CN106333907A - Bath crystal composition and preparation method thereof - Google Patents

Abstract

The invention relates to the bath appliance field, and specifically discloses a bath crystal composition, wherein the bath crystal composition comprises sodium sulfate, edible salt, plant extract, borax and alum; the plant extract includes 5 to 18 parts by weight of sophora flower/rose/Calendula officinalis/honeysuckle mixed extract; 1 to 5 parts by weight of lily extract; 0.1 to 2 parts by weight of Saussurea involucrata extract; 0.1 to 3 parts by weight of Rhodiola extract; 1 to 5 parts by weight of pomelo peel extract; 0.1 to 1 part by weight of grape seed extract; 0.01 to 0.1 part by weight of Roselle extract; 1 to 13 parts by weight of raw ginger extract; 1 to 10 parts by weight of wormwood extract; 1 to 5 parts by weight of Camellia extract; 1 to 10 parts by weight of aloe extract; 1 to 3 parts by weight of eucalyptus extract, 1 to 8 parts by weight of wolfberry extract, 0.01 to 0.5 part by weight of pseudo-ginseng flower extract and 0.05 part by weight of vanilla extract.

Description

Bath crystal composite and preparation method thereof

Technical field

The present invention relates to bath article field, and in particular to a kind of bath crystal composite, further relates to bathe the preparation of crystal composite Method.

Background technology

Now, each follow the fashion, beautiful girl, she when selecting article of everyday use, no longer merely values effect, and more note Their composition of weight.As exquisite nature of wearing the clothes, arbitrarily, article of everyday use then be particular about composition natural content." bath is brilliant " is then suitable Reason becomes the good merchantable brand of skin care with coming out as an article, because its natural composition, light fragrance, charming color, effect free from worldly cares, Become the skin protection new lover of beautiful girls.In many countries, people have been accustomed to being washed one's face with bath crystalline substance, foot bath, have a bath, reduce weight, strong While body, beauty treatment, improve life grade.

It is said that find earliest that " salt " have skin-care effect is European sailor.Though they tan by the sun for a long time in the sun, sea salt Cleaning and antiinflammation their skin can be made to get well in time state.Dutchman is inspired by this, taking from deep-sea Salt is refined into bath salt, people can be washed one's face with it, foot bath.Fact proved, the micro salinity in bath salt can promote skin newly old Metabolism, to skin sterilization, antiinflammatory, deoil, pore refining, make the soft and smooth exquisiteness of skin.Hong Kong skin protection expert it is further proposed that, use Bath salt is bathed just as having done a whole body massage.Because human body is just as a small power generation body, and salt is good electrolyte, will Body steeps in the water containing micro salinity, and the little electric field energy of formation produces to the peripheral nerve in skin and stimulates, thus promoting Blood circulation and metabolism.In the presence of this " electric field ", the dirt on horny layer and skin is more easy to fall off, benefits skin Cleaning and self renewal.

With growth in the living standard, people constantly strengthen to the maintenance consciousness of skin.Bath salt life in the market Produce high cost and single function is it is impossible to meet the demand of people well.Thus, it is brilliant that urgent need will develop a multi-functional bath Compositionss are meeting the demand of people.

Content of the invention

In order to solve the above problems, the invention provides a kind of bath crystal composite, in parts by weight, the brilliant combination of described bath Thing includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 5～18 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extraction Thing；The Bulbus Lilii extract of 1～5 weight portion；The Herba Saussureae Involueratae extract of 0.1～2 weight portion；The Radix Rhodiolae of 0.1～3 weight portion extracts Thing；The Pericarpium Citri grandis extract of 1～5 weight portion；The Proflavanol of 0.1～1 weight portion；The Hibiscus Sabdariffa Linn of 0.01～0.1 weight portion Extract；The Rhizoma Zingiberis Recens extract of 1～13 weight portion；The wormwood extract of 1～10 weight portion；The Flos Camelliae Japonicae of 1～5 weight portion extracts Thing；The Aloe extract of 1～10 weight portion, the eucalyptus extracts of 1～3 weight portion, the wolfberry fruit extract of 1～8 weight portion, 0.01 The pseudo-ginseng flower extract of～0.5 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

In a preferred embodiment, in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 8～15 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extraction Thing；The Bulbus Lilii extract of 3～5 weight portions；The Herba Saussureae Involueratae extract of 1～2 weight portion；The Radix Rhodiolae extract of 1～2 weight portion；2 The Pericarpium Citri grandis extract of～5 weight portions；The Proflavanol of 0.1～0.8 weight portion；The Hibiscus Sabdariffa Linn of 0.01～0.05 weight portion carries Take thing；The Rhizoma Zingiberis Recens extract of 1～10 weight portion；The wormwood extract of 4～7 weight portions；The Flos Camelliae Japonicae flower extract of 1～4 weight portion； The Aloe extract of 3～8 weight portions, the eucalyptus extracts of 1～3 weight portion, the wolfberry fruit extract of 2～7 weight portions, 0.01～ The pseudo-ginseng flower extract of 0.3 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

In a preferred embodiment, in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 10 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；5 The Bulbus Lilii extract of weight portion；The Herba Saussureae Involueratae extract of 1 weight portion；The Radix Rhodiolae extract of 2 weight portions；The Fructus Citri grandiss of 4 weight portions Peel extract；The Proflavanol of 0.5 weight portion；The Hibiscus Sabdariffa Linn extract of 0.05 weight portion；The Rhizoma Zingiberis Recens extract of 8 weight portions；6 The wormwood extract of weight portion；The Flos Camelliae Japonicae flower extract of 3 weight portions；The Aloe extract of 6 weight portions, the Eucalyptuss of 2 weight portions carry Take the Herba vanillae Planifoliae extract of thing, the wolfberry fruit extract of 5 weight portions, the pseudo-ginseng flower extract of 0.2 weight portion, 0.05 weight portion.

In a preferred embodiment, described edible salt is selected from: sea salt, lake salt, rock salt, well salt, bamboo salt, mineral Any one or a few mixing in salt, hot spring salt, Flos Rosae Rugosae salt, Truffe salt.

In a preferred embodiment, the carrying of described Flos Rosae Rugosae/Flos Sophorae/Calendula officinaliss flower/Flos Lonicerae mixed extract The method is taken to be:

(1) weigh: weigh dry Flos Rosae Rugosae, Flos Sophorae, Calendula officinaliss flower, Flos Lonicerae for 10:1:5:0.5 by weight, mix Grind into powder after conjunction；

(2) extract: the powder in step (1) adds refined honey to mix post-heating to 50 DEG C, is incubated 5h, with matter after cooling Measuring the ethanol that concentration is 60% is solvent, with ultrasonic extraction 2～5h, extracts 3 times, united extraction liquid, is concentrated into no after filtration Ethanol, obtains final product.

In a preferred embodiment, in described bath crystal composite, the extracting method of described Herba vanillae Planifoliae extract For:

Weigh Herba vanillae Planifoliae powder, add the ethanol that mass concentration is 95%, using extracting through microwave heating 2 after immersion 1～3h ～3 times, filter, filtrate, through being evaporated to no ethanol, obtains final product.

In a preferred embodiment, also include the quintessence oil of 0.5～1 weight portion in described bath crystal composite.

In a preferred embodiment, described quintessence oil is selected from: tea tree ethereal oil, orange blossom quintessence oil, rose ethereal oil, smokes clothing Any one or a few mixing in careless quintessence oil, jasmin quintessence oil.

Another aspect provides the preparation method of bath crystal composite, at least comprise the following steps:

(1) pulverize after sodium sulfate, edible salt mixing, with the sieve of 30～100 mesh, obtain component a；

(2) by after plant extract mix homogeneously, at 30～50 DEG C, stir 1～10h, obtain component b；

(3) component a and component b are mixed at 20～35 DEG C, be stirred until homogeneous, obtain final product.

The another aspect of the present invention provides the bath application in bath article field for the crystal composite.

It is more readily understood the above-mentioned of the application and other features, aspect and advantage with reference to described further below.

Specific embodiment

The embodiment of the participation in the election detailed description being preferable to carry out method of the invention below and inclusion can be more easily understood this Bright content.Unless otherwise defined, all technology used herein and scientific terminology have common with art of the present invention The identical implication that technical staff is generally understood that.When there is contradiction, the definition in this specification is defined.

As used herein term " by ... preparation " synonymous with "comprising".Term "comprising" used herein, " inclusion ", " having ", " containing " or its any other deformation it is intended that cover non-exclusionism inclusion.For example, comprise the combination of listed elements Thing, step, method, product or device are not necessarily solely those key elements, but can include not expressly listed other key elements or This kind of compositionss, step, method, product or the intrinsic key element of device.

Conjunction " Consists of " excludes any key element do not pointed out, step or component.If be used in claim, this Phrase will make claim be closed so as to not comprise the material in addition to the material that those describe, but relative normal Except rule impurity.When phrase " Consists of " occurs in and is rather than immediately following after theme in the clause of claim main body, It is only limited to the key element described in this clause；Other key elements are not excluded outside as overall described claim.

Equivalent, concentration or other value or parameter are excellent with scope, preferred scope or a series of upper limit preferred value and lower limit During the Range Representation that choosing value limits, this is appreciated that and specifically discloses by any range limit or preferred value and any scope All scopes that arbitrary pairing of lower limit or preferred value is formed, regardless of whether whether this scope separately discloses.For example, when open During scope " 1 to 5 ", described scope should be interpreted as including scope " 1 to 4 ", " 1 to 3 ", " 1 to 2 ", " 1 to 2 and 4 to 5 ", " 1 to 3 and 5 " etc..When numerical range is herein described, unless otherwise indicated, otherwise this scope is intended to include its end Value and all integers within the range and fraction.

Singulative includes plural number and object is discussed, unless the context clearly dictates otherwise." optional " or " arbitrarily A kind of " refer to that the item describing thereafter or event may or may not occur, and this description include event generation situation and The situation that event does not occur.

Approximate term in specification and claims is used for modifying quantity, represents that the present invention is not limited to this concrete Quantity, also includes the part of the correction of acceptable change without lead to related basic function close to this quantity.Phase Answer, modify a numerical value with " about ", " about " etc., mean and the invention is not restricted to this exact numerical.In some examples, approximately Term likely corresponds to the precision of the instrument of measured value.In present specification and claims, scope limits permissible Combination and/or exchange, these scopes include all subranges contained therebetween if not stated otherwise.

Additionally, the quantitative requirement to key element or component for the indefinite article " a kind of " and " one " before key element of the present invention or component (i.e. occurrence number) unrestriction.Therefore " one " or " a kind of " should be read as including one or at least one, and odd number The key element of form or component also include plural form, unless the obvious purport of described quantity refers to singulative.

In order to solve the above problems, the invention provides a kind of bath crystal composite, in parts by weight, the brilliant combination of described bath Thing includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 5～18 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extraction Thing；The Bulbus Lilii extract of 1～5 weight portion；The Herba Saussureae Involueratae extract of 0.1～2 weight portion；The Radix Rhodiolae of 0.1～3 weight portion extracts Thing；The Pericarpium Citri grandis extract of 1～5 weight portion；The Proflavanol of 0.1～1 weight portion；The Hibiscus Sabdariffa Linn of 0.01～0.1 weight portion Extract；The Rhizoma Zingiberis Recens extract of 1～13 weight portion；The wormwood extract of 1～10 weight portion；The Flos Camelliae Japonicae of 1～5 weight portion extracts Thing；The Aloe extract of 1～10 weight portion, the eucalyptus extracts of 1～3 weight portion, the wolfberry fruit extract of 1～8 weight portion, 0.01 The pseudo-ginseng flower extract of～0.5 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

In a preferred embodiment, in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 8～15 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extraction Thing；The Bulbus Lilii extract of 3～5 weight portions；The Herba Saussureae Involueratae extract of 1～2 weight portion；The Radix Rhodiolae extract of 1～2 weight portion；2 The Pericarpium Citri grandis extract of～5 weight portions；The Proflavanol of 0.1～0.8 weight portion；The Hibiscus Sabdariffa Linn of 0.01～0.05 weight portion carries Take thing；The Rhizoma Zingiberis Recens extract of 1～10 weight portion；The wormwood extract of 4～7 weight portions；The Flos Camelliae Japonicae flower extract of 1～4 weight portion； The Aloe extract of 3～8 weight portions, the eucalyptus extracts of 1～3 weight portion, the wolfberry fruit extract of 2～7 weight portions, 0.01～ The pseudo-ginseng flower extract of 0.3 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

In a preferred embodiment, in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 10 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；5 The Bulbus Lilii extract of weight portion；The Herba Saussureae Involueratae extract of 1 weight portion；The Radix Rhodiolae extract of 2 weight portions；The Fructus Citri grandiss of 4 weight portions Peel extract；The Proflavanol of 0.5 weight portion；The Hibiscus Sabdariffa Linn extract of 0.05 weight portion；The Rhizoma Zingiberis Recens extract of 8 weight portions；6 The wormwood extract of weight portion；The Flos Camelliae Japonicae flower extract of 3 weight portions；The Aloe extract of 6 weight portions, the Eucalyptuss of 2 weight portions carry Take the Herba vanillae Planifoliae extract of thing, the wolfberry fruit extract of 5 weight portions, the pseudo-ginseng flower extract of 0.2 weight portion, 0.05 weight portion.

Sodium sulfate

In the present invention, described " sodium sulfate " can be Disodium sulfate decahydrate also known as Natrii Sulfas, the thin anhydride of high-purity, granule Referred to as Matrii Sulfas Exsiccatus.Profile is colourless, transparent, big crystallization or graininess little crystallization.

In the present invention, described " sodium sulfate " can also be dehydration sodium sulfate.

In the present invention, described " sodium sulfate " primarily serves the effect of carrier.

In the present invention, described " sodium sulfate " is commercially available acquisition.

Edible salt

In the present invention, described " edible salt " is water white transparency；Generally white or canescence, translucent.Tool hyaloid Gloss.Body is heavier, and matter is hard, easily smashes.Feeble QI, salty in the mouth.Dew puts the easy deliquescence of in the air.Water can be dissolved in, insoluble in ethanol, colourless Burn on flame, flame is in foresythia.So that color is white, pure, free from admixture person is preferred.

Wherein, " detailed outline " is recorded: " the salty raw meat of abnormal smells from the patient of salt, the blood also salty raw meat of people, salty flavor acting on blood, unsuitable for blood disease to treat with salty drugs, polyphagia is then Arteries and veins coagulates weeps and variable color, from its class.Boiling salt person, receives it with Fructus Gleditsia.Therefore the taste micro-pungent of salt, pungent walk lung, salty walk kidney, breathe heavily cough, edema, The person of quenching one's thirst, salt is to avoid greatly, or draws expectorant and tell, or tears blood vessels, or help pathogenic water therefore.So salt is the master of all kinds of diseases and ailments, all kinds of diseases and ailments invariably with it, therefore Take the kidney invigorating pharmaceutical salts soup person, salty return kidney, it is dirty that priming gas enters this；Reinforcing the heart is medicinal to fry salt person, and the bitter void of the heart is with salty benefit；Spleen reinforcing medicine With frying salt person, reinforcing the mother-organ for treating deficiency of the son-organ, spleen is the son of the heart；Control the person of accumulation tuberculosis use, salt energy softening the hard mass；All carbuncle eyes and disorders of blood With person, salty flavor acting on blood；The person of all wind heat disease use, cold prevailing over heat；The person of defecation disease use, salty energy relaxing the bowels with lubricant drugs；Osteopathia tooth disease is used Person, kidney governing bones, salty to the marrow；The person of insect bite use, takes its removing toxic substances."

" Chongqing hall random notes " are recorded: " saline taste is the most salty, taste over-salty i.e. thirsty person, levying of dry liquid, both can do liquid, then saline taste belongs to Fire is undoubtedly.Though but taste belong to fire and property is descending, hyperactivity of deficient fire person, drink dilute salt water drop, therefore for guiding fire to origin quality goods.Tell nosebleed more than Person, salt brine leaching foot is healed."

In the present invention, the main component of described " edible salt " edible salt is sodium chloride, contains a small amount of moisture content and impurity simultaneously And the element such as other ferrum, phosphorus, iodine.

In a preferred embodiment, described edible salt is selected from: sea salt, lake salt, rock salt, well salt, bamboo salt, mineral Any one or a few mixing in salt, hot spring salt, Flos Rosae Rugosae salt, Truffe salt.

Described sea salt can also be able to be dead sea salts selected from the sea salt of any one commercially available brand.

In the present invention, the preparation method of the sea salt that can enumerate produces sea salt for solarization method.

Solarization method produce crude salt, its technological process be generally divided into receive tide, brewed brine, crystallization, receive the big operation of salt four.

(1) receive tide

Exactly using tidal motion, the sea water of high for off-lying sea salinity is pushed extract to salt manufacturing raw material during coastal waters.At present, employing Damp mode of receiving has two kinds, and one is that nature receives tide, and two is that power receives tide.Naturally tide of receiving is to allow sea water natural along drawing tidal creek at the incoming tide Flow into；Power is received tide and is typically introduced sea water using axial-flow pump, is characterized in not limited by natural conditions.

(2) brewed brine

Brewed brine is to carry out in the evaporation tank of vast area, according to every daily evaporation amount, suitably grasps evaporation tank and walks the depth of water Degree, makes bittern concentration step up, is finally condensed into saturation halogen.

(3) crystallize

In continuous evaporating concentration process, various salt densities constantly increase sea water, when salt density reaches saturation, salt Just separated out with crystal form, supersaturated solution constantly maintains solution degree of supersaturation, crystal just can continued growth.

(4) receive salt

By the salt growing up to, sticked together using manually or mechanically packing up heap.

What in the present invention, sea salt can be enumerated originates in Liaoning, Hebei, Shandong, Jiangsu, Zhejiang, Fujian, Guangdong, Guangxi, platform Gulf etc. is it is also possible to originate in external.

In the present invention, the lake salt being used is all achievable present invention of any one lake salt of commercially available acquisition.

In the present invention, the lake salt being used can also make acquisition by oneself, it is possible to use method commonly used in the art prepares, The method that can enumerate has: attack method, beach solarization method etc..

Attack method: lake is evaporated through long-term, Sodium chloride deposit lakebed, is not required to can directly fish for through processing.As bavin reaches The salt lake on tub ground, changed after tens million of years；Define dry lake, its salt is exposed to surface.Various places are at present with Salt miner or adopt salt Ship is produced, and its technological process is substantially: stripping covering and adopts salt pipeline (or automobile conveying) washing, takes off Water one belt feeder conveys a finished product salt people and sticks together.Shine method as beach similar with Salt production technique.

In the present invention, the well salt being used is all achievable present invention of any one well salt of commercially available acquisition, preferably certainly Gongjing salt.

In the present invention, the well salt being used can also make acquisition by oneself, it is possible to use method commonly used in the art prepares, The preparation of well salt mainly includes adopting halogen and two links of salt manufacturing.Different ore deposit types adopts halogen method using different.Extract natural halogen Method have that bailing method, gas lift method, oil pumping adopt halogen, the methods such as halogen are adopted in deep-well Submerged bittern pump, blowing.

Rock salt in the present invention, bamboo salt, mineral salt, hot spring salt, Flos Rosae Rugosae salt, Truffe salt are all commercially available.

Plant extract

In the present invention, described " plant extract " includes: the Flos Rosae Rugosae/Flos Sophorae/Calendula officinaliss flower/gold silver of 5～18 weight portions Flower mixed extract；The Bulbus Lilii extract of 1～5 weight portion；The Herba Saussureae Involueratae extract of 0.1～2 weight portion；0.1～3 weight portion Radix Rhodiolae extract；The Pericarpium Citri grandis extract of 1～5 weight portion；The Proflavanol of 0.1～1 weight portion；0.01～0.1 weight The Hibiscus Sabdariffa Linn extract of part；The Rhizoma Zingiberis Recens extract of 1～13 weight portion；The wormwood extract of 1～10 weight portion；1～5 weight portion Three Flos Camelliae Japonicae extracts；The Aloe extract of 1～10 weight portion, the eucalyptus extracts of 1～3 weight portion, the Fructus Lycii of 1～8 weight portion Extract, the pseudo-ginseng flower extract of 0.01～0.5 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

Flos Rosae Rugosae

In the present invention, described " Flos Rosae Rugosae " is flower to be dried slightly become hemispherical or irregular bulk, 1.5～2 centimetres of diameter.Flower Lobe is intensive, short and justify, and color is purplish red and bright-coloured, and central authorities are yellow pistil, and green calyx is arranged at bottom, and its tip splits into 5.Lower end There is the holder expanding planet-shaped.Light weight and crisp.Gas Li is aromatic strongly fragrant, mildly bitter flavor.With piece big, lobe is thick, color is purple, bright-coloured, the dense person of fragrance It is preferred.

Flos Rosae Rugosae contain volatile oil, interior master (linalool) containing linalool, linalool formic acid esters (linalyl formate), β-citronellol (β-citronellol), geraniol formate (citronellyl formate), geraniol acetate (citronellyl acetate), geraniol (geraniol), gemic acid formic acid esters (geranyl formate), cattle Youngster's acid acetass (geranyl acetate), phenethanol (phenylethanol), nerol (nerol) and 3- methyl isophthalic acid- Butanol (3-methyl-1-butanol), trauls-ss-Ocimene (trans β-ocimene), pentadecane (pentadecane), 2- Tridecane ketone (2-tridecanone), l- amylalcohol (1-pentanol), l- hexanol (1-hexanol), 3- hexenol (- Hexenol), Exceed 600 (hexyl acetat), acetic acid -3- hexene ester (3-hexenyl acetate), benzyl alcohol (benzyl alcohol), eugenol (eugenol), methyleugenol (methyl eugenol) etc..The volatilization of pollen Composition is: 6- methyl -5 hepten-2-one (6-methyl-5-hepten-2-one), geranyl acetate, neral (neral), geranial (geranial), geraniol, citronellic acid acetass, neryl acetate (neryfacetate), Cattle benzylacetone (geranyl acetone), pentadecane, methyln nonyl ketone (2-undecanone), methyl n-undecyl ketone, 2- 15 Alkanone (2-pentadecanone), myristic aldehyde (tetradecanal), hexadecanyl aldehyde (hexadecanal), the acetic acid tetradecane Alcohol ester (tetradecyl acetate) bata-phenethyl alcohol, eugenol, methyleugenol, acetic acid-bata-phenethyl alcohol ester (β- phenylethyl acetate).The micro constitutent that Flos Rosae Rugosae fragrance is played an important role is: β-damascone (β-damascone), Rose oxide (roseoxide), a- common perilla alkene (a-naginatene).Flower also (quercetin) containing Quercetin, the double glycoside of Centaurea cyanus (cyanin), organic acid, beta-carotene (β-carotene), fatty oil etc..Holder contains tannin compositions: Flos Rosae Rugosae tannin (rugosin) a, b, c, d, e, f, g, casurin strictinin), different 1-O-Galloyl-4,6-hexahydroxydiphenoyl-beta-D-glucose (isostrictinin), long stalk horse Semen Oroxyli element (pedunculagin), Casuarina equisetifolia L. tan booth (casuarictin), new suona horn element (tellimagrandin) and, 1, 2,3- tri--o- galloyl glucoses (1,2,3-tri-o-galloyl- β-d-glucose), 1,2,6- tri--o- nutgall acyl Glucose (1,2,6-tri-o-galloyl- β-d-glucose)；Wherein Pedunculagin and new suona horn element i tool anti-retrovirus Effect.Fruit (citric acid) containing citric acid, malic acid (malic acid), quininic acid (quinic acid), ascorbic acid (ascorbic acid), Quercetin, isoquercitin (isoquercetin), Phytoxanthine (phytoxanthin), rubixanthin (rubixanthin), lycopene (lycopene), gamma carotene (γ-carotene), glucose (glucose), Fructose (fructose), xylose (xylose), sucrose (sucrose) etc..Contain the unsaturated fatty acid of many stars in seed oil, and contain β-paddy Sterol (β-sitosterol).Seed contains vitamin (vitamin) e and f.Stem and leaf contains Quercetin, the flavone such as globulariacitrin (rutin) Class compound.Leaf contains isoquercitin, the flavones ingredient such as apigenin (apigenin) and 6- de-methoxy -4-o- methyl Herba Artemisiae Scopariae color Former ketone (6-demethoxy-4-o-methylcapillarisin), 6- de-methoxy capillarisin (6- The chromogen ketones component such as demethoxycapillarisin).Again containing multiple sesquiterpenoidss compositions: Flos Rosae Rugosae terpene aldehyde (rugosal) a, D, table Flos Rosae Rugosae terpene aldehyde (epirugosal) d, roseolic acid (rugosic acid) a, b, c, d, Isosorbide-5-Nitrae-Radix Dauci Sativae two olefine aldehydr (carota- L, 4-dienal), Isosorbide-5-Nitrae-Radix Dauci Sativae dienoic acid (carota-1,4-dienoic acid), Flos Rosae Rugosae commiferin (bisaborosaol) a, b1, b2, c1, c2, d, e1, e2, f2, Hamann draws uncommon acid (hamanasic acid) a, Radix Dauci Sativae olefine aldehydr (dancenal), epoxy Radix Dauci Sativae olefine aldehydr (epoxydaucenal) a, b, different Radix Dauci Sativae olefine aldehydr (isodaucenal), different daucene Sour (isodaucenoic acid), 11,12- dehydrogenations Radix Dauci Sativae olefine aldehydr (11,12-dehydrodaucenal), 11,12- dehydrogenations are recklessly Radix Raphani olefin(e) acid (11,12-dehydrodaucenoic acid), hydroxyl different Radix Dauci Sativae olefin(e) acid (hydroxyisodaucenal), different Hu Radix Raphani olefin(e) acid (isodaucenol), Rhodinol (carotarosal) a, Flos Rosae Rugosae helicene ketone (rosacorenone), Flos Rosae Rugosae helicene alcohol (rosacorenol), disconnected Rhodinol (secocarotanal), daucene (daucene), different daucene (isodaucene), Isosorbide-5-Nitrae-Radix Dauci Sativae diene (carota-l, 4-diene), 3 (4), 8 (15)-acoradienes [accra-3 (4), 8 (15)-diene], 3 (4), 7 (8)-acoradienes (acora3 (4), 7 (8)-diene].Also contain lactone component: 4-hydroxyl-cis- cinnamic acid 22 Alcohol ester (4-hydroxy-cis-cinnamic acid docpsul ester), 4-hydroxyl-2,3- dihydro cinnamic acid 25 Alcohol ester (4-hydroxy-2,3-dihydrocinnamic acid pentacosyl ester), 4-hydroxyl-cis- cinnamic acid Hexacosyl alcohol ester (4-hydroxy-cis-cinnamic acid hexacosyl ester), 4-hydroxyl-cis- cinnamic acid two Octadecane ester (4-hydroxy-cis-cinnamic acid octacosyl ester).Root ambiguous skin element, cachou extract (catechin), daucosterol (daucosterol), campesterol glycoside (campesterol glucoside), mound of entrusting Dish acid -28-o- glucose ester glycoside (tormentic acid 28-o-glucoside), wild refined Chinese toon acid -28-o- glucose ester glycoside (euscaphicacid 28-o-glucoside), different arjunolic acid -28-o- glucose ester glycoside (aujunic acid 28- o-glucoside).

Flos Sophorae

In the present invention, described " Flos Sophorae " crimps for many shrinkages, is scattered petal more.Complete person's Calyx mitriform, yellow green, first 5 are held shallow to split；Petal 5, yellow or yellow-white, 1 larger, subcircular, tip nick, remaining 4 Long Circle；Stamen 10, wherein 9 Individual base portion joint, filigree is elongated；Gynoecium is cylindrical, bending.With individual big, tighten, yellow skin is green, no stalk leaf person is preferred.

Flos Sophorae is essentially identical with Flos Sophorae Immaturus ingredient, and main soap containing triterpene becomes: Semen Phaseoli Saponin (azukisaponin), , soyasaponinss (soyasaponin) i, Flos Sophorae Saponin (kaikasaponin),.Also contain flavonoid: Quercetin (quercetin), globulariacitrin (rutin), isorhamnetin (isorhamnetin), isorhamnetin-3-rutinoside (isorhamnetin-3-rutinoside), kaempferol -3- rutinoside (kaempferol-3-rutinoside).Contain white again Pine gum alcohol (betulin), sophoradiol (sophoradiol).(lauric acid) containing lauric acid in caul-fat, dodecenoic acid (dodecenoic acid), myristic acid (myristic acid), tetradecenoic acid (tetradecenoic acid) 14 Carbon dienoic acid (teradecadienoic acid), Palmic acid (palmitic acid), hexadecenoic acid (hexadecenoic Acid), stearic acid (stearic acid), octadecadienoic acid (octadecadienoic acid), ten make carbon trienic acid (octadecatrienoic acid), the fatty acid such as arachidic acid (arachidic acid) and cupreol (β- Sitosterol), separately contain tannin.

Calendula officinaliss are spent

In the present invention, described " Calendula officinaliss flower " be annual or more year SHENGCAO this, high 30-60cm, Herb has undercoat.Stem is straight Vertical, there is vertical rib, branch is arranged at top.Single leaf alternate；Inferior leads cochlear, full edge；Upper leaf oblong extremely long ellipticity obovate, Long 5-9cm, wide 1-2cm, tip is blunt or sharp, and base portion is slightly heart-shaped, slightly embraces stem, edge full edge or the sparse serration of tool.Head Inflorescence list is born in an end, diameter 2.5-5cm, has stalk；Involucre has bract 1-2 layer, and bract is linear, and tip is tapering, edge film quality；Tongue Shape flower yellow or crocus, female, 1-2 layer, breeds, tongue piece full edge or tip 3 fissure；Guan Guanhua both sexes, do not breed, sliver 5, Style does not split.Achene is long compared with bract, and inside hook is bent, and back has flakey tuck crape, and both sides have the narrow wing；No pappus.Florescence 4-7 Month.

Flower (stismasterol) containing stigmasterol, cupreol (β-silosterol), campesterol (campesterol), cholesterol (cholesterol), 24- methylenecholesterol (24-methylenecholesterol), 4 Beta-methyl Ergota steroid -7,24 (28)-diene -3 β -ol [4 β-methyler-gasta-7,24 (28)-diene-3 beta -ol], methyl Sterol (methyl sterol), avenasterol (avenasterol), α-Amyrin (α-amyrin), β-Amyrin, Pu Herba Taraxaci sterol (taraxasterol), ψ-taraxasterol (ψ-taraxasterol), lupeol (lupeol), elemi resin Alcohol (brein), Calendula officinaliss glycol (calenduladiol), Arnica (srnidiol), faradiol (faradiol), Usu enediol (ursa-diol).Erythrodiol (erythrodiol), maniladiol (manilladiol), lupene three Alcohol (lupenetriol), Ladanum triol (heliantriol) f, c, Usu alkene triol (ursatriol), longispinogenin (longispinogenine), p-hydroxy Benzoic Acid (phydroxybenzoic acid), p-coumaric acid (p-coumaric ), acid gentisic acid (gen-tisic acid), vanillic acid (vanillic acid), syringic acid (syringic acid), coffee Sour (caffeic acid), o- hydroxyl phenylacetic acid (o-hydroxyphenyl acetic acid), salicylic acid (salicylic ), acid protocatechuic acid (protocatechuic acid), umbelliferone (umbelliferone), horse chestnut bark glycoside (esculetin), scopoletin (scopoletin), Calendula officinaliss florigen (calendin), the double rhamnoside of Calendula officinaliss flavone (calendoflaside), Calendula officinaliss flavonoid glycoside (calendoflavoside), demethyl Calendula officinaliss flavonoid glycoside (calendoflavobioside), narcissin (narcissoside, narcissin), Quercetin (quercetin), isoquercitrin Glycoside (isoquercetin), rutinoside (rutinoside), isorhamnetin (isorhamnetin), isorhamnetin -3-o- Portugal Grape glucoside (isorhamnetin-3-o-glucoside), quercetin glucoside (quercetin glucoside), Cortex querci dentatae Element -2g- rhamanopyranosyl rutinoside (quercetin-2g-rhamnosylrutlnoside), Quercetin -3-o- new dried orange peel glycoside (quercetin-3-o-neohesperidoside), isorhamnetin -3-o- α-l- rhamnopyranosyl (1 → 2)-o [α-l- pyrrole Mutter rhamanopyranosyl (1 → 6)]-β-d- glucopyanoside.

Flos Lonicerae

Flos Lonicerae is the flower that caprifoliaceae plant Radix Ophiopogoniss (lonicerajaponicathunb) dry flower or band are just opened, and is Conventional Chinese medicine, has the effect of heat-clearing and toxic substances removing, wind-heat dissipating, cures mainly carbuncle, sore throat, erysipelas, toxic-heat and blood stasis, anemopyretic cold, temperature The diseases such as disease heating, applicating history is long.From Tang Materia Medica to " Wenbing Tiaobian, Detailed Analysis of Epidemic Warm Diseases ", until " the Chinese medicine sea " of modern publishing etc., in Medical science is progressively goed deep into the research of Flos Lonicerae, and application is more and more wider.Flos Lonicerae heat-clearing and toxic substances removing, performance is led off, thoroughly dissipates pathogenic factor in the exterior, often with The partner treatment affection due to external wind and heat such as Fructus Forsythiae, Fructus Arctii, Herba Schizonepetae or epidemic febrile disease from the beginning of.As anemopyretic cold, influenza, mumps, spring-warm syndrome, autumn Temperature etc. symptoms include heating slight chill, head-body-pain, chickenpox initial stage.

Flos Lonicerae and its congener pharmacological research show, its have antibacterial, antiviral, antipyretic, antiinflammatory, liver protection, Hemostasis, antioxidation etc. act on.

Chemical constitution study about Flos Lonicerae shows, Flos Lonicerae is rich in volatile oil (linalool, Flos Lonicerae alcohol etc.), additionally Containing chemical compositions such as organic acid (chlorogenic acid, isochlorogenic acid, caffeic acid, Palmic acid etc.), flavonoid, saponinss.

In a preferred embodiment, the carrying of described Flos Rosae Rugosae/Flos Sophorae/Calendula officinaliss flower/Flos Lonicerae mixed extract The method is taken to be:

(1) weigh: weigh dry Flos Rosae Rugosae, Flos Sophorae, Calendula officinaliss flower, Flos Lonicerae for 10:1:5:0.5 by weight, mix Grind into powder after conjunction；

(2) extract: the powder in step (1) adds refined honey to mix post-heating to 50 DEG C, is incubated 5h, with matter after cooling Measuring the ethanol that concentration is 60% is solvent, with ultrasonic extraction 2～5h, extracts 3 times, united extraction liquid, is concentrated into no after filtration Ethanol, obtains final product.

Bulbus Lilii

In the present invention, described " Bulbus Lilii " is perennial herb, high 70-150cm.Purple fringe, no hair are had on stem；Bulb ball Shape, diameter about 5cm, bulb lobe is extensively opened up, and no saves, white.Leaf is scattered, has short handle；Upper leaf is often less than middle leaf, and blade drapes over one's shoulders pin Shape to obovate, long 7-10cm, wide 2-3cm, the anxious point of tip, narrow, full edge, no hair more than base portion, have 3-5 bar arteries and veins.1-4, flower, loudspeaker Shape, savory；Tapel 6, obovate, long 15-20cm, wide 3-4.5cm, mostly white, back side band puce, immaculate, Tip is curved and do not roll up, nectary both sides have papilla；Stamen 6, antecurvature, the long 9.58-11cm of filigree, have pubescence, flower pesticide is ellipse Circle, T-shaped raw, pollen grain maroon；The long cylindricality of ovary, is about 3.5cm, the long 11cm of style, no hair, and stigma 3 splits.Capsule Long Circle, is about 5cm, wide about 3cm, has rib.Seed is most.Flower, the fruiting period 6-9 month.2. tiger lily perennial herb, high 1-1.5m. Bulb oval shape oblate spheroid, high 4-7cm, diameter 5-8cm.Stem is upright, and lavender, by white MIAOMAO.Leaf alternate, stockless；Blade Lanceolar or long round shape lanceolar, long 5-20cm, wide 0.5-2cm, gradually little one-tenth bracteal upwards, often there are atropurpureuss in the axil of top Bulbil.3-6 or more, flower, is born in proximal portion, sagging, Chinese red, by white MIAOMAO during alabastrum；Tapel lanceolar is outside Warp, inner face close by atropurpureuss speckle；Stamen 6, is shorter than perianth, flower pesticide purple；Ovary is about 1.5cm, and stigma 3 splits, purple.Capsule Fruit Long Circle to obovate, long 3-4cm.Seed is most.The month at florescence 6-7, the fruiting period 8-10 month.3. Bulbus lilii concoloris perennial herb, high 20- 60cm.Bulb cone or long avette, diameter 1.8-3.5cm, tool thin film, cuiller Long Circle or long avette, long 2-3.5cm, wide 0.7-1.2cm, white.Leaf scattered in the middle part of stem, stockless；Blade bar shaped, long 3-10cm, wide 1-3mm, no hair, the sharp point of tip, base Portion is tapered, has 1 obvious arteries and veins.Spend one to several, be born in stem top or between the axil of stem end, bow vertical, cerise or aubergine；Flower By piece 6, long 3-4.5cm, wide 5-7mm, interior tapel is slightly wider, warp, immaculate or have minority speckle, and there is mamillary on nectary both sides Projection；Stamen 6, is shorter than perianth, filigree no hair, flower pesticide oblong, yellow, the red pollen grain of tool；Ovary is cylindrical, is about 9mm, style is longer 1.5-2 times than ovary.Capsule Long Circle.The month at florescence 7-8, the fruiting period 8-10 month.4. Bulbus Lilii perennial herb is high About 1.5m.Bulb is spherical, diameter 2-4cm, white.Stem is upright, has kick or sparse bright and beautiful hair.Leaf is scattered, and middle part is intensive；Leaf Piece bar shaped, long 6-10cm, wide 2-3mm, two sides no hair, edge warp simultaneously has obvious papilla, has white at axil MIAOMAO, middle arteries are obvious.Hua Dansheng or 2-8 becomes total shape arrangement, sagging, orange-yellow, diameter 5-8cm；The long 3-6cm of bennet, tool drapes over one's shoulders The lobate bract of aciculiform；Tapel 6, Long Circle, long 4-6cm, wide 1cm, outside warp, have a purple dot, the dilute silk floss of outer mask Hair, nectary both sides tool hair and papillae；Filigree no hair, flower pesticide Long Circle, long 1.4-1.6cm, pollen depth Chinese red；Style 2 times of a length of ovary.Capsule oblong, long 3.5cm, diameter 1.7-2cm.The month at florescence 7-8, fruiting period September.

Lily bulb Bulbus Lilii containing Ming River glycoside (regaloside) a, d, 3,6'-o- bis- Resina Ferulae acyl sucrose (3,6'-o- Diferuloylsucrose), 1-o- Resina Ferulae acyl glycerol (1-o-feruloylglycerol), 1-o- p- coumaric acyl glycerol (1- O-p-coumaroylglycerol), 26-o- β-d- glucopyranosyl-slave's Ah's ruscogenin -3-o- α-l- rhamnopyranosyl - (1 → 2)-β-d- glucopyanoside-β-d-glucopyranoside), 26-o- β-d- glucopyranosyl-slave's Ah's Saponin Unit's -3-o- α-l- rhamnopyranosyl-(1 → 2)-o- [β-d- glucopyranosyl (1 → 4)]-β-d- glucopyanoside.

In a preferred embodiment, the extracting method of described Bulbus Lilii extract is: take the Bulbus Lilii that 10g is dried, plus Enter refined honey, after soaking 2h, with white vinegar as solvent, at 20 DEG C, extracting through microwave heating 5 times, filters, filtrate is through being evaporated to no White vinegar, obtains final product.

Term " refined honey " refers to: Mel is put in pot, after being heated to slowly seething with excitement, uses slow fire instead, keep micro-boiling, and remove Foam and floating waxiness, then filter off dead honeybee, impurity with sieve sieve or gauze, then are poured in pot, be heated to 100 DEG C -118 DEG C, full Pot plays flake bubble, with the toughness of handss sth. made by twisting, when there is no long white silk to occur between two fingers, takes the dish out of the pot rapidly.

Herba Saussureae Involueratae

In the present invention, described " Herba Saussureae Involueratae " is Saussurea laniceps perennial herb, high 15-30cm.Rhizome is thick, and cervical region is brown Color row deposit petiole.Stem is sturdy, and uprightly, white close MIAOMAO is arranged at top.Leaf is extremely intensive, blade lanceolar or cochlear, long 8-15cm, Wide 1.5-2cm, tip is slightly sharp, base portion gradually narrow one-tenth petiole, and there is wavy sawtooth at edge, has spider's thread shape MIAOMAO above, after gradually come off, under The close raw brown fine hair in face.Head inflorescence is most, no obstructs, lines up oval spike on stem top；Bract strip lanceolar is white Close MIAOMAO；Involucre is hemispherical；Outer layer phyllary strip lanceolar, is about 2.5cm, and tip length is tapering, has white close MIAOMAO, internal layer Phyllary lanceolar, top strip length is tapering, has pitchy to become mildewed；Floral white, long 10-12mm, eaves portion is cylindric, long about cylinder Three times of portion.Achene is about 3mm；Pappus pitchy, outer layer is short, coarse wool shape, easy to fall off, internal layer featheriness.Florescence 6-7.

Saussurea laniceps herb (scopoletin) containing scopoletin, umbelliferone (umbelliferone), p- hydroxyl Benzoylformaldoxime (p-hy-droxyacetophenone), positive hentriacontane (n-hentriacontane), physcione , and cupreol (β-istosterol) (physcion).

In a preferred embodiment, the extracting method of described Herba Saussureae Involueratae extract is: takes the Herba Saussureae Involueratae that 10g is dried Flower, add refined honey, soak 2h after, with mass concentration be 75% ethanol as solvent, at 20 DEG C, extracting through microwave heating 5 times, mistake Filter, filtrate, through being evaporated to no ethanol, obtains final product.

Radix Rhodiolae

In the present invention, described " Radix Rhodiolae " is perennial herb, all close by white or faint yellow long pubescence, high by 10～25 Centimetre.The normal hollow of stem, bar-shaped, base portion has brownish black remaining blade.Leaf alternate, intensive, stockless, lanceolar or narrow obovate, long 2 ～10 centimetres, wide 0.5～1.5 centimetre, edge plumage split or tool bastard, close by white villus.Head inflorescence is most, intensive, often 15～25 millimeters of sequence length；The long and narrow lanceolar of phyllary, is about 12 millimeters, wide about 2 millimeters, no hair, glossy, central herbaceous stem, Edge film quality, has 3 obvious longitudinal veins；Flower both sexes, are all tubular flower, are about 1 centimetre, uprightly, corolla pipe is isometric with eaves portion, splits Piece lanceolar；Flower pesticide base portion flechette-type；Style is linear.Achene, is about 7 millimeters, and flat, brown has unconspicuous 4 ribs；Pappus 2 Layer, outer layer pappus is shorter, upper tool undercoat, and internal layer is pinniform.6～July of florescence.

Apigenin -7-o- beta -d-glucose- glycoside is mainly contained in the extract of Radix Rhodiolae, glucopyanoside, apigenin - 7-o- α-l- rhamnopyranosyl (1 → 2)-β d- glucopyanoside, Quercetin -3-o- β-d- glucopyanoside (quercetin-3-o- β-d-glucopyranoside), apigenin (apigenin), luteolin (luteolin), Fructus Arctii Glycoside (arctiin).

In a preferred embodiment, the extracting method of described Radix Rhodiolae extract is: take the Radix Rhodiolae that 8g is dried, With mass concentration be 40% ethanol soak 2h after, then with mass concentration be 80% ethanol as solvent, extracting through microwave heating 5 Secondary, filter, filtrate, through being evaporated to no ethanol, obtains final product.

Pomelo peel

In the present invention, described " pomelo peel " is grapefruit peel, and grapefruit peel is the peel of Citrus paradisi Macfadyen.Qiu Mo, winter Just collect, cut open into the peel that is dried of 5～7 lobes, the skin graft diameter after elongation is about 25～32 centimetres, 10～13 lis of every single-lobe length Rice, wide 5～7 centimetres, thick 0.5～1 centimetre.Skin graft edge curls slightly inward；Outer surface yellowish-brown or withered yellow, are in micro- gold sometimes Yellow, extremely rough, there is the oil drop of most recessed round dots and projection；Inner surface white, is in slightly flocculence.Matter is soft, has dense Fructus Citri grandiss fragrance.

In a preferred embodiment, the extracting method of described Pericarpium Citri grandis extract is: takes the pomelo peel that 5g is dried It is dried after being soaked using vinegar, then with water as solvent, at 50 DEG C, extracting through microwave heating 5 times, filters, filtrate is through concentrating under reduced pressure To anhydrous, obtain final product.

Semen Vitis viniferae

" Semen Vitis viniferae " of the present invention is powder.Described Semen Vitis viniferae powder is commercially available acquisition.

Hibiscus Sabdariffa Linn

In the present invention, described " Hibiscus Sabdariffa Linn " also known as Calyx Hibisci Sabdariffae, the annual upright draft of Calyx Hibisci Sabdariffae, up to 2m.Stem lavender, No hair.Leaf abnormity；The long 2-8cm of petiole, thin villosity；Stipule is linear, is about 1cm, thin villosity；The leaf of bottom is avette, Do not divide, leaf palmate 3 drastic crack on top, sliver lanceolar, long 2-8cm, wide 5-15mm, have sawtooth, tip is blunt or tapering, base portion Circular to wide wedge shape, two sides all no hairs；Master pulse 3-5 bar, back side middle rib has gland.Hua Dan is born in axil, closely no obstructs；Squamella 8-12 Redness, meat, lanceolar, long 5-10mm, wide 2-3mm, dredge by long bristle, nearly top has thorn-like appurtenance, base portion and calyx symphysis； Calyx cup-shaped, lavender, diameter about 1cm, dredge and pierced and coarse wool, symphysis at base portion 1/3, sliver 5, the tapering shape of triangular shape, long 1- 2cm；Flower yellow, inner face base portion peony, diameter 6-7cm.Capsule ovoid, diameter about 1.5cm, close by coarse wool.Seed kidney shape, No hair.Summer at florescence, autumn.

In a preferred embodiment, the extracting method of described Hibiscus Sabdariffa Linn extract is: takes the Lip river god that 10g is dried Flower, add refined honey, soak 2h after, with mass concentration be 80% ethanol as solvent, extracting through microwave heating 5 times, filter, filtrate warp It is evaporated to no ethanol, obtain final product.

Rhizoma Zingiberis Recenss

In the present invention, described " Rhizoma Zingiberis Recenss " are perennial herb, high 50-80cm.Rhizome is plump, and section yellow-white has dense Acrid odors.Leaf alternate, lines up 2 row, stockless, several armfuls of stems；The long 2-4mm of the tip of a leaf；Blade lanceolar is to wire lanceolar, long 15-30cm, wide 1.5-2.2cm, tip is tapering, and base portion is narrow, and leaf leather sheath shape embraces stem, no hair.Scape is extracted out from rhizome, long 15- 25cm；Spike is oval, long 4-5cm；Bract is avette, is about 2.5cm, light green, edge is faint yellow, and tip has little point Head；Calyx tube is about 1cm, has 3 short pointed tooths；Corolla yellow green, pipe range 2-2.5cm, sliver 3, lanceolar, long too late 2cm, lip The long round shape of middle sliver fall ovum open, short compared with corolla lobe, have purple fringe and faint yellow speckle, two side slivers are avette, yellowish green Color, has purple edge；Stamen 1, mulberry, flower pesticide is about 9m, and connective appendage wraps style；Ovary 3 Room, no hair, style 1, stigma is subsphaeroidal.Capsule.Seed is most, black.Florescence August.

In a preferred embodiment, the extracting method of described Rhizoma Zingiberis Recens extract is: weighs the Rhizoma Zingiberis Recenss that 7g is dried, powder Broken, add the white vinegar that mass concentration is 40%, soak after 1～3h using extracting through microwave heating 2-3 time, filter, filtrate is through reducing pressure It is concentrated into no white vinegar, obtain final product.

Folium Artemisiae Argyi

In the present invention, described " Folium Artemisiae Argyi " is also called Folium Artemisiae Argyi, Chinese mugwort, Radix Artemisia ordosicae, family Chinese mugwort.

Folium Artemisiae Argyi shrinkage, crushes, has short handle.It is in ovate-elliptic after intact leaf flattening, pinniform is molten to be split, and sliver ellipticity is draped over one's shoulders Aciculiform, there are irregular rough sawn tooth, upper surface celadon work dark yellow-green in edge, has sparse pubescence and gland point, the close life of lower surface Canescence fine hair.Matter is soft.Gas delicate fragrance, bitter in the mouth.With leaf thickness, color green grass or young crops, back side canescence, fine hair are many, matter is soft, the person of giving off a strong fragrance It is preferred.

In wormwood extract, containing 2- methyl butanol (2-methylbutanol), 2- olefine aldehydr (2-hexenal), suitable Formula -3- alkene -1- alcohol (cis-3-hexene-1-ol), tricyclene (tcmlibicyclene), α-thujene (α-thujene), Australene (α-pinene), lauro lene (camphene), sabinene (sabinene), nopinene (β-pinene), 1-OCOL (1-octen-3-ol), 2,4 (8)-p- Meng's diene [2,4 (8)-pinthadiene], cymol (p-cymene), 1, 8- Folium eucalypti globueli (Eucalyptus globulus Labill.) is mutual (1,8-cineole), γ-terpinene (γ-terpinene), artemisol (artemisia alcohol), α Oleum Pini Alkene (α-terpinene), dimethyl styrene (dimethylstyrene), Camphora (camphor), Borneolum Syntheticum (borneol), Isoborneol (dioborneol), 4- terpinenol (terpinen-4-ol), p- poly- umbrella flower-α -ol (p-cymen- α-ol), α- Terpineol, cis piperitol, cordovan orders oxalene ketone, myrtanol, trans small jar menthol, trans noon reed alcohol, cis-fragrant reed Alcohol, acetic acid-cis -3- enol ester, p- propylbenzyl aldehyde, Eucarvone (carvone), fragrant reed ketenes (carvenone), Perillaldehyde (perillaldehyde), borneol acetate (bornyl acetate), perilla alcohol (perilla-al-cohol) is fragrant Herba Schizonepetae phenol (carvacrol), eugenol (eugenol), (king is ancient) (king's bar) alkene (copaene), the other alkene of beta waves (β- Borbonene), β-sill perfume alkene (β-elemene), methyleugenol (methyleugenol), trans-Flos Caryophylli alkene, β-gold closes Joyous alkene, oxalene (humulene), β-Fructus Canarii albi alkene (β-maaliene), trans-β-farnesene (tcmlibans- β- Farnescene), β-selinene (β-selinene), γ-muurolene (γ-muurolene), γ-elemene (γ- Elemene), α-muurolene, propanoic acid orange blossom alcohol ester (neryl propionate), ξ-cadinene, Flos Caryophylli olefinic oxide, cough Alcohol (ledol), pentadecane aldehyde (pentadecanal), hexahydro farnesene benzylacetone, o- phthalic acid dibutyl ester, brown sample Acid etc..

In a preferred embodiment, the extracting method of described wormwood extract is: weigh the Folium Artemisiae Argyi that 15g is dried, Pulverize, add the ethanol that mass concentration is 70%, soak after 1～3h using extracting through microwave heating 2-3 time, filtration, filtrate is through subtracting Pressure is concentrated into no ethanol, obtains final product.

Flos Camelliae Japonicae

In the present invention, described " Flos Camelliae Japonicae " is alabastrum oval, and open flower is in irregularly flat plate-like, disk footpath 5-8cm.Table Flushing color, yellowish-brown or sepia, sepal 5, brownish red, keratin, gather canescence spun silk sample fine hair at the back side；Petal 5-7 Or more, top oval, tip nick, bottom color is deeper, and base portion is integrated, papery；Stamen is most, 2 wheels, and foreign steamer is spent Silk is integrated.Feeble QI, sweet in the mouth.With color red, do not open person be preferred.

Flower (anthocyanin) containing anthocyanin, grey glycoside (leucoan-thocyanin), globulariacitrin (rutin), Rhizoma Kaempferiae Phenol -3-o- rutinoside (kaempferol-3-o-rhamnoglucoside), myricetin -3-o- glycoside (myricetin-3-oglucoside), cyanidin -3- galactoside (cyanidin-3-galactoside), Centaurea cyanus Element -3- glycoside (cyanidin-3-glucoside), cyanidin -3- (6- p-coumaroyl) glycoside (cyanidin-3-o- β-d (6-o-p-coumaroyl) glucoside] it is hyacinth glycoside (hyacinthin), Quercetin (quercetin), nimbecetin (kaempferol), 3,4,5,7- tetrahydroxys -8- methoxy flavone (sexangularetin), right Hydroxy benzoic acid (p-hydroxybenzoic acid), protocatechuic acid (protocatechuic acid), gallic acid (gallic acid) and 3 beta-hydroxy -28- nor- olive -17- alkene -16- ketone -12,13- epoxide (3 β-hydroxy- 28-norolean-l7-en-16-on-12,13-epoxide), Flos Camelliae Japonicae diketoalcohol (camellendionol), Flos Camelliae Japonicae ketone two Alcohol (camellenodiol), the triterpenes components such as horse auspicious glycoside unit (maragenin).Tannin containing Herba Diclipterae Chinensises (gemin) d length again Stalk aristin (peduncula-gin), new miterwort element (tellimagrandin), Flos Camelliae Japonicae tannin (camelliin) a and b Etc. tannin and a- chondrillasterol (a-spinasterol), cupreol-d- glycoside, stigmasterol-d- glycoside (stigmasteryl-d-glucoside), bean steroid -7- alkene -3 β -ol.Near get again tsubakisaponin (camellidin),. Also contain Theobromine.

In a preferred embodiment, the extracting method of described Flos Camelliae Japonicae flower extract is: weighs 10g Flos Camelliae Japonicae, cuts Broken, add the ethanol that mass concentration is 60%, soak after 1～3h using extracting through microwave heating 2-3 time, filter, filtrate is through reducing pressure It is concentrated into no ethanol, obtain final product.

Aloe

In the present invention, described " Aloe " is Liliaceae drought tolerance herbaceous plant, and scientific name is aloevera, is distributed mainly on non- The ground such as continent, have the effect of antibacterial, antiinflammatory and relieving constipation, are usually used in treating liver-heat, flatulence, constipation, headache, exudative dermatitis and calculus etc.. Polysaccharide and anthraquinones rich content in fresh aloe, are chief active positions.Aloe gel contains substantial amounts of saccharide Composition, is different types of glucomannoglycan mostly, and wherein acetylizad mannan has higher biological activity.The other containing Monosaccharide is then common arabinose, galactose, glucose, mannose and rhamnose etc..Being distributed in subcutaneous anthraquinones more In palisade tissue, based on barbaloin and aloe-emodin, they are partly combined into glycoprotein with polysaccharide, partly in the form of enzyme Exist, such as hydroxyl peptidase, peroxidating oxygenase, cellulase and superoxide dismutase etc., in Aloe, also contain lactic acid, succinum Acid, malic acid, P-coumaric acid, succinic acid and citric acid etc..

In a preferred embodiment, the extracting method of described Aloe extract is: 10g fresh aloe is cleaned Afterwards, shred, mass concentration be 50% ethanol in soak 2h, then using water as solvent, use ultrasonic extraction 3-5h, extract 3 Secondary, united extraction liquid, it is concentrated into anhydrous after filtration, obtain final product.

Eucalyptuss

In the present invention, described Eucalyptuss are Myrtaceae cup fruit tree genus, umbrella room belongs to and the general designation of eucalyptus, and original producton location prints The ground such as Buddhist nun and Australia.Eucalyptuss have many types, for example, have arid sclerophyll high forest type, moistening sclerophyll arbor type, dilute Tree Types of Grassland, arid sclerophyll arbor type, mesophorbium, coryphile type.

What the species of described " Eucalyptuss " can be enumerated has: Eucalyptus globulus Labill, directly dry Eucalyptus globulus Labill, eucalyptus citriodora, Folium Eucalypti Robustae, sight blade profile copper coin Eucalyptus globuluss, Eucalyptus urophylla, alpine ash, gray gum, Eucalyptus globulus Labill, E. dunnii, Liu An, tail alpine ash, Eucalyptus urophylla-grandis, tail Eucalyptus eamalducensis Dehnd．, tail Eucalyptus eamalducensis Dehnd．, Eucalyptus eamalducensis Dehnd．, Dunne Eucalyptus globuluss etc..

Macrocarpal (macrocarpal) a, b, c, d, e, Tritriacontane -16,18- diketone (n- is contained in eucalyptus leaveses Tritriacontane-16,18-dione), contain Eucalyptus globulus Labill aldehyde (euglobal) in leaf and alabastrum, in leaf, also contain flavonoid Compound: Quercetin (quercetol is quercetin), quercitrin (querictrin), globulariacitrin (rutin), hyperin (hyperoside), quercetin glucoside (quercetol-3-glucoside), and gallic acid (gallic acid), Caffeic acid (caffeic acid), ferulic acid (ferulic acid), gentisic acid (gallic acid), protocatechuic acid (protocate-chuic acid).5,4- dihydroxy -7- methoxy flavone (5,4- is contained in the wax on blade face Dihydroxy-7-methoxy-6-methylflavone), chrysin (chrysin), Eucalyptin (eucalyptin), 8- goes Methyl Eucalyptin (8-demethyleu-calyptin), and 4,5- dihydroxy -7- methoxyl group -6,8- dimethyl flavone (sideroxylin).In leaf by hair oil master (cineole) containing cineole, separately have Flos Caryophylli alkene (caryophyllene).Bark Be separated to tritriacontane -16,18- diketone, 3-o- methyl benzoaric acid -4- rhamnoside (3-o- in xylem Methylellagic acid-4-rhamnoside), benzoaric acid (ellagic acid) and ellagitannin (el- lagitannin).

In a preferred embodiment, the extracting method of described eucalyptus extracts is: weighs weight than for 1:50 altogether Mixed eucalyptus citriodora leaveves and the powder of Folium Eucalypti Robustae leaveves, addition mass concentration is 60% ethanol, using microwave heating after immersion 3h Extract 3 times, filter, filtrate, through being evaporated to no ethanol, obtains final product.

Fructus Lycii

In the present invention, described " Fructus Lycii " is lycium barbarum.

The mature fruit of lycium barbarum (betane) containing glycine betaine, atropine (atcmlibopine), hyoscyamine (gyoscyamine).Contain Semen Maydiss Huang matter, physalin, kryptoxanthin (cryptosxanthin), scopoletin again (scopo-letin), carotene, thiamine, riboflavin, nicotinic acid, vitamin c.Seed contains aminoacid: aspartic acid, dried meat ammonia Acid, alanine, leucine, Phenylalanine (pheny-lalanine), serine (serine), glycine, glutamic acid (glutamic acid), cysteine (cysteine), lysine (lysine), arginine (arginine), isoleucine (isoleucine), threonine (threonine), histidine, cruel propylhomoserin, tryptophan, Methionine (methionine).Also contain The elements such as potassium, calcium, sodium, zinc, ferrum, copper, chromium, strontium, lead, nickel, cadmium, cobalt, magnesium.Separately contain the polysaccharide that tool promotes immunization, content is 7.09%.Contain taurine, γ-aminobutyric acid again.

The mature fruit of congener Fructus Lycii contains glycine betaine, Semen Maydiss Huang matter) zeax-anthin), physalin (physalien), also contain aminoacid: leucine (leucine), L-Valine (valine), proline (proline), alanine (alanine), tyrosine (tyro-sine), L-Glutamine (glutamine), glycine (glycine), glutamic acid (glutaminc acid), aspartic acid (sapartic acid), agedoite (asparagine), histidine (histideine), tryptophan (tcmlibyptophan).Again containing volatile ingredient, mainly safranal (safranal), Alpha, beta-lonone (β-, 3- hydroxy-beta-ionoionone (3-hydroxy- β-ionone), left-handed 1,2- dehydrogenation-α-Rhizoma Cyperi alkene (1,2-dehydrox- α-cyperene), Rhizoma Solani tuber osi spiral shell dienone (solavetivone).Another report, 100g fruit contains Radix Dauci Sativae Plain (carotene) 3.39mg, thiamine (thiamine) 0.23mg, riboflavin (* riboflavine) 0.33mg, nicotinic acid (nicotinic acid) 1.7mg, vitamin (vi-tamin) c3.0mg.Seed oil-containing, wherein non-saponified portions contain multiple Sterol: belong to 4- demethyl sterols has cholesterol (cholesterol), 7- cholestenol (cholest-7-enol) vegetable oil steroid Alcohol (campesterol), 24- methylenecholesterol (24-methylenecholesterol), isofucosterol (isofucoterol), stigmasterol (isofucosterol), stigmasterol (stig-masterol), cupreol (β- Sitosterol), 24-lhnhad-5,24- cholestadienol, 24- ethyl-cholestadienol (24-ethyl-cholesta-5, 24-dienol), Dihydrocholesterol (cholestanol), 24- methylcholestane alcohol (24-methylcholestanol), 24- second Base -22- cholestenol (24-ehtylcholest-22-enol)；Belong to 4- methyl sterol alcohols has 31- demethyl cycloartane Alcohol (31-norcycloartanol), 31- demethyl cycloartenol (31-norcycloartenol), cycloeucalenol (cycloeucalenol), 31- demethyl -8- lanostenol (31-norlanost-8-enol), 4 α, 14 α, 24- front three Base -8,24- cholestadienol, 31- demethyl -9 (11)-lanostenol [24-methyl-31-norlanost-9 (11) - Enol], 4 Alpha-Methyls, -8- cholestenol (4 α-methylcholest-8-enol), 4- methyl -7- cholestenol (4- ), methylcholest-7-enol 4- methyl -24 ethyl -7- cholestenol (24-ethylolphenol), 4,24- dimethyl - Cholestenol (4,24-methyllophenol), grass sterol, citrostadienol (citcmlibostadienol), 4 α, 24- methyl 7,24- cholestadienol (α, 24-dimethylcholesta-7,24-dienol (, 4 Alpha-Methyl ethyl -7,24- gallbladder Steroid dienol, 4,4- dimethylsterols classes have a 8- lanostenol (lanost-8-enol), ring wood Herba Spinaciae trailing plants alkanol (cycloartanol), cycloartenol (cycloartenol), lanosterol (lanosterol), β-Amyrin (β- Amyrin), lupeol, 24- methylene -8- lanostenol, 24- methylene basic ring wood Herba Spinaciae trailing plants alkanol etc..

In a preferred embodiment, the extracting method of described wolfberry fruit extract is: the Fructus Lycii that 15g is dried, plus Enter refined honey, after soaking 5h, with water as solvent, at 50 DEG C, extracting through microwave heating 3 times, filters, filtrate is through being evaporated to no Water, obtains final product.

Term " refined honey " refers to: Mel is put in pot, after being heated to slowly seething with excitement, uses slow fire instead, keep micro-boiling, and remove Foam and floating waxiness, then filter off dead honeybee, impurity with sieve sieve or gauze, then are poured in pot, be heated to 100 DEG C -118 DEG C, full Pot plays flake bubble, with the toughness of handss sth. made by twisting, when there is no long white silk to occur between two fingers, takes the dish out of the pot rapidly.

Flower of Radix Notoginseng

In the present invention, described " flower of Radix Notoginseng ", cry Radix Notoginseng again, sweet in the mouth, cool in nature, there are flat liver improving eyesight, promoting the production of body fluid to quench thirst, heat clearing away solution Malicious the effect of.

In a preferred embodiment, the extracting method of described pseudo-ginseng flower extract is: the flower of Radix Notoginseng that 5g is dried, With water as solvent, at 80 DEG C, extracting through microwave heating 3 times, filters, filtrate is anhydrous through being evaporated to, and obtains final product.

Herba vanillae Planifoliae

In the present invention, described " Herba vanillae Planifoliae ", it is a kind of perennial climbing vine plant, be in typical Tropical rain forest Plant large-scale orchid family spice berry.Stem slightly plumpness or meat, often save raw 1 piece of leaf and 1 aerial root.Ye great, meat, have short handle, have When deteriorate to flakey.Raceme is born in axil, and tool number flower is to spending more；Spend generally larger, reverse, often ovary and perianth it Between have 1 absciss layer；Sepal is similar to petal, from life, launches；The Chang Yurui post edge symphysis of hypochil edge, symphysis part sometimes Several reach whole stamen column length, thus lip is in often horn-like, and front portion does not conform to first portion and often expands, and 3 split sometimes.Fruit is pod Shape, meat, does not ftracture or ftractures.The thick episperm of seed tool, is in often black, aptery.

Vanilla Bean contain vanillin (or claim vanillon) and carbon hydrocarbon compound, alcohols, carboxyl compound, esters, The 150-170 kind composition such as phenols, acids, 2, 2-Oxydiphenol class and heterocyclic compound.The seed of vanilla contains:

1st, volatile oil composition: vanilla, vanillic acid, cephrol, Acetovanillone, cinnamic acid, cinnamyl alcohol, methyl cinnamic acid Ester, myristic acid, anisic acid, anise alcohol, Fructus Foeniculi methyl ester, guaiacol, 4- methyl guaiacol and 4, hydroxy benzaldehyde.

2nd, glucosides constituents: glucovanillin glycosides, vanillic acid glucoside, guaiacyl-beta -d-glucose- glycosides, right Tolyl-beta -d-glucose- glycosides, phenethyl -2- glucoside, p-nitrophenyl glucoside etc..The extract of vanilla also contains Have: ethyl vanillin ether, methyl Rhizoma et radix valerianae ether, to hydroxybenzyl ethyl ester etc..

In a preferred embodiment, the extracting method of described Herba vanillae Planifoliae extract is: weighs the Rhizoma et radix valerianae that 5g is dried Orchid, chopping, add the ethanol that mass concentration is 65%, soak after 1～3h using extracting through microwave heating 2～3 times, filter, filtrate Through being evaporated to no ethanol, obtain final product.

Borax

In the present invention, described " Borax ", structural formula is na₂b₄o₇·10h₂O, is very important containing boron mineral and boronation Compound.It is usually the white powder containing clear crystal, soluble in water.

In the present invention, Borax can play the effect of anti-inflammation and sterilization, and in the present invention, Borax can be risen with plant extract To interacting, further enhancing its bactericidal effect.

Alumen

In the present invention, described " Alumen " is also called Alumen, arcanite, potassium aluminium alum, potassium alum, and composition is 12 hydrazine aluminum sulfates Potassium, is the double salt of the potassium sulfate containing water of crystallization and aluminum sulfate.Colourless cubic crystal, appearance often be in octahedron, or with cube, Granatohedron forms combinate form, is sometimes invested with { 111 } face and is similar to six square plate shapes on chamber wall, belongs to α type Alumen class multiple Salt, has glassy lustre.Density 1.757g/cm3,92.5 DEG C of fusing point.Lose 9 molecular crystalline water when 92.5 DEG C, lose when 200 DEG C 12 molecular crystalline water, are dissolved in water, insoluble in ethanol.Alumen nature and flavor are sour and astringent, tremble with fear, poisonous.Therefore have antibacterial action, astriction Deng can be used as Chinese medicine.

The present inventor is found surprisingly that, after ethanol extraction long-time placement in bath crystal composite of single Flos Rosae Rugosae The situation of inefficacy occurs, leads to the shelf-life bathing crystal composite shorter, affect using effect.But by Flos Rosae Rugosae/Flos Sophorae/gold After small cup Flos Chrysanthemi/Flos Lonicerae mixture mixed extraction, can solve the problem that shelf-life shorter, the unstable technology of Flos Rosae Rugosae extract is asked Topic.The present inventor speculate its may the reason for Flos Sophorae, Calendula officinaliss flower, ethanol extraction and Flos Rosae Rugosae extract can in Flos Lonicerae To interact, forming the structure of similar complex, have adjusted the ph value in compositionss simultaneously, stoping its hydrolysis, thus extending Shelf-life, improve stability.

Embodiment

Embodiment 1: embodiments of the present invention 1 provide a kind of bath crystal composite, in parts by weight, described bath is brilliant Compositionss include,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 5～18 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extraction Thing；The Bulbus Lilii extract of 1～5 weight portion；The Herba Saussureae Involueratae extract of 0.1～2 weight portion；The Radix Rhodiolae of 0.1～3 weight portion extracts Thing；The Pericarpium Citri grandis extract of 1～5 weight portion；The Proflavanol of 0.1～1 weight portion；The Hibiscus Sabdariffa Linn of 0.01～0.1 weight portion Extract；The Rhizoma Zingiberis Recens extract of 1～13 weight portion；The wormwood extract of 1～10 weight portion；The Flos Camelliae Japonicae of 1～5 weight portion extracts Thing；The Aloe extract of 1～10 weight portion, the eucalyptus extracts of 1～3 weight portion, the wolfberry fruit extract of 1～8 weight portion, 0.01 The pseudo-ginseng flower extract of～0.5 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

Embodiment 2: embodiment 2 is identical with embodiment 1, and difference is, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 8～15 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extraction Thing；The Bulbus Lilii extract of 3～5 weight portions；The Herba Saussureae Involueratae extract of 1～2 weight portion；The Radix Rhodiolae extract of 1～2 weight portion；2 The Pericarpium Citri grandis extract of～5 weight portions；The Proflavanol of 0.1～0.8 weight portion；The Hibiscus Sabdariffa Linn of 0.01～0.05 weight portion carries Take thing；The Rhizoma Zingiberis Recens extract of 1～10 weight portion；The wormwood extract of 4～7 weight portions；The Flos Camelliae Japonicae flower extract of 1～4 weight portion； The Aloe extract of 3～8 weight portions, the eucalyptus extracts of 1～3 weight portion, the wolfberry fruit extract of 2～7 weight portions, 0.01～ The pseudo-ginseng flower extract of 0.3 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

Embodiment 3: embodiment 3 is identical with embodiment 1, and difference is, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 10 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；5 The Bulbus Lilii extract of weight portion；The Herba Saussureae Involueratae extract of 1 weight portion；The Radix Rhodiolae extract of 2 weight portions；The Fructus Citri grandiss of 4 weight portions Peel extract；The Proflavanol of 0.5 weight portion；The Hibiscus Sabdariffa Linn extract of 0.05 weight portion；The Rhizoma Zingiberis Recens extract of 8 weight portions；6 The wormwood extract of weight portion；The Flos Camelliae Japonicae flower extract of 3 weight portions；The Aloe extract of 6 weight portions, the Eucalyptuss of 2 weight portions carry Take the Herba vanillae Planifoliae extract of thing, the wolfberry fruit extract of 5 weight portions, the pseudo-ginseng flower extract of 0.2 weight portion, 0.05 weight portion.

Embodiment 4: embodiment 4 is identical with embodiment 1, and difference is, described edible salt is selected from: sea salt, lake Any one or a few mixing in salt, rock salt, well salt, bamboo salt, mineral salt, hot spring salt, Flos Rosae Rugosae salt, Truffe salt.

Embodiment 5: embodiment 5 is identical with embodiment 1, and difference is, described Flos Rosae Rugosae/Flos Sophorae/Calendula officinaliss The extracting method of flower/Flos Lonicerae mixed extract is:

(1) weigh: weigh dry Flos Rosae Rugosae, Flos Sophorae, Calendula officinaliss flower, Flos Lonicerae for 10:1:5:0.5 by weight, mix Grind into powder after conjunction；

(2) extract: the powder in step (1) adds refined honey to mix post-heating to 50 DEG C, is incubated 5h, with matter after cooling Measuring the ethanol that concentration is 60% is solvent, with ultrasonic extraction 2～5h, extracts 3 times, united extraction liquid, is concentrated into no after filtration Ethanol, obtains final product.

Embodiment 6: embodiment 6 is identical with embodiment 1, and difference is, the extraction of described Herba vanillae Planifoliae extract Method is:

Weigh Herba vanillae Planifoliae powder, add the ethanol that mass concentration is 95%, using extracting through microwave heating 2 after immersion 1～3h ～3 times, filter, filtrate, through being evaporated to no ethanol, obtains final product.

Embodiment 7: embodiment 7 is identical with embodiment 1, and difference is, also includes in described bath crystal composite The quintessence oil of 0.5～1 weight portion.

Embodiment 8: embodiment 8 is identical with embodiment 1, and difference is, described quintessence oil is selected from: tea tree ethereal oil, Any one or a few mixing in orange blossom quintessence oil, rose ethereal oil, Herba Lysimachiae foenum-graeci quintessence oil, jasmin quintessence oil.

Embodiment 9: embodiment 9 provides the preparation method bathing crystal composite described in embodiment 1～8, its feature It is, at least comprise the following steps:

(1) pulverize after sodium sulfate, edible salt mixing, with the sieve of 30～100 mesh, obtain component a；

(2) by after plant extract mix homogeneously, at 30～50 DEG C, stir 1～10h, obtain component b；

(3) component a and component b are mixed at 20～35 DEG C, be stirred until homogeneous, obtain final product.

Embodiment 10: embodiment 10 provides bath crystal composite described in embodiment 1～8 in bath article field Application.

Below by embodiment, the present invention is specifically described.Be necessary it is pointed out here that, following examples are only used In the invention will be further described it is impossible to be interpreted as limiting the scope of the invention, professional and technical personnel in the field Some the nonessential improvement made according to the content of the invention described above and adjustment, still fall within protection scope of the present invention.

In addition, if not having other explanations, raw materials used is all commercially available, and number used by following material is weight Part.

Embodiment 1

Embodiments of the invention 1 provide a kind of bath crystal composite, and in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 5 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；5 weights The Bulbus Lilii extract of amount part；The Herba Saussureae Involueratae extract of 0.1 weight portion；The Radix Rhodiolae extract of 0.1 weight portion；The Fructus Citri grandiss of 5 weight portions Sub- peel extract；The Proflavanol of 0.1 weight portion；The Hibiscus Sabdariffa Linn extract of 0.1 weight portion；The Rhizoma Zingiberis Recens extract of 1 weight portion； The wormwood extract of 10 weight portions；The Flos Camelliae Japonicae flower extract of 1 weight portion；The Aloe extract of 10 weight portions, the Eucalyptuss of 1 weight portion Extract, the wolfberry fruit extract of 8 weight portions, the pseudo-ginseng flower extract of 0.01 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

Extracting method:

The extracting method of Flos Rosae Rugosae/Flos Sophorae/Calendula officinaliss flower/Flos Lonicerae mixed extract is:

(1) weigh: weigh dry Flos Rosae Rugosae, Flos Sophorae, Calendula officinaliss flower, Flos Lonicerae for 10:1:5:0.5 by weight, mix Grind into powder after conjunction；

(2) extract: the powder in step (1) adds refined honey to mix post-heating to 50 DEG C, is incubated 5h, with matter after cooling Measuring the ethanol that concentration is 60% is solvent, uses ultrasonic extraction 5h, extracts 3 times, united extraction liquid, be concentrated into no second after filtration Alcohol, obtains final product.

The extracting method of Bulbus Lilii extract is:

Take the Bulbus Lilii that 10g is dried, add refined honey, after soaking 2h, with white vinegar (Zhenjiang white vinegar) as solvent, at 20 DEG C, micro- Wave heating extracts 5 times, filters, and filtrate, through being evaporated to no white vinegar, obtains final product.

The extracting method of Herba Saussureae Involueratae extract is:

Take 10g be dried Herba Saussureae Involueratae, add refined honey, soak 2h after, with mass concentration be 75% ethanol as solvent, 20 At DEG C, extracting through microwave heating 5 times, filters, filtrate, through being evaporated to no ethanol, obtains final product.

The extracting method of Radix Rhodiolae extract is:

Take the Radix Rhodiolae that 8g is dried, soaked after 2h with the ethanol that mass concentration is 40%, then be 80% with mass concentration Ethanol is solvent, and extracting through microwave heating 5 times filters, and filtrate, through being evaporated to no ethanol, obtains final product.

The extracting method of Pericarpium Citri grandis extract is:

The pomelo peel that 5g is dried is taken to be dried after adopting vinegar immersion, then with water as solvent, at 50 DEG C, extracting through microwave heating 5 times, filter, filtrate is anhydrous through being evaporated to, and obtains final product.

The extracting method of Hibiscus Sabdariffa Linn extract is:

Take 10g be dried Hibiscus Sabdariffa Linn, add refined honey, soak 2h after, with mass concentration be 80% ethanol as solvent, microwave Heating extraction 5 times, filters, and filtrate, through being evaporated to no ethanol, obtains final product.

The extracting method of Rhizoma Zingiberis Recens extract is:

Weigh the Rhizoma Zingiberis Recenss that 7g is dried, pulverize, add the white vinegar that mass concentration is 40%, carried using microwave heating after soaking 2h Take 2 times, filter, filtrate, through being evaporated to no white vinegar, obtains final product.

The extracting method of wormwood extract is:

Weigh the Folium Artemisiae Argyi that 15g is dried, pulverize, add the ethanol that mass concentration is 70%, using microwave heating after immersion 1h Extract 3 times, filter, filtrate, through being evaporated to no ethanol, obtains final product.

The extracting method of Flos Camelliae Japonicae flower extract is:

Weigh 10g and Flos Camelliae Japonicae be dried and after 1g is dried the mixing of Flos Camelliae Japonicae floral leaf, chopping, add the second that mass concentration is 60% Alcohol, soaks after 3h using extracting through microwave heating 2 times, filters, filtrate, through being evaporated to no ethanol, obtains final product.

The extracting method of Aloe extract is:

After 10g fresh aloe is cleaned, chopping, mass concentration be 50% ethanol in soak 2h, then using water as molten Agent, uses ultrasonic extraction 5h, extracts 3 times, united extraction liquid, is concentrated into anhydrous, obtains final product after filtration.

The extracting method of eucalyptus extracts is:

Weigh the powder that weight is than the eucalyptus citriodora leaveves being blended for 1:50 and Folium Eucalypti Robustae leaveves, add mass concentration to be 60% Ethanol, soaks after 3h using extracting through microwave heating 3 times, filters, filtrate, through being evaporated to no ethanol, obtains final product.

The extracting method of wolfberry fruit extract is:

The Fructus Lycii that 15g is dried, adds refined honey, after soaking 5h, with water as solvent, at 50 DEG C, extracting through microwave heating 3 Secondary, filter, filtrate is anhydrous through being evaporated to, and obtains final product.

The extracting method of pseudo-ginseng flower extract is:

The flower of Radix Notoginseng that 5g is dried, with water as solvent, at 80 DEG C, extracting through microwave heating 3 times, filters, filtrate is through decompression It is concentrated into anhydrous, obtain final product.

The extracting method of Herba vanillae Planifoliae extract is:

Weigh the Herba vanillae Planifoliae that 5g is dried, chopping, add the ethanol that mass concentration is 65%, using microwave heating after immersion 3h Extract 2 times, filter, filtrate, through being evaporated to no ethanol, obtains final product.

Proflavanol is commercially available Australia swisse brand.

Preparation method:

(1) pulverize after sodium sulfate, edible salt mixing, with the sieve of 100 mesh, obtain component a；

(2) by after above-mentioned plant extract mix homogeneously, at 30 DEG C, stir 10h, obtain component b；

(3) component a and component b are mixed at 35 DEG C, be stirred until homogeneous, obtain final product.

Embodiment 2

Embodiments of the invention 2 provide a kind of bath crystal composite, and in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 18 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；1 The Bulbus Lilii extract of weight portion；The Herba Saussureae Involueratae extract of 2 weight portions；The Radix Rhodiolae extract of 3 weight portions；The Fructus Citri grandiss of 1 weight portion Peel extract；The Proflavanol of 1 weight portion；The Hibiscus Sabdariffa Linn extract of 0.01 weight portion；The Rhizoma Zingiberis Recens extract of 13 weight portions；1 The wormwood extract of weight portion；The Flos Camelliae Japonicae flower extract of 5 weight portions；The Aloe extract of 1 weight portion, the Eucalyptuss of 3 weight portions carry Take the Herba vanillae Planifoliae extract of thing, the wolfberry fruit extract of 1 weight portion, the pseudo-ginseng flower extract of 0.5 weight portion, 0.05 weight portion.

Plant extract and preparation method are with embodiment 1.

Embodiment 3

Embodiments of the invention 3 provide a kind of bath crystal composite, and in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 8 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；3 weights The Bulbus Lilii extract of amount part；The Herba Saussureae Involueratae extract of 2 weight portions；The Radix Rhodiolae extract of 2 weight portions；The pomelo peel of 5 weight portions Extract；The Proflavanol of 0.1 weight portion；The Hibiscus Sabdariffa Linn extract of 0.05 weight portion；The Rhizoma Zingiberis Recens extract of 1 weight portion；7 weights The wormwood extract of amount part；The Flos Camelliae Japonicae flower extract of 1 weight portion；The Aloe extract of 8 weight portions, the Eucalyptuss of 3 weight portions are extracted Thing, the wolfberry fruit extract of 7 weight portions, the pseudo-ginseng flower extract of 0.3 weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

Plant extract and preparation method are with embodiment 1.

Embodiment 4

Embodiments of the invention 4 provide a kind of bath crystal composite, and in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 15 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；5 The Bulbus Lilii extract of weight portion；The Herba Saussureae Involueratae extract of 1 weight portion；The Radix Rhodiolae extract of 1 weight portion；The Fructus Citri grandiss of 2 weight portions Peel extract；The Proflavanol of 0.8 weight portion；The Hibiscus Sabdariffa Linn extract of 0.01 weight portion；The Rhizoma Zingiberis Recens extract of 10 weight portions； The wormwood extract of 4 weight portions；The Flos Camelliae Japonicae flower extract of 4 weight portions；The Aloe extract of 3 weight portions, the Eucalyptuss of 1 weight portion carry Take the Herba vanillae Planifoliae extract of thing, the wolfberry fruit extract of 2 weight portions, the pseudo-ginseng flower extract of 0.01 weight portion, 0.05 weight portion.

Plant extract and preparation method are with embodiment 1.

Embodiment 5

Embodiments of the invention 5 provide a kind of bath crystal composite, and in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 10 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；5 The Bulbus Lilii extract of weight portion；The Herba Saussureae Involueratae extract of 1 weight portion；The Radix Rhodiolae extract of 2 weight portions；The Fructus Citri grandiss of 4 weight portions Peel extract；The Proflavanol of 0.5 weight portion；The Hibiscus Sabdariffa Linn extract of 0.05 weight portion；The Rhizoma Zingiberis Recens extract of 8 weight portions；6 The wormwood extract of weight portion；The Flos Camelliae Japonicae flower extract of 3 weight portions；The Aloe extract of 6 weight portions, the Eucalyptuss of 2 weight portions carry Take the Herba vanillae Planifoliae extract of thing, the wolfberry fruit extract of 5 weight portions, the pseudo-ginseng flower extract of 0.2 weight portion, 0.05 weight portion.

Plant extract and preparation method are with embodiment 1.

Embodiment 6

Embodiments of the invention 6 provide a kind of bath crystal composite, and in parts by weight, described bath crystal composite includes,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 10 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；5 The Bulbus Lilii extract of weight portion；The Herba Saussureae Involueratae extract of 1 weight portion；The Radix Rhodiolae extract of 2 weight portions；The Fructus Citri grandiss of 4 weight portions Peel extract；The Proflavanol of 0.5 weight portion；The Hibiscus Sabdariffa Linn extract of 0.05 weight portion；The Rhizoma Zingiberis Recens extract of 8 weight portions；6 The wormwood extract of weight portion；The Flos Camelliae Japonicae flower extract of 3 weight portions；The Aloe extract of 6 weight portions, the Eucalyptuss of 2 weight portions carry Take the Herba vanillae Planifoliae extract of thing, the wolfberry fruit extract of 5 weight portions, the pseudo-ginseng flower extract of 0.2 weight portion, 0.05 weight portion.

Plant extract and preparation method are with embodiment 1.

Comparative example 1

With embodiment 6, difference is comparative example 1, and described bath crystal composite only includes sea salt.

Comparative example 2

With embodiment 6, difference is comparative example 2, and described bath crystal composite only includes the sodium sulfate of 98 weight portions, 2 weights Amount part sea salt.

Comparative example 3

With embodiment 6, difference is comparative example 3, and described bath crystal composite only includes plant extract.

Comparative example 4

With embodiment 6, difference is comparative example 4, described Flos Rosae Rugosae/Flos Sophorae/Calendula officinaliss flower/Flos Lonicerae mixed extract It is replaced by Flos Rosae Rugosae extract, Flos Sophorae extract, Calendula officinaliss flower extract, Flos Lonicerae extract.

Flos Rosae Rugosae extract extracting method:

By the dry Flos Rosae Rugosae of 10 weight portions, add refined honey to mix post-heating to 50 DEG C, be incubated 5h, with mass concentration after cooling Ethanol for 60% is solvent, uses ultrasonic extraction 5h, extracts 3 times, united extraction liquid, is concentrated into no ethanol, obtains final product after filtration.

Flos Sophorae extract extracting method:

By the dry Flos Sophorae of 10 weight portions, add refined honey to mix post-heating to 50 DEG C, be incubated 5h, after cooling with mass concentration be 60% ethanol is solvent, uses ultrasonic extraction 5h, extracts 3 times, united extraction liquid, is concentrated into no ethanol, obtains final product after filtration.

Calendula officinaliss flower extract extracting method:

By the dry Calendula officinaliss flower of 10 weight portions, add refined honey to mix post-heating to 50 DEG C, be incubated 5h, dense with quality after cooling The ethanol spent for 60% is solvent, uses ultrasonic extraction 5h, extracts 3 times, united extraction liquid, is concentrated into no ethanol, that is, after filtration ?.

Flos Lonicerae extract extracting method:

By the dry Flos Lonicerae of 10 weight portions, add refined honey to mix post-heating to 50 DEG C, be incubated 5h, with mass concentration after cooling Ethanol for 60% is solvent, uses ultrasonic extraction 5h, extracts 3 times, united extraction liquid, is concentrated into no ethanol, obtains final product after filtration.

Comparative example 5

With embodiment 6, difference is comparative example 5, and described plant extract does not include Flos Camelliae Japonicae flower extract.

Comparative example 6

With embodiment 6, difference is comparative example 6, and described plant extract does not include Herba vanillae Planifoliae extract.

The embodiment 1～6 being obtained and comparative example 1～6 are used for comprehensive skin protection cleaning effect test.

The people choosing 120 20～70 years old age brackets, as object on probation, is divided into 12 groups, uses embodiment 1～6 respectively And the bath of comparative example 1～6 preparation is brilliant.Every night, use time was 1 month using once.

Every using effect total score is divided into best result for 5 etc.: 5, represents very well；4 are divided into preferably；3 are divided into and can accept；3 It is bad below point it is impossible to accept.It is below every average, the results are shown in Table 1:

Table 1 comprehensive performance evaluation

Embodiment	Whitening	Moisture retention	Foaming characteristic	Massage property	Spatter property	Anti-acne
							Embodiment 1	4.0	4.3	3.7	4.2	4.0	4.5
Embodiment 2	4.3	4.3	3.8	4.4	4.1	4.5
							Embodiment 3	4.1	4.3	3.8	4.5	4.0	4.8
Embodiment 4	4.2	4.5	4.0	4.8	4.2	4.5
							Embodiment 5	5.0	5.0	4.6	5.0	4.2	5.0
Embodiment 6	5.0	5.0	4.9	5.0	4.9	5.0
							Comparative example 1	1.2	0.8	1.0	0.6	0.5	0.7
Comparative example 2	1.5	1.0	1.3	1.0	0.9	1.0
							Comparative example 3	3.5	3.6	1.1	0.5	2.3	1.3
Comparative example 4	4.1	4.2	4.1	4.3	3.8	4.2
							Comparative example 5	5.0	4.6	4.7	4.6	4.6	4.9
Comparative example 6	4.8	4.9	4.8	4.2	4.8	5.0

From table 1 it follows that the bath crystal composite in the present invention, with sodium sulfate as carrier, add and contain particular order Preparation method and knockdown extraction plant extract the plant extract that obtains of method, skin is had extraordinary comprehensive Close performance, such as whitening, moisture retention, foaming characteristic, massage property, spatter property, anti-acne are respectively provided with preferable effect.

Aforesaid example is merely illustrative, for explaining some features of the feature of the disclosure.Appended claim It is intended to the scope as wide as possible requiring to be contemplated that, and embodiments as presented herein is only according to all possible embodiment The embodiment of the selection of combination explanation.Therefore, the purpose of applicant is appended claim not by the explanation present invention The example of feature selectional restriction.And the progress in science and technology will be formed due to language performance inaccurate reason and not The possible equivalent being presently considered or son are replaced, and these changes also should be interpreted by appended in the conceived case Claim covers.

Claims (10)

1. it is characterised in that in parts by weight, described bath crystal composite includes a kind of bath crystal composite,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 5～18 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；1～ The Bulbus Lilii extract of 5 weight portions；The Herba Saussureae Involueratae extract of 0.1～2 weight portion；The Radix Rhodiolae extract of 0.1～3 weight portion；1～ The Pericarpium Citri grandis extract of 5 weight portions；The Proflavanol of 0.1～1 weight portion；The Hibiscus Sabdariffa Linn extract of 0.01～0.1 weight portion； The Rhizoma Zingiberis Recens extract of 1～13 weight portion；The wormwood extract of 1～10 weight portion；The Flos Camelliae Japonicae flower extract of 1～5 weight portion；1～ The Aloe extract of 10 weight portions, the eucalyptus extracts of 1～3 weight portion, the wolfberry fruit extract of 1～8 weight portion, 0.01～0.5 The pseudo-ginseng flower extract of weight portion, the Herba vanillae Planifoliae extract of 0.05 weight portion.

2. it is characterised in that in parts by weight, described bath crystal composite includes bath crystal composite as claimed in claim 1,

Described plant extract includes: the Flos Rosae Rugosae/Flos Sophorae of 8～15 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；3～ The Bulbus Lilii extract of 5 weight portions；The Herba Saussureae Involueratae extract of 1～2 weight portion；The Radix Rhodiolae extract of 1～2 weight portion；2～5 weights The Pericarpium Citri grandis extract of amount part；The Proflavanol of 0.1～0.8 weight portion；The Hibiscus Sabdariffa Linn extract of 0.01～0.05 weight portion； The Rhizoma Zingiberis Recens extract of 1～10 weight portion；The wormwood extract of 4～7 weight portions；The Flos Camelliae Japonicae flower extract of 1～4 weight portion；3～8 The Aloe extract of weight portion, the eucalyptus extracts of 1～3 weight portion, the wolfberry fruit extract of 2～7 weight portions, 0.01～0.3 weight The pseudo-ginseng flower extract of amount part, the Herba vanillae Planifoliae extract of 0.05 weight portion.

3. it is characterised in that in parts by weight, described bath crystal composite includes bath crystal composite as claimed in claim 2,

Described plant extract at least includes: the Flos Rosae Rugosae/Flos Sophorae of 10 weight portions/Calendula officinaliss flower/Flos Lonicerae mixed extract；5 The Bulbus Lilii extract of weight portion；The Herba Saussureae Involueratae extract of 1 weight portion；The Radix Rhodiolae extract of 2 weight portions；The Fructus Citri grandiss of 4 weight portions Peel extract；The Proflavanol of 0.5 weight portion；The Hibiscus Sabdariffa Linn extract of 0.05 weight portion；The Rhizoma Zingiberis Recens extract of 8 weight portions；6 The wormwood extract of weight portion；The Flos Camelliae Japonicae flower extract of 3 weight portions；The Aloe extract of 6 weight portions, the Eucalyptuss of 2 weight portions carry Take the Herba vanillae Planifoliae extract of thing, the wolfberry fruit extract of 5 weight portions, the pseudo-ginseng flower extract of 0.2 weight portion, 0.05 weight portion.

4. bath crystal composite as claimed in claim 1 is it is characterised in that described edible salt is selected from: sea salt, lake salt, rock salt, well Any one or a few mixing in salt, bamboo salt, mineral salt, hot spring salt, Flos Rosae Rugosae salt, Truffe salt.

5. bath crystal composite as claimed in claim 1 is it is characterised in that described Flos Rosae Rugosae/Flos Sophorae/Calendula officinaliss flower/Flos Lonicerae The extracting method of mixed extract is:

(1) weigh: weigh dry Flos Rosae Rugosae, Flos Sophorae, Calendula officinaliss flower, Flos Lonicerae for 10:1:5:0.5 by weight, after mixing Grind into powder；

(2) extract: the powder in step (1) adds refined honey to mix post-heating to 50 DEG C, is incubated 5h, dense with quality after cooling Spending the ethanol for 60% is solvent, with ultrasonic extraction 2～5h, extracts 3 times, united extraction liquid, is concentrated into no ethanol after filtration, Obtain final product.

6. bath crystal composite as claimed in claim 1 is it is characterised in that the extracting method of described Herba vanillae Planifoliae extract is:

Weigh Herba vanillae Planifoliae powder, add the ethanol that mass concentration is 95%, using extracting through microwave heating 2～3 after immersion 1～3h Secondary, filter, filtrate, through being evaporated to no ethanol, obtains final product.

7. bath crystal composite as claimed in claim 1 is it is characterised in that also include 0.5～1 weight in described bath crystal composite The quintessence oil of part.

8. as claimed in claim 1 bath crystal composite it is characterised in that described quintessence oil is selected from: tea tree ethereal oil, orange blossom quintessence oil, Any one or a few mixing in rose ethereal oil, Herba Lysimachiae foenum-graeci quintessence oil, jasmin quintessence oil.

9. the preparation method of the bath crystal composite as described in claim 1～8 is it is characterised in that at least comprise the following steps:

(1) pulverize after sodium sulfate, edible salt mixing, with the sieve of 30～100 mesh, obtain component a；

(2) by after plant extract mix homogeneously, at 30～50 DEG C, stir 1～10h, obtain component b；

(3) component a and component b are mixed at 20～35 DEG C, be stirred until homogeneous, obtain final product.

10. the bath application in bath article field for the crystal composite as described in claim 1～8.