CN106368069A - Heating non-combustible cigarette paper and preparation method thereof - Google Patents

Heating non-combustible cigarette paper and preparation method thereof Download PDF

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Publication number
CN106368069A
CN106368069A CN201610913140.7A CN201610913140A CN106368069A CN 106368069 A CN106368069 A CN 106368069A CN 201610913140 A CN201610913140 A CN 201610913140A CN 106368069 A CN106368069 A CN 106368069A
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China
Prior art keywords
cigarette paper
heating non
preparation
burning
paper
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CN201610913140.7A
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CN106368069B (en
Inventor
肖翠翠
黄启志
陈泽亮
王小平
游志强
朱星宇
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ZHONGYAN MODI (JIANGMEN) PAPER INDUSTRY Co Ltd
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ZHONGYAN MODI (JIANGMEN) PAPER INDUSTRY Co Ltd
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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H27/00Special paper not otherwise provided for, e.g. made by multi-step processes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D1/00Methods of beating or refining; Beaters of the Hollander type
    • D21D1/02Methods of beating; Beaters of the Hollander type
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D21H11/12Pulp from non-woody plants or crops, e.g. cotton, flax, straw, bagasse
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H13/00Pulp or paper, comprising synthetic cellulose or non-cellulose fibres or web-forming material
    • D21H13/36Inorganic fibres or flakes
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H15/00Pulp or paper, comprising fibres or web-forming material characterised by features other than their chemical constitution
    • D21H15/02Pulp or paper, comprising fibres or web-forming material characterised by features other than their chemical constitution characterised by configuration
    • D21H15/10Composite fibres
    • D21H15/12Composite fibres partly organic, partly inorganic
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/21Macromolecular organic compounds of natural origin; Derivatives thereof
    • D21H17/24Polysaccharides
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/21Macromolecular organic compounds of natural origin; Derivatives thereof
    • D21H17/24Polysaccharides
    • D21H17/28Starch
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20Macromolecular organic compounds
    • D21H17/21Macromolecular organic compounds of natural origin; Derivatives thereof
    • D21H17/24Polysaccharides
    • D21H17/28Starch
    • D21H17/29Starch cationic
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63Inorganic compounds
    • D21H17/67Water-insoluble compounds, e.g. fillers, pigments
    • D21H17/675Oxides, hydroxides or carbonates
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63Inorganic compounds
    • D21H17/67Water-insoluble compounds, e.g. fillers, pigments
    • D21H17/68Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H19/00Coated paper; Coating material
    • D21H19/10Coatings without pigments
    • D21H19/14Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12
    • D21H19/20Coatings without pigments applied in a form other than the aqueous solution defined in group D21H19/12 comprising macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/06Paper forming aids
    • D21H21/10Retention agents or drainage improvers
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/16Sizing or water-repelling agents
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/18Reinforcing agents
    • D21H21/20Wet strength agents

Abstract

The invention discloses heating non-combustible cigarette paper and a preparation method thereof. The preparation method of the heating non-burning cigarette paper comprises the following steps: 1) pulping the plant fiber with the length of 0.5 to 4mm, or adding the appropriate proportion of inorganic fiber; 2) adding the inorganic filler in the process of dilution of the pulp, wherein the addition ratio of the inorganic filler is 5 to 50% of the mass of the pulp; 3) sizing the paper to improve water and oil resistance, and cigarette paper is quantified at 50 to 120 g/m<2>. Compared with the existing heated non-combustible cigarette paper that is heated at 350 DEG C, the non-combustible cigarette paper of the present invention has very few yellow stitches, and no tar spots and carbonization, while the entire surface of the existing non-combustible cigarette paper turns yellow, with large tar penetrating and carbonized. In addition, the non-combustible cigarette paper of the present invention is rarely present broken in actual production, and there is almost no deformation and wrinkling after being sucked as the heated cigarette paper.

Description

A kind of heating non-burning cigarette paper and preparation method thereof
Technical field
The present invention relates to a kind of heating non-burning cigarette paper and preparation method thereof, particularly to a kind of heating non-burning Nicotiana tabacum L. Non-burning cigarette paper used by product.
Background technology
Step with international Tobacco Control campaign is more accelerated, the limit to smoking especially smoking in public places for the Chinese government System is further strict, and has gradually formed social consensus.Under increasingly strict Tobacco Control environment, Partial Tobacco article consumer may New non-traditional tobacco product can be selected, and this variation tendency is day by day clear.Show according to statistical data in 2015, in the world While scope inner wrap strip volume of production and marketing has declined, other types tobacco product assumes rapid growth trend, World tobacco market Constantly there is profound change in product structure, positive Development of Novel tobacco product is increasingly becoming the strategy of each transnational tobacco company Orientation.
Traditional cigarette produces multiple harmful components due to result of combustion of tobacco and thermal cracking, and heating non-combustion-type Medicated cigarette produces Flue gas is closer to traditional cigarette, and avoids because of 900 DEG C of high temperature above cracking substantial amounts of harmful components of generation, side-stream smoke Substantially reduce with part harmful components, decrease the harm to body while consumer obtains gratification, and reduce The pollution of environment flue gas.In addition, heating non-burning Medicated cigarette as most potential replacement traditional cigarette novel tobacco product, closely The sales volume growth rate of 2 years is very swift and violent.And cigarette paper, as one of Medicated cigarette emphasis material, is heating non-burning Medicated cigarette In research and development essential it is necessary to there be the cigarette paper complete sets of Techniques that can meet it head-on, could power-assisted Chinese-style cigarette product upgrading wound Newly.
Existing heating non-burning cigarette paper technology is also disclosed, and such as " a kind of low-temperature heat type Medicated cigarette is not with for Chinese patent Combustion cigarette paper and preparation method thereof ", application number cn201410437696.4.This patented technology pass through slurry in be filled with magnesium hydroxide, Aluminium hydroxide and be coated with phosphorus flame retardant to reach the purpose do not fired when cigarette paper uses on paper substrate surface.Its disclosed embodiment Testing result show, can accomplish that 350 DEG C do not fire (carbonization when 450 DEG C), but whole turn to be yellow.
Applicant is tested according to the cigarette paper that do not fire that the method that patent cn201410437696.4 provides obtains, and finds There is during actually used blackened appearance, tar stain, Folding Deformation;Further, since quantitative low, low intensity, shape are steady Property difference the problems such as easily cause during production processing curly course in frequently break paper problem.Obviously, existing do not fire cigarette paper skill Art index is far from the actually used demand meeting heating non-burning Medicated cigarette.
Content of the invention
The purpose of the present invention solves the existing cigarette paper that do not fire to be existed when being applied to and heating non-burning Medicated cigarette Drawbacks described above, provides a kind of Novel heating non-burning cigarette paper and preparation method thereof.
For reaching above-mentioned purpose, the technical scheme that the present invention takes is as follows:
A kind of preparation method of heating non-burning cigarette paper, comprises the steps:
1) choose Plant fiber's making beating that length is 0.5~4mm, or the inorfil mixing proper proportion;
2) add inorganic filler after grinding during thick stock dilution, the adding proportion of inorganic filler be stock quality 5~ 50%;
3) applying glue after copy paper, improves water resistant, the grease resistance of body paper;
Quantification of 50~the 120g/ of cigarette paper.
Further, above-mentioned step 1), to length be 0.5~1.5mm, 3~4mm Plant fiber beating degree be 20~ 40 ° of sr, fibre length is the beating degree of 1.5~3mm Plant fiber is 40~90 ° of sr.Described Plant fiber can be wood pulp, The mixing slurry of one or more of jute pulp, straw pulp, described wood pulp include but are not limited to birch, Eucalyptus, Zelkova schneideriana Hand.-Mazz., Lignum seu Ramulus Cunninghamiae Lanceolatae or Masson Pine, described ramie pulp fiber includes Fructus Cannabiss or Caulis et Folium Lini, and described straw pulp fiber includes but are not limited to Caulis et Folium Oryzae, straw or dragon Grass.
Further, above-mentioned step 1), described inorfil includes but are not limited to alumina silicate fibre, shepardite fibre Dimension, Calcium Carbonate fiber etc., further, the inorfil Particle size requirements 0.1~4mm of interpolation.Using Plant fiber and inorganic fibre During the mixed slurry of dimension, the mass mixing ratio preferably 0.5~4:1 of Plant fiber and inorfil.
Further, above-mentioned step 2), described inorganic filler includes caco3, Pulvis Talci, caso4、al(oh)3.3h2o、 al2o3、mg(oh)2Deng one or more of mixture, preferably ca co3Or mg (oh)2;Inorganic filler Particle size requirements 0.3~ 20 microns.The adding proportion of inorganic filler is preferably the 15~20% of stock quality.
Further, above-mentioned step 3), the sizing agent that applying glue adopts is stearic acid, calcium stearate, styrene-acrylate Polymer, alkyl ketene dimer (akd), styrene acrylic polymers, styrene maleic anhydride copolymer, carboxymethyl cellulose The single sizing agent such as element, polyvinyl alcohol, polyacrylamide, polyurethane or the mixture of multiple sizing agent, preferably alkyl alkene Ketone dimer (akd) or styrene-acrylate polymers.
Further, in order to optimize follow-up papermaking properties, in step 2) add reinforcing agent afterwards, described reinforcing agent is oxidation Starch, phosphate ester starch, hydroxyalkyl starch, acetate starch, cationic starch, guar gum, xanthan gum, casein, polyethylene One of alcohol, polyacrylamide etc. or multiple mixture.The consumption of reinforcing agent is 5~30kg paper per ton, specifically can be Add before pressurized screen.
Further, in order to optimize follow-up papermaking properties, in step 2) also can add a small amount of general cigarette paper afterwards with helping Stay the process assistants such as agent, such as cationic starch etc., the ratio of interpolation is 1~5kg paper per ton.Specifically can add after pressurized screen.
Beneficial effects of the present invention:
The present invention is manufactured paper with pulp body paper using the fiber through making beating, after being filled with, then through glue-applying technique, body paper is changed in slurry Property, reduce the cracking of cigarette paper and hydrophilic, reach that raising cigarette paper is heat-resisting, anti-deformation, the purpose of impermeabilisation ability.
The present invention is not burnt with existing heating compared with cigarette paper, with 350 DEG C heat when, the non-burning Medicated cigarette of the present invention The stitching of the only few jaundice of paper, existing cigarette paper whole surface of not firing all is turned to be yellow;The non-burning cigarette paper of the present invention does not have There is tar stain and start carbonization phenomenon, and the existing cigarette paper that do not fire has the infiltration of bulk tar and starts carbonization.In addition, the present invention Non-burning cigarette paper disconnected paper phenomenon also seldom occurs in actual production, almost do not have as after the cigarette paper suction of hot type There are deformation and gauffer.
Below in conjunction with drawings and Examples, the specific implementation method of the present invention is elaborated.
Brief description
Fig. 1 is that the prepared heating non-burning cigarette paper of embodiment 1 heats the outward appearance after 6 mouthfuls of suction in 350 DEG C of heaters Picture.Heating non-burning cigarette paper whiteness conservation rate is 90%, and the problems such as tar stain, deformation.
Fig. 2 heats the outward appearance picture after 6 mouthfuls of suction for cigarette paper prepared by comparative example 1 in 350 DEG C of heaters.Cigarette paper Whiteness conservation rate is 44%, and the problems such as serious tar stain, deformation.
Specific embodiment
Embodiment 1: prepare quantification of 90g/m2Heating non-burning cigarette paper
Using fibrous raw material, inorganic filler, reinforcing agent, sizing agent and, retention agent and some processes index see table 1, Inorfil Particle size requirements 0.1~4mm, 0.3~20 micron of inorganic filler Particle size requirements.
Table 1
Other slurrying and copy paper technique are carried out according to the production technology of general cigarette paper.
By the quantification of 90g/m obtaining2Heating non-burning cigarette paper, with 350 DEG C heating non-burning cigarette heater enter Row heats and aspirates, and after 6 mouthfuls of suction, the whiteness taking out photographic analysis cigarette paper is 80%, and whiteness conservation rate is 90%;Additionally, After 6 mouthfuls of continuous sucking, the problems such as tar stain, deformation in outward appearance.Illustrate using adding that the inventive method prepares Hot non-burning cigarette paper can be actually used in 350 DEG C of heating non-burning Medicated cigarette.
Embodiment 2: prepare quantification of 120g/m2Heating non-burning cigarette paper
Using fibrous raw material, inorganic filler, reinforcing agent, sizing agent and, retention agent and some processes index see table 2, Inorfil Particle size requirements 0.1~4mm, 0.3~20 micron of inorganic filler Particle size requirements.
Table 2
Other slurrying and copy paper technique are carried out according to the production technology of general cigarette paper.
By the quantification of 120g/m obtaining2Heating non-burning cigarette paper, with 350 DEG C heating non-burning cigarette heater enter Row heats and aspirates, and after 6 mouthfuls of suction, the whiteness taking out photographic analysis cigarette paper is 88%, and whiteness conservation rate is 98%;Additionally, After 6 mouthfuls of continuous sucking, the problems such as tar stain, deformation in outward appearance.The heating being prepared using inventive method is described Non-burning cigarette paper can be actually used in 350 DEG C of heating non-burning Medicated cigarette, and indices are excellent.
Embodiment 3: prepare quantification of 90g/m2Heating non-burning cigarette paper
Using fibrous raw material, inorganic filler, reinforcing agent, sizing agent and, retention agent and some processes index see table 3, Inorfil Particle size requirements 0.1~4mm, 0.3~20 micron of inorganic filler Particle size requirements.
Table 3
Other slurrying and copy paper technique are carried out according to the production technology of general cigarette paper.
By the quantification of 90g/m obtaining2Heating non-burning cigarette paper, with 350 DEG C heating non-burning cigarette heater enter Row heats and aspirates, and after 6 mouthfuls of suction, the whiteness taking out photographic analysis cigarette paper is 86%, and whiteness conservation rate is 96%;Additionally, After 6 mouthfuls of continuous sucking, the problems such as tar stain, deformation in outward appearance.Illustrate using adding that the inventive method prepares Hot non-burning cigarette paper successfully can use in 350 DEG C of heating non-burning Medicated cigarette, and effect is fine.
Embodiment 4: prepare quantification of 100g/m2Heating non-burning cigarette paper
Using fibrous raw material, inorganic filler, reinforcing agent, sizing agent and, retention agent and some processes index see table 4, Inorfil Particle size requirements 0.1~4mm, 0.3~20 micron of inorganic filler Particle size requirements.
Table 4
Other slurrying and copy paper technique are carried out according to the production technology of general cigarette paper.
By the quantification of 100g/m obtaining2Heating non-burning cigarette paper, with 350 DEG C heating non-burning cigarette heater enter Row heats and aspirates, and after 6 mouthfuls of suction, the whiteness taking out photographic analysis cigarette paper is 86%, and whiteness conservation rate is 96%;Additionally, After 6 mouthfuls of continuous sucking, the problems such as tar stain, deformation in outward appearance.Heating non-burning using this method preparation is described Cigarette paper can heat at 350 DEG C can practical application in non-burning Medicated cigarette.
Embodiment 5: prepare quantification of 50g/m2Heating non-burning cigarette paper
Using fibrous raw material, inorganic filler, reinforcing agent, sizing agent and, retention agent and some processes index see table 5, Inorfil Particle size requirements 0.1~4mm, 0.3~20 micron of inorganic filler Particle size requirements.
Table 5
Other slurrying and copy paper technique are carried out according to the production technology of general cigarette paper.
By the quantification of 50g/m obtaining2Heating non-burning cigarette paper, with 350 DEG C heating non-burning cigarette heater enter Row heats and aspirates, and after 6 mouthfuls of suction, the whiteness taking out photographic analysis cigarette paper is 80%, and whiteness conservation rate is 90%;Additionally, After 6 mouthfuls of continuous sucking, the problems such as tar stain, deformation in outward appearance.Heating non-burning using this method preparation is described Cigarette paper successfully can use in 350 DEG C of heating non-burning Medicated cigarette.
Comparative example 1:
Table 6 does not fire cigarette paper composition
Quantification of 32g/m prepared by comparative example 12Do not fire cigarette paper, with 350 DEG C heating non-burning cigarette heater enter Row heats and aspirates, and after 6 mouthfuls of continuous sucking, the whiteness taking out photographic analysis cigarette paper is 40%, and whiteness conservation rate is 44%, and And by accompanying drawing as can be seen that comparative example method be obtained do not fire cigarette paper after 6 mouthfuls of continuous sucking, occur serious tar stain, The problems such as blackened appearance, is it is impossible to enough use in 350 DEG C of heating non-burning cigarette heater.Illustrate to use ammonium polyphosphate flame retardant Although can be fire-retardant, cigarette paper has turned yellow blackening, and has serious tar stain it is impossible to practical application.
The heating non-burning cigarette paper that the inventive method is obtained, carries out adding with 350 DEG C of heating non-burning cigarette heater Heat is simultaneously aspirated, and after 6 mouthfuls of continuous sucking, taking-up is taken pictures, and the whiteness using cigarette paper after Instrumental Analysis suction, and analysis result shows After 6 mouthfuls of continuous sucking, the whiteness scope of cigarette paper is 80~88%, and whiteness conservation rate is 85~98%;Additionally, by illustrating The attached Fig. 1 and 2 of book can be seen that the prepared heating non-burning cigarette paper of the inventive method after 6 mouthfuls of continuous sucking, Jiao The problems such as oil mark, deformation.Illustrate to add at 350 DEG C and less than 350 DEG C using the heating non-burning cigarette paper of this method preparation Successfully use in hot non-burning Medicated cigarette.
In addition, the heating non-burning cigarette paper of the present invention is in production and follow-up processing curly course, do not occur existing The common paper phenomenon of frequently breaking of some cigarette paper.

Claims (11)

1. a kind of preparation method of heating non-burning cigarette paper, comprises the steps:
1) choose Plant fiber's making beating that length is 0.5~4mm, or the inorfil mixing proper proportion;
2) add inorganic filler during thick stock dilution after grinding, the adding proportion of inorganic filler is the 5~50% of stock quality;
3) applying glue after copy paper, improves water resistant, the grease resistance of body paper;
Quantification of 50~the 120g/ of cigarette paper.
2. as claimed in claim 1 heating non-burning cigarette paper preparation method it is characterised in that: described step 1), right Length is 0.5~1.5mm, the beating degree of 3~4mm Plant fiber is 20~40 ° of sr, and length is beating of 1.5~3mm Plant fiber The degree of beating is 40~90 ° of sr.
3. as claimed in claim 1 heating non-burning cigarette paper preparation method it is characterised in that: described step 1), Inorfil is mixed, the mass mixing ratio of Plant fiber and inorfil is 0.5~4:1 in vegetable-fibre slurry.
4. as claimed in claim 1 heating non-burning cigarette paper preparation method it is characterised in that: described inorfil bag Include alumina silicate fibre, brucite fiber or Calcium Carbonate.
5. as claimed in claim 1 heating non-burning cigarette paper preparation method it is characterised in that: described inorfil grain Footpath requires 0.1~4mm.
6. as claimed in claim 1 heating non-burning cigarette paper preparation method it is characterised in that: step 2) described in inorganic Filler is caco3, Pulvis Talci, caso4、al(oh)3.3h2o、al2o3、mg(oh)2One or more of mixture.
7. as claimed in claim 1 heating non-burning cigarette paper preparation method it is characterised in that: inorganic filler Particle size requirements 0.3~20 micron.
8. heating non-burning cigarette paper as claimed in claim 1 preparation method it is characterised in that: step 3) applying glue that adopts Agent is stearic acid, calcium stearate, styrene-acrylate polymers, alkyl ketene dimer, styrene acrylic polymers, benzene The single sizing agent such as ethenyl maleic anhydride copolymer, carboxymethyl cellulose, polyvinyl alcohol, polyacrylamide, polyurethane or The mixture of multiple sizing agents.
9. as claimed in claim 1 heating non-burning cigarette paper preparation method it is characterised in that: before pressurized screen add increase Strong agent, described reinforcing agent is Oxytarch, phosphate ester starch, hydroxyalkyl starch, acetate starch, cationic starch, Guar One of glue, xanthan gum, casein, polyvinyl alcohol, polyacrylamide etc. or multiple mixture.
10. as claimed in claim 1 heating non-burning cigarette paper preparation method it is characterised in that: after pressurized screen add Retention agent, addition is 1~5kg paper per ton.
The heating non-burning Medicated cigarette that the preparation method of the arbitrary described heating non-burning cigarette paper of 11. claim 1-10 obtains Paper.
CN201610913140.7A 2016-10-19 2016-10-19 It is a kind of to heat non-burning cigarette paper and preparation method thereof Active CN106368069B (en)

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Cited By (18)

* Cited by examiner, † Cited by third party
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WO2019001014A1 (en) * 2017-06-28 2019-01-03 上海新型烟草制品研究院有限公司 Heat-resistant paper for tobacco products capable of not burning under heating
CN109567271A (en) * 2018-12-26 2019-04-05 湖南中烟工业有限责任公司 One kind, which has to reduce, heats the cigarette smoke temperature filter stick additive and preparation method thereof that do not burn
CN109588770A (en) * 2018-12-26 2019-04-09 湖南中烟工业有限责任公司 A kind of cooling mouth stick and cigarette
CN109594411A (en) * 2018-12-27 2019-04-09 牡丹江恒丰纸业股份有限公司 Impermeable low-temperature heat is not burnt cigarette paper combustion inhibitor, cigarette paper and preparation method
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CN110172868A (en) * 2019-04-30 2019-08-27 安徽中烟工业有限责任公司 A kind of composite cigarette paper for magnetic grain soaking tobacco product
CN110284370A (en) * 2019-06-20 2019-09-27 云南中烟工业有限责任公司 It is a kind of for heating the heatproof cigarette paper and its preparation method and application for the cigarette that do not burn
WO2020008510A1 (en) * 2018-07-02 2020-01-09 日本たばこ産業株式会社 Wrapping paper for non-combustible heated type smoking article, non-combustible heated type smoking article, and electrically-heated smoking system
WO2020026311A1 (en) * 2018-07-30 2020-02-06 日本たばこ産業株式会社 Rolling paper for non-combusted heated smoking article, non-combusted heated smoking article, and electric heated smoking system
CN112779818A (en) * 2021-01-08 2021-05-11 中烟施伟策(云南)再造烟叶有限公司 Heating tobacco cigarette paper and preparation method thereof
TWI746873B (en) * 2018-07-31 2021-11-21 日商日本煙草產業股份有限公司 Wrapper for non-burning heating type smoking article, non-buring heating type smoking article and electrically heating type smoking system
EP3779042A4 (en) * 2018-05-29 2021-11-24 Japan Tobacco Inc. Rolling paper for non-combustion heating-type smoking article, non-combustion heating-type smoking article, and electric heating-type smoking system
CN113957746A (en) * 2020-07-20 2022-01-21 福建中烟工业有限责任公司 Sepiolite composite paper, preparation method and application thereof
TWI757519B (en) * 2018-07-02 2022-03-11 日商日本煙草產業股份有限公司 Wrapping paper for non-burning heating type smoking article, non-burning heating type smoking article and electrically heating type smoking system
RU2771820C1 (en) * 2018-07-30 2022-05-12 Джапан Тобакко Инк. Cigarette paper for a non-burned heated smoking article, non-burned heated smoking article, and electrically heated smoking system
CN115852731A (en) * 2022-12-28 2023-03-28 广东中烟工业有限责任公司 Whole hemp pulp for heating non-combustible cigarettes and application thereof
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WO2019001014A1 (en) * 2017-06-28 2019-01-03 上海新型烟草制品研究院有限公司 Heat-resistant paper for tobacco products capable of not burning under heating
CN107587382A (en) * 2017-09-07 2018-01-16 滁州市光威化工有限公司 A kind of cigarette paper with the inflammable function that eliminates smoke
EP3779042A4 (en) * 2018-05-29 2021-11-24 Japan Tobacco Inc. Rolling paper for non-combustion heating-type smoking article, non-combustion heating-type smoking article, and electric heating-type smoking system
JP7021351B2 (en) 2018-07-02 2022-02-16 日本たばこ産業株式会社 Rolling paper for non-combustion-heated smoking articles, non-combustion-heated smoking articles and electric-heated smoking systems
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WO2020008510A1 (en) * 2018-07-02 2020-01-09 日本たばこ産業株式会社 Wrapping paper for non-combustible heated type smoking article, non-combustible heated type smoking article, and electrically-heated smoking system
JPWO2020008510A1 (en) * 2018-07-02 2021-06-24 日本たばこ産業株式会社 Rolling paper for non-combustion heating type smoking articles, non-combustion heating type smoking articles and electric heating type smoking system
KR20210014139A (en) * 2018-07-02 2021-02-08 니뽄 다바코 산교 가부시키가이샤 Non-combustible heated smoking article wrapper, non-combusted heated smoking article and electric heated smoking system
CN112368444A (en) * 2018-07-02 2021-02-12 日本烟草产业株式会社 Cigarette paper for non-combustion heating type smoking article, non-combustion heating type smoking article and electric heating type smoking system
US20210120867A1 (en) * 2018-07-02 2021-04-29 Japan Tobacco Inc. Wrapping paper for non-combustible heated type smoking article, non-combustible heated type smoking article, and electrically-heated smoking system
EP3832013A4 (en) * 2018-07-30 2022-03-23 Japan Tobacco Inc. Rolling paper for non-combusted heated smoking article, non-combusted heated smoking article, and electric heated smoking system
WO2020026311A1 (en) * 2018-07-30 2020-02-06 日本たばこ産業株式会社 Rolling paper for non-combusted heated smoking article, non-combusted heated smoking article, and electric heated smoking system
JPWO2020026311A1 (en) * 2018-07-30 2021-08-02 日本たばこ産業株式会社 Rolling paper for non-combustion heating type smoking articles, non-combustion heating type smoking articles and electric heating type smoking system
JP7105889B2 (en) 2018-07-30 2022-07-25 日本たばこ産業株式会社 Paper wrapping for non-combustion heating smoking articles, non-combustion heating smoking articles and electrically heated smoking systems
RU2771820C1 (en) * 2018-07-30 2022-05-12 Джапан Тобакко Инк. Cigarette paper for a non-burned heated smoking article, non-burned heated smoking article, and electrically heated smoking system
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CN109680540A (en) * 2018-11-23 2019-04-26 山东中烟工业有限责任公司 A kind of package periphery hot type heats the paper and preparation method thereof of non-burning cigarette core material
CN109588770A (en) * 2018-12-26 2019-04-09 湖南中烟工业有限责任公司 A kind of cooling mouth stick and cigarette
CN109567271A (en) * 2018-12-26 2019-04-05 湖南中烟工业有限责任公司 One kind, which has to reduce, heats the cigarette smoke temperature filter stick additive and preparation method thereof that do not burn
CN109594411A (en) * 2018-12-27 2019-04-09 牡丹江恒丰纸业股份有限公司 Impermeable low-temperature heat is not burnt cigarette paper combustion inhibitor, cigarette paper and preparation method
CN109594411B (en) * 2018-12-27 2021-12-14 牡丹江恒丰纸业股份有限公司 Anti-permeation low-temperature heating non-combustion cigarette paper combustion inhibitor, cigarette paper and preparation method
CN110172868A (en) * 2019-04-30 2019-08-27 安徽中烟工业有限责任公司 A kind of composite cigarette paper for magnetic grain soaking tobacco product
CN110284370A (en) * 2019-06-20 2019-09-27 云南中烟工业有限责任公司 It is a kind of for heating the heatproof cigarette paper and its preparation method and application for the cigarette that do not burn
US11712059B2 (en) 2020-02-24 2023-08-01 Nicoventures Trading Limited Beaded tobacco material and related method of manufacture
CN113957746A (en) * 2020-07-20 2022-01-21 福建中烟工业有限责任公司 Sepiolite composite paper, preparation method and application thereof
CN112779818A (en) * 2021-01-08 2021-05-11 中烟施伟策(云南)再造烟叶有限公司 Heating tobacco cigarette paper and preparation method thereof
CN115852731A (en) * 2022-12-28 2023-03-28 广东中烟工业有限责任公司 Whole hemp pulp for heating non-combustible cigarettes and application thereof

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