CN105859136B - A kind of crystal bead blank of amber color and preparation method thereof - Google Patents
A kind of crystal bead blank of amber color and preparation method thereof Download PDFInfo
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- CN105859136B CN105859136B CN201610431554.6A CN201610431554A CN105859136B CN 105859136 B CN105859136 B CN 105859136B CN 201610431554 A CN201610431554 A CN 201610431554A CN 105859136 B CN105859136 B CN 105859136B
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- bead blank
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C12/00—Powdered glass; Bead compositions
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C4/00—Compositions for glass with special properties
- C03C4/02—Compositions for glass with special properties for coloured glass
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Road Signs Or Road Markings (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
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Abstract
The present invention discloses a kind of crystal bead blank of amber color, includes the raw material of following parts by weight：1.32 8.5 parts of fiery 100 150 parts of polishing powder, 100 200 parts of soda ash, 90 150 parts of quartz sand, 70 180 parts of cullet, 17 parts of salt, 18 70 parts of sodium nitrate, 10 40 parts of calcium carbonate, 5 25 parts of piece alkali, 10 35 parts of borax decahydrate, 2 15 parts of sodium chlorate, 0.5 2 parts of iron oxide red, 3 12 parts of ilmenite concentrate, 3.5 12 parts of manganese dioxide, 0.35 7 parts of sulphur and coal；The crystal bead blank coloring of the amber color is good, stable quality, productivity effect are high, is adapted to produce in enormous quantities, and will not cause environmental pollution.
Description
Technical field
Present invention relates particularly to a kind of crystal bead blank of amber color and preparation method thereof.
Background technology
Amber color crystal bead blank is the semi-finished product for manufacturing black crystal product, existing amber color crystal bead blank
In technique, crucible manufacture is used, there are this coloring is poor, irregular colour is even, there is decorative pattern, unstable product quality, productivity effect
It is low, be not suitable for continuous mass production, in addition, containing aluminium, environmental pollution is easily caused with coal.
The content of the invention
It is an object of the invention in view of the shortcomings of the prior art, providing a kind of good coloring, stable quality, productivity effect
It is high, suitable to produce in enormous quantities, and crystal bead blank of amber color of environmental pollution and preparation method thereof will not be caused.
It is as follows in order to solve the problem above-mentioned the technology of the use of the present invention and method：
A kind of crystal bead blank of amber color, includes the raw material of following parts by weight：Fiery polishing powder 100-150 parts, soda ash 100-
200 parts, 90-150 parts of quartz sand, 70-180 parts of cullet, 1-7 parts of salt, 18-70 parts of sodium nitrate, 10-40 parts of calcium carbonate, piece
5-25 parts of alkali, 10-35 parts of borax decahydrate, 2-15 parts of sodium chlorate, 0.5-2 parts of iron oxide red, 3-12 parts of ilmenite concentrate, manganese dioxide
1.32-8.5 parts of 3.5-12 parts, 0.35-7 parts of sulphur and coal.
Another technical problem to be solved by the invention is a kind of preparation method of the crystal bead blank of amber color of offer, including
Following steps：
1) 100-150 parts of polishing powder of getting fire, 100-200 parts of soda ash, 90-150 parts of quartz sand, 70-180 parts of cullet, salt
1-7 parts, 18-70 parts of sodium nitrate, 10-40 parts of calcium carbonate, 5-25 parts of piece alkali, 10-35 parts of borax decahydrate, 2-15 parts of sodium chlorate, oxygen
Change 1.32-8.5 parts of 0.5-2 parts of iron oxide red, 3-12 parts of ilmenite concentrate, 3.5-12 parts of manganese dioxide, 0.35-7 parts of sulphur and coal, mixing is equal
It is even；
2) it is put into comminutor and is granulated, granular size 0.5-2.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1350-1400 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross compression molding after material path cooling, temperature control exists
900-1000℃；
5) stove polishing shaping is thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 840-860 DEG C, is turned
200 revolutions per seconds of speed, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of amber color.
Beneficial effects of the present invention are：Stablize with performance, glossiness is good, and color is neat, unleaded pollution-free, productivity effect
It is good, it can be mass, using the optical requirement of Na-B-Si system highs index of refraction.
Embodiment
With reference to embodiment, the present invention is described in further detail, but they are not to technical solution of the present invention
Restriction, based on present invention teach that any conversion made, all falls within protection scope of the present invention.
Embodiment
A kind of preparation method of the crystal bead blank of amber color, comprises the following steps：
1) 110 parts of polishing powder of getting fire, 120 parts of soda ash, 90 parts of quartz sand, 90 parts of cullet, 2 parts of salt, 18 parts of sodium nitrate, carbon
Sour 15 parts of calcium, 5.5 parts of piece alkali, 1.2 parts of borax decahydrate, 3.3 parts of sodium chlorate, 0.5 part of iron oxide red, 5 parts of ilmenite concentrate, manganese dioxide
1.78 parts of 4.5 parts, 0.55 part of sulphur and coal, are uniformly mixed；
2) it is put into comminutor and is granulated, granular size 0.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1350 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross compression molding after material path cooling, temperature control exists
900℃；
5) stove polishing shaping is thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 840 DEG C, rotating speed 200
Revolutions per second, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of amber color.
Embodiment 2
A kind of preparation method of the crystal bead blank of amber color, comprises the following steps：
1) 150 parts of polishing powder of getting fire, 200 parts of soda ash, 150 parts of quartz sand, 180 parts of cullet, 7 parts of salt, 70 parts of sodium nitrate,
40 parts of calcium carbonate, 25 parts of piece alkali, 35 parts of borax decahydrate, 15 parts of sodium chlorate, 2 parts of iron oxide red, 12 parts of ilmenite concentrate, manganese dioxide 12
8.5 parts of part, 7 parts of sulphur and coal, are uniformly mixed；
2) it is put into comminutor and is granulated, granular size 2.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1400 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross compression molding after material path cooling, temperature control exists
1000℃；
5) stove polishing shaping is thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 860 DEG C, rotating speed 200
Revolutions per second, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of amber color.
Embodiment 3
A kind of preparation method of the crystal bead blank of amber color, comprises the following steps：
1) 125 parts of polishing powder of getting fire, 150 parts of soda ash, 120 parts of quartz sand, 135 parts of cullet, 4 parts of salt, 39 parts of sodium nitrate,
25 parts of calcium carbonate, 20 parts of piece alkali, 25 parts of borax decahydrate, 9 parts of sodium chlorate, 1 part of iron oxide red, 8 parts of ilmenite concentrate, 8 parts of manganese dioxide,
4 parts of 4 parts of sulphur and coal, are uniformly mixed；
2) it is put into comminutor and is granulated, granular size 1.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1375 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross compression molding after material path cooling, temperature control exists
950℃；
5) stove polishing shaping is thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 850 DEG C, rotating speed 200
Revolutions per second, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of amber color.
Beneficial effects of the present invention are：Stablize with performance, glossiness is good, and color is neat, unleaded pollution-free, productivity effect
It is good, it can be mass, using the optical requirement of Na-B-Si system highs index of refraction.
The above description is merely a specific embodiment, but protection scope of the present invention is not limited thereto, any
The change or replacement expected without creative work, should be covered by the protection scope of the present invention, therefore, of the invention
Protection domain should be determined by the scope of protection defined in the claims.
Claims (1)
1. a kind of crystal bead blank of amber color, it is characterised in that include the raw material of following parts by weight：Fiery 125 parts of polishing powder, soda ash
150 parts, 120 parts of quartz sand, 135 parts of cullet, 4 parts of salt, 39 parts of sodium nitrate, 25 parts of calcium carbonate, 20 parts of piece alkali, borax decahydrate
4 parts of 25 parts, 9 parts of sodium chlorate, 1 part of iron oxide red, 8 parts of ilmenite concentrate, 8 parts of manganese dioxide, 4 parts of sulphur and coal, the amber face
The preparation method of the crystal bead blank of color, comprises the following steps：
1) 125 parts of polishing powder of getting fire, 150 parts of soda ash, 120 parts of quartz sand, 135 parts of cullet, 4 parts of salt, 39 parts of sodium nitrate, carbonic acid
25 parts of calcium, 20 parts of piece alkali, 25 parts of borax decahydrate, 9 parts of sodium chlorate, 1 part of iron oxide red, 8 parts of ilmenite concentrate, 8 parts of manganese dioxide, sulphur
4 parts and 4 parts of coal, are uniformly mixed；
2) it is put into comminutor and is granulated, granular size 1.5cm；
3) by batch charger input crystal pond, liquid level stabilizing being kept when melted, temperature control is at 1375 DEG C；
4) in crystal pond 12 it is small when after, into clarifying basin 2 it is small when, cross material path cooling after compression molding, temperature control is 950
℃；
5) stove polishing shaping to be thrown through fire, then at the uniform velocity enters stainless steel pipes, pipe temperature is controlled at 850 DEG C, 200 turns of rotating speed/
Second, pipeline duration 5 minutes；
6) pipeline enters extinction tank after coming out, out the as crystal bead blank of amber color.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610431554.6A CN105859136B (en) | 2016-06-15 | 2016-06-15 | A kind of crystal bead blank of amber color and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610431554.6A CN105859136B (en) | 2016-06-15 | 2016-06-15 | A kind of crystal bead blank of amber color and preparation method thereof |
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| CN105859136A CN105859136A (en) | 2016-08-17 |
| CN105859136B true CN105859136B (en) | 2018-05-11 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106242278A (en) * | 2016-08-29 | 2016-12-21 | 浙江伟兴水晶有限公司 | A kind of white colour crystal bead blank and preparation method thereof |
| CN106365447A (en) * | 2016-08-29 | 2017-02-01 | 浙江伟兴水晶有限公司 | Peacock blue crystal bead blank and preparation method thereof |
| CN106380074A (en) * | 2016-08-29 | 2017-02-08 | 浙江伟兴水晶有限公司 | Cymbidium sinensis-color crystal ball blank and preparation method thereof |
| CN106277780A (en) * | 2016-08-29 | 2017-01-04 | 浙江伟兴水晶有限公司 | A kind of Flos Nelumbinis color purple crystal bead blank and preparation method thereof |
| CN106365446A (en) * | 2016-08-29 | 2017-02-01 | 浙江伟兴水晶有限公司 | Light-blue colored crystal bead blank and preparation method thereof |
| CN106396376A (en) * | 2016-08-29 | 2017-02-15 | 浙江伟兴水晶有限公司 | Capri blue crystal bead rough and preparation method thereof |
| CN108545934B (en) * | 2018-05-15 | 2021-01-12 | 张怀民 | Iron-titanium-carbon colored medical water-resistant glass |
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| CN102838277A (en) * | 2012-09-17 | 2012-12-26 | 江苏锦程集团科技有限公司 | Production process of honey peach CZ diamond |
| CN104556696B (en) * | 2015-01-06 | 2016-03-23 | 浙江伟兴水晶有限公司 | A kind of rosy quartz pearl embryo and preparation method thereof |
| CN104556698B (en) * | 2015-01-06 | 2016-03-23 | 浙江伟兴水晶有限公司 | A kind of cigarette yellow crystal pearl embryo and preparation method thereof |
| CN104556697B (en) * | 2015-01-06 | 2016-03-23 | 浙江伟兴水晶有限公司 | A kind of golden yellow crystal bead blank and preparation method thereof |
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Effective date of registration: 20220210 Address after: 321000 No. 668, Xuecheng East Road, Hanxiang Industrial Park, Tangya Town, Jindong District, Jinhua City, Zhejiang Province Patentee after: Zhejiang xinweixing crystal Co.,Ltd. Address before: 321000 Jindong comprehensive development park, Jinhua City, Zhejiang Province Patentee before: ZHEJIANG WEIXING CRYSTAL Co.,Ltd. |