CN106380074A - Cymbidium sinensis-color crystal ball blank and preparation method thereof - Google Patents
Cymbidium sinensis-color crystal ball blank and preparation method thereof Download PDFInfo
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- CN106380074A CN106380074A CN201610745218.9A CN201610745218A CN106380074A CN 106380074 A CN106380074 A CN 106380074A CN 201610745218 A CN201610745218 A CN 201610745218A CN 106380074 A CN106380074 A CN 106380074A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/10—Forming beads
- C03B19/1005—Forming solid beads
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
- C03C1/04—Opacifiers, e.g. fluorides or phosphates; Pigments
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C12/00—Powdered glass; Bead compositions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
- C03C4/0028—Compositions for glass with special properties for crystal glass, e.g. lead-free crystal glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
- C03C4/02—Compositions for glass with special properties for coloured glass
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses cymbidium sinensis-color crystal ball blank and a preparation method thereof. The cymbidium sinensis-color crystal ball blank is composed of the following ingredients (by weight): 150-300 parts of quartz sand, 150-300 parts of fire polishing powder, 130-280 parts of soda ash, 100-280 parts of glass, 20-70 parts of sodium nitrate, 15-55 parts of borax decahydrate, 16-60 parts of calcium carbonate, 4-12 parts of salt, 7-25 parts of potassium nitrate, 0.05-3.2 parts of cobalt oxide, 0.06-1.7 parts of nickel protoxide and 0.09-3.3 parts of copper oxide. During preparation of the cymbidium sinensis-color crystal ball blank, nickel protoxide and copper oxide are used as a colorant so as to obtain good dyeing property. Without lead-containing raw materials, the product has advantages of good glossiness, bright color, tidiness, no color difference, no spot, high yield, no lead or dust pollution, good productivity benefits and batch production. By using many recyclable wastes as raw materials, production cost is greatly reduced and energy consumption and environmental pollution are also minimized.
Description
Technical field
The present invention relates to a kind of Chinese cymbidium color crystal bead blank and preparation method thereof.
Background technology
Chinese cymbidium color crystal bead blank is used to prepare the semi-finished product of Chinese cymbidium color crystal product, existing Chinese cymbidium color crystal
Pearl embryo technique adopts crucible manufacture, there is aberration, spottiness, unstable product quality, low production efficiency, is not suitable for continuously big
Batch production, in addition leaded harmful, and burnt with coal and cause environmental pollution.
Content of the invention
The technical problem to be solved is to provide a kind of color reproduction good, solid colour no color differnece, immaculate,
Unleaded, no dust pollution, product quality is stable, and production efficiency is high, can be suitable for the Chinese cymbidium color water of the production operation of continuous tank furnace
Brilliant pearl embryo.
For solving the above problems, the present invention is achieved through the following technical solutions：A kind of Chinese cymbidium color crystal bead blank,
This Chinese cymbidium color crystal bead blank is made up of following weight composition:Quartz sand 150-300 part, fiery polishing powder 150-300 part,
Soda 130-280 part, glass 100-280 part, sodium nitrate 20-70 part, borax decahydrate 15-55 part, Calcium Carbonate 16-60 part, Sal
4-12 part, potassium nitrate 7-25 part, cobalt oxide 0.05-3.2 part, nickel protoxide 0.06-1.7 part and copper oxide 0.09-3.3 part.
Another technical problem to be solved by this invention is to provide a kind of preparation method of Chinese cymbidium color crystal bead blank,
The present invention is achieved through the following technical solutions：The preparation process of described Chinese cymbidium color crystal bead blank is as follows：
1) quartz sand 150-300 part, fiery polishing powder 150-300 part, soda 130-280 part, glass are extracted by weight ratio
100-280 part, sodium nitrate 20-70 part, borax decahydrate 15-55 part, Calcium Carbonate 16-60 part, Sal 4-12 part, potassium nitrate 7-25
Part, cobalt oxide 0.05-3.2 part, nickel protoxide 0.06-1.7 part and copper oxide 0.09-3.3 part mix homogeneously；
2) the Chinese cymbidium color crystal bead blank raw material of mix homogeneously is carried out pelletize by comminutor；
3) granular Chinese cymbidium color crystal bead blank raw material will be made put in glass quartz tank furnace and found, put into by several times,
Put into per hour once, when founding, keep oxidizing atmosphere and liquid level of solution stable；
4) crystal solution is molded into Chinese cymbidium color crystal bead blank after the cooling of material road homogenizing；
5) molding pearl embryo is put into fire and throws stove polishing, integer, uniform coloring, during polishing, first allow blank be stained with composite,
Molding pearl embryo is allowed at the uniform velocity to enter stainless steel pipes again, pipe temperature controls at 870 DEG C -1000 DEG C, 150 revolutions per seconds of rotating speed, and pipeline is long
Spend for 7.5 meters, 7 minutes in pipeline；
6) pipeline out enters tank of giving a dinner of welcome, from tank of giving a dinner of welcome be exactly out through integer, beautiful, no color differnece, no decorative pattern ink
Blue color crystal bead blank.
Further, in the described preparation process 3 in Chinese cymbidium color crystal bead blank, when founding temperature control 1360 DEG C-
1410℃.
Further, in the described preparation process 4 in Chinese cymbidium color crystal bead blank, chilling temperature controls at 870 DEG C -1000
℃.
The beneficial effect of Chinese cymbidium color crystal bead blank of the present invention is：Using oxidation during described Chinese cymbidium color crystal bead blank preparation
Sub- nickel and copper oxide are coloring agent, thus obtaining good coloring；Do not adopt leaded raw material, it is good to have a glossiness, color
Bright-coloured, neat, no color differnece, immaculate, yield is high, unleaded no dust pollution, and productivity effect is good, the advantage that can be mass；Adopt
With much callable waste materials as raw material, greatly reduce production cost and decrease energy resource consumption and environmental pollution.
Specific embodiment
Following examples are used for the present invention is described, but are not limited to the scope of the present invention.
Embodiment 1
A kind of Chinese cymbidium color crystal bead blank of the present invention, this Chinese cymbidium color crystal bead blank is by following weight composition
Composition:300 parts of quartz sand, fiery 300 parts of polishing powder, 280 parts of soda, 280 parts of glass, 70 parts of sodium nitrate, 55 parts of borax decahydrate, carbonic acid
60 parts of calcium, 12 parts of Sal, 25 parts of potassium nitrate, 3.2 parts of cobalt oxide, 1.7 parts of nickel protoxide and 3.3 parts of copper oxide.
The preparation process of described Chinese cymbidium color crystal bead blank is as follows：
1) 300 parts of quartz sand, fiery 300 parts of polishing powder, 280 parts of soda, 280 parts of glass, sodium nitrate are extracted by weight ratio
70 parts, 55 parts of borax decahydrate, 60 parts of Calcium Carbonate, 12 parts of Sal, 25 parts of potassium nitrate, 3.2 parts of cobalt oxide, 1.7 parts of nickel protoxide and
3.3 parts of mix homogeneously of copper oxide；
2) the Chinese cymbidium color crystal bead blank raw material of mix homogeneously is carried out pelletize by comminutor；
3) granular Chinese cymbidium color crystal bead blank raw material will be made put in glass quartz tank furnace and found, put into by several times,
Put into per hour once, keep oxidizing atmosphere and liquid level of solution to stablize when founding, temperature control is at 1360 DEG C -1410 DEG C；
4) by crystal solution through material road homogenizing cooling after be molded into Chinese cymbidium color crystal bead blank, temperature control 870 DEG C-
1000℃；
5) molding pearl embryo is put into fire and throws stove polishing, integer, uniform coloring, during polishing, first allow blank be stained with composite,
Molding pearl embryo is allowed at the uniform velocity to enter stainless steel pipes again, pipe temperature controls at 870 DEG C -1000 DEG C, 150 revolutions per seconds of rotating speed, and pipeline is long
Spend for 7.5 meters, 7 minutes in pipeline；
6) pipeline out enters tank of giving a dinner of welcome, from tank of giving a dinner of welcome be exactly out through integer, beautiful, no color differnece, no decorative pattern ink
Blue color crystal bead blank.
Embodiment 2
Its difference from Example 1 is, this Chinese cymbidium color crystal bead blank is made up of following weight composition:
150 parts of quartz sand, fiery 150 parts of polishing powder, 130 parts of soda, 100 parts of glass, 20 parts of sodium nitrate, 15 parts of borax decahydrate, Calcium Carbonate 16
Part, 4 parts of Sal, 7 parts of potassium nitrate, 0.05 part of cobalt oxide, 0.06 part of nickel protoxide and 0.09 part of copper oxide.
Embodiment 3
Its difference from Example 1 is, this Chinese cymbidium color crystal bead blank is made up of following weight composition:
230 parts of quartz sand, fiery 200 parts of polishing powder, 190 parts of soda, 185 parts of glass, 50 parts of sodium nitrate, 30 parts of borax decahydrate, Calcium Carbonate 35
Part, 8 parts of Sal, 17 parts of potassium nitrate, 1.6 parts of cobalt oxide, 0.8 part of nickel protoxide and 2.1 parts of copper oxide.
Embodiment 4
Its difference from Example 1 is, this Chinese cymbidium color crystal bead blank is made up of following weight composition:
165 parts of quartz sand, fiery 158 parts of polishing powder, 145 parts of soda, 111 parts of glass, 27 parts of sodium nitrate, 18 parts of borax decahydrate, Calcium Carbonate 19
Part, 5 parts of Sal, 9 parts of potassium nitrate, 0.15 part of cobalt oxide, 0.23 part of nickel protoxide and 0.26 part of copper oxide.
Embodiment 5
Its difference from Example 1 is, this Chinese cymbidium color crystal bead blank is made up of following weight composition:
285 parts of quartz sand, fiery 267 parts of polishing powder, 255 parts of soda, 241 parts of glass, 66 parts of sodium nitrate, 51 parts of borax decahydrate, Calcium Carbonate 49
Part, 11 parts of Sal, 22 parts of potassium nitrate, 2.9 parts of cobalt oxide, 1.5 parts of nickel protoxide and 3 parts of copper oxide.
Embodiment 6
Its difference from Example 1 is, this Chinese cymbidium color crystal bead blank is made up of following weight composition:
150 parts of quartz sand, fiery 155 parts of polishing powder, 150 parts of soda, 120 parts of glass, 35 parts of sodium nitrate, 17 parts of borax decahydrate, Calcium Carbonate 46
Part, 7 parts of Sal, 12 parts of potassium nitrate, 0.21 part of cobalt oxide, 0.1 part of nickel protoxide and 1.4 parts of copper oxide.
Embodiment 7
Its difference from Example 1 is, this Chinese cymbidium color crystal bead blank is made up of following weight composition:
197 parts of quartz sand, fiery 269 parts of polishing powder, 222 parts of soda, 155 parts of glass, 27 parts of sodium nitrate, 38 parts of borax decahydrate, Calcium Carbonate 39
Part, 7.4 parts of Sal, 14 parts of potassium nitrate, 1.3 parts of cobalt oxide, 1.1 parts of nickel protoxide and 1.68 parts of copper oxide.
Embodiment 8
Its difference from Example 1 is, this Chinese cymbidium color crystal bead blank is made up of following weight composition:
250 parts of quartz sand, fiery 200 parts of polishing powder, 150 parts of soda, 250 parts of glass, 50 parts of sodium nitrate, 45 parts of borax decahydrate, Calcium Carbonate 50
Part, 10 parts of Sal, 15 parts of potassium nitrate, 2 parts of cobalt oxide, 1 part of nickel protoxide and 1.5 parts of copper oxide.
The present invention is not limited to above-mentioned preferred forms, anyone draw under the enlightenment of the present invention other any with
Product as the present invention is same or like, is within the scope of the present invention.
Claims (4)
1. a kind of Chinese cymbidium color crystal bead blank it is characterised in that：This Chinese cymbidium color crystal bead blank is to be become by following weight
Part composition:Quartz sand 150-300 part, fiery polishing powder 150-300 part, soda 130-280 part, glass 100-280 part, sodium nitrate 20-
70 parts, borax decahydrate 15-55 part, Calcium Carbonate 16-60 part, Sal 4-12 part, potassium nitrate 7-25 part, cobalt oxide 0.05-3.2 part,
Nickel protoxide 0.06-1.7 part and copper oxide 0.09-3.3 part.
2. a kind of preparation method of the Chinese cymbidium color crystal bead blank prepared described in claim 1 it is characterised in that：The method includes
Following steps：
1) quartz sand 150-300 part, fiery polishing powder 150-300 part, soda 130-280 part, glass 100- are extracted by weight ratio
280 parts, sodium nitrate 20-70 part, borax decahydrate 15-55 part, Calcium Carbonate 16-60 part, Sal 4-12 part, potassium nitrate 7-25 part, oxygen
Change cobalt 0.05-3.2 part, nickel protoxide 0.06-1.7 part and copper oxide 0.09-3.3 part mix homogeneously；
2) the Chinese cymbidium color crystal bead blank raw material of mix homogeneously is carried out pelletize by comminutor；
3) granular Chinese cymbidium color crystal bead blank raw material will be made put in glass quartz tank furnace and found, put into by several times, often little
When put into once, keep oxidizing atmosphere and liquid level of solution stable when founding；
4) crystal solution is molded into Chinese cymbidium color crystal bead blank after the cooling of material road homogenizing；
5) molding pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, first allow blank be stained with composite during polishing, then allow
Molding pearl embryo at the uniform velocity enters stainless steel pipes, and pipe temperature controls at 870 DEG C -1000 DEG C, 150 revolutions per seconds of rotating speed, and duct length is
7.5 meters, 7 minutes in pipeline；
6) pipeline out enters tank of giving a dinner of welcome, from tank of giving a dinner of welcome be exactly out through integer, beautiful, no color differnece, no decorative pattern Chinese cymbidium face
Color crystal bead blank.
3. Chinese cymbidium color crystal bead blank preparation method according to claim 2 it is characterised in that：Described in Chinese cymbidium color water
In the preparation process 3 of brilliant pearl embryo, when founding, temperature control is at 1360 DEG C -1410 DEG C.
4. Chinese cymbidium color crystal bead blank preparation method according to claim 2 it is characterised in that：Described in Chinese cymbidium color water
In the preparation process 4 of brilliant pearl embryo, chilling temperature controls at 870 DEG C -1000 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610745218.9A CN106380074A (en) | 2016-08-29 | 2016-08-29 | Cymbidium sinensis-color crystal ball blank and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610745218.9A CN106380074A (en) | 2016-08-29 | 2016-08-29 | Cymbidium sinensis-color crystal ball blank and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106380074A true CN106380074A (en) | 2017-02-08 |
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ID=57917514
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610745218.9A Pending CN106380074A (en) | 2016-08-29 | 2016-08-29 | Cymbidium sinensis-color crystal ball blank and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080041103A1 (en) * | 2006-08-21 | 2008-02-21 | 3M Innovative Properties Company | Method of making inorganic, metal oxide spheres using microstructured molds |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN105859136A (en) * | 2016-06-15 | 2016-08-17 | 浙江伟兴水晶有限公司 | Amber crystal bead blank and preparation method thereof |
-
2016
- 2016-08-29 CN CN201610745218.9A patent/CN106380074A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080041103A1 (en) * | 2006-08-21 | 2008-02-21 | 3M Innovative Properties Company | Method of making inorganic, metal oxide spheres using microstructured molds |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN105859136A (en) * | 2016-06-15 | 2016-08-17 | 浙江伟兴水晶有限公司 | Amber crystal bead blank and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 西北轻工业学院: "《玻璃工艺学》", 31 January 2000, 中国轻工业出版社 * |
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Application publication date: 20170208 |
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