CN106380315B - 一种改性生物蜡包膜控释肥料及其制备方法 - Google Patents
一种改性生物蜡包膜控释肥料及其制备方法 Download PDFInfo
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- CN106380315B CN106380315B CN201610787847.8A CN201610787847A CN106380315B CN 106380315 B CN106380315 B CN 106380315B CN 201610787847 A CN201610787847 A CN 201610787847A CN 106380315 B CN106380315 B CN 106380315B
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- wax
- fertilizer
- biological wax
- modified biological
- coating agent
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- 239000003337 fertilizer Substances 0.000 title claims abstract description 136
- 238000013270 controlled release Methods 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000011248 coating agent Substances 0.000 claims abstract description 123
- 238000000576 coating method Methods 0.000 claims abstract description 57
- 238000002844 melting Methods 0.000 claims abstract description 42
- 230000008018 melting Effects 0.000 claims abstract description 42
- 239000000463 material Substances 0.000 claims abstract description 22
- 238000001816 cooling Methods 0.000 claims abstract description 17
- 239000003607 modifier Substances 0.000 claims abstract description 13
- 239000002245 particle Substances 0.000 claims abstract description 7
- 238000012986 modification Methods 0.000 claims abstract description 4
- 230000004048 modification Effects 0.000 claims abstract description 4
- 239000001993 wax Substances 0.000 claims description 151
- 238000010438 heat treatment Methods 0.000 claims description 48
- 229920005989 resin Polymers 0.000 claims description 38
- 239000011347 resin Substances 0.000 claims description 38
- 239000003208 petroleum Substances 0.000 claims description 37
- 229920002367 Polyisobutene Polymers 0.000 claims description 32
- 238000003756 stirring Methods 0.000 claims description 27
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 claims description 16
- 150000001875 compounds Chemical class 0.000 claims description 16
- 239000004021 humic acid Substances 0.000 claims description 16
- 239000012188 paraffin wax Substances 0.000 claims description 15
- 244000068988 Glycine max Species 0.000 claims description 12
- 235000010469 Glycine max Nutrition 0.000 claims description 12
- 239000004203 carnauba wax Substances 0.000 claims description 12
- 239000004359 castor oil Substances 0.000 claims description 12
- 235000019438 castor oil Nutrition 0.000 claims description 12
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 12
- 239000005038 ethylene vinyl acetate Substances 0.000 claims description 7
- -1 jojoba wax Substances 0.000 claims description 7
- 229920001200 poly(ethylene-vinyl acetate) Polymers 0.000 claims description 7
- 235000019482 Palm oil Nutrition 0.000 claims description 6
- 239000003795 chemical substances by application Substances 0.000 claims description 6
- 239000008173 hydrogenated soybean oil Substances 0.000 claims description 6
- 239000002540 palm oil Substances 0.000 claims description 6
- 239000004698 Polyethylene Substances 0.000 claims description 5
- 229920000573 polyethylene Polymers 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- 239000010453 quartz Substances 0.000 claims description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 5
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 4
- DOIRQSBPFJWKBE-UHFFFAOYSA-N dibutyl phthalate Chemical compound CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims description 4
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims description 4
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 2
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 claims description 2
- 239000005696 Diammonium phosphate Substances 0.000 claims description 2
- 235000014466 Douglas bleu Nutrition 0.000 claims description 2
- 240000001416 Pseudotsuga menziesii Species 0.000 claims description 2
- 235000005386 Pseudotsuga menziesii var menziesii Nutrition 0.000 claims description 2
- 240000000528 Ricinus communis Species 0.000 claims description 2
- 235000004443 Ricinus communis Nutrition 0.000 claims description 2
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 2
- 240000000111 Saccharum officinarum Species 0.000 claims description 2
- 235000007201 Saccharum officinarum Nutrition 0.000 claims description 2
- 239000004163 Spermaceti wax Substances 0.000 claims description 2
- 235000021355 Stearic acid Nutrition 0.000 claims description 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 2
- 235000013871 bee wax Nutrition 0.000 claims description 2
- 239000012166 beeswax Substances 0.000 claims description 2
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 claims description 2
- CJZGTCYPCWQAJB-UHFFFAOYSA-L calcium stearate Chemical compound [Ca+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O CJZGTCYPCWQAJB-UHFFFAOYSA-L 0.000 claims description 2
- 239000008116 calcium stearate Substances 0.000 claims description 2
- 235000013539 calcium stearate Nutrition 0.000 claims description 2
- 239000004204 candelilla wax Substances 0.000 claims description 2
- 235000013868 candelilla wax Nutrition 0.000 claims description 2
- 229940073532 candelilla wax Drugs 0.000 claims description 2
- 239000004202 carbamide Substances 0.000 claims description 2
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims description 2
- 229910000388 diammonium phosphate Inorganic materials 0.000 claims description 2
- 235000019838 diammonium phosphate Nutrition 0.000 claims description 2
- IUJAMGNYPWYUPM-UHFFFAOYSA-N hentriacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC IUJAMGNYPWYUPM-UHFFFAOYSA-N 0.000 claims description 2
- 229920006007 hydrogenated polyisobutylene Polymers 0.000 claims description 2
- 229940119170 jojoba wax Drugs 0.000 claims description 2
- 239000004922 lacquer Substances 0.000 claims description 2
- 235000019359 magnesium stearate Nutrition 0.000 claims description 2
- 239000004200 microcrystalline wax Substances 0.000 claims description 2
- 235000019808 microcrystalline wax Nutrition 0.000 claims description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 2
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 2
- 239000012168 ouricury wax Substances 0.000 claims description 2
- 239000001103 potassium chloride Substances 0.000 claims description 2
- 235000011164 potassium chloride Nutrition 0.000 claims description 2
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 claims description 2
- 229910052939 potassium sulfate Inorganic materials 0.000 claims description 2
- 235000011151 potassium sulphates Nutrition 0.000 claims description 2
- 239000004170 rice bran wax Substances 0.000 claims description 2
- 235000019384 rice bran wax Nutrition 0.000 claims description 2
- 235000019385 spermaceti wax Nutrition 0.000 claims description 2
- 239000008117 stearic acid Substances 0.000 claims description 2
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 14
- 239000000126 substance Substances 0.000 description 11
- 230000004720 fertilization Effects 0.000 description 10
- 238000005516 engineering process Methods 0.000 description 9
- 235000015097 nutrients Nutrition 0.000 description 9
- 230000015556 catabolic process Effects 0.000 description 7
- 238000006731 degradation reaction Methods 0.000 description 7
- 229910052757 nitrogen Inorganic materials 0.000 description 7
- 238000001514 detection method Methods 0.000 description 6
- 230000000694 effects Effects 0.000 description 4
- 239000002689 soil Substances 0.000 description 3
- 230000002459 sustained effect Effects 0.000 description 3
- 238000013268 sustained release Methods 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- ZSWFCLXCOIISFI-UHFFFAOYSA-N cyclopentadiene Chemical compound C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 244000037666 field crops Species 0.000 description 2
- 230000007774 longterm Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000005445 natural material Substances 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 235000017060 Arachis glabrata Nutrition 0.000 description 1
- 244000105624 Arachis hypogaea Species 0.000 description 1
- 235000010777 Arachis hypogaea Nutrition 0.000 description 1
- 235000018262 Arachis monticola Nutrition 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- 244000017020 Ipomoea batatas Species 0.000 description 1
- 235000002678 Ipomoea batatas Nutrition 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 244000061456 Solanum tuberosum Species 0.000 description 1
- 235000002595 Solanum tuberosum Nutrition 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000007667 floating Methods 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000015816 nutrient absorption Nutrition 0.000 description 1
- 235000020232 peanut Nutrition 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F11/00—Other organic fertilisers
- C05F11/02—Other organic fertilisers from peat, brown coal, and similar vegetable deposits
Abstract
Description
Claims (2)
Priority Applications (2)
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CN201610787847.8A CN106380315B (zh) | 2016-08-31 | 2016-08-31 | 一种改性生物蜡包膜控释肥料及其制备方法 |
CN201911043881.4A CN110803962B (zh) | 2016-08-31 | 2016-08-31 | 一种用于制备控释肥料的改性生物蜡包膜材料 |
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CN201610787847.8A CN106380315B (zh) | 2016-08-31 | 2016-08-31 | 一种改性生物蜡包膜控释肥料及其制备方法 |
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CN201911043881.4A Division CN110803962B (zh) | 2016-08-31 | 2016-08-31 | 一种用于制备控释肥料的改性生物蜡包膜材料 |
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CN106380315B true CN106380315B (zh) | 2020-01-10 |
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CN201610787847.8A Active CN106380315B (zh) | 2016-08-31 | 2016-08-31 | 一种改性生物蜡包膜控释肥料及其制备方法 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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DE102020006130A1 (de) | 2020-10-07 | 2022-04-07 | WACHS-CHEMIE Elsteraue e. K. | Ersatz für Polymere - EU 2019/1009 |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110803962B (zh) * | 2016-08-31 | 2021-11-26 | 山东农大肥业科技有限公司 | 一种用于制备控释肥料的改性生物蜡包膜材料 |
CN110256167A (zh) * | 2019-08-07 | 2019-09-20 | 大连隆星新材料有限公司 | 一种由精制费托蜡与石蜡制备控释肥包膜专用蜡的方法 |
CN110372446A (zh) * | 2019-08-07 | 2019-10-25 | 大连隆星新材料有限公司 | 一种由精制费托蜡、微晶蜡与石蜡制备控释肥包膜专用蜡的方法 |
CN113023868B (zh) * | 2021-02-27 | 2023-09-01 | 安徽久吾天虹环保科技有限公司 | 一种生物蜡包埋微生物的生物活性填料及制备方法与应用 |
CN114456011A (zh) * | 2021-11-22 | 2022-05-10 | 中国科学院南京土壤研究所 | 表面生物蜡修饰的水基聚合物包膜控释肥料及其制备方法 |
CN115958054B (zh) * | 2022-12-26 | 2024-01-26 | 仲销农业科技发展(江苏)有限公司 | 一种微生物菌剂修复土壤及制备方法 |
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CN1145059A (zh) * | 1994-12-12 | 1997-03-12 | 宋美莹 | 可控制释放的基质型肥料及其制备方法 |
CN1948227A (zh) * | 2005-10-11 | 2007-04-18 | 上海汉枫缓释肥料有限公司 | 一种改进的涂硫尿素缓释肥料及制造方法 |
WO2009143656A1 (zh) * | 2008-05-30 | 2009-12-03 | 山东金正大生态工程股份有限公司 | 水溶性醇酸树脂-蜡复合包膜控释肥料及其制备方法 |
CN103708963A (zh) * | 2013-12-26 | 2014-04-09 | 大连汉枫集团有限公司 | 硫包控释钾肥及其制造方法 |
CN104003784A (zh) * | 2013-02-25 | 2014-08-27 | 大连宁化微晶化工有限公司 | 一种高效缓释复合肥料的缓释包膜蜡 |
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JPS4816299B1 (zh) * | 1969-09-04 | 1973-05-21 | ||
JPH062632B2 (ja) * | 1985-01-14 | 1994-01-12 | 三井東圧化学株式会社 | 粒子状吸湿性肥料用物質の固結防止方法 |
US6475259B1 (en) * | 1999-10-29 | 2002-11-05 | Mississippi Chemical Corporation | Coating agent and coated particulate fertilizers |
CN1657512A (zh) * | 2005-02-05 | 2005-08-24 | 方连明 | 包膜控释肥料及其组合以及制备方法 |
CN100558682C (zh) * | 2007-05-14 | 2009-11-11 | 中国农业大学 | 一种聚合物包膜控释肥料及其生产方法与专用包膜材料 |
CN101289350B (zh) * | 2008-05-30 | 2012-10-24 | 山东金正大生态工程股份有限公司 | 水溶性醇酸树脂-蜡复合包膜控释肥料及其制备方法 |
CN102001890B (zh) * | 2010-12-10 | 2013-01-09 | 合肥工业大学 | 一种松香-凹凸棒石-石蜡复合包膜缓释氮肥及其制备方法 |
CN103819292B (zh) * | 2014-02-25 | 2015-09-30 | 北京市农林科学院 | 一种无溶剂包膜控释肥料及其制备方法 |
US20150376077A1 (en) * | 2014-06-27 | 2015-12-31 | Koch Biological Solutions, Llc | Polymer coated fertilizer compositions and methods of making thereof |
CN110803962B (zh) * | 2016-08-31 | 2021-11-26 | 山东农大肥业科技有限公司 | 一种用于制备控释肥料的改性生物蜡包膜材料 |
-
2016
- 2016-08-31 CN CN201911043881.4A patent/CN110803962B/zh active Active
- 2016-08-31 CN CN201610787847.8A patent/CN106380315B/zh active Active
Patent Citations (5)
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CN1145059A (zh) * | 1994-12-12 | 1997-03-12 | 宋美莹 | 可控制释放的基质型肥料及其制备方法 |
CN1948227A (zh) * | 2005-10-11 | 2007-04-18 | 上海汉枫缓释肥料有限公司 | 一种改进的涂硫尿素缓释肥料及制造方法 |
WO2009143656A1 (zh) * | 2008-05-30 | 2009-12-03 | 山东金正大生态工程股份有限公司 | 水溶性醇酸树脂-蜡复合包膜控释肥料及其制备方法 |
CN104003784A (zh) * | 2013-02-25 | 2014-08-27 | 大连宁化微晶化工有限公司 | 一种高效缓释复合肥料的缓释包膜蜡 |
CN103708963A (zh) * | 2013-12-26 | 2014-04-09 | 大连汉枫集团有限公司 | 硫包控释钾肥及其制造方法 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102020006130A1 (de) | 2020-10-07 | 2022-04-07 | WACHS-CHEMIE Elsteraue e. K. | Ersatz für Polymere - EU 2019/1009 |
Also Published As
Publication number | Publication date |
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CN110803962B (zh) | 2021-11-26 |
CN106380315A (zh) | 2017-02-08 |
CN110803962A (zh) | 2020-02-18 |
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