CN106281771A - A kind of delicate fragrance type laundry detergent compositions and preparation method thereof - Google Patents
A kind of delicate fragrance type laundry detergent compositions and preparation method thereof Download PDFInfo
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- CN106281771A CN106281771A CN201610643330.1A CN201610643330A CN106281771A CN 106281771 A CN106281771 A CN 106281771A CN 201610643330 A CN201610643330 A CN 201610643330A CN 106281771 A CN106281771 A CN 106281771A
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- Prior art keywords
- delicate fragrance
- detergent compositions
- laundry detergent
- isomery
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- 239000003599 detergent Substances 0.000 title claims abstract description 20
- 239000000203 mixture Substances 0.000 title claims abstract description 18
- 239000003205 fragrance Substances 0.000 title claims abstract description 15
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- VMHLLURERBWHNL-UHFFFAOYSA-M Sodium acetate Chemical compound [Na+].CC([O-])=O VMHLLURERBWHNL-UHFFFAOYSA-M 0.000 claims abstract description 8
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 claims abstract description 8
- 229940070800 myristoyl glutamate Drugs 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 235000017281 sodium acetate Nutrition 0.000 claims abstract description 8
- 239000001632 sodium acetate Substances 0.000 claims abstract description 8
- -1 propyl hydroxy sulfobetaine Chemical compound 0.000 claims abstract description 7
- 229930183111 sapindoside Natural products 0.000 claims abstract description 7
- KHSLHYAUZSPBIU-UHFFFAOYSA-M benzododecinium bromide Chemical compound [Br-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 KHSLHYAUZSPBIU-UHFFFAOYSA-M 0.000 claims abstract description 6
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims abstract description 6
- 235000018185 Betula X alpestris Nutrition 0.000 claims abstract description 5
- 235000018212 Betula X uliginosa Nutrition 0.000 claims abstract description 5
- CCRCUPLGCSFEDV-UHFFFAOYSA-N cinnamic acid methyl ester Natural products COC(=O)C=CC1=CC=CC=C1 CCRCUPLGCSFEDV-UHFFFAOYSA-N 0.000 claims abstract description 5
- CCRCUPLGCSFEDV-BQYQJAHWSA-N methyl trans-cinnamate Chemical compound COC(=O)\C=C\C1=CC=CC=C1 CCRCUPLGCSFEDV-BQYQJAHWSA-N 0.000 claims abstract description 5
- TVACALAUIQMRDF-UHFFFAOYSA-N dodecyl dihydrogen phosphate Chemical compound CCCCCCCCCCCCOP(O)(O)=O TVACALAUIQMRDF-UHFFFAOYSA-N 0.000 claims abstract description 4
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 4
- 238000010438 heat treatment Methods 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 7
- 229940126062 Compound A Drugs 0.000 claims description 6
- NLDMNSXOCDLTTB-UHFFFAOYSA-N Heterophylliin A Natural products O1C2COC(=O)C3=CC(O)=C(O)C(O)=C3C3=C(O)C(O)=C(O)C=C3C(=O)OC2C(OC(=O)C=2C=C(O)C(O)=C(O)C=2)C(O)C1OC(=O)C1=CC(O)=C(O)C(O)=C1 NLDMNSXOCDLTTB-UHFFFAOYSA-N 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 238000010907 mechanical stirring Methods 0.000 claims description 6
- 238000013019 agitation Methods 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
- 239000011734 sodium Substances 0.000 claims description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- 239000005864 Sulphur Substances 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 239000003513 alkali Substances 0.000 claims 1
- 150000001336 alkenes Chemical class 0.000 claims 1
- 230000003115 biocidal effect Effects 0.000 abstract description 2
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 229940117986 sulfobetaine Drugs 0.000 abstract description 2
- 239000004094 surface-active agent Substances 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 235000019082 Osmanthus Nutrition 0.000 description 2
- 241000333181 Osmanthus Species 0.000 description 2
- 230000031709 bromination Effects 0.000 description 2
- 238000005893 bromination reaction Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- VYVKAVOEYGTNNY-UHFFFAOYSA-N C(CCCCCCCCCCC)C1=C(C([N+](C)(C)CCCCCCCCCCCCCCCC)(C)C)C=CC=C1 Chemical compound C(CCCCCCCCCCC)C1=C(C([N+](C)(C)CCCCCCCCCCCCCCCC)(C)C)C=CC=C1 VYVKAVOEYGTNNY-UHFFFAOYSA-N 0.000 description 1
- 239000010022 Myron Substances 0.000 description 1
- 241001439614 Myron Species 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 230000016507 interphase Effects 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 101150067879 sas-6 gene Proteins 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/36—Organic compounds containing phosphorus
- C11D3/362—Phosphates or phosphites
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/04—Carboxylic acids or salts thereof
- C11D1/10—Amino carboxylic acids; Imino carboxylic acids; Fatty acid condensates thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/143—Sulfonic acid esters
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/38—Cationic compounds
- C11D1/62—Quaternary ammonium compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
- C11D1/721—End blocked ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/12—Soft surfaces, e.g. textile
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a kind of delicate fragrance type laundry detergent compositions and preparation method thereof, be made up of the raw material of following weight portion: C14 17 SAS 47, lauryl both sexes sodium acetate 8 11, myristoyl glutamate sodium 69, methyl cinnamate 36, isomery ten polyoxyethylenated alcohol 58, birch juice 47, dodecylphosphoric acid monoesters 10 12, sapindoside 48, cocoamido propyl hydroxy sulfobetaine 69, dodecyl dimethyl benzyl ammonium bromide 7 10, water 55 65.Detergent clean result of the present invention is good, and dirt-removing power is strong, has certain natural delicate fragrance and preferable antibiotic property and antistatic behaviour, to human body skin nonirritant, safety and environmental protection simultaneously.
Description
Technical field
The present invention relates to a kind of delicate fragrance type laundry detergent compositions and preparation method thereof, belong to articles for washing technical field.
Background technology
Modern detergent is the complex mixture containing Multiple components, and wherein surfactant has been the main of cleaning action
Composition, other compositions or for improving and increase the clenaing effect of surfactant or some is special in order to adapt in detergent
Need or add for making required and product form.Various surfactants and various auxiliary agent have respective characteristic,
These distinct compositions mix, owing to their interphase interaction will produce more preferably clean result.Existing
It is not strong that some laundry detergent compositions also exist dirt-removing power, and function singleness does not possess the multiple demand such as delicate fragrance, antibacterial, antistatic, nothing
Method meets the use requirement of people.
Summary of the invention
For the deficiencies in the prior art, the problem to be solved in the present invention is to provide the delicate fragrance type clothing that a kind of dirt-removing power is strong
Thing detergent and preparation method thereof.
For solving prior art problem, the present invention provides following technical scheme:
A kind of delicate fragrance type laundry detergent compositions, is made up of the raw material of following weight portion: C14-17 SAS 4-7, the moon
Osmanthus base both sexes sodium acetate 8-11, myristoyl glutamate sodium 6-9, methyl cinnamate 3-6, isomery ten polyoxyethylenated alcohol 5-8, birch
Myron 4-7, dodecylphosphoric acid monoesters 10-12, sapindoside 4-8, cocoamido propyl hydroxy sulfobetaine 6-9, bromination
Dodecyl dimethyl hexadecyldimethyl benzyl ammonium 7-10, water 55-65.
The preparation method of a kind of delicate fragrance type laundry detergent compositions, comprises the following steps:
(1) take 1/2-1/3 amount water heating in water bath to 45-50 DEG C, be sequentially added into the secondary alkyl of C14-17 under mechanical stirring
Sodium sulfonate, isomery ten polyoxyethylenated alcohol and dodecyl dimethyl benzyl ammonium bromide, be then 300-400W at heating power,
Rotating speed is magnetic agitation 3-6min under conditions of 400-500r/min, obtains compound A；
(2) take remaining water heating in water bath to 50-55 DEG C, be sequentially added under mechanical stirring lauryl both sexes sodium acetate,
Isomery ten polyoxyethylenated alcohol, myristoyl glutamate sodium and sapindoside, be then 250-350W at microwave power, rotating speed
For microwave stirring 2-4min under conditions of 300-400r/min, obtain compound B；
(3) compound A and compound B being mixed, be 850-950W at power, frequency is ultrasonic under conditions of 30-40KHz
Stirring 4-8min, then adjustment solution temperature is to 40-45 DEG C, adds remaining raw material, is the condition of 500-600r/min at rotating speed
Lower stirring 3-6min, gets product.
The method have the benefit that
The C14-17 SAS of present invention interpolation, lauryl both sexes sodium acetate, myristoyl glutamate sodium, nothing are suffered from
The surfactants such as sub-saponin, can strengthen the dirt-removing power of detergent, the raw material such as the birch juice of interpolation, methyl cinnamate, can
To increase the aromatic odor of detergent, the dodecyl dimethyl benzyl ammonium bromide of interpolation, the antibiotic property of detergent can be improved
And antistatic behaviour.Detergent clean result of the present invention is good, and dirt-removing power is strong, has certain natural delicate fragrance simultaneously and preferably resists
Bacterium property and antistatic behaviour, to human body skin nonirritant, safety and environmental protection.
Detailed description of the invention
Embodiment
A kind of delicate fragrance type laundry detergent compositions, is made up of the raw material of following weight (kg): C14-17 SAS 6, the moon
Osmanthus base both sexes sodium acetate 9, myristoyl glutamate sodium 7, methyl cinnamate 4.5, isomery ten polyoxyethylenated alcohol 6, birch juice 5,
Dodecylphosphoric acid monoesters 11, sapindoside 5, cocoamido propyl hydroxy sulfobetaine 8, bromination dodecyl dimethyl benzyl
Base ammonium 9, water 60.
The preparation method of a kind of delicate fragrance type laundry detergent compositions, comprises the following steps:
(1) take the water heating in water bath of 1/2 amount to 47 DEG C, be sequentially added under mechanical stirring C14-17 SAS,
Isomery ten polyoxyethylenated alcohol and dodecyl dimethyl benzyl ammonium bromide, be then 350W at heating power, and rotating speed is 450r/
Magnetic agitation 5min under conditions of min, obtains compound A；
(2) take remaining water heating in water bath to 52 DEG C, be sequentially added into lauryl both sexes sodium acetate, isomery under mechanical stirring
Ten polyoxyethylenated alcohol, myristoyl glutamate sodium and sapindoside, be then 300W at microwave power, and rotating speed is 350r/
Under conditions of min, microwave stirring 3min, obtains compound B；
(3) being mixed by compound A and compound B, be 900W at power, frequency is ultrasonic agitation under conditions of 35KHz
6min, then adjustment solution temperature is to 42 DEG C, adds remaining raw material, stirs 4min, i.e. under conditions of rotating speed is 550r/min
Obtain finished product.
The main performance testing result of the delicate fragrance type laundry detergent compositions that above-described embodiment prepares is as shown in the table:
| Project | Soil removal efficiency (%) | Foam volume (mL) |
| Result | 76.4 | 390 |
Claims (2)
1. a delicate fragrance type laundry detergent compositions, it is characterised in that be made up of the raw material of following weight portion: C14-17 secondary alkyl sulphur
Acid sodium 4-7, lauryl both sexes sodium acetate 8-11, myristoyl glutamate sodium 6-9, methyl cinnamate 3-6, isomery ten alcohol polyoxy second
Alkene ether 5-8, birch juice 4-7, dodecylphosphoric acid monoesters 10-12, sapindoside 4-8, cocamidopropyl propyl amide hydroxyl sulfobetaines
Alkali 6-9, dodecyl dimethyl benzyl ammonium bromide 7-10, water 55-65.
The preparation method of a kind of delicate fragrance type laundry detergent compositions the most according to claim 1, it is characterised in that include following step
Rapid:
(1) take 1/2-1/3 amount water heating in water bath to 45-50 DEG C, be sequentially added into the secondary alkyl sulfonic acid of C14-17 under mechanical stirring
Sodium, isomery ten polyoxyethylenated alcohol and dodecyl dimethyl benzyl ammonium bromide, be then 300-400W at heating power, rotating speed
For magnetic agitation 3-6min under conditions of 400-500r/min, obtain compound A；
(2) take remaining water heating in water bath to 50-55 DEG C, be sequentially added into lauryl both sexes sodium acetate, isomery under mechanical stirring
Ten polyoxyethylenated alcohol, myristoyl glutamate sodium and sapindoside, be then 250-350W at microwave power, and rotating speed is
Under conditions of 300-400r/min, microwave stirring 2-4min, obtains compound B；
(3) being mixed by compound A and compound B, be 850-950W at power, frequency is ultrasonic agitation under conditions of 30-40KHz
4-8min, then adjustment solution temperature is to 40-45 DEG C, adds remaining raw material, stirs under conditions of rotating speed is 500-600r/min
Mix 3-6min, get product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610643330.1A CN106281771A (en) | 2016-08-08 | 2016-08-08 | A kind of delicate fragrance type laundry detergent compositions and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610643330.1A CN106281771A (en) | 2016-08-08 | 2016-08-08 | A kind of delicate fragrance type laundry detergent compositions and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106281771A true CN106281771A (en) | 2017-01-04 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022042977A1 (en) * | 2020-08-28 | 2022-03-03 | Unilever Ip Holdings B.V. | Detergent composition |
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|---|---|---|---|---|
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| CN101225349A (en) * | 2007-01-18 | 2008-07-23 | 郭景龙 | Liquid detergent and method for preparing same |
| CN104818147A (en) * | 2015-03-25 | 2015-08-05 | 上海应用技术学院 | Compound liquid laundry detergent and preparation method thereof |
| CN105779158A (en) * | 2016-03-04 | 2016-07-20 | 俞尧芳 | Clothes ink removing method |
-
2016
- 2016-08-08 CN CN201610643330.1A patent/CN106281771A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1290739A (en) * | 2000-10-20 | 2001-04-11 | 崔凤瑞 | Multipurpose concentrated washing and protecting liquid |
| CN101225349A (en) * | 2007-01-18 | 2008-07-23 | 郭景龙 | Liquid detergent and method for preparing same |
| CN104818147A (en) * | 2015-03-25 | 2015-08-05 | 上海应用技术学院 | Compound liquid laundry detergent and preparation method thereof |
| CN105779158A (en) * | 2016-03-04 | 2016-07-20 | 俞尧芳 | Clothes ink removing method |
Non-Patent Citations (1)
| Title |
|---|
| 李慕南等: "《青少年爱科学 匪夷所思的植物》", 31 May 2012, 北方妇女儿童出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2022042977A1 (en) * | 2020-08-28 | 2022-03-03 | Unilever Ip Holdings B.V. | Detergent composition |
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