CN103936282B - A kind of shallow large red color crystal bead blank and preparation method thereof - Google Patents

A kind of shallow large red color crystal bead blank and preparation method thereof Download PDF

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Publication number
CN103936282B
CN103936282B CN201410104051.9A CN201410104051A CN103936282B CN 103936282 B CN103936282 B CN 103936282B CN 201410104051 A CN201410104051 A CN 201410104051A CN 103936282 B CN103936282 B CN 103936282B
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parts
red color
bead blank
large red
color crystal
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CN103936282A (en
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杨鑫法
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Zhejiang Xinweixing Crystal Co ltd
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浙江伟兴水晶有限公司
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Abstract

The invention discloses a kind of shallow large red color crystal bead blank and preparation method thereof, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 120-230 part, zinc oxide 15-40 part, soda ash 30-90 part, salt of wormwood 15-45 part, boric acid 10-30 part, calcium carbonate 2-12 part, aluminium hydroxide 0.5-4 part, salt 1-5 part, cadmium yellow 3-3.5 part, selenium powder 0.5-3 part and cadmium red 0.5-8 part.The redox equilibrium that the present invention's shallow large red color crystal bead blank makes cupric ion in melting process when preparing keeps stable, thus obtains good tint permanence; Do not adopt leaded raw material, have glossiness good, bright-colored, neat, no color differnece, without decorative pattern, output is high, unleaded pollution-free, the advantage that productivity effect is good.

Description

A kind of shallow large red color crystal bead blank and preparation method thereof
Technical field
The present invention relates to a kind of shallow large red color crystal bead blank and preparation method thereof.
Background technology
Shallow large red color crystal bead blank is used to the work in-process preparing shallow large red color crystal product, existing shallow large red color crystal bead blank technique adopts crucible manufacture, there is aberration, color is uneven, have decorative pattern, unstable product quality, production efficiency is low, be not suitable for continuous production in enormous quantities, and cause environmental pollution by coal burning.
Summary of the invention
It is good that technical problem to be solved by this invention is to provide a kind of color reproduction, and solid colour no color differnece, without decorative pattern, constant product quality, production efficiency is high, can be applicable to the shallow large red color crystal bead blank of the production operation of continuous tank furnace.
For solving the problem, the present invention is achieved through the following technical solutions: a kind of shallow large red color crystal bead blank, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 120-230 part, zinc oxide 15-40 part, soda ash 30-90 part, salt of wormwood 15-45 part, boric acid 10-30 part, calcium carbonate 2-12 part, aluminium hydroxide 0.5-4 part, salt 1-5 part, cadmium yellow 3-3.5 part, selenium powder 0.5-3 part and cadmium red 0.5-8 part.
Another technical problem to be solved by this invention is to provide a kind of preparation method of shallow large red color crystal bead blank,
The present invention is achieved through the following technical solutions: the preparation process of described shallow large red color crystal bead blank is as follows:
1) extract quartz sand quartz sand 120-230 part, zinc oxide 15-40 part, soda ash 30-90 part, salt of wormwood 15-45 part, boric acid 10-30 part, calcium carbonate 2-12 part, aluminium hydroxide 0.5-4 part, salt 1-5 part, cadmium yellow 3-3.5 part, selenium powder 0.5-3 part and cadmium red 0.5-8 part by weight ratio to mix;
2) the shallow large red color crystal bead blank raw material mixed is carried out granulation by tablets press;
3) granular shallow large red color crystal bead blank raw material will be made put into glass quartz tank furnace and found, and when founding, keep neutral atmosphere and liquid level of solution to stablize;
4) crystal solution is molded into shallow large red color crystal bead blank after the homogenizing cooling of material road;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 850 DEG C, rotating speed 200 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, shallow large red color crystal bead blank without decorative pattern.
Further, described in the preparation process 3 of shallow large red color crystal bead blank, when founding, temperature controls at 1310 DEG C-1350 DEG C.
Further, described in the preparation process 4 of shallow large red color crystal bead blank, cooling temperature controls at 800 DEG C-1000 DEG C.
The beneficial effect of the shallow large red color crystal bead blank of the present invention is: the redox equilibrium making cupric ion in melting process time prepared by described shallow large red color crystal bead blank keeps stable, thus obtains good tint permanence; Do not adopt leaded raw material, have glossiness good, bright-colored, neat, no color differnece, without decorative pattern, output is high, unleaded pollution-free, the advantage that productivity effect is good.
Embodiment
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1
The shallow large red color crystal bead blank of one of the present invention, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 120 parts, 15 parts, zinc oxide, soda ash 30 parts, 15 parts, salt of wormwood, boric acid 10 parts, 2 parts, calcium carbonate, 0.5 part, aluminium hydroxide, salt 1 part, cadmium yellow 3 parts, selenium powder 0.5 part and cadmium red 0.5 part.
The preparation process of described shallow large red color crystal bead blank is as follows:
1) extract quartz sand 120 parts, 15 parts, zinc oxide, soda ash 30 parts, 15 parts, salt of wormwood, boric acid 10 parts, 2 parts, calcium carbonate, 0.5 part, aluminium hydroxide, salt 1 part, cadmium yellow 3 parts, selenium powder 0.5 part and cadmium red 0.5 part by weight ratio to mix;
2) the shallow large red color crystal bead blank raw material mixed is carried out granulation by tablets press;
3) will make granular shallow large red color crystal bead blank raw material to put into glass quartz tank furnace and found, keep neutral atmosphere and liquid level of solution to stablize when founding, temperature controls at 1310 DEG C-1350 DEG C;
4) crystal solution is molded into shallow large red color crystal bead blank after the homogenizing cooling of material road, temperature controls at 800 DEG C-1000 DEG C;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 850 DEG C, rotating speed 200 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, shallow large red color crystal bead blank without decorative pattern.
Embodiment 2
Its difference from Example 1 is, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 230 parts, 40 parts, zinc oxide, soda ash 90 parts, 45 parts, salt of wormwood, boric acid 30 parts, 12 parts, calcium carbonate, 4 parts, aluminium hydroxide, salt 5 parts, cadmium yellow 3.5 parts, selenium powder 3 parts and cadmium red 8 parts.
Embodiment 3
Its difference from Example 1 is, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 200 parts, 25 parts, zinc oxide, soda ash 55 parts, 40 parts, salt of wormwood, boric acid 28 parts, 10 parts, calcium carbonate, 3 parts, aluminium hydroxide, salt 2 parts, cadmium yellow 2 parts, selenium powder 1 part and cadmium red 4 parts.
Embodiment 4
Its difference from Example 1 is, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 165 parts, 23 parts, zinc oxide, soda ash 42 parts, 25 parts, salt of wormwood, boric acid 24 parts, 8 parts, calcium carbonate, 3.7 parts, aluminium hydroxide, salt 2.8 parts, cadmium yellow 3.3 parts, selenium powder 2.3 parts and cadmium red 6.5 parts.
Embodiment 5
Its difference from Example 1 is, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 215 parts, 36 parts, zinc oxide, soda ash 49 parts, carbonic acid K43 part, boric acid 28 parts, 10.5 parts, calcium carbonate, 3.5 parts, aluminium hydroxide, salt 1.5 parts, cadmium yellow 3.4 parts, selenium powder 1.9 parts and cadmium red 5.3 parts.
Embodiment 6
Its difference from Example 1 is, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 170 parts, 28 parts, zinc oxide, soda ash 83 parts, 23 parts, salt of wormwood, boric acid 16 parts, 3 parts, calcium carbonate, 4.5 parts, aluminium hydroxide, salt 4.1 parts, cadmium yellow 3.2 parts, selenium powder 2.5 parts and cadmium red 7.1 parts.
Embodiment 7
Its difference from Example 1 is, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 133 parts, 17 parts, zinc oxide, soda ash 52 parts, 36 parts, salt of wormwood, boric acid 23 parts, 4.8 parts, calcium carbonate, 3.5 parts, aluminium hydroxide, salt 2.5 parts, cadmium yellow 3.4 parts, selenium powder 2.9 parts and cadmium red 2.5 parts.
Embodiment 8
Its difference from Example 1 is, this shallow large red color crystal bead blank is made up of following weight composition: quartz sand 195 parts, 35 parts, zinc oxide, soda ash 66 parts, 33 parts, salt of wormwood, boric acid 22 parts, 11 parts, calcium carbonate, 0.8 part, aluminium hydroxide, salt 1.3 parts, cadmium yellow 3 parts, selenium powder 2.4 parts and cadmium red 4.9 parts.
The present invention is not limited to above-mentioned preferred forms, anyone other any or akin products identical with the present invention drawn under enlightenment of the present invention, all drops within protection scope of the present invention.

Claims (1)

1. a shallow large red color crystal bead blank, is characterized in that: be made up of following weight composition: quartz sand 120 parts, 15 parts, zinc oxide, soda ash 30 parts, 15 parts, salt of wormwood, boric acid 10 parts, 2 parts, calcium carbonate, 0.5 part, aluminium hydroxide, salt 1 part, cadmium yellow 3 parts, selenium powder 0.5 part and cadmium red 0.5 part; The preparation process of described shallow large red color crystal bead blank is as follows: 1) extract quartz sand 120 parts, 15 parts, zinc oxide, soda ash 30 parts, 15 parts, salt of wormwood, boric acid 10 parts, 2 parts, calcium carbonate, 0.5 part, aluminium hydroxide, salt 1 part, cadmium yellow 3 parts, selenium powder 0.5 part and cadmium red 0.5 part by weight ratio and mix; 2) the shallow large red color crystal bead blank raw material mixed is carried out granulation by tablets press; 3) will make granular shallow large red color crystal bead blank raw material to put into glass quartz tank furnace and found, keep neutral atmosphere and liquid level of solution to stablize when founding, temperature controls at 1310 DEG C-1350 DEG C; 4) crystal solution is molded into shallow large red color crystal bead blank after the homogenizing cooling of material road, temperature controls at 800 DEG C-1000 DEG C; 5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 850 DEG C, rotating speed 200 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, shallow large red color crystal bead blank without decorative pattern.
CN201410104051.9A 2014-03-20 2014-03-20 A kind of shallow large red color crystal bead blank and preparation method thereof Active CN103936282B (en)

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WO2016185450A1 (en) 2015-05-21 2016-11-24 Laurus Labs Private Limited An improved processes for the preparation of carfilzomib or pharmaceutically acceptable salts thereof
CN105924004B (en) * 2016-04-29 2019-02-12 浦江县乾坤工贸有限公司 A kind of production method of porcelain red quartz stick

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US5656559A (en) * 1994-06-23 1997-08-12 Saint-Gobain Vitrage Clear glass composition intended for the production of panes
CN101186425A (en) * 2007-12-17 2008-05-28 山西晋城九州玻璃制品有限公司 Method for fabricating flashed glass ware
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CN102837251A (en) * 2012-09-17 2012-12-26 江苏锦程集团科技有限公司 Diamond bead blank fire polishing furnace

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CN101186425A (en) * 2007-12-17 2008-05-28 山西晋城九州玻璃制品有限公司 Method for fabricating flashed glass ware
CN101648773A (en) * 2009-09-04 2010-02-17 常熟市万利特种玻璃厂 Processing technology of Chinese red glass metal
CN102211869A (en) * 2011-04-12 2011-10-12 姚晓春 Primary pressure-sizing molding crystalloid glass and preparation method thereof
CN102503126A (en) * 2011-10-08 2012-06-20 浙江伟兴水晶有限公司 Preparation method for smoky yellow crystal bead blanks
CN102838277A (en) * 2012-09-17 2012-12-26 江苏锦程集团科技有限公司 Production process of honey peach CZ diamond
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Patentee before: ZHEJIANG WEIXING CRYSTAL Co.,Ltd.