CN106420384A - Anti-dandruff itching relieving shampoo and preparation method thereof - Google Patents
Anti-dandruff itching relieving shampoo and preparation method thereof Download PDFInfo
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- CN106420384A CN106420384A CN201611222866.2A CN201611222866A CN106420384A CN 106420384 A CN106420384 A CN 106420384A CN 201611222866 A CN201611222866 A CN 201611222866A CN 106420384 A CN106420384 A CN 106420384A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4913—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having five membered rings, e.g. pyrrolidone carboxylic acid
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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Abstract
The invention belongs to the technical field of daily chemical preparations, and particularly relates to anti-dandruff itching relieving shampoo and a preparation method thereof. The shampoo mainly comprises, in weight percentage, 7-15% of lauryl polyoxyethylene ether ammonium sulfate, 2-7% of cetearyl glucoside, 3-10% of cocamidopropylamine oxide, 7-12% of lecithin, 2-6% of dipropylene glycol, 2-4% of pyrrolidone carboxylic acid zinc, 1-3% of ethyl alcohol, 0.1-0.2% of acetic acid, 0.5-1% of nanometer titania, 0.5-1% of dipotassium glycyrrhizinate, 0.2-0.4% of preservatives and 50-70% of water. The shampoo has simple and mild components, good cleaning power, good dandruff removing and itching relieving functions and a good inhibiting effect on fungous dandruff. Moreover, the shampoo is faintly acid, scalp sebum cannot be damaged, and a normal metabolism environment of scalp is maintained.
Description
Technical field
The invention belongs to daily use chemicals preparation technical field, and in particular to a kind of antidandruff and antipruritic shampoo and its preparation side
Method.
Background technology
The dandruff is more common in adult, and the scalp environment that living habit or hormone cause changes, sebaceous gland activity
Level reduces, and causes substantial amounts of pityrosporum ovale amount reproduction, forms the substantial amounts of dandruff, and this is sending out for the pathogenic dandruff
Raw reason；Some is that scalp environment is unbalance as life-time service alkalescence shampoo is caused, and drying causes the dandruff
Occur.
It is attractive in appearance that the dandruff has had a strong impact on human body, has increased to ceremony aspect now, and the even dandruff is led
The scalp itch of cause has had a strong impact on the orthobiosiss of people, therefore, selects a kind of suitable antidandruff and antipruritic shampoo very heavy
Will.
At present, the method for solving the fungoids dandruff is washed hair using TPIATOP, can locally use daktarin soft
Cream external, but persistently can not use for a long time using medicine is anti-dandruff, may develop immunity to drugs or injure scalp；Another kind side
Method is the shampoo using alkalescence, can find that the dandruff is reduced a lot of after use, but the time more long on the contrary can be before producing ratio
More dandruffs, because alkalescence can stimulate scalp epithelial cell keratinization, produce the dandruff.
Therefore, increasing research institution is devoted to studying faintly acid shampoo, and scalp pH is about on a 5.5-6.0 left side
The right side, the pH of shampoo should be more or less the same with scalp environment.
Notification number discloses a kind of dandruff control shampoo containing for the Chinese patent of 103370044A, including：A) 0.1-5wt.%
Anti-dandruff zinc salt；B) the branched alkoyl isethionates of 1-8wt.%；C) fatty acyl isethionate of 1-10wt.%
Product, the product is comprising the fatty acyl hydroxy sulfonate of 40-80wt% and free fatty and/or the fat of 15-50wt%
Hydrochlorate；And d) the cosurfactant of 0.5-14wt%；Exist to improving anti-dandruff zinc salt with branched alkoyl isethionates
The purposes for depositing on scalp, but, substantial amounts of sulfonate belongs to weak base salt, can stimulate scalp, dries scalp hydropenia, makes for a long time
With more dandruffs can be produced.
The Chinese patent application of Publication No. 104306182A discloses a kind of weak acid amino acid shampoo, comprising following group
Become part：Alanine 4-5 part, L-Valine 3-10 part, Leucine 10-15 part, isoleucine 2-8 part, proline 6-11 part, phenylpropyl alcohol
Propylhomoserin 7-13 part, L-Tryptophan 2-9 part, methionine 11-15 part, Glycine 12-15 part, serine 10-16 part, threonine 3-9 part,
Cysteine 7-10 part, acidic amino acid mixture 40-45 part, Oleum Cocois 4-5 part, wheat protein 2-11 part, detergent alkylate
Sodium sulfonate 2-6 part..The weak acid amino acid shampoo formula containing acidic amino acid mixture described in the invention, with anti-dandruff,
Antipruritic effect, and Controlling oil effect is obvious, is very suitable for the client of oiliness scalp tissue, and wherein the patent employs substantial amounts of
Aminoacid, first from cost for, aminoacid extract and separate not be simple flow process, on the market commonly use be not list
The aminoacid of one composition, configuration cost is too high, and secondly, a large amount of aminoacid, albumen and the lubricant component for containing in shampoo belongs to
Organic nutrient substance, easily going mouldy during storage makes shampoo fail, and finally, the cleansing for using is detergent alkylate
Sodium sulfonate, very little, cleaning dynamics is too weak, is only suitable for nursing function for content.
Content of the invention
In order to solve disadvantages mentioned above present in prior art and deficiency, the invention provides a kind of antidandruff and antipruritic shampoo
And preparation method thereof, the hair washing water constituent is simply gentle, and cleaning force is good, with good removing scurf and relieving itching function, to fungoids head
Scurf has good inhibitory action, and water of washing hair does not have destructiveness to scalp sebum, maintains scalp normal for faintly acid
Metabolism environment.
Concrete technical scheme of the present invention is as follows.
A kind of antidandruff and antipruritic shampoo, mainly is become to be grouped into by following mass fraction：Laureth sulphuric acid
Ammonium 7-15%, cetearyl glucoside 2-7%, cocamidopropyl propyl amide amine oxide 3-10%, lecithin 7-12%, double third sweet
Alcohol 2-6%, zinc pyrrolidone carboxylate 2-4%, ethanol 1-3%, acetic acid 0.1-0.2%, nano titanium oxide 0.5-1%, Radix Glycyrrhizae
Sour dipotassium 0.5-1%, preservative 0.2-0.4% and water 50-70%.
Zinc pyrrolidone carboxylate CAS：15454-75-8；Dipropylene glycol CAS：110-98-5.
Zinc pyrrolidone carboxylate can be used to control excessive fat secretion, make scalp salubriouser, and with good
Antibacterium, antifungal, the effect of antiinflammatory；Glycyrrhizic acid dipotassium has the effects such as antiinflammatory, antiallergic, moisturizing, with the use of ketopyrrolidine
Zinc polycarboxylate, can prevent zinc pyrrolidone carboxylate to be deposited on scalp surface, and beneficial to the cleaning function of shampoo, the present invention also adds
Nano titanium oxide, finds there is suppression bactericidal action well to the fungoids dandruff, and some tinea bacterium is had relatively
Good antibacterial effect.
Preferably, described antidandruff and antipruritic shampoo, is become to be grouped into by following mass fraction：Laureth
Ammonium sulfate 10%, cetearyl glucoside 4%, cocamidopropyl propyl amide amine oxide 6%, lecithin 9%, dipropylene glycol 4%,
Zinc pyrrolidone carboxylate 3%, ethanol 2%, acetic acid 0.15%, nano titanium oxide 0.75%, glycyrrhizic acid dipotassium 0.8%, anti-corrosion
Agent 0.3% and water 60%.
Further, described preservative is Kazon.
Further, present invention also offers the preparation method of described antidandruff and antipruritic shampoo, step is：
S1：Acetic acid is added in ethanol, after fully dissolving, obtains pH adjusting agent A；
S2：Make after water, dipropylene glycol, zinc pyrrolidone carboxylate, glycyrrhizic acid dipotassium and nano titanium oxide are sufficiently mixed
With in vacuum pump suction emulsifying pot, 80-90 DEG C is heated to, constant temperature stirs 10-15min, mixing speed is 250-400r/min, to obtain
Aqueous phase B；
S3：The aqueous phase B that step S2 is obtained is cooled to after 60-70 DEG C, sucks laureth using vacuum pump
Ammonium sulfate, cetearyl glucoside, cocamidopropyl propyl amide amine oxide, lecithin, constant temperature stirs 20-30min, mixing speed
For 250-400r/min, mastic C is obtained；
S4：The pH to 5.6-6.0 of the mastic C for being obtained using pH adjusting agent A regulating step S3 obtained in step S1, is then dropped
Temperature sucks preservative to 45-55 DEG C, and constant temperature stirs 15-20min, and mixing speed is 250-400r/min, homogeneous 10-15min,
Room temperature is down to, discharging, obtain final product.
Further, pH to 5.8 is adjusted in described step S4.
The hair washing water constituent that the present invention is provided is simply gentle, is faintly acid, and damaged scalp, can preferably not maintain scalp
Normal metabolism environment.The formula that the present invention is provided has good compatibility, uses cooperatively, and sterilizing and itch-relieving effect is strong.
Compared with prior art, the present invention has advantages below：
1st, faintly acid：Replace traditional alkaline dandruff control shampoo containing using weakly acidic dandruff control shampoo containing, not damaged scalp, can
Preferably to maintain the normal metabolism environment of scalp.
2nd, sterilizing and itch-relieving effect：Glycyrrhizic acid dipotassium is used cooperatively using zinc pyrrolidone carboxylate, nano titanium oxide, to thin
Bacterium, funguses have good sterilization effect, further removing the dandruff, while not injuring scalp, not developing immunity to drugs.
Specific embodiment
Below by specific embodiment, the present invention is described in further details, these embodiments are only used for the mesh of illustration
, it is in no way intended to limit protection scope of the present invention.The present invention using become to belong to conventional products, nano titanium oxide：Shanghai permits
Multiple nanosecond science and technology company limited, article No. YFO04-N30；Lauryl polyethenoxy ether sodium sulfate (CAS.32612-48-9)：Hubei
Ju Sheng Science and Technology Ltd.；Cetearyl glucoside (CAS.68439-49-6)：The happy Industrial Co., Ltd. of Shanghai Jin Jin；Cocos nucifera oil
Amido propyl amine oxide cocamidopropyl propyl amide amine oxide (CAS.68155-09-9)：The chemical limited public affairs of Jin Jinle (Hunan)
Department；Lecithin (CAS.8002-43-5)：Henan Hua Yue chemical products company limited.
Embodiment 1
A kind of antidandruff and antipruritic shampoo, is become to be grouped into by following mass fraction：Lauryl polyethenoxy ether sodium sulfate
10%th, cetearyl glucoside 4%, cocamidopropyl propyl amide amine oxide 6%, lecithin 9%, dipropylene glycol 4%, pyrrolidine
Keto carboxylic acid zinc 3%, ethanol 2%, acetic acid 0.15%, nano titanium oxide 0.75%, glycyrrhizic acid dipotassium 0.8%, Preservative Kathon CG(Methylchloroisothiazolinone/Methylisothiazolinone combination)
0.3% and water 60%.
The preparation method of described antidandruff and antipruritic shampoo, step is：
S1：Acetic acid is added in ethanol, after fully dissolving, obtains pH adjusting agent A；
S2：Make after water, dipropylene glycol, zinc pyrrolidone carboxylate, glycyrrhizic acid dipotassium and nano titanium oxide are sufficiently mixed
With in vacuum pump suction emulsifying pot, 85 DEG C are heated to, constant temperature stirs 13min, mixing speed is 300r/min, to obtain aqueous phase B；
S3：After the aqueous phase B that step S2 is obtained is cooled to 65 DEG C, laureth sulphuric acid is sucked using vacuum pump
Ammonium, cetearyl glucoside, cocamidopropyl propyl amide amine oxide, lecithin, constant temperature stirs 25min, and mixing speed is 300r/
Min, obtains mastic C；
S4：The pH to 5.8 of the mastic C for being obtained using pH adjusting agent A regulating step S3 obtained in step S1, is then cooled to
50 DEG C, preservative is sucked, constant temperature stirs 18min, mixing speed is 300r/min, homogeneous 13min, room temperature to be down to, discharging, i.e.,
?.
Embodiment 2
A kind of antidandruff and antipruritic shampoo, is become to be grouped into by following mass fraction：Lauryl polyethenoxy ether sodium sulfate
15%th, cetearyl glucoside 2%, cocamidopropyl propyl amide amine oxide 10%, lecithin 7%, dipropylene glycol 6%, pyrroles
Alkanone zinc polycarboxylate 2%, ethanol 3%, acetic acid 0.1%, nano titanium oxide 1%, glycyrrhizic acid dipotassium 0.5%, Preservative Kathon CG(Methylchloroisothiazolinone/Methylisothiazolinone combination)
0.4% and water 53%.
The preparation method of the antidandruff and antipruritic shampoo is similar to Example 1.
Embodiment 3
A kind of antidandruff and antipruritic shampoo, is become to be grouped into by following mass fraction：Lauryl polyethenoxy ether sodium sulfate
7%th, cetearyl glucoside 7%, cocamidopropyl propyl amide amine oxide 3%, lecithin 12%, dipropylene glycol 2%, pyrrolidine
Keto carboxylic acid zinc 4%, ethanol 1%, acetic acid 0.2%, nano titanium oxide 0.5%, glycyrrhizic acid dipotassium 1%, Preservative Kathon CG(Methylchloroisothiazolinone/Methylisothiazolinone combination) 0.2%
With water 62.1%.
The preparation method of the antidandruff and antipruritic shampoo is similar to Example 1.
Comparative example 1
A kind of antidandruff and antipruritic shampoo, is become to be grouped into by following mass fraction：Lauryl polyethenoxy ether sodium sulfate
10%th, cetearyl glucoside 4%, cocamidopropyl propyl amide amine oxide 6%, lecithin 9%, dipropylene glycol 4%, pyrrolidine
Keto carboxylic acid zinc 3.75%, ethanol 2%, acetic acid 0.15%, glycyrrhizic acid dipotassium 0.8%, Preservative Kathon CG(Methylchloroisothiazolinone/Methylisothiazolinone combination) 0.3% and water 60.0%.
Difference with embodiment 1 is：Without nano titanium oxide, increase the content of zinc pyrrolidone carboxylate.
The preparation method of the antidandruff and antipruritic shampoo is similar to Example 1.
Comparative example 2
A kind of antidandruff and antipruritic shampoo, is become to be grouped into by following mass fraction：Lauryl polyethenoxy ether sodium sulfate
10%th, cetearyl glucoside 4%, cocamidopropyl propyl amide amine oxide 6%, lecithin 9%, dipropylene glycol 4%, pyrrolidine
Keto carboxylic acid zinc 3%, ethanol 2%, nano titanium oxide 0.75%, glycyrrhizic acid dipotassium 0.95%, Kazon 0.3% and water 60.0%.
The preparation method of described antidandruff and antipruritic shampoo, step is：
S1：Water, ethanol, dipropylene glycol, zinc pyrrolidone carboxylate, glycyrrhizic acid dipotassium and nano titanium oxide are sufficiently mixed
Afterwards using in vacuum pump suction emulsifying pot, 85 DEG C are heated to, constant temperature stirs 13min, mixing speed is 300r/min, to obtain water phase A；
S2：Water phase A that step S1 is obtained is cooled to after 65 DEG C, sucks laureth sulphuric acid using vacuum pump
Ammonium, cetearyl glucoside, cocamidopropyl propyl amide amine oxide, lecithin, constant temperature stirs 25min, and mixing speed is 300r/
Min, obtains mastic B；
S3：The mastic B that step S2 is obtained continues to be cooled to 50 DEG C, sucks preservative, and constant temperature stirs 18min, stirring speed
Spend for 300r/min, homogeneous 13min, room temperature is down to, discharging, obtain final product.
Difference with embodiment 1 is：Without acetic acid, increase the content of glycyrrhizic acid dipotassium.
1 skin patch test of test example
1st, tested material：The antidandruff and antipruritic shampoo that embodiment 1-3 is prepared with comparative example 1-2.
2nd, subjects：Male 25 people, 25 people of female, each 5 people of men and women is 1 group, experimenter's no dermatosiss allergies, meets tested
Person volunteers inclusion criteria.
3rd, test method：Device is tried from qualified speckle, with closed patch experiment method, by tested material about 0.020ml～
0.025ml is dripped in speckle examination device, and external special adhesive tape is covered on subjects back, removes tested material, wash with water after 0.5 hour
Only, dermoreaction after observing 0.5,2,6 hours respectively.
Human skin patch result shows：50 experimenters are by stopping itching shampoo (embodiment of the present invention
1-3), reference substance (comparative example 1-2) patch test, observed dermoreaction at 0.5,2,6 hours, and wherein 0 skin occur bad
Reaction, illustrates to test antidandruff and antipruritic shampoo safety used.While it can also be observed that embodiment of the present invention 1-3 and comparative example
There is no dry-out phenomenon after removing 6 hours in 1 antidandruff and antipruritic shampoo for preparing, but after comparative example 2 is dispelled 6 hours, skin is slightly
There is drying property skin effect phenomenon, illustrate that the antidandruff and antipruritic shampoo moisture retention that comparative example 2 is prepared is poor.
2 effect test of test example
1st, test products：The antidandruff and antipruritic shampoo that embodiment 1-3 is prepared with comparative example 1-2.
2nd, subjects：Male 25 people, 25 people of female, each 5 people of men and women is 1 group, and all subjects are all that the dandruff is sent out
Itch hair quality.
3rd, test method：Per two days using 1 shampoo hair washing, continuously use 2 months, observation experiment effect, test knot
3 grades of fruit point, cure：The dandruff be can't see completely using rear；Effectively：Reduced using the rear dandruff, but do not remove dry
Only；Invalid：Completely without anti-dandruff effect, observation result is simultaneously recorded, concrete as shown in table 1.
1 effect test of table
From table 1 it follows that the shampoo removing scurf and relieving itching effect is significant that embodiment of the present invention 1-3 is prepared, and right
Ratio 1-2 is to carry out simple plus-minus on the basis of the present invention to replace to formula, and effect changes, and illustrates that inventive formulation has
There is good compatibility, arbitrarily can not add and subtract.
Above-described embodiment only principle of the illustrative present invention and its effect, not for the restriction present invention.Any ripe
The personage for knowing this technology all can carry out modifications and changes to above-described embodiment, still without prejudice under the spirit and the scope of the present invention
Should be covered by the claim of the present invention.
Claims (5)
1. a kind of antidandruff and antipruritic shampoo, it is characterised in that main become to be grouped into by following mass fraction：Lauryl polyoxy second
Alkene ether ammonium sulfate 7-15%, cetearyl glucoside 2-7%, cocamidopropyl propyl amide amine oxide 3-10%, lecithin 7-
12%th, dipropylene glycol 2-6%, zinc pyrrolidone carboxylate 2-4%, ethanol 1-3%, acetic acid 0.1-0.2%, nano titanium oxide
0.5-1%, glycyrrhizic acid dipotassium 0.5-1%, preservative 0.2-0.4% and water 50-70%.
2. antidandruff and antipruritic shampoo according to claim 1, it is characterised in that become to be grouped into by following mass fraction：
Lauryl polyethenoxy ether sodium sulfate 10%, cetearyl glucoside 4%, cocamidopropyl propyl amide amine oxide 6%, lecithin
9%th, dipropylene glycol 4%, zinc pyrrolidone carboxylate 3%, ethanol 2%, acetic acid 0.15%, nano titanium oxide 0.75%, Radix Glycyrrhizae
Sour dipotassium 0.8%, preservative 0.3% and water 60%.
3. antidandruff and antipruritic shampoo according to claim 1 and 2, it is characterised in that described preservative be.
4. the preparation method of the antidandruff and antipruritic shampoo according to any one of claim 1-3, it is characterised in that step is,
S1：Acetic acid is added in ethanol, after fully dissolving, obtains pH adjusting agent A；
S2：Using true after water, dipropylene glycol, zinc pyrrolidone carboxylate, glycyrrhizic acid dipotassium and nano titanium oxide are sufficiently mixed
Empty pumping enters in emulsifying pot, is heated to 80-90 DEG C, and constant temperature stirs 10-15min, and mixing speed is 250-400r/min, to obtain water phase
B；
S3：The aqueous phase B that step S2 is obtained is cooled to after 60-70 DEG C, sucks laureth sulphuric acid using vacuum pump
Ammonium, cetearyl glucoside, cocamidopropyl propyl amide amine oxide, lecithin, constant temperature stirs 20-30min, and mixing speed is
250-400r/min, obtains mastic C；
S4：The pH to 5.6-6.0 of the mastic C for being obtained using pH adjusting agent A regulating step S3 obtained in step S1, is then cooled to
45-55 DEG C, preservative is sucked, constant temperature stirs 15-20min, mixing speed is 250-400r/min, homogeneous 10-15min, to be down to
Room temperature, discharging, obtain final product.
5. the preparation method of antidandruff and antipruritic shampoo according to claim 4, it is characterised in that adjust in step S4 pH to
5.8.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108524363A (en) * | 2018-06-05 | 2018-09-14 | 苏州睿烁环境科技有限公司 | A kind of shampoo and preparation method thereof improving hair quality |
| CN108743614A (en) * | 2018-06-29 | 2018-11-06 | 方安轩 | A kind of preparation method and application of nano-titanium dioxide suspension |
| CN110709059A (en) * | 2018-12-26 | 2020-01-17 | 拉芳家化股份有限公司 | Dandruff-removing and itching-relieving shampoo composition containing multi-element zinc |
| CN110960434A (en) * | 2019-12-23 | 2020-04-07 | 广州市科能化妆品科研有限公司 | Scalp care shampoo composition and preparation method thereof |
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