CN106314002A - Ceramic overglazed pearlescent relief pigment, ceramic overglazed pearlescent relief color decal paper and manufacturing method thereof - Google Patents
Ceramic overglazed pearlescent relief pigment, ceramic overglazed pearlescent relief color decal paper and manufacturing method thereof Download PDFInfo
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- CN106314002A CN106314002A CN201610747641.2A CN201610747641A CN106314002A CN 106314002 A CN106314002 A CN 106314002A CN 201610747641 A CN201610747641 A CN 201610747641A CN 106314002 A CN106314002 A CN 106314002A
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- lustre
- pearly
- embossment
- ceramic
- pigment
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B44—DECORATIVE ARTS
- B44C—PRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
- B44C1/00—Processes, not specifically provided for elsewhere, for producing decorative surface effects
- B44C1/16—Processes, not specifically provided for elsewhere, for producing decorative surface effects for applying transfer pictures or the like
Abstract
The invention relates to a ceramic overglazed pearlescent relief pigment, a ceramic overglazed pearlescent relief color decal paper and a manufacturing method thereof and belongs to the technical field of ceramic overglazed color printing. The ceramic overglazed pearlescent relief pigment comprises the following components in percentage by mass: 30-40% of feldspar, 15-25% of borax, 5-15% of kaoline and 20-50% of low-temperature lead-free frits, wherein the percentage sum of all the components is 100%. After a ceramic product is decaled by using the ceramic overglazed pearlescent relief color decal paper prepared by the manufacturing method, an overglazed pearlescent relief has a relatively strong adhesive force and favorable glossiness, the ceramic product is enabled to have excellent stain resistance, scrubbing resistance and wear resistance and is also enabled to have an excellent metal pearlescent colorating effect, and the ceramic product can show pearlescent metal effects with different degrees under rays with different angles; in addition, the manufactured decal paper is attractive in appearance, environment-friendly and extremely low in lead and cadmium dissolution quantity and conforms to the standards of China and each of Europe and America.
Description
Technical field
The invention belongs to color printing technology on ceramic glaze, be specifically related to pearly-lustre embossment pigment and pottery on a kind of ceramic glaze
Pearly-lustre embossment firework paper and manufacture method on enamel.
Background technology
Pottery pearly-lustre embossment pigment is the embossment cap layer pigment being exclusively used in marble paper on ceramic glaze, is characterized in burning till in making
After can reach stronger metal sense, and different metal effects can be shown under the light of different angles, it is color transformed
Abundant, substantially close to the color development of organic pigment.Traditional pearly-lustre its composition of embossment pigment is mainly the titanium oxide cloud of synthetic
Master slice, it burns till fusing point is about 1500 DEG C, although titanium oxide mica sheet cost is relatively low, but has the disadvantage that first, attached
Put forth effort poor；Second, rough surface five gloss；3rd, resistance to soiling is poor and not wash resistant；Current solution is in printing
Overprint transparent cap layer on complete pearly-lustre pattern again, thus improve glossiness and the wear resistence of surface of ceramic products, but due to
Pearlescent pigment is poor with the matching of transparent cap layer, brings again new problem: surface of ceramic products not only loses pearl simultaneously
Delustering pigment due metal sense, also affects the color of pearlescent pigment itself.
Although and prior art has many reports of embossment on associated ceramic glaze, but there are no the report of pearly-lustre embossment
Road, and at present embossment marble paper only has the single colour systems such as transparent and milky white, limitation is relatively big, and above-mentioned many deficiencies mainly by
The limitation of embossment pigment formula and processing technology causes, and the embossment pigment of a lot of marble paper is being pasted onto on ceramic
There will be pigment distribution after drying uneven, affect the outward appearance of ceramic, because the embossment composition to embossment pigment on glaze
And processing technology requires that in relatively glaze, pigment is higher.The China of Application No. 201410243698.X that applicant submitted in 2014
Patent, discloses the processing technology of famille-rose embossment printed matter on a kind of glaze, although it has filled up on glaze embossment on colour system
Blank, but applicant finds the color effect of this marble paper its famille-rose embossment in actual use not in follow-up research
Substantially, firing temperature is higher, and its toning is the most cumbersome, is still further improved.
Summary of the invention
The invention aims to solve the deficiencies in the prior art, and provide on a kind of ceramic glaze pearly-lustre embossment pigment and
Pearly-lustre embossment firework paper and manufacture method on ceramic glaze, the method is easy and simple to handle, and the firing temperature of embossment pigment is relatively low, and pearly-lustre floats
The adhesive force of carving is relatively strong, and resistance to soiling and washing fastness are preferable, and glossiness and wear resistence are preferably, can give ceramic excellence
Pearly-lustre anaglyph.
The present invention adopts the following technical scheme that
Pearly-lustre embossment pigment on ceramic glaze, the following component including according to mass percent: Anhydrite 30%-40%, Borax 15%-
25%, Kaolin 5%-15%, low-temperature lead-free frit 20%-50%, wherein said each component percentages adds up to 100%.
Further, pearly-lustre embossment pigment on described ceramic glaze, wherein said Anhydrite is in orthoclase or plagioclase
One.
Further, pearly-lustre embossment pigment on described ceramic glaze, wherein said Anhydrite is potassium feldspar, albite or Austria
One in Anhydrite.
On ceramic glaze, the manufacture method of pearly-lustre embossment firework paper, comprises the steps:
Step one, the preparation of pearl essence: according to mass percent, by pearl essence and the low-temperature lead-free of 10%-30% of 70%-90%
Add the ethanol ball milling 2-4h of equal in quality after frit mixing, pulverize 200 mesh sieves after drying standby；
Step 2, the preparation of pearly-lustre embossment pigment: according to described mass percent, by Anhydrite, Borax, Kaolin and low-temperature lead-free
Frit mix homogeneously, by calcining, ball milling, dries and pulverizes and i.e. obtain described pearly-lustre embossment pigment, and wherein said calcining is specially
It is gradually heating to 1050 DEG C, is incubated 20-30min；Described ball milling is specially and adds the ethanol identical with raw material gross weight, in ball milling
Ball milling 120h under the rotating speed of 1000r/min；Described drying is specially dries at 50-60 DEG C, crosses 350 mesh sieves after described pulverizing；
Step 3, printing:
A: be screen printed onto on transcription base stock with 250 mesh by background color lead and cadmium free pigment, is dried more than 6h, obtains background color marble paper；
B: stirred with ink by described pearl essence, pearl essence is 1:1-1:2 with the mass ratio of ink, uses 200 mesh after rolling ink
It is screen printed onto on the background color of step a gained background color marble paper, naturally dries more than 4h, obtain pearly-lustre marble paper；
C: described pearly-lustre embossment pigment is mixed homogeneously with ink, pearly-lustre embossment pigment is 10:6-10:8 with the mass ratio of ink,
Being screen printed onto with 120 mesh after rolling ink on the pearly-lustre color of step b gained pearly-lustre marble paper, print pass is as needed for 1-3 time, certainly
So dry more than 12h, obtain pearly-lustre embossment marble paper；
D: front cover glue is screen printed onto on the pearly-lustre embossing pattern of step c gained pearly-lustre embossment marble paper with 80 mesh, is drying to obtain
Pearly-lustre embossment firework paper on described ceramic glaze.
Further, the manufacture method of pearly-lustre embossment firework paper, wherein ball described in step one on described ceramic glaze
Grind ball milling 2-4h under 1500r/min rotating speed.
Further, on described ceramic glaze, the manufacture method of pearly-lustre embossment firework paper, wherein forges described in step 2
Burn and be specially gradually heating to 1050 DEG C, be incubated 20-30min；Described ball milling is specially and adds the second identical with raw material gross weight
Alcohol, ball milling 120h under the rotating speed of ball milling 1000r/min；Described drying is specially dries at 50-60 DEG C, mistake after described pulverizing
350 mesh sieves.
Further, the manufacture method of pearly-lustre embossment firework paper on described ceramic glaze, wherein institute in step 3 b and c
State and be dried as naturally drying.
The present invention also provides for a kind of ceramic glaze prepared by the manufacture method of pearly-lustre embossment firework paper on described ceramic glaze
Upper pearly-lustre embossment firework paper.
On the ceramic glaze that the present invention prepares, pearly-lustre embossment firework paper applique is after ceramic surface, and first dry in the air more than 6h naturally, then
At 1100-1150 DEG C, roasting 30-40min can give pearly-lustre anaglyph on the glaze that ceramic is excellent.
Compared with prior art, it has the beneficial effect that the present invention
After on the glaze prepared by the present invention, pearly-lustre embossment firework paper carries out applique to ceramic, on glaze, pearly-lustre embossment has stronger
Adhesive force and good glossiness, and give resistance to soiling, scrub resistance and the wear resistence that ceramic is excellent, also impart pottery
The metal pearly-lustre colouring effect that ceramic products is excellent, and under the light of different angles, ceramic can demonstrate different journey
The pearly-lustre metal effect of degree, additionally, the marble paper environmental protection attractive in appearance prepared, its lead-indium alloy is extremely low, respectively less than 0.005mg/L, symbol
Close China and the standard of European and American countries.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example is merely to illustrate the present invention, and should not be regarded as limiting this
Bright scope.The pearl essence used in the present invention is the pearl essence that Merck KGaA produces, and the low-temperature lead-free frit of use is purchased from English
Village letter Wan Feng company of state.
Embodiment 1
Pearly-lustre embossment pigment on ceramic glaze, the following component including according to mass percent: potassium feldspar 35%, Borax 20%, height
Ridge soil 10%, low-temperature lead-free frit 35%, wherein said each component percentages adds up to 100%.
On ceramic glaze, the manufacture method of pearly-lustre embossment firework paper, comprises the steps:
Step one, the preparation of pearl essence: according to mass percent, the pearl essence by 80% and the low-temperature lead-free frit mixing of 20%
The ethanol of rear addition equal in quality ball milling 3h under 1500r/min rotating speed, pulverized 200 mesh sieves standby after drying；
Step 2, the preparation of pearly-lustre embossment pigment: according to described mass percent, by Anhydrite, Borax, Kaolin and low-temperature lead-free
Frit mix homogeneously, by calcining, ball milling, dries and pulverizes and i.e. obtain described pearly-lustre embossment pigment；
Step 3, printing:
A: be screen printed onto on transcription base stock with 250 mesh by background color lead and cadmium free pigment, is dried more than 6h, obtains background color marble paper；
B: stirred with ink by described pearl essence, the mass ratio of pearl essence and ink is 1:1, rolls after ink with 200 mesh silk screens
Print to the background color of step a gained background color marble paper, be dried more than 4h, obtain pearly-lustre marble paper；
C: mixed homogeneously with ink by described pearly-lustre embossment pigment, pearly-lustre embossment pigment is 10:7 with the mass ratio of ink, rolls ink
Being screen printed onto with 120 mesh afterwards on the pearly-lustre color of step b gained pearly-lustre marble paper, print pass, as needed for 1-3 time, is dried
More than 12h, obtains pearly-lustre embossment marble paper；
D: front cover glue is screen printed onto on the pearly-lustre embossing pattern of step c gained pearly-lustre embossment marble paper with 80 mesh, is drying to obtain
Pearly-lustre embossment firework paper on described ceramic glaze.
Embodiment 2
Pearly-lustre embossment pigment on ceramic glaze, the following component including according to mass percent: albite 30%, Borax 15%, height
Ridge soil 5%, low-temperature lead-free frit 50%, wherein said each component percentages adds up to 100%.
On ceramic glaze, the manufacture method of pearly-lustre embossment firework paper, comprises the steps:
Step one, the preparation of pearl essence: according to mass percent, the pearl essence by 70% and the low-temperature lead-free frit mixing of 30%
The ethanol of rear addition equal in quality ball milling 2h under 1500r/min rotating speed, pulverized 200 mesh sieves standby after drying；
Step 2, the preparation of pearly-lustre embossment pigment: according to described mass percent, by Anhydrite, Borax, Kaolin and low-temperature lead-free
Frit mix homogeneously, by calcining, ball milling, dries and pulverizes and i.e. obtain described pearly-lustre embossment pigment；
Step 3, printing:
A: be screen printed onto on transcription base stock with 250 mesh by background color lead and cadmium free pigment, is dried more than 6h, obtains background color marble paper；
B: stirred with ink by described pearl essence, the mass ratio of pearl essence and ink is 1:1.5, rolls after ink with 200 mesh silks
Wire mark brush, on the background color of step a gained background color marble paper, is dried more than 4h, obtains pearly-lustre marble paper；
C: mixed homogeneously with ink by described pearly-lustre embossment pigment, pearly-lustre embossment pigment is 10:6 with the mass ratio of ink, rolls ink
Being screen printed onto with 120 mesh afterwards on the pearly-lustre color of step b gained pearly-lustre marble paper, print pass, as needed for 1-3 time, is dried
More than 12h, obtains pearly-lustre embossment marble paper；
D: front cover glue is screen printed onto on the pearly-lustre embossing pattern of step c gained pearly-lustre embossment marble paper with 80 mesh, is drying to obtain
Pearly-lustre embossment firework paper on described ceramic glaze.
Embodiment 3
Pearly-lustre embossment pigment on ceramic glaze, the following component including according to mass percent: oligoclase 40%, Borax 25%, height
Ridge soil 15%, low-temperature lead-free frit 20%, wherein said each component percentages adds up to 100%.
On ceramic glaze, the manufacture method of pearly-lustre embossment firework paper, comprises the steps:
Step one, the preparation of pearl essence: according to mass percent, the pearl essence by 90% and the low-temperature lead-free frit mixing of 10%
The ethanol of rear addition equal in quality ball milling 4h under 1500r/min rotating speed, pulverized 200 mesh sieves standby after drying；
Step 2, the preparation of pearly-lustre embossment pigment: according to described mass percent, by Anhydrite, Borax, Kaolin and low-temperature lead-free
Frit frit mix homogeneously, by calcining, ball milling, dries and pulverizes and i.e. obtain described pearly-lustre embossment pigment；
Step 3, printing:
A: be screen printed onto on transcription base stock with 250 mesh by background color lead and cadmium free pigment, is dried more than 6h, obtains background color marble paper；
B: stirred with ink by described pearl essence, the mass ratio of pearl essence and ink is 1:2, rolls after ink with 200 mesh silk screens
Print to the background color of step a gained background color marble paper, be dried more than 4h, obtain pearly-lustre marble paper；
C: mixed homogeneously with ink by described pearly-lustre embossment pigment, pearly-lustre embossment pigment is 10:8 with the mass ratio of ink, rolls ink
Being screen printed onto with 120 mesh afterwards on the pearly-lustre color of step b gained pearly-lustre marble paper, print pass, as needed for 1-3 time, is dried
More than 12h, obtains pearly-lustre embossment marble paper；
D: front cover glue is screen printed onto on the pearly-lustre embossing pattern of step c gained pearly-lustre embossment marble paper with 80 mesh, is drying to obtain
Pearly-lustre embossment firework paper on described ceramic glaze.
On the ceramic glaze prepare the embodiment of the present invention 1 to 3, pearly-lustre embossment firework paper applique is behind ceramic surface, first
Naturally dry in the air more than 6h, roasting 6h at 780-820 DEG C, the performance of test ceramic, and test result see table 1:
Table 1 performance test data
| Detection project | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Resistance to soiling (acid of resistance to low concentration) | GLA | GLA | GLA |
| Scrub resistance (wet rubbing), secondary | 10000 | 10000 | 10000 |
| Wear resistence | 6000 turns, level Four | 6000 turns, level Four | 6000 turns, level Four |
| Adhesive force (cross-hatching) | 4B | 4B | 4B |
As seen from the above table, on the glaze prepared according to the present invention, pearly-lustre embossment firework paper can give the excellent resistance to soiling of pottery, resistance to
Scrubbing character, wear resistence, and pearly-lustre embossment pigment is relatively strong with the adhesive force of pottery, can reach 4B level.
Skilled person will appreciate that of the industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation
The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention, the present invention also has
Various changes and modifications, these changes and improvements both fall within scope of the claimed invention.Claimed scope
Defined by appending claims and equivalent thereof.
Claims (8)
1. pearly-lustre embossment pigment on ceramic glaze, it is characterised in that include the following component according to mass percent: Anhydrite 30%-
40%, Borax 15%-25%, Kaolin 5%-15%, low-temperature lead-free frit 20%-50%, wherein said each component percentages adds up to
100%。
Pearly-lustre embossment pigment on ceramic glaze the most according to claim 1, it is characterised in that described Anhydrite is orthoclase or oblique
One in Anhydrite.
Pearly-lustre embossment pigment on ceramic glaze the most according to claim 2, it is characterised in that described Anhydrite is potassium feldspar, sodium
One in Anhydrite or oligoclase.
4. the manufacture method of pearly-lustre embossment firework paper on ceramic glaze, it is characterised in that comprise the steps:
Step one, the preparation of pearl essence: according to mass percent, by pearl essence and the low-temperature lead-free of 10%-30% of 70%-90%
Add the ethanol ball milling 2-4h of equal in quality after frit mixing, pulverize 200 mesh sieves after drying standby；
Step 2, the preparation of pearly-lustre embossment pigment: according to described mass percent, by Anhydrite, Borax, Kaolin and low-temperature lead-free
Frit mix homogeneously, by calcining, ball milling, dries and pulverizes and i.e. obtain described pearly-lustre embossment pigment；
Step 3, printing:
A: be screen printed onto on transcription base stock with 250 mesh by background color lead and cadmium free pigment, is dried more than 6h, obtains background color marble paper；
B: stirred with ink by described pearl essence, pearl essence is 1:1-1:2 with the mass ratio of ink, uses 200 mesh after rolling ink
It is screen printed onto on the background color of step a gained background color marble paper, is dried more than 4h, obtains pearly-lustre marble paper；
C: described pearly-lustre embossment pigment is mixed homogeneously with ink, pearly-lustre embossment pigment is 10:6-10:8 with the mass ratio of ink,
Being screen printed onto with 120 mesh after rolling ink on the pearly-lustre color of step b gained pearly-lustre marble paper, print pass is as needed for 1-3 time, dry
Dry more than 12h, obtains pearly-lustre embossment marble paper；
D: front cover glue is screen printed onto on the pearly-lustre embossing pattern of step c gained pearly-lustre embossment marble paper with 80 mesh, is drying to obtain
Pearly-lustre embossment firework paper on described ceramic glaze.
5. according to the manufacture method of pearly-lustre embossment firework paper on the ceramic glaze described in right 4, it is characterised in that described in step one
Ball milling is ball milling 2-4h under 1500r/min rotating speed.
The manufacture method of pearly-lustre embossment firework paper on ceramic glaze the most according to claim 4, it is characterised in that in step 2
Described calcining is specially gradually heating to 1050 DEG C, is incubated 20-30min；Described ball milling is specially and adds and raw material gross weight phase
Same ethanol, ball milling 120h under the rotating speed of ball milling 1000r/min；Described drying is specially dries at 50-60 DEG C, described powder
350 mesh sieves are crossed after broken.
The manufacture method of pearly-lustre embossment firework paper on ceramic glaze the most according to claim 4, it is characterised in that step 3 b
Be dried described in c as naturally drying.
8. pearly-lustre embossment on the ceramic glaze prepared by the manufacture method of pearly-lustre embossment firework paper on the ceramic glaze described in claim 4
Firework paper.
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| CN201610747641.2A CN106314002B (en) | 2016-08-30 | 2016-08-30 | Pearly-lustre embossment firework paper and production method on pearly-lustre embossment pigment and ceramic glaze on ceramic glaze |
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| CN201610747641.2A CN106314002B (en) | 2016-08-30 | 2016-08-30 | Pearly-lustre embossment firework paper and production method on pearly-lustre embossment pigment and ceramic glaze on ceramic glaze |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107827363A (en) * | 2017-11-24 | 2018-03-23 | 广东道氏技术股份有限公司 | A kind of high temperature golden yellow pearly-lustre glaze and its application |
| CN111072283A (en) * | 2019-12-28 | 2020-04-28 | 福建省德化县溢茂工艺有限公司 | Preparation process for preparing high-alkali-resistance ceramic glazing solvent by grinding and adding silica sol |
| CN111070952A (en) * | 2019-12-28 | 2020-04-28 | 福建省德化县华兴陶瓷有限公司 | Ceramic-glazed pearlescent relief color paper and manufacturing method thereof |
| CN111675936A (en) * | 2020-05-11 | 2020-09-18 | 醴陵市精陶瓷业有限公司 | Ceramic three-dimensional stained paper and preparation method and application thereof |
| CN111731019A (en) * | 2020-05-11 | 2020-10-02 | 醴陵市精陶瓷业有限公司 | Embossed stained paper and preparation method and application thereof |
| CN113698233A (en) * | 2021-08-31 | 2021-11-26 | 深圳市国瓷永丰源瓷业有限公司 | Pearlescent interference color combination product and preparation method thereof, stained paper and one-time color firing process |
| CN113844189A (en) * | 2021-09-16 | 2021-12-28 | 德化县新佳兴印刷有限公司 | One-time firing embossed gold stained paper and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107827363A (en) * | 2017-11-24 | 2018-03-23 | 广东道氏技术股份有限公司 | A kind of high temperature golden yellow pearly-lustre glaze and its application |
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| CN111072283A (en) * | 2019-12-28 | 2020-04-28 | 福建省德化县溢茂工艺有限公司 | Preparation process for preparing high-alkali-resistance ceramic glazing solvent by grinding and adding silica sol |
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| CN111731019A (en) * | 2020-05-11 | 2020-10-02 | 醴陵市精陶瓷业有限公司 | Embossed stained paper and preparation method and application thereof |
| CN113698233A (en) * | 2021-08-31 | 2021-11-26 | 深圳市国瓷永丰源瓷业有限公司 | Pearlescent interference color combination product and preparation method thereof, stained paper and one-time color firing process |
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Denomination of invention: Ceramic overglazed pearlescent relief pigment, ceramic overglazed pearlescent relief color decal paper and manufacturing method thereof Effective date of registration: 20190820 Granted publication date: 20190409 Pledgee: Industrial Commercial Bank of China Ltd Dehua branch Pledgor: Dehua, Fujian Province Ming Fengjin marble paper company limited Registration number: Y2019990000098 |
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