CN106280664A - A kind of using earth as the external reinforcement agent of decorating inner and external walls and preparation technology thereof - Google Patents

A kind of using earth as the external reinforcement agent of decorating inner and external walls and preparation technology thereof Download PDF

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CN106280664A
CN106280664A CN201610654849.XA CN201610654849A CN106280664A CN 106280664 A CN106280664 A CN 106280664A CN 201610654849 A CN201610654849 A CN 201610654849A CN 106280664 A CN106280664 A CN 106280664A
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earth
external
reinforcement agent
preparation technology
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蒋黔湘
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/10Esters
    • C08F220/12Esters of monohydric alcohols or phenols
    • C08F220/16Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms
    • C08F220/18Esters of monohydric alcohols or phenols of phenols or of alcohols containing two or more carbon atoms with acrylic or methacrylic acids
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L33/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • C08L33/04Homopolymers or copolymers of esters
    • C08L33/06Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, which oxygen atoms are present only as part of the carboxyl radical
    • C08L33/10Homopolymers or copolymers of methacrylic acid esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D1/00Coating compositions, e.g. paints, varnishes or lacquers, based on inorganic substances
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40Additives
    • C09D7/65Additives macromolecular
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Inorganic Chemistry (AREA)
  • Cosmetics (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

nullThe invention discloses a kind of using earth as the external reinforcement agent of decorating inner and external walls,Relate to building field,It is made up of the raw material of following weight portion: it is made up of the raw material of following weight portion: methacrylate 20 23 parts,Butyl acrylate 10 15 parts,Methylcellulose 1.5 2 parts,Sodium lauryl sulphate anion 1.5 2 parts,Alcohol ester 12 parts,Sodium methyl silicate 23 parts,Ammonium persulfate. 0.5 1 parts,Ethylene glycol 0.5 1 parts,Allyl glycidol 1.5 2 parts,2.5 3 parts of animal collagen powder,Organic polymer rubber powder 1.5 2 parts,Deionized water 40 50 parts,The invention also discloses the preparation technology of this kind of firming agent,The firming agent water-resistance of the present invention is good,Surface strength is high、Frost resistance is good、Can mix with most soil,Simultaneously,It is simple that the present invention has preparation technology、Cheap、The feature such as be easily mastered easy to use.

Description

A kind of using earth as the external reinforcement agent of decorating inner and external walls and preparation technology thereof
Technical field
The present invention relates to building field, be specifically related to a kind of using earth as the external reinforcement agent of decorating inner and external walls and one Using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls.
Background technology
At present, building decoration field, cement, ceramic tile, glass, marble, the coating of shades of colour have made people produce Visual fatigue.And ecosystem building allows people that the pise of simple and unsophisticated ecosystem creates fine hope, along with this skill The art this pseudo-classic earth decoration of applying in various places is the most gradually favored by people.The application of the present invention is either from economy side For face is still in terms of ecological environment, meaning is the most great.
Earth reconciles into thin pulp shape, and (or adding grass muscle or starch) paints on the inside and outside metope of building, and this is me State has continued to use a kind of decoration technology of thousands of years, and this technique is rarely employed now, and main cause is, water-resistance is not and wall The bond degree in face is bad, low fragile, the defect such as the frequency of maintenance high use time is short of surface strength.The present invention solves emphatically earth The too high problem of liquid limit index, solid after the problem of surface strength.Using the metope of the technology of the present invention brushing, rainwater soaks No longer reverse, do not fall mud do not fall ash cohesive force good, directly can brush on cement brick, fired brick, cement wall, the thickness of brushing is only Needing 1-3mm, metope intensity height is difficult to aging, and Acceptable life, can the rendering of affected coarse exterior wall earth more than 30 years Also the interior wall brushing of smooth exquisiteness can be made by the way of sand papering.Thus the ancient method building decoration side of thousands of years will be used Arriving of method passes on and improvement.Can be widely applied to building in the style of the ancients, ecological folk house, scenic spot building, country villa, characteristic Real Estate Development Inner-outer wall earth rendering in building.
Also there is the coating of imitative earth in market, but be all titanium dioxide, zinc oxide and the allochromatic colour essence pigment thereof of admixture, free Content of beary metal is high, and containing materials such as harmful formaldehyde, benzene, TVOC.
Summary of the invention
The present invention be directed to use earth to paint effect the best as building inside and outside wall and provide using earth as building Build external reinforcement agent and the preparation technology of decorating inner and external walls.
To achieve these goals, the technical scheme that the present invention takes by: the one provided using earth as inner-outer wall The external reinforcement agent of decoration, it is made up of the raw material of following weight portion: methacrylate 20-23 part, butyl acrylate 10-15 Part, methylcellulose 1.5-2 part, sodium lauryl sulphate anion 1.5-2 part, alcohol ester 12 0.8-1 part, sodium methyl silicate 2- 3 parts, Ammonium persulfate. 0.5-1 part, ethylene glycol 0.5-1 part, allyl glycidol 1.5-2 part, animal collagen powder 2.5-3 part, have Machine macromolecule rubber powder 1.5-2 part, deionized water 40-50 part.
Preferably, described Ammonium persulfate. uses potassium peroxydisulfate to replace.
A kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, comprise the following steps:
(1) pre-emulsification solution is prepared: first by the water of 20-30 weight portion, methacrylate, butyl acrylate, dodecane Base sodium sulfate anion emulsifier adds pre-emulsification in emulsator, through being slowly heated, after insulation 0.5h, is cooled to 65 DEG C, obtains Pre-emulsification solution;
(2) seeding polymerization solution is prepared: take the 10-15% of pre-emulsification solution obtained above, with Ammonium persulfate. at 60-65 High-speed stirred at a temperature of DEG C, obtains seeding polymerization solution;
(3) polymerization: by pre-emulsification solution remaining in step (1) and seeding polymerization solution within the 3h time, with cellulose, Animal collagen powder, organic polymer rubber powder, allyl glycidol, sodium silicate, the deionized water of 20-30 weight portion, the most all In even addition reactor, temperature controls at 86-120 DEG C, insulation reaction 1-2h, is cooled to 65 DEG C of sustained responses 0.5h, finally drops Alcohol ester 12 and ethylene glycol, to less than 40 DEG C, are added solution and carry out high-speed stirred 0.5h, then filter, obtain finished product by temperature.
Preferably, in described step (1), heating process is: is slowly heated in 1-1.5h and reaches 90-95 DEG C.
Preferably, described step (2) high speed mixing time is no less than 0.5h.
Preferably, in described step (3), the purity of alcohol ester 12 is more than 95%, and the purity of ethylene glycol is 99%.
Preferably, the equipment that described step (2) and the stirring of step (3) high speed use is planetary stirring machine, from rotating speed Degree is 200RPM, and revolution speed is 180RPM.
The component material that the present invention uses is the material of low toxicity and nonhazardous, without formaldehyde, is not spiked with color essence and a huge sum of money Belong to stain, use the mode of high temperature polymerization, during use, directly use earth to admix as main brushing base material, external reinforcement agent Use ratio is little, the most no matter all goes out almost without the wash rice polluted with harmful toxic matter after solid as exterior wall or interior wall, from this The hazardness contrasting general coating in matter is negligible;The firming agent water-resistance of the present invention is good, and surface strength is high, anti- Freezing property is good, can mix with most soil;It is simple, cheap, easy to use easily that the present invention has preparation technology The features such as grasp.
Detailed description of the invention
Embodiment 1:
A kind of using earth as the external reinforcement agent of decorating inner and external walls, it is made up of the raw material of following weight portion: methyl-prop Olefin(e) acid hydroxyl ethyl ester 22 parts, butyl acrylate 10 parts, methylcellulose 2 parts, sodium lauryl sulphate anion 2 parts, alcohol ester 12 Part, sodium methyl silicate 2 parts, Ammonium persulfate. 1 part, ethylene glycol 1 part, allyl glycidol 1.5 parts, 3 parts of animal collagen powder, organic Macromolecule rubber powder 2 parts, deionized water 43 parts.
A kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, comprise the following steps:
(1) pre-emulsification solution is prepared: first by the water of 20 weight portions, methacrylate, butyl acrylate, dodecyl sulfur Acid sodium anion emulsifier adds pre-emulsification in emulsator, through being slowly heated, after insulation 0.5h, is cooled to 65 DEG C, obtains pre-breast Change solution;
(2) seeding polymerization solution is prepared: take the 10-15% of pre-emulsification solution obtained above, with Ammonium persulfate. at 60-65 High-speed stirred at a temperature of DEG C, obtains seeding polymerization solution;
(3) polymerization: by pre-emulsification solution remaining in step (1) and seeding polymerization solution within the 3h time, with cellulose, Animal collagen powder, organic polymer rubber powder, allyl glycidol, sodium silicate, the deionized water of 23 weight portions, the most uniformly add Entering in reactor, temperature controls at 86 DEG C, and insulation reaction 1-2h is cooled to 65 DEG C of sustained responses 0.5h, is finally cooled to 40 DEG C Hereinafter, alcohol ester 12 and ethylene glycol are added solution and carries out high-speed stirred 0.5h, then filter, obtain finished product.
In the present embodiment, in described step (1), heating process is: is slowly heated in 1-1.5h and reaches 90-95 DEG C, described Step (2) high speed mixing time is that in described step (3), the purity of alcohol ester 12 is more than 95%, second two no less than 0.5h The purity of alcohol is 99%, and the equipment that described step (2) and the stirring of step (3) high speed use is planetary stirring machine, from rotating speed Degree is 200RPM, and revolution speed is 180RPM.
Additionally, described Ammonium persulfate. can use potassium peroxydisulfate to replace.
Embodiment 2:
A kind of using earth as the external reinforcement agent of decorating inner and external walls, it is made up of the raw material of following weight portion: methyl-prop Olefin(e) acid hydroxyl ethyl ester 20 parts, butyl acrylate 12 parts, methylcellulose 1.5 parts, anion sodium lauryl sulphate 2 parts, alcohol ester ten 21 parts, sodium methyl silicate 2 parts, Ammonium persulfate. 0.5 part, ethylene glycol 0.5 part, allyl glycidol 1.5 parts, animal collagen powder 3 Part, organic polymer rubber powder 2 parts, deionized water 45 parts.
A kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, comprise the following steps:
(1) pre-emulsification solution is prepared: first by the water of 20 weight portions, methacrylate, butyl acrylate, dodecyl sulfur Acid sodium anion emulsifier adds pre-emulsification in emulsator, through being slowly heated, after insulation 0.5h, is cooled to 65 DEG C, obtains pre-breast Change solution;
(2) seeding polymerization solution is prepared: take the 10% of pre-emulsification solution obtained above, with Ammonium persulfate. 60 DEG C of temperature Lower high-speed stirred, obtains seeding polymerization solution;
(3) polymerization: by pre-emulsification solution remaining in step (1) and seeding polymerization solution within the 3h time, with cellulose, Animal collagen powder, organic polymer rubber powder, allyl glycidol, sodium silicate, the deionized water of 23 weight portions, the most uniformly add Entering in reactor, temperature controls at 100 DEG C, and insulation reaction 2h is cooled to 65 DEG C of sustained responses 0.5h, is finally cooled to 35 DEG C, Alcohol ester 12 and ethylene glycol are added solution and carries out high-speed stirred 0.5h, then filter, obtain finished product.
In the present embodiment, in described step (1), heating process is: is slowly heated in 1.5h and reaches 90 DEG C, described step (2) high speed mixing time is 0.7h, and in described step (3), the purity of alcohol ester 12 is more than 95%, and the purity of ethylene glycol is 99%, the equipment that described step (2) and the stirring of step (3) high speed use is planetary stirring machine, and rotational velocity is 200RPM, Revolution speed is 180RPM.
Additionally, described Ammonium persulfate. can use potassium peroxydisulfate to replace.
Embodiment 3:
A kind of using earth as the external reinforcement agent of decorating inner and external walls, it is made up of the raw material of following weight portion: methyl-prop Olefin(e) acid hydroxyl ethyl ester 20 parts, butyl acrylate 12 parts, methylcellulose 1.8 parts, anion sodium lauryl sulphate 2 parts, alcohol ester ten 21 parts, sodium methyl silicate 2 parts, Ammonium persulfate. 0.5 part, ethylene glycol 0.5 part, allyl glycidol 1.5 parts, animal collagen powder 3 Part, organic polymer rubber powder 2 parts, deionized water 45 parts.
A kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, comprise the following steps:
(1) pre-emulsification solution is prepared: first by the water of 22 weight portions, methacrylate, butyl acrylate, dodecyl sulfur Acid sodium anion emulsifier adds pre-emulsification in emulsator, through being slowly heated, after insulation 0.5h, is cooled to 65 DEG C, obtains pre-breast Change solution;
(2) seeding polymerization solution is prepared: take the 12% of pre-emulsification solution obtained above, with Ammonium persulfate. 63 DEG C of temperature Lower high-speed stirred, obtains seeding polymerization solution;
(3) polymerization: by pre-emulsification solution remaining in step (1) and seeding polymerization solution within the 3h time, with cellulose, Animal collagen powder, organic polymer rubber powder, allyl glycidol, sodium silicate, the deionized water of 23 weight portions, the most uniformly add Entering in reactor, temperature controls at 120 DEG C, and insulation reaction 1.5h is cooled to 65 DEG C of sustained responses 0.5h, is finally cooled to 36 DEG C, alcohol ester 12 and ethylene glycol are added solution and carries out high-speed stirred 0.5h, then filter, obtain finished product.
Additionally, described Ammonium persulfate. can use potassium peroxydisulfate to replace.
Embodiment 4:
A kind of using earth as the external reinforcement agent of decorating inner and external walls, it is made up of the raw material of following weight portion: methyl-prop Olefin(e) acid hydroxyl ethyl ester 23 parts, butyl acrylate 10 parts, methylcellulose 1.5 parts, anion sodium lauryl sulphate 1.5 parts, alcohol ester 12 parts, sodium methyl silicate 1.5 parts, Ammonium persulfate. 0.5 part, ethylene glycol 0.5 part, allyl glycidol 2 parts, animal glue 2.5 parts of former powder, organic polymer rubber powder 1.5 parts, deionized water 40 parts.
A kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, comprise the following steps:
(1) pre-emulsification solution is prepared: first by the water of 20 weight portions, methacrylate, butyl acrylate, dodecyl sulfur Acid sodium anion emulsifier adds pre-emulsification in emulsator, through being slowly heated, after insulation 0.5h, is cooled to 65 DEG C, obtains pre-breast Change solution;
(2) seeding polymerization solution is prepared: take the 12% of pre-emulsification solution obtained above, with Ammonium persulfate. 63 DEG C of temperature Lower high-speed stirred, obtains seeding polymerization solution;
(3) polymerization: by pre-emulsification solution remaining in step (1) and seeding polymerization solution within the 3h time, with cellulose, Animal collagen powder, organic polymer rubber powder, allyl glycidol, sodium silicate, the deionized water of 20 weight portions, the most uniformly add Entering in reactor, temperature controls at 100 DEG C, and insulation reaction 1.5h is cooled to 65 DEG C of sustained responses 0.5h, is finally cooled to 36 DEG C, alcohol ester 12 and ethylene glycol are added solution and carries out high-speed stirred 0.5h, then filter, obtain finished product.
In the present embodiment, in described step (1), heating process is: is slowly heated in 1.2h and reaches 92 DEG C, described step (2) high speed mixing time is 0.8h, and in described step (3), the purity of alcohol ester 12 is more than 95%, and the purity of ethylene glycol is 99%, the equipment that described step (2) and the stirring of step (3) high speed use is planetary stirring machine, and rotational velocity is 200RPM, Revolution speed is 180RPM.
Additionally, described Ammonium persulfate. can use potassium peroxydisulfate to replace.
Present invention earth additive practices its feature and is: when described additive carries out wall construction, wherein, mud Soil, water, the mixing of additive weigh quality and than scope are: (10-15): (90-80): (10-15).When needing exterior wall to have harsh feeling, The uniform fine sand of below the 1mm of 1-2% can be added, or the rice husk grass muscle amount increased does not exceeds 1-2%, during operation, first by earth Use clear water to be diluted to mud, use the mode of brushing as far as possible, carry out the brushing of about three times.When carrying out interior wall construction, brushing Twice, solid after, use sand papering smooth after, use 1:10 ratio additive at external coating once (uncomfortable earth).
Application examples 1:
Foregoing invention polymerization external reinforcement agent is used to carry out what indoor brushing was applied in November, 2015 in Wangcheng, Hunan Test: after using the water of the additive of 10%, (particle diameter the is less than 1mm) earth of 10% and 75% to be sufficiently stirred for, first carry out 2 The brushing of secondary interior wall, uses the sand paper of 360-400 to polish after 10h, then use the additive diluent of 1:10 ratio (no Adjust earth) at external coating once, earth color does not change, and surfacing does not has light tone.Having construction simple, cost is low Honest and clean, the advantage such as quick-drying, colour-fast, can to wash.Contrast is not spiked with traditional earth decoration technology of additive, and thickness reduces 70%, Surface determination of pencil hardness is H, after soaked 96h without turning white, bubble, coating shedding phenomenon.
Application examples 2:
The polymerization external reinforcement agent using above-mentioned application examples to invent has carried out exterior wall application in July, 2015 in Chenggong, Kunming Test: after using the additive of 10%, the water of particle diameter 1mm earth, the rice husk of 1% and 74% of 15% to be sufficiently stirred for, point The brushing that three times carry out exterior wall, maintains the genuine simple and unsophisticated style of earth, operation thickness 2-2.5mm, after 12 months, and wall Face without luming, going mouldy, flawless, obscission.
Obviously the present invention implements and is not subject to the restrictions described above, as long as have employed method design and the skill of the present invention The improvement of the various unsubstantialities that art scheme is carried out, or the most improved design by the present invention and technical scheme directly apply to it Its occasion, all within protection scope of the present invention.

Claims (7)

1. one kind using earth as the external reinforcement agent of decorating inner and external walls, it is characterised in that it is by the raw material group of following weight portion Become: methacrylate 20-23 part, butyl acrylate 10-15 part, methylcellulose 1.5-2 part, sodium lauryl sulphate cloudy from Sub-1.5-2 part, alcohol ester 12 0.8-1 part, sodium methyl silicate 2-3 part, Ammonium persulfate. 0.5-1 part, ethylene glycol 0.5-1 part, allyl Base (+)-2,3-Epoxy-1-propanol 1.5-2 part, animal collagen powder 2.5-3 part, organic polymer rubber powder 1.5-2 part, deionized water 40-50 part.
2. according to claim 1 using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, it is special Levy and be, comprise the steps:
(1) pre-emulsification solution is prepared: first by the water of 20-30 weight portion, methacrylate, butyl acrylate, dodecyl sulfur Acid sodium anion emulsifier adds pre-emulsification in emulsator, through being slowly heated, after insulation 0.5h, is cooled to 65 DEG C, obtains pre-breast Change solution;
(2) seeding polymerization solution is prepared: take the 10-15% of pre-emulsification solution obtained above, with Ammonium persulfate. 60-65 DEG C of temperature The lower high-speed stirred of degree, obtains seeding polymerization solution;
(3) polymerization: by pre-emulsification solution remaining in step (1) and seeding polymerization solution within the 3h time, with cellulose, animal Collagen powder, organic polymer rubber powder, allyl glycidol, sodium silicate, the deionized water of 20-30 weight portion, the most uniformly add Entering in reactor, temperature controls at 86-120 DEG C, insulation reaction 1-2h, is cooled to 65 DEG C of sustained responses 0.5h, is finally cooled to Less than 40 DEG C, alcohol ester 12 and ethylene glycol are added solution and carries out high-speed stirred 0.5h, then filter, obtain finished product.
The most according to claim 2 a kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, it is special Levying and be, in described step (1), heating process is: is slowly heated in 1-1.5h and reaches 90-95 DEG C.
The most according to claim 2 a kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, it is special Levying and be, described step (2) high speed mixing time is no less than 0.5h.
The most according to claim 2 a kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, it is special Levying and be, in described step (3), the purity of alcohol ester 12 is more than 95%, and the purity of ethylene glycol is 99%.
The most according to claim 2 a kind of using earth as the preparation technology of the external reinforcement agent of decorating inner and external walls, it is special Levying and be, the equipment that described step (2) and the stirring of step (3) high speed use is planetary stirring machine, and rotational velocity is 200RPM, revolution speed is 180RPM.
The most according to claim 1 a kind of using earth as the external reinforcement agent of decorating inner and external walls, it is characterised in that described Ammonium persulfate. uses potassium peroxydisulfate to replace.
CN201610654849.XA 2016-08-10 2016-08-10 A kind of using earth as the external reinforcement agent of decorating inner and external walls and preparation technology thereof Pending CN106280664A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116515330A (en) * 2023-05-24 2023-08-01 奈拓新材料(杭州)有限公司 Water-proof zero-formaldehyde inorganic interior wall coating

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101037597A (en) * 2007-04-18 2007-09-19 南京大学 Ecological soil stabilizer and preparation method thereof
JP2009046542A (en) * 2007-08-16 2009-03-05 Koyo Sangyo Co Ltd Putty composition, and decoration plywood repaired using the same
CN102020990A (en) * 2009-09-22 2011-04-20 山东宏艺科技股份有限公司 Novel high-strength waterproof composite solid curing agent
CN103194241A (en) * 2013-04-26 2013-07-10 潘志刚 Polymer aggregation agent for high order aggregate spray seeding greening, and preparation method thereof
CN104497776A (en) * 2014-02-21 2015-04-08 井冈山大学 Reinforcement protection agent for mud wall and attached mortar layer surface slogans and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101037597A (en) * 2007-04-18 2007-09-19 南京大学 Ecological soil stabilizer and preparation method thereof
JP2009046542A (en) * 2007-08-16 2009-03-05 Koyo Sangyo Co Ltd Putty composition, and decoration plywood repaired using the same
CN102020990A (en) * 2009-09-22 2011-04-20 山东宏艺科技股份有限公司 Novel high-strength waterproof composite solid curing agent
CN103194241A (en) * 2013-04-26 2013-07-10 潘志刚 Polymer aggregation agent for high order aggregate spray seeding greening, and preparation method thereof
CN104497776A (en) * 2014-02-21 2015-04-08 井冈山大学 Reinforcement protection agent for mud wall and attached mortar layer surface slogans and preparation method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN116515330A (en) * 2023-05-24 2023-08-01 奈拓新材料(杭州)有限公司 Water-proof zero-formaldehyde inorganic interior wall coating

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