CN106082643B - A kind of crystal bead blank of black color and preparation method thereof - Google Patents
A kind of crystal bead blank of black color and preparation method thereof Download PDFInfo
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- CN106082643B CN106082643B CN201610424195.1A CN201610424195A CN106082643B CN 106082643 B CN106082643 B CN 106082643B CN 201610424195 A CN201610424195 A CN 201610424195A CN 106082643 B CN106082643 B CN 106082643B
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
- C03C4/0028—Compositions for glass with special properties for crystal glass, e.g. lead-free crystal glass
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B11/00—Pressing molten glass or performed glass reheated to equivalent low viscosity without blowing
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Crystallography & Structural Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Glass Compositions (AREA)
Abstract
The present invention discloses a kind of crystal bead blank of black color, includes the raw material of following parts by weight：5 17 parts of fiery 100 200 parts of polishing powder, 70 180 parts of quartz sand, 80 180 parts of cullet, 50 170 parts of soda ash, 10 25 parts of sodium nitrate, 15 parts of sodium chloride, 5 15 parts of calcium carbonate, 2 10 parts of piece alkali, 5 20 parts of borax decahydrate, 10 24 parts of manganese dioxide and weight potassium caseinate；The crystal bead blank coloring of the black color is good, stable quality, productivity effect are high, is adapted to produce in enormous quantities, and will not cause environmental pollution.
Description
Technical field
Present invention relates particularly to a kind of crystal bead blank of black color and preparation method thereof.
Background technology
Black color crystal bead blank is the semi-finished product for manufacturing black crystal product, existing black color crystal bead blank
In technique, crucible manufacture is used, there are this coloring is poor, irregular colour is even, there is decorative pattern, unstable product quality, productivity effect
It is low, be not suitable for continuous mass production, in addition, containing aluminium, environmental pollution is easily caused with coal.
The content of the invention
It is an object of the invention in view of the shortcomings of the prior art, providing a kind of good coloring, stable quality, productivity effect
It is high, suitable to produce in enormous quantities, and crystal bead blank of black color of environmental pollution and preparation method thereof will not be caused.
It is as follows in order to solve the problem above-mentioned the technology of the use of the present invention and method：
A kind of crystal bead blank of black color, includes the raw material of following parts by weight：Fiery polishing powder 100-200 parts, quartz sand 70-
180 parts, 80-180 parts of cullet, 50-170 parts of soda ash, 10-25 parts of sodium nitrate, 1-5 parts of sodium chloride, 5-15 parts of calcium carbonate, piece alkali
2-10 parts, 5-20 parts of borax decahydrate, 10-24 parts of manganese dioxide and 5-17 parts of potassium caseinate of weight.
Another technical problem to be solved by the invention is a kind of preparation method of the crystal bead blank of black color of offer, including
Following steps：
1) 100-200 parts of polishing powder of getting fire, 70-180 parts of quartz sand, 80-180 parts of cullet, 50-170 parts of soda ash, sodium nitrate
10-25 parts, 1-5 parts of sodium chloride, 5-15 parts of calcium carbonate, 2-10 parts of piece alkali, 5-20 parts of borax decahydrate, 10-24 parts of manganese dioxide and
5-17 parts of potassium caseinate of weight, is uniformly mixed；
2) it is put into comminutor and is granulated, granular size 0.5-2.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1350-1400 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross compression molding after material path cooling, temperature control exists
800-1000℃；
5) stove polishing shaping is thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 840-860 DEG C, is turned
200 revolutions per seconds of speed, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of black color.
Beneficial effects of the present invention are：Stablize with performance, glossiness is good, and color is neat, unleaded pollution-free, productivity effect
It is good, it can be mass, using the optical requirement of Na-B-Si system highs index of refraction.
Embodiment
With reference to embodiment, the present invention is described in further detail, but they are not to technical solution of the present invention
Restriction, based on present invention teach that any conversion made, all falls within protection scope of the present invention.
Embodiment 1
A kind of preparation method of the crystal bead blank of black color, comprises the following steps：
1) 110 parts of polishing powder of getting fire, 75 parts of quartz sand, 85 parts of cullet, 70 parts of soda ash, 12 parts of sodium nitrate, sodium chloride 1.5
Part, 6 parts of calcium carbonate, 2 parts of piece alkali, 6 parts of borax decahydrate, 11 parts of manganese dioxide and 5.4 parts of weight potassium caseinate, are uniformly mixed；
2) it is put into comminutor and is granulated, granular size 0.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1350 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross compression molding after material path cooling, temperature control exists
800℃；
5) stove polishing shaping is thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 840 DEG C, rotating speed 200
Revolutions per second, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of black color.
Embodiment 2
A kind of preparation method of the crystal bead blank of black color, comprises the following steps：
1) 200 parts of polishing powder of getting fire, 180 parts of quartz sand, 180 parts of cullet, 170 parts of soda ash, 25 parts of sodium nitrate, sodium chloride 5
Part, 15 parts of calcium carbonate, 10 parts of piece alkali, 20 parts of borax decahydrate, 24 parts of manganese dioxide and 17 parts of weight potassium caseinate, are uniformly mixed；
2) it is put into comminutor and is granulated, granular size 2.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1400 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross compression molding after material path cooling, temperature control exists
1000℃；
5) stove polishing shaping is thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 860 DEG C, rotating speed 200
Revolutions per second, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of black color.
Embodiment 3
A kind of preparation method of the crystal bead blank of black color, comprises the following steps：
1) 150 parts of polishing powder of getting fire, 120 parts of quartz sand, 130 parts of cullet, 110 parts of soda ash, 20 parts of sodium nitrate, sodium chloride 3
Part, 10 parts of calcium carbonate, 6 parts of piece alkali, 15 parts of borax decahydrate, 17 parts of manganese dioxide and 11 parts of weight potassium caseinate, are uniformly mixed；
2) it is put into comminutor and is granulated, granular size 1.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1375 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross compression molding after material path cooling, temperature control exists
900℃；
5) stove polishing shaping is thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 850 DEG C, rotating speed 200
Revolutions per second, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of black color.
Beneficial effects of the present invention are：Stablize with performance, glossiness is good, and color is neat, unleaded pollution-free, productivity effect
It is good, it can be mass, using the optical requirement of Na-B-Si system highs index of refraction.
The above description is merely a specific embodiment, but protection scope of the present invention is not limited thereto, any
The change or replacement expected without creative work, should be covered by the protection scope of the present invention, therefore, of the invention
Protection domain should be determined by the scope of protection defined in the claims.
Claims (1)
- A kind of 1. crystal bead blank of black color, it is characterised in that：Include the raw material of following parts by weight：Fiery 200 parts of polishing powder, quartz 180 parts of sand, 180 parts of cullet, 170 parts of soda ash, 25 parts of sodium nitrate, 5 parts of sodium chloride, 15 parts of calcium carbonate, 10 parts of piece alkali, ten water boron 17 parts of 20 parts of sand, 24 parts of manganese dioxide and weight potassium caseinate, the preparation method of the black color crystal bead blank, including following step Suddenly：1) 200 parts of polishing powder of getting fire, 180 parts of quartz sand, 180 parts of cullet, 170 parts of soda ash, 25 parts of sodium nitrate, 5 parts of sodium chloride, carbon 17 parts of sour 15 parts of calcium, 10 parts of piece alkali, 20 parts of borax decahydrate, 24 parts of manganese dioxide and weight potassium caseinate, are uniformly mixed；2) it is put into comminutor and is granulated, granular size 2.5cm；3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1400 DEG C；4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross material path cooling after compression molding, temperature control is 1000 ℃；5) stove polishing shaping to be thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 860 DEG C, 200 turns of rotating speed/ Second, pipeline duration 5 minutes；6) pipeline enters extinction tank after coming out, out the as crystal bead blank of black color.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610424195.1A CN106082643B (en) | 2016-06-15 | 2016-06-15 | A kind of crystal bead blank of black color and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610424195.1A CN106082643B (en) | 2016-06-15 | 2016-06-15 | A kind of crystal bead blank of black color and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106082643A CN106082643A (en) | 2016-11-09 |
| CN106082643B true CN106082643B (en) | 2018-05-08 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610424195.1A Active CN106082643B (en) | 2016-06-15 | 2016-06-15 | A kind of crystal bead blank of black color and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102515473A (en) * | 2011-12-06 | 2012-06-27 | 浙江伟兴水晶有限公司 | Preparation method for transparent black crystal ball blank |
| CN102718387A (en) * | 2011-12-06 | 2012-10-10 | 浙江伟兴水晶有限公司 | Preparation method of large black crystal bead semi-finished product |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN104496179A (en) * | 2015-01-06 | 2015-04-08 | 浙江伟兴水晶有限公司 | Transparent black crystal bead embryo and preparation method thereof |
-
2016
- 2016-06-15 CN CN201610424195.1A patent/CN106082643B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102515473A (en) * | 2011-12-06 | 2012-06-27 | 浙江伟兴水晶有限公司 | Preparation method for transparent black crystal ball blank |
| CN102718387A (en) * | 2011-12-06 | 2012-10-10 | 浙江伟兴水晶有限公司 | Preparation method of large black crystal bead semi-finished product |
| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN104496179A (en) * | 2015-01-06 | 2015-04-08 | 浙江伟兴水晶有限公司 | Transparent black crystal bead embryo and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN106082643A (en) | 2016-11-09 |
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Effective date of registration: 20220214 Address after: 321000 No. 668, Xuecheng East Road, Hanxiang Industrial Park, Tangya Town, Jindong District, Jinhua City, Zhejiang Province Patentee after: Zhejiang xinweixing crystal Co.,Ltd. Address before: 321000 Jindong comprehensive development park, Jinhua City, Zhejiang Province Patentee before: ZHEJIANG WEIXING CRYSTAL Co.,Ltd. |
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