CN104478214B - A kind of pale pink look crystal bead blank and preparation method thereof - Google Patents
A kind of pale pink look crystal bead blank and preparation method thereof Download PDFInfo
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- CN104478214B CN104478214B CN201510003548.6A CN201510003548A CN104478214B CN 104478214 B CN104478214 B CN 104478214B CN 201510003548 A CN201510003548 A CN 201510003548A CN 104478214 B CN104478214 B CN 104478214B
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Abstract
The invention discloses a kind of pale pink look crystal bead blank and preparation method thereof, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 90-160 part, zinc oxide 9-17 part, soda ash 27-51 part, salt of wormwood 16-30 part, boric acid 6.5-17 part, calcium carbonate 3-5 part, aluminium hydroxide 0.8-3.2 part, salt 1-2 part, antimonous oxide 2-5 part, saltpetre 0.1-2 part, Sodium Selenite 0.02-0.2 part and Iron sulfuret 0.001-0.003 part.Pale pink look crystal bead blank of the present invention does not consume the compound of a large amount of rare earth erbiums when preparing, obtain stable painted, solve discoloration problem during thermal treatment in selenium colored glass with the selenium compound of minute quantity; Adopt unleaded raw material, have glossiness good, bright-colored, neat, no color differnece, without decorative pattern, output is high, unleaded pollution-free, the advantage that productivity effect is good.
Description
Technical field
The present invention relates to a kind of pale pink look crystal bead blank and preparation method thereof.
Background technology
Pale pink look crystal bead blank is used to the work in-process preparing pale pink look crystal product, existing pale pink look crystal bead blank technique adopts crucible manufacture, there is aberration, color is uneven, have decorative pattern, unstable product quality, production efficiency is low, be not suitable for continuous production in enormous quantities, and cause environmental pollution by coal burning.And the rare-earth oxidation erbium of the consumption costliness had in existing technical recipe, but some selenium powders are painted unstable, the lead compound containing contaminate environment had.
Summary of the invention
It is good that technical problem to be solved by this invention is to provide a kind of color reproduction, solid colour no color differnece, without decorative pattern, constant product quality, production efficiency is high, can be applicable to the production operation of continuous tank furnace, production cost is low, the pale pink look crystal bead blank of non-environmental-pollution.
For solving the problem, the present invention is achieved through the following technical solutions: a kind of pale pink look crystal bead blank, and this pale pink look crystal bead blank is made up of following weight composition: quartz sand 90-160 part, zinc oxide 9-17 part, soda ash 27-51 part, salt of wormwood 16-30 part, boric acid 6.5-17 part, calcium carbonate 3-5 part, aluminium hydroxide 0.8-3.2 part, salt 1-2 part, antimonous oxide 2-5 part, saltpetre 0.1-2 part, Sodium Selenite 0.02-0.2 part and Iron sulfuret 0.001-0.003 part.
Another technical problem to be solved by this invention is to provide a kind of preparation method of pale pink look crystal bead blank,
The present invention is achieved through the following technical solutions: the preparation process of described pale pink look crystal bead blank is as follows:
1) extract quartz sand 90-160 part, zinc oxide 9-17 part, soda ash 27-51 part, salt of wormwood 16-30 part, boric acid 6.5-17 part, calcium carbonate 3-5 part, aluminium hydroxide 0.8-3.2 part, salt 1-2 part, antimonous oxide 2-5 part, saltpetre 0.1-2 part, Sodium Selenite 0.02-0.2 part and Iron sulfuret 0.001-0.003 part by weight ratio to mix;
2) the pale pink look crystal bead blank raw material mixed is carried out granulation by tablets press;
3) granular pale pink look crystal bead blank raw material will be made put into glass quartz tank furnace and found, and when founding, keep weak oxide atmosphere and liquid level of solution to stablize;
4) crystal solution is molded into pale pink look crystal bead blank after the homogenizing cooling of material road;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, pale pink look crystal bead blank without decorative pattern.
Further, described in the preparation process 3 of pale pink look crystal bead blank, when founding, temperature controls at 1320 DEG C-1380 DEG C.
Further, described in the preparation process 4 of pale pink look crystal bead blank, cooling temperature controls at 800 DEG C-1000 DEG C.
The beneficial effect of pale pink look crystal bead blank of the present invention is: the compound not consuming a large amount of rare earth erbiums time prepared by described pale pink look crystal bead blank, obtain with the selenium compound of minute quantity stable painted, solve discoloration problem during thermal treatment in selenium colored glass; Adopt unleaded raw material, have glossiness good, bright-colored, neat, no color differnece, without decorative pattern, output is high, unleaded pollution-free, the advantage that productivity effect is good.
Embodiment
Following examples for illustration of the present invention, but are not used for limiting the scope of the invention.
Embodiment 1
A kind of pale pink look crystal bead blank of the present invention, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 150 parts, 11 parts, zinc oxide, soda ash 28 parts, 22 parts, salt of wormwood, boric acid 13 parts, 3.8 parts, calcium carbonate, 2.6 parts, aluminium hydroxide, salt 1.8 parts, antimonous oxide 3.5 parts, 0.7 part, saltpetre, Sodium Selenite 0.03 part and Iron sulfuret 0.002 part.
The preparation process of described pale pink look crystal bead blank is as follows:
1) extract quartz sand 150 parts, 11 parts, zinc oxide, soda ash 28 parts, 22 parts, salt of wormwood, boric acid 13 parts, 3.8 parts, calcium carbonate, 2.6 parts, aluminium hydroxide, salt 1.8 parts, antimonous oxide 3.5 parts, 0.7 part, saltpetre, Sodium Selenite 0.03 part and Iron sulfuret 0.002 part by weight ratio to mix;
2) the pale pink look crystal bead blank raw material mixed is carried out granulation by tablets press;
3) will make granular pale pink look crystal bead blank raw material to put into glass quartz tank furnace and found, keep weak oxide atmosphere and liquid level of solution to stablize when founding, glass melting temperature controls at 1320 DEG C-1380 DEG C;
4) crystal solution is molded into pale pink look crystal bead blank after the homogenizing cooling of material road, cooling temperature controls at 800 DEG C-1000 DEG C;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, pale pink look crystal bead blank without decorative pattern.
Embodiment 2
Its difference from Example 1 is, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 160 parts, 17 parts, zinc oxide, soda ash 51 parts, 30 parts, salt of wormwood, boric acid 17 parts, 5 parts, calcium carbonate, 3.2 parts, aluminium hydroxide, salt 2 parts, antimonous oxide 5 parts, 2 parts, saltpetre, Sodium Selenite 0.2 part and Iron sulfuret 0.003 part.
Embodiment 3
Its difference from Example 1 is, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 90 parts, 9 parts, zinc oxide, soda ash 27 parts, 16 parts, salt of wormwood, boric acid 6.5 parts, 3 parts, calcium carbonate, 0.8 part, aluminium hydroxide, salt 1 part, antimonous oxide 2 parts, 0.1 part, saltpetre, Sodium Selenite 0.02 part and Iron sulfuret 0.001 part.
Embodiment 4
Its difference from Example 1 is, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 100 parts, 10 parts, zinc oxide, soda ash 29 parts, 18 parts, salt of wormwood, boric acid 6.9 parts, 3.4 parts, calcium carbonate, 1 part, aluminium hydroxide, salt 1.2 parts, antimonous oxide 2.7 parts, 0.8 part, saltpetre, Sodium Selenite 0.09 part and Iron sulfuret 0.0017 part.
Embodiment 5
Its difference from Example 1 is, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 145 parts, 15 parts, zinc oxide, soda ash 46 parts, 27 parts, salt of wormwood, boric acid 14 parts, 4.2 parts, calcium carbonate, 3 parts, aluminium hydroxide, salt 1.8 parts, antimonous oxide 4.4 parts, 1.6 parts, saltpetre, Sodium Selenite 0.13 part and Iron sulfuret 0.0024 part.
Embodiment 6
Its difference from Example 1 is, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 130 parts, 13 parts, zinc oxide, soda ash 33 parts, 21 parts, salt of wormwood, boric acid 10 parts, 3.8 parts, calcium carbonate, 1.6 parts, aluminium hydroxide, salt 1.4 parts, antimonous oxide 3.9 parts, 1.1 parts, saltpetre, Sodium Selenite 0.13 part and Iron sulfuret 0.0021 part.
Embodiment 7
Its difference from Example 1 is, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 115 parts, 12 parts, zinc oxide, soda ash 29 parts, 26 parts, salt of wormwood, boric acid 7 parts, 3.7 parts, calcium carbonate, 2.2 parts, aluminium hydroxide, salt 1.2 parts, antimonous oxide 2.8 parts, 1.6 parts, saltpetre, Sodium Selenite 0.09 part and Iron sulfuret 0.0017 part.
Embodiment 8
Its difference from Example 1 is, this pale pink look crystal bead blank is made up of following weight composition: quartz sand 143 parts, 16 parts, zinc oxide, soda ash 39 parts, 19 parts, salt of wormwood, boric acid 8 parts, 4.1 parts, calcium carbonate, 2.9 parts, aluminium hydroxide, salt 1.3 parts, antimonous oxide 2.9 parts, 0.25 part, saltpetre, Sodium Selenite 0.12 part and Iron sulfuret 0.002 part.
The present invention is not limited to above-mentioned preferred forms, anyone other any or akin products identical with the present invention drawn under enlightenment of the present invention, all drops within protection scope of the present invention.
Claims (1)
1. a pale pink look crystal bead blank, it is characterized in that: this pale pink look crystal bead blank is made up of following weight composition: quartz sand 150 parts, 11 parts, zinc oxide, soda ash 28 parts, 22 parts, salt of wormwood, boric acid 13 parts, 3.8 parts, calcium carbonate, 2.6 parts, aluminium hydroxide, salt 1.8 parts, antimonous oxide 3.5 parts, 0.7 part, saltpetre, Sodium Selenite 0.03 part and Iron sulfuret 0.002 part, the preparation process of described pale pink look crystal bead blank is as follows:
1) extract quartz sand 150 parts, 11 parts, zinc oxide, soda ash 28 parts, 22 parts, salt of wormwood, boric acid 13 parts, 3.8 parts, calcium carbonate, 2.6 parts, aluminium hydroxide, salt 1.8 parts, antimonous oxide 3.5 parts, 0.7 part, saltpetre, Sodium Selenite 0.03 part and Iron sulfuret 0.002 part by weight ratio to mix;
2) the pale pink look crystal bead blank raw material mixed is carried out granulation by tablets press;
3) will make granular pale pink look crystal bead blank raw material to put into glass quartz tank furnace and found, keep weak oxide atmosphere and liquid level of solution to stablize when founding, glass melting temperature controls at 1320 DEG C-1380 DEG C;
4) crystal solution is molded into pale pink look crystal bead blank after the homogenizing cooling of material road, cooling temperature controls at 800 DEG C-1000 DEG C;
5) shaping pearl embryo is put into fire and throw stove polishing, integer, uniform coloring, shaping pearl embryo is allowed at the uniform velocity to enter stainless steel pipes, pipe temperature controls at 800 DEG C-900 DEG C, rotating speed 180 revolutions per seconds, in pipeline 5 minutes, pipeline was out just through integer, solid colour, no color differnece, pale pink look crystal bead blank without decorative pattern.
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| CN201510003548.6A CN104478214B (en) | 2015-01-06 | 2015-01-06 | A kind of pale pink look crystal bead blank and preparation method thereof |
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| CN201510003548.6A CN104478214B (en) | 2015-01-06 | 2015-01-06 | A kind of pale pink look crystal bead blank and preparation method thereof |
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| CN104478214B true CN104478214B (en) | 2016-03-23 |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106082648B (en) * | 2016-06-15 | 2018-06-26 | 浙江伟兴水晶有限公司 | A kind of crystal bead blank of lake water orchid color and preparation method thereof |
| CN110128009A (en) * | 2019-06-25 | 2019-08-16 | 中国耀华玻璃集团有限公司 | Pink colour body-tinted glass composition |
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| CN1095696A (en) * | 1993-05-22 | 1994-11-30 | 陈才 | A kind of crystal glass |
| US5656559A (en) * | 1994-06-23 | 1997-08-12 | Saint-Gobain Vitrage | Clear glass composition intended for the production of panes |
| CN101648773A (en) * | 2009-09-04 | 2010-02-17 | 常熟市万利特种玻璃厂 | Processing technology of Chinese red glass metal |
| CN102211869A (en) * | 2011-04-12 | 2011-10-12 | 姚晓春 | Primary pressure-sizing molding crystalloid glass and preparation method thereof |
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| JP2010083721A (en) * | 2008-09-30 | 2010-04-15 | Reiseki:Kk | Method for storing granulate or powdery object to be stored |
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2015
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| CN1095696A (en) * | 1993-05-22 | 1994-11-30 | 陈才 | A kind of crystal glass |
| US5656559A (en) * | 1994-06-23 | 1997-08-12 | Saint-Gobain Vitrage | Clear glass composition intended for the production of panes |
| CN101648773A (en) * | 2009-09-04 | 2010-02-17 | 常熟市万利特种玻璃厂 | Processing technology of Chinese red glass metal |
| CN102211869A (en) * | 2011-04-12 | 2011-10-12 | 姚晓春 | Primary pressure-sizing molding crystalloid glass and preparation method thereof |
| CN102503126A (en) * | 2011-10-08 | 2012-06-20 | 浙江伟兴水晶有限公司 | Preparation method for smoky yellow crystal bead blanks |
| CN102837251A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Diamond bead blank fire polishing furnace |
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Effective date of registration: 20220209 Address after: 321000 No. 668, Xuecheng East Road, Hanxiang Industrial Park, Tangya Town, Jindong District, Jinhua City, Zhejiang Province Patentee after: Zhejiang xinweixing crystal Co.,Ltd. Address before: 321000 Jindong comprehensive development park, Jinhua City, Zhejiang Province Patentee before: ZHEJIANG WEIXING CRYSTAL Co.,Ltd. |
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