the degree of compacting of the skin of embodiment, humidity and smoothnesses
Index be obviously improved, and do not improved significantly using the skin of reference examples, or even smoothness have also appeared down
The phenomenon of fall, as shown in Figure 2.
In addition, we have also carried out same test to embodiment 2, embodiment 3, all occur in that similar experimental result,
Fully demonstrate the crease-resistant composite skin care product of the present invention and have really improving the aspects such as degree of compacting, humidity and the smoothness of skin
The effect cut.
The above, be only presently preferred embodiments of the present invention, not the present invention is made with any pro forma restriction, therefore
Every without departing from technical solution of the present invention content, any simply repaiied according to what the technical spirit of the present invention made to above example
Change, equivalent variations and modification, all still fall within the range of technical solution of the present invention.
Claims (9)
1. a kind of multi-functional crease-resistant composite skin care product it is characterised in that by weight percentage, comprises following components：
The NMF of 0.01-15%；The milk thistle berry extract of 0.5-5%；The carnosine of 1-5%；The thickener of 0.5-2.5%；
The chelating agent of 0.01-0.5%；The emulsifying agent of 0.1-5.0%；The additive of 1-16%；Deionized water surplus.
2. multi-functional crease-resistant composite skin care product according to claim 1 it is characterised in that by weight percentage, wraps
Containing following components：
The NMF of 0.5-5%；The milk thistle berry extract of 0.5-4%；The carnosine of 1-4%；The thickener of 0.8-1.5%；
The chelating agent of 0.01-0.1%；The emulsifying agent of 0.5-3.0%；The additive of 2-10%；Deionized water surplus.
3. multi-functional crease-resistant composite skin care product according to claim 1 it is characterised in that：Described NMF is hyalomitome
One or more of sour sodium, butanediol, ring five dimethyl silicone polymer, pungent glycol.
4. multi-functional crease-resistant composite skin care product according to claim 1 it is characterised in that：Described thickener is acrylic acid
One or more of sodium/sodium acryloyldimethyl taurate copolymers, xanthan gum, Carbomer, cellulose.
5. multi-functional crease-resistant composite skin care product according to claim 1 it is characterised in that：Described chelating agent is EDTA-
2Na.
6. multi-functional crease-resistant composite skin care product according to claim 1 it is characterised in that：Described emulsifying agent is that spermaceti is hard
Aliphatic radical glucoside, stearine, PEG-40 Span60, Phosphoric acid monohexadecyl ester potassium, C12-20 alkyl Portugal
Glucosides, PEG-20 methyl sesquistearate, methyl sesquistearate, sorbitan sesquioleate, C20-C22
One or more of alkyl phosphate.
7. multi-functional crease-resistant composite skin care product according to claim 1 it is characterised in that：Described additive is carbonic acid two
Octyl Nitrite, marine algae extract, dried tremella extract, tea (CAMELLIA SINENSIS) leaf extract, pomegranate (PUNICA
GRANATUM) one or more of extract, bacopa monnieri (BACOPA MONNIERA) extract, ubiquinone.
8. the multi-functional crease-resistant composite skin care product according to any one of claim 1-7 is it is characterised in that by weight hundred
Divide than meter, comprise following tri- components of A, B, C：
Described component A comprises：Sodium Hyaluronate 0.01%～0.15%, butanediol 1.0%～8.0%, cetearyl glucose
Glycosides 0.5%～3.0%, marine algae extract 1.0%～8.0%, EDTA-2Na 0.01%～0.1%, balance of deionized water；
Described B component comprises：Ring five dimethyl silicone polymer 1.0%～5.0%, PAA/acryloyldimethyl taurine
Sodium copolymer 0.5%～1.5%, diethyl hexylcarbonate 1.0%～8.0%；
Described component C comprises：Pungent glycol 0.5%～1.0%, carnosine 1.0%～4.0%, milk thistle berry extract 0.5%～
4.0%.
9. multi-functional crease-resistant composite skin care product according to claim 8 is it is characterised in that be by following processing step system
Standby obtain：
1) deionized water is added in emulsification pot, then will soak in Sodium Hyaluronate butanediol, add in emulsification pot, open
Stirring, sequentially adds other remaining component A, is warming up to 80 DEG C, is incubated 10 minutes, high speed homogenization 5 minutes；
2) raw material of B component is mixed, add in oil phase pot, and when being warming up to 75 DEG C, oil phase pot material is passed through vacuum
In suction emulsification pot, high speed homogenization 8 minutes, cooling；
3) component C is mixed, add emulsification pot, high speed homogenization 2 minutes when 50 DEG C；
4) cooling, filtering and discharging when being down to 38 DEG C are continued；
5) inspection is qualified, filling.
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Cited By (6)
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| CN107881216A (en) * | 2017-12-12 | 2018-04-06 | 杜立波 | A kind of anti-aging skin care product method for customizing |
| CN107929206A (en) * | 2017-12-20 | 2018-04-20 | 上海东晟源日化有限公司 | One kind has the intensive anti-oxidant skin care item of crease-resistant activated polysaccharide albumen |
| CN112807255A (en) * | 2020-03-23 | 2021-05-18 | 上海铮信生物科技有限公司 | Anti-wrinkle composition and application thereof in cosmetics |
| CN113384507A (en) * | 2021-07-22 | 2021-09-14 | 广东丸美生物技术股份有限公司 | Anti-aging composition and preparation method and application thereof |
| CN116370361A (en) * | 2023-06-06 | 2023-07-04 | 珠海远大美业生物科技有限公司 | Anti-aging composition and preparation method and application thereof |
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| CN107661262A (en) * | 2017-10-28 | 2018-02-06 | 安徽孔氏奇医药科技有限公司 | One kind is compacted radioresistance eye cream and preparation method thereof |
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| CN107929206A (en) * | 2017-12-20 | 2018-04-20 | 上海东晟源日化有限公司 | One kind has the intensive anti-oxidant skin care item of crease-resistant activated polysaccharide albumen |
| CN112807255A (en) * | 2020-03-23 | 2021-05-18 | 上海铮信生物科技有限公司 | Anti-wrinkle composition and application thereof in cosmetics |
| CN113384507A (en) * | 2021-07-22 | 2021-09-14 | 广东丸美生物技术股份有限公司 | Anti-aging composition and preparation method and application thereof |
| CN113384507B (en) * | 2021-07-22 | 2022-05-27 | 广东丸美生物技术股份有限公司 | Anti-aging composition and preparation method and application thereof |
| CN116370361A (en) * | 2023-06-06 | 2023-07-04 | 珠海远大美业生物科技有限公司 | Anti-aging composition and preparation method and application thereof |
| CN116370361B (en) * | 2023-06-06 | 2023-09-12 | 珠海远大美业生物科技有限公司 | Anti-aging composition and preparation method and application thereof |
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