CN106279570A - 一种改性栲胶陶瓷减水剂及其制备方法 - Google Patents
一种改性栲胶陶瓷减水剂及其制备方法 Download PDFInfo
- Publication number
- CN106279570A CN106279570A CN201610556518.2A CN201610556518A CN106279570A CN 106279570 A CN106279570 A CN 106279570A CN 201610556518 A CN201610556518 A CN 201610556518A CN 106279570 A CN106279570 A CN 106279570A
- Authority
- CN
- China
- Prior art keywords
- reducing agent
- water reducing
- preparation
- tannin extract
- modified tannin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 62
- 239000000919 ceramic Substances 0.000 title claims abstract description 47
- 239000003638 chemical reducing agent Substances 0.000 title claims abstract description 41
- 239000000284 extract Substances 0.000 title claims abstract description 37
- 235000018553 tannin Nutrition 0.000 title claims abstract description 27
- 229920001864 tannin Polymers 0.000 title claims abstract description 27
- 239000001648 tannin Substances 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 238000003756 stirring Methods 0.000 claims abstract description 20
- -1 allyloxy 2 hydroxypropionate Chemical compound 0.000 claims abstract description 12
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 10
- 235000011149 sulphuric acid Nutrition 0.000 claims abstract description 10
- 150000001412 amines Chemical class 0.000 claims abstract description 9
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Natural products P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229910000073 phosphorus hydride Inorganic materials 0.000 claims abstract description 8
- 239000003999 initiator Substances 0.000 claims abstract description 7
- 229920002554 vinyl polymer Polymers 0.000 claims abstract description 7
- 239000001117 sulphuric acid Substances 0.000 claims abstract description 4
- CHQMHPLRPQMAMX-UHFFFAOYSA-L sodium persulfate Chemical compound [Na+].[Na+].[O-]S(=O)(=O)OOS([O-])(=O)=O CHQMHPLRPQMAMX-UHFFFAOYSA-L 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 17
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- VVJKKWFAADXIJK-UHFFFAOYSA-N Allylamine Chemical compound NCC=C VVJKKWFAADXIJK-UHFFFAOYSA-N 0.000 claims description 14
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 10
- USHAGKDGDHPEEY-UHFFFAOYSA-L potassium persulfate Chemical compound [K+].[K+].[O-]S(=O)(=O)OOS([O-])(=O)=O USHAGKDGDHPEEY-UHFFFAOYSA-L 0.000 claims description 9
- 235000019394 potassium persulphate Nutrition 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 8
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 claims description 6
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical compound OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 claims description 6
- YPJHXRAHMUKXAE-UHFFFAOYSA-N 3-diethoxyphosphorylprop-1-ene Chemical compound CCOP(=O)(CC=C)OCC YPJHXRAHMUKXAE-UHFFFAOYSA-N 0.000 claims description 5
- DYUWTXWIYMHBQS-UHFFFAOYSA-N n-prop-2-enylprop-2-en-1-amine Chemical compound C=CCNCC=C DYUWTXWIYMHBQS-UHFFFAOYSA-N 0.000 claims description 5
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 5
- 229910001870 ammonium persulfate Inorganic materials 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
- 230000003467 diminishing effect Effects 0.000 claims description 3
- VPYJNCGUESNPMV-UHFFFAOYSA-N triallylamine Chemical compound C=CCN(CC=C)CC=C VPYJNCGUESNPMV-UHFFFAOYSA-N 0.000 claims description 3
- 235000003642 hunger Nutrition 0.000 claims 1
- 230000000977 initiatory effect Effects 0.000 claims 1
- 235000015424 sodium Nutrition 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 description 8
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 3
- 239000000654 additive Substances 0.000 description 3
- 230000008901 benefit Effects 0.000 description 3
- YLFBFPXKTIQSSY-UHFFFAOYSA-N dimethoxy(oxo)phosphanium Chemical compound CO[P+](=O)OC YLFBFPXKTIQSSY-UHFFFAOYSA-N 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- 239000002002 slurry Substances 0.000 description 3
- NIQCNGHVCWTJSM-UHFFFAOYSA-N Dimethyl phthalate Chemical compound COC(=O)C1=CC=CC=C1C(=O)OC NIQCNGHVCWTJSM-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- FLKPEMZONWLCSK-UHFFFAOYSA-N diethyl phthalate Chemical compound CCOC(=O)C1=CC=CC=C1C(=O)OCC FLKPEMZONWLCSK-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 125000000524 functional group Chemical group 0.000 description 2
- RZKYDQNMAUSEDZ-UHFFFAOYSA-N prop-2-enylphosphonic acid Chemical compound OP(O)(=O)CC=C RZKYDQNMAUSEDZ-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 125000003368 amide group Chemical group 0.000 description 1
- 229910052925 anhydrite Inorganic materials 0.000 description 1
- 235000015895 biscuits Nutrition 0.000 description 1
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 150000001993 dienes Chemical class 0.000 description 1
- LXCYSACZTOKNNS-UHFFFAOYSA-N diethoxy(oxo)phosphanium Chemical compound CCO[P+](=O)OCC LXCYSACZTOKNNS-UHFFFAOYSA-N 0.000 description 1
- 239000003085 diluting agent Substances 0.000 description 1
- FBSAITBEAPNWJG-UHFFFAOYSA-N dimethyl phthalate Natural products CC(=O)OC1=CC=CC=C1OC(C)=O FBSAITBEAPNWJG-UHFFFAOYSA-N 0.000 description 1
- 229960001826 dimethylphthalate Drugs 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 230000005661 hydrophobic surface Effects 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 description 1
- 235000013923 monosodium glutamate Nutrition 0.000 description 1
- 239000004223 monosodium glutamate Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 235000019832 sodium triphosphate Nutrition 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F289/00—Macromolecular compounds obtained by polymerising monomers on to macromolecular compounds not provided for in groups C08F251/00 - C08F287/00
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/632—Organic additives
- C04B35/634—Polymers
- C04B35/63404—Polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C04B35/63444—Nitrogen-containing polymers, e.g. polyacrylamides, polyacrylonitriles, polyvinylpyrrolidone [PVP], polyethylenimine [PEI]
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Compounds Of Unknown Constitution (AREA)
Abstract
Description
粘土 | 高岭土 | 长石 | 石英粉 |
40% | 15% | 30% | 15% |
Claims (6)
Priority Applications (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201811082480.5A CN109467652A (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂的制备方法 |
CN201811082486.2A CN109320672A (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂的制备方法 |
CN201610556518.2A CN106279570B (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610556518.2A CN106279570B (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂及其制备方法 |
Related Child Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201811082486.2A Division CN109320672A (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂的制备方法 |
CN201811082480.5A Division CN109467652A (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106279570A true CN106279570A (zh) | 2017-01-04 |
CN106279570B CN106279570B (zh) | 2018-12-07 |
Family
ID=57651606
Family Applications (3)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201811082480.5A Pending CN109467652A (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂的制备方法 |
CN201811082486.2A Pending CN109320672A (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂的制备方法 |
CN201610556518.2A Expired - Fee Related CN106279570B (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂及其制备方法 |
Family Applications Before (2)
Application Number | Title | Priority Date | Filing Date |
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CN201811082480.5A Pending CN109467652A (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂的制备方法 |
CN201811082486.2A Pending CN109320672A (zh) | 2016-07-15 | 2016-07-15 | 一种改性栲胶陶瓷减水剂的制备方法 |
Country Status (1)
Country | Link |
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CN (3) | CN109467652A (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108640693A (zh) * | 2018-06-17 | 2018-10-12 | 刘玉清 | 一种高分子陶瓷解凝剂及其制备方法 |
CN108675800A (zh) * | 2018-06-17 | 2018-10-19 | 刘玉清 | 一种改性茶皂素陶瓷解凝剂及其制备方法 |
CN108715552A (zh) * | 2018-06-17 | 2018-10-30 | 刘玉清 | 一种陶瓷解凝剂及其制备方法 |
CN111454065A (zh) * | 2020-03-20 | 2020-07-28 | 肇庆市欧陶新型材料有限公司 | 一种N、P、Si化合物有机无机复合陶瓷解胶剂 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102675560A (zh) * | 2012-05-02 | 2012-09-19 | 陆明富 | 一种抗高温降粘剂的制备方法 |
CN105384380A (zh) * | 2015-12-07 | 2016-03-09 | 安徽省阜南绿原化工有限公司 | 一种栲胶/聚羧酸混凝土减水剂及其制备方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104610514B (zh) * | 2014-12-30 | 2017-08-29 | 福建清源科技有限公司 | 一种改性木质素磺酸盐减水剂及其制备方法 |
-
2016
- 2016-07-15 CN CN201811082480.5A patent/CN109467652A/zh active Pending
- 2016-07-15 CN CN201811082486.2A patent/CN109320672A/zh active Pending
- 2016-07-15 CN CN201610556518.2A patent/CN106279570B/zh not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102675560A (zh) * | 2012-05-02 | 2012-09-19 | 陆明富 | 一种抗高温降粘剂的制备方法 |
CN105384380A (zh) * | 2015-12-07 | 2016-03-09 | 安徽省阜南绿原化工有限公司 | 一种栲胶/聚羧酸混凝土减水剂及其制备方法 |
Non-Patent Citations (2)
Title |
---|
刘程等: "《表面活性剂应用手册 第三版》", 30 September 2004, 化学工业出版社 * |
李松林: "《混凝土涉及与施工简明手册》", 31 May 2011, 中国电力出版社 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108640693A (zh) * | 2018-06-17 | 2018-10-12 | 刘玉清 | 一种高分子陶瓷解凝剂及其制备方法 |
CN108675800A (zh) * | 2018-06-17 | 2018-10-19 | 刘玉清 | 一种改性茶皂素陶瓷解凝剂及其制备方法 |
CN108715552A (zh) * | 2018-06-17 | 2018-10-30 | 刘玉清 | 一种陶瓷解凝剂及其制备方法 |
CN111454065A (zh) * | 2020-03-20 | 2020-07-28 | 肇庆市欧陶新型材料有限公司 | 一种N、P、Si化合物有机无机复合陶瓷解胶剂 |
Also Published As
Publication number | Publication date |
---|---|
CN106279570B (zh) | 2018-12-07 |
CN109320672A (zh) | 2019-02-12 |
CN109467652A (zh) | 2019-03-15 |
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Effective date of registration: 20191212 Address after: 214500 No.27, jujiadai, Yujia village, Xilai Town, Jingjiang City, Taizhou City, Jiangsu Province Patentee after: Wang Xiulan Address before: Shishi Haojiang road Quanzhou City, Fujian province 362700 No. 707 Building 1 Room 102 Patentee before: Li Bicha |
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TR01 | Transfer of patent right | ||
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Effective date of registration: 20201009 Address after: Room j2050, No. 912, Yecheng Road, Jiading Industrial Zone, Jiading District, Shanghai, 201800 Patentee after: Shanghai zhongang Industrial Co.,Ltd. Address before: 214500 No.27, jujiadai, Yujia village, Xilai Town, Jingjiang City, Taizhou City, Jiangsu Province Patentee before: Wang Xiulan |
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Effective date of registration: 20201204 Address after: 214537, No. 28 River Road, Xinqiao Town, Jingjiang City, Jiangsu, Taizhou Patentee after: NAIR ENERGY EQUIPMENT Co.,Ltd. Address before: Room j2050, No. 912, Yecheng Road, Jiading Industrial Zone, Jiading District, Shanghai, 201800 Patentee before: Shanghai zhongang Industrial Co.,Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20181207 |