CN106361920A - Preparation method of long-acting medical disinfection cotton balls - Google Patents
Preparation method of long-acting medical disinfection cotton balls Download PDFInfo
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- CN106361920A CN106361920A CN201610923009.9A CN201610923009A CN106361920A CN 106361920 A CN106361920 A CN 106361920A CN 201610923009 A CN201610923009 A CN 201610923009A CN 106361920 A CN106361920 A CN 106361920A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/481—Astragalus (milkvetch)
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- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/618—Molluscs, e.g. fresh-water molluscs, oysters, clams, squids, octopus, cuttlefish, snails or slugs
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- A61K36/23—Apiaceae or Umbelliferae (Carrot family), e.g. dill, chervil, coriander or cumin
- A61K36/236—Ligusticum (licorice-root)
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- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/886—Aloeaceae (Aloe family), e.g. aloe vera
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- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
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- A61M35/00—Devices for applying media, e.g. remedies, on the human body
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- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
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Abstract
The invention relates to a preparation method of long-acting medical disinfection cotton balls, belonging to the technical field of medical disinfection and sterilization. According to the preparation method, anthraquinone substances, polysaccharides and soluble salt in radix astragali seu hedysari, rhizoma chuanxiong and aluminite are extracted by using an ethanol solution for promoting healing of a wound and protecting the wound by sterilization; filtered liquid and aloe vera leaves are cooked for extracting aloe vera gel, and the extracted aloe vera gel is oxidized by using hydrogen peroxide for improving the film-forming property, so that a basic disinfectant is prepared; then, the basic disinfectant is mixed with freshwater pearl powder, potassium iodide and the like so as to obtain a disinfectant; absorbent balls are soaked in the obtained disinfectant, so that the long-acting medical disinfection cotton balls are obtained. The long-acting medical disinfection cotton balls can be used for disinfecting and sterilizing the wound by means of bactericidal substances in natural products so as to avoid the irritation to the skin, and using the aloe vera gel to protect the wound in a film-forming way; by using a principle that nutrient substances provided by pearl powder accelerate the wound healing, after the long-acting medical disinfection cotton balls are used, the problem that disinfection cotton balls have skin irritation since the disinfectant in the cotton balls easily volatilizes so as to lead to decrement of concentration is effectively solved, and the effects of enabling the disinfection cotton balls to be long-acting and accelerating the wound healing are realized.
Description
Technical field
The present invention relates to a kind of preparation method of long-acting medical disinfecting cotton ball, belong to medical disinfecting technical field.
Background technology
Sterilized cotton ball is to draw medical alcohol by the rayon balls of sterilized process to be made, and has and human body skin is disappeared
Poison, prevents the effect infecting.People, through test repeatedly, learn that the ethanol sterilizing power that concentration is 75% is the strongest, so medical disappear
Poisonous wine essence typically all contains 75% absolute alcohol and 25% water.
Existing sterilized cotton ball is typically medicining liquid dipping rayon balls, medical by intensified glutaraldehyde, antirust agent, buffer agent
After soaking in the medicinal liquid of distilled water configuration, dehydration and cotton swab immersion iodine tincture, the method for ethanol are obtained, and are generally required for protecting
Exist in the container quite sealing.
Soak prepared sterilized cotton ball, because of iodine preparation, there is stronger zest to human body skin in iodine tincture, therefore, facing
Typically carry out second wiping with alcoholic cotton balls again on bed, to dilute the iodine number on skin, normally referred to as take off iodine, to subtract
Few stimulation to human body skin for the iodine, but because iodide ion is extremely active, oxidability is strong, distils quickly, meet it after meeting light
Its material, also easily generates precipitation, and after being especially formed into cotton balls, the effect tool of its sterilizing significantly decreases.And in wine
Soak in essence prepared sterilized cotton ball because ethanol readily volatilized, be difficult to keep the concentration of cotton balls and humidity constant it is easy to cut
Weak so lose Disinfection Effect.This several sterilized cotton ball all must be placed in the container of sealing, once container goes wrong, very
It is easily caused cotton balls cannot use.
Content of the invention
The technical problem to be solved: volatile and lead to for the disinfectant solution in existing sterilized cotton ball at present
Lowering of concentration, it is impossible to long-acting use, has stronger irritating problem simultaneously to human body skin, there is provided a kind of long-acting medical
The preparation method of sterilized cotton ball, the present invention utilize ethanol solution extract the Radix Astragali, the anthraquinones in Rhizoma Chuanxiong and Alumen, polysaccharide and
Soluble-salt, promotes wound healing, wound is carried out with sterilizing protection, then extracts Aloe glue by filtrate with Folium Aloe steaming and decocting,
Using hydrogen peroxide to extract Aloe glue aoxidize, increase film property, be obtained basis disinfectant solution, then with mussel pearl powder, iodine
Change potassium etc. and be mixed to prepare disinfectant solution, rayon balls are soaked, long-acting medical disinfecting cotton ball is obtained, the present invention passes through in natural goodses
Fungicidal substance carries out sterilizing to wound, it is to avoid the stimulation to skin, carries out film forming protection with Aloe glue to wound, uses
Margarita powder provides nutrient substance to accelerate the principle of wound healing, efficiently solves the disinfectant solution in sterilized cotton ball volatile and lead to
It is impossible to long-acting use, the problem of being irritating to the skin property, it is achieved that sterilized cotton ball can long-acting use, accelerates wound to lowering of concentration
The effect of healing.
For solving above-mentioned technical problem, the present invention using technical scheme as described below is:
(1) count by weight, take 25～30 parts of Radixs Astragali, 18～22 parts of Rhizoma Chuanxiongs, 17～19 parts of Alumen and 60～70 parts of quality to divide
Several 15% ethanol solution, put into the Radix Astragali, Rhizoma Chuanxiong and Alumen in 80 DEG C of baking ovens first and 10～15min are dried, place into pulverizer
Middle pulverizing, crosses 200 mesh sieves, collects and sieves granule, and with mass fraction 15% ethanol solution, put in digester, design temperature
70～80 DEG C, steaming and decocting 9～12h；
(2) after above-mentioned steaming and decocting terminates, naturally cool to room temperature, the cooking mixture in digester is filtered, collected
Filtrate, in mass ratio 2:5, filtrate are put in juice extractor with fresh aloe leaf and are squeezed the juice, and collect squeezeding juice, and will squeeze the juice
The 1.1mol/l hydrogen peroxide of liquid and its volume 10～15% is put in blender, stirs 30～50min with 200r/min；
(3) after above-mentioned stirring terminates, the mixture in blender is put in centrifuge, with 1200r/min centrifugation 10～
15min, collects supernatant, puts in vacuum concentration pot, vacuum is set as 0.08～0.09mpa, be concentrated into the 60 of original volume
～70%, collect concentrated solution, use quality fraction 40% citric acid solution adjusts ph to 6.0～6.5, obtains basic disinfectant solution；
(4) count by weight, take 40～45 parts of basic disinfectant solution, 12～16 parts of sterilized water, 7～9 part of 200 mesh mussel pearl
Powder, 3～6 parts of dodecylbenzene sodium sulfonate and 5～8 parts of potassium iodide, put in blender and stir, obtain disinfectant solution, extracting degreasing
Cotton balls is soaked in disinfectant solution, stands 40～50min, takes out the rayon balls after soaking, and is sterilized using ultraviolet sterilizing lamp
Sterilization, you can obtain long-acting medical disinfecting cotton ball.
The application process of the present invention: clean wound surface with clear water first, then long-acting medical disappeared with what the present invention was obtained
Malicious cotton balls wipes wound, after testing, wipes wound 3～5 times, and sterilization rate can reach 99～100%, no anaphylaxiss, at normal temperatures
After placing 60～90min, sterilization rate still can reach 80～90%.
Compared with additive method, Advantageous Effects are the present invention:
(1) the long-acting medical disinfecting cotton ball disinfectant solution that the present invention is obtained is not volatile, can reasonable holding concentration, Ke Yichang
Effect uses；
(2) the long-acting medical disinfecting cotton ball sterilization rate that the present invention is obtained is good, and human body is difficult allergy, non-stimulated to human body skin.
Specific embodiment
Count by weight, take 25～30 parts of Radixs Astragali, 18～22 parts of Rhizoma Chuanxiongs, 17～19 parts of Alumen and 60～70 parts of quality to divide
Several 15% ethanol solution, put into the Radix Astragali, Rhizoma Chuanxiong and Alumen in 80 DEG C of baking ovens first and 10～15min are dried, place into pulverizer
Middle pulverizing, crosses 200 mesh sieves, collects and sieves granule, and with mass fraction 15% ethanol solution, put in digester, design temperature
70～80 DEG C, steaming and decocting 9～12h；After above-mentioned steaming and decocting terminates, naturally cool to room temperature, the cooking mixture in digester is entered
Row filters, and collects filtrate, 2:5 in mass ratio, filtrate is put in juice extractor with fresh aloe leaf and is squeezed the juice, and collects and squeezes
Juice, and the 1.1mol/l hydrogen peroxide of squeezeding juice and its volume 10～15% is put in blender, stir 30 with 200r/min
～50min；After above-mentioned stirring terminates, the mixture in blender is put in centrifuge, with 1200r/min centrifugation 10～
15min, collects supernatant, puts in vacuum concentration pot, vacuum is set as 0.08～0.09mpa, be concentrated into the 60 of original volume
～70%, collect concentrated solution, use quality fraction 40% citric acid solution adjusts ph to 6.0～6.5, obtains basic disinfectant solution；Press
Parts by weight meter, take 40～45 parts of basic disinfectant solution, 12～16 parts of sterilized water, 7～9 part of 200 mesh mussel pearl powder, 3～6 part ten
Dialkyl benzene sulfonic acids sodium and 5～8 parts of potassium iodide, put in blender and stir, and obtain disinfectant solution, and extracting degreasing cotton balls is soaked in and disappears
In venom, stand 40～50min, take out the rayon balls after soaking, and use ultraviolet sterilizing lamp sterilizing, you can must be long
Effect medical disinfecting cotton ball.
Example 1
Count by weight, take 25 parts of Radixs Astragali, 18 parts of Rhizoma Chuanxiongs, 17 parts of Alumen and 60 parts of mass fraction 15% ethanol solution, first
The Radix Astragali, Rhizoma Chuanxiong and Alumen are put in 80 DEG C of baking ovens 10min is dried, place in pulverizer and pulverize, cross 200 mesh sieves, collected
Sieve granule, and with mass fraction 15% ethanol solution, put in digester, 70 DEG C of design temperature, steaming and decocting 9h；In above-mentioned steaming and decocting knot
Shu Hou, naturally cools to room temperature, and the cooking mixture in digester is filtered, collection filtrate, and 2:5 in mass ratio will
Filtrate is put in juice extractor with fresh aloe leaf and is squeezed the juice, and collects squeezeding juice, and by squeezeding juice and its volume 10%
1.1mol/l hydrogen peroxide is put in blender, stirs 30min with 200r/min；After above-mentioned stirring terminates, by blender
Mixture is put in centrifuge, is centrifuged 10min with 1200r/min, collects supernatant, puts in vacuum concentration pot, vacuum sets
Be set to 0.08mpa, be concentrated into the 60% of original volume, collect concentrated solution, use quality fraction 40% citric acid solution adjust ph to
6.0, obtain basic disinfectant solution；Count by weight, take 40 parts of basic disinfectant solution, 12 parts of sterilized water, 7 part of 200 mesh mussel pearl powder,
3 parts of dodecylbenzene sodium sulfonate and 5 parts of potassium iodide, put in blender and stir, and obtain disinfectant solution, and extracting degreasing cotton balls is soaked in
In disinfectant solution, stand 40min, take out the rayon balls after soaking, and use ultraviolet sterilizing lamp sterilizing, you can obtain long-acting
Medical disinfecting cotton ball.
The application process of the present invention: clean wound surface with clear water first, then long-acting medical disappeared with what the present invention was obtained
Malicious cotton balls wipes wound, after testing, wipes wound 3 times, and sterilization rate can reach 99%, and no anaphylaxiss are placed at normal temperatures
After 60min, sterilization rate still can reach 80%.
Example 2
Count by weight, take 30 parts of Radixs Astragali, 22 parts of Rhizoma Chuanxiongs, 19 parts of Alumen and 70 parts of mass fraction 15% ethanol solution, first
The Radix Astragali, Rhizoma Chuanxiong and Alumen are put in 80 DEG C of baking ovens 15min is dried, place in pulverizer and pulverize, cross 200 mesh sieves, collected
Sieve granule, and with mass fraction 15% ethanol solution, put in digester, 80 DEG C of design temperature, steaming and decocting 12h；In above-mentioned steaming and decocting
After end, naturally cool to room temperature, the cooking mixture in digester is filtered, collection filtrate, 2:5 in mass ratio,
Filtrate is put in juice extractor with fresh aloe leaf and is squeezed the juice, collect squeezeding juice, and by squeezeding juice and its volume 15%
1.1mol/l hydrogen peroxide is put in blender, stirs 50min with 200r/min；After above-mentioned stirring terminates, by blender
Mixture is put in centrifuge, is centrifuged 15min with 1200r/min, collects supernatant, puts in vacuum concentration pot, vacuum sets
Be set to 0.09mpa, be concentrated into the 70% of original volume, collect concentrated solution, use quality fraction 40% citric acid solution adjust ph to
6.5, obtain basic disinfectant solution；Count by weight, take 45 parts of basic disinfectant solution, 16 parts of sterilized water, 9 part of 200 mesh mussel pearl powder,
6 parts of dodecylbenzene sodium sulfonate and 8 parts of potassium iodide, put in blender and stir, and obtain disinfectant solution, and extracting degreasing cotton balls is soaked in
In disinfectant solution, stand 50min, take out the rayon balls after soaking, and use ultraviolet sterilizing lamp sterilizing, you can obtain long-acting
Medical disinfecting cotton ball.
The application process of the present invention: clean wound surface with clear water first, then long-acting medical disappeared with what the present invention was obtained
Malicious cotton balls wipes wound, after testing, wipes wound 5 times, and sterilization rate can reach 100%, and no anaphylaxiss are placed at normal temperatures
After 90min, sterilization rate still can reach 90%.
Example 3
Count by weight, take 28 parts of Radixs Astragali, 20 parts of Rhizoma Chuanxiongs, 18 parts of Alumen and 65 parts of mass fraction 15% ethanol solution, first
The Radix Astragali, Rhizoma Chuanxiong and Alumen are put in 80 DEG C of baking ovens 12min is dried, place in pulverizer and pulverize, cross 200 mesh sieves, collected
Sieve granule, and with mass fraction 15% ethanol solution, put in digester, 75 DEG C of design temperature, steaming and decocting 11h；In above-mentioned steaming and decocting
After end, naturally cool to room temperature, the cooking mixture in digester is filtered, collection filtrate, 2:5 in mass ratio,
Filtrate is put in juice extractor with fresh aloe leaf and is squeezed the juice, collect squeezeding juice, and by squeezeding juice and its volume 13%
1.1mol/l hydrogen peroxide is put in blender, stirs 40min with 200r/min；After above-mentioned stirring terminates, by blender
Mixture is put in centrifuge, is centrifuged 12min with 1200r/min, collects supernatant, puts in vacuum concentration pot, vacuum sets
Be set to 0.07mpa, be concentrated into the 65% of original volume, collect concentrated solution, use quality fraction 40% citric acid solution adjust ph to
6.3, obtain basic disinfectant solution；Count by weight, take 42 parts of basic disinfectant solution, 15 parts of sterilized water, 8 part of 200 mesh mussel pearl powder,
4 parts of dodecylbenzene sodium sulfonate and 7 parts of potassium iodide, put in blender and stir, and obtain disinfectant solution, and extracting degreasing cotton balls is soaked in
In disinfectant solution, stand 45min, take out the rayon balls after soaking, and use ultraviolet sterilizing lamp sterilizing, you can obtain long-acting
Medical disinfecting cotton ball.
The application process of the present invention: clean wound surface with clear water first, then long-acting medical disappeared with what the present invention was obtained
Malicious cotton balls wipes wound, after testing, wipes wound 4 times, and sterilization rate can reach 99.5%, and no anaphylaxiss are placed at normal temperatures
After 75min, sterilization rate still can reach 85%.
Claims (1)
1. a kind of preparation method of long-acting medical disinfecting cotton ball is it is characterised in that concrete preparation process is:
(1) count by weight, take 25～30 parts of Radixs Astragali, 18～22 parts of Rhizoma Chuanxiongs, 17～19 parts of Alumen and 60～70 parts of quality to divide
Several 15% ethanol solution, put into the Radix Astragali, Rhizoma Chuanxiong and Alumen in 80 DEG C of baking ovens first and 10～15min are dried, place into pulverizer
Middle pulverizing, crosses 200 mesh sieves, collects and sieves granule, and with mass fraction 15% ethanol solution, put in digester, design temperature
70～80 DEG C, steaming and decocting 9～12h；
(2) after above-mentioned steaming and decocting terminates, naturally cool to room temperature, the cooking mixture in digester is filtered, collected
Filtrate, in mass ratio 2:5, filtrate are put in juice extractor with fresh aloe leaf and are squeezed the juice, and collect squeezeding juice, and will squeeze the juice
The 1.1mol/l hydrogen peroxide of liquid and its volume 10～15% is put in blender, stirs 30～50min with 200r/min；
(3) after above-mentioned stirring terminates, the mixture in blender is put in centrifuge, with 1200r/min centrifugation 10～
15min, collects supernatant, puts in vacuum concentration pot, vacuum is set as 0.08～0.09mpa, be concentrated into the 60 of original volume
～70%, collect concentrated solution, use quality fraction 40% citric acid solution adjusts ph to 6.0～6.5, obtains basic disinfectant solution；
(4) count by weight, take 40～45 parts of basic disinfectant solution, 12～16 parts of sterilized water, 7～9 part of 200 mesh mussel pearl
Powder, 3～6 parts of dodecylbenzene sodium sulfonate and 5～8 parts of potassium iodide, put in blender and stir, obtain disinfectant solution, extracting degreasing
Cotton balls is soaked in disinfectant solution, stands 40～50min, takes out the rayon balls after soaking, and is sterilized using ultraviolet sterilizing lamp
Sterilization, you can obtain long-acting medical disinfecting cotton ball.
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| CN201610923009.9A CN106361920A (en) | 2016-10-29 | 2016-10-29 | Preparation method of long-acting medical disinfection cotton balls |
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| CN201610923009.9A CN106361920A (en) | 2016-10-29 | 2016-10-29 | Preparation method of long-acting medical disinfection cotton balls |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109505116A (en) * | 2018-11-07 | 2019-03-22 | 四川省遂宁市康达卫生材料有限公司 | A kind of production method of medical cotton ball |
| CN112370244A (en) * | 2020-11-24 | 2021-02-19 | 中南大学湘雅三医院 | Automatic pressing medical application and control method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1126523C (en) * | 2000-01-27 | 2003-11-05 | 杭州杨驰医疗用品有限公司 | Medical disinfecting cotton ball and its preparing method |
| CN201213842Y (en) * | 2008-06-11 | 2009-04-01 | 王艳 | Novel skin sterilizer |
| CN102258803B (en) * | 2011-07-20 | 2013-12-04 | 安立 | Long-acting medical skin sterilization cotton ball |
-
2016
- 2016-10-29 CN CN201610923009.9A patent/CN106361920A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1126523C (en) * | 2000-01-27 | 2003-11-05 | 杭州杨驰医疗用品有限公司 | Medical disinfecting cotton ball and its preparing method |
| CN201213842Y (en) * | 2008-06-11 | 2009-04-01 | 王艳 | Novel skin sterilizer |
| CN102258803B (en) * | 2011-07-20 | 2013-12-04 | 安立 | Long-acting medical skin sterilization cotton ball |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109505116A (en) * | 2018-11-07 | 2019-03-22 | 四川省遂宁市康达卫生材料有限公司 | A kind of production method of medical cotton ball |
| CN112370244A (en) * | 2020-11-24 | 2021-02-19 | 中南大学湘雅三医院 | Automatic pressing medical application and control method thereof |
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