CN106277785A - A kind of black matrix erythema pottery glaze - Google Patents
A kind of black matrix erythema pottery glaze Download PDFInfo
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- CN106277785A CN106277785A CN201610680523.4A CN201610680523A CN106277785A CN 106277785 A CN106277785 A CN 106277785A CN 201610680523 A CN201610680523 A CN 201610680523A CN 106277785 A CN106277785 A CN 106277785A
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- black matrix
- erythema
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Glass Compositions (AREA)
Abstract
A kind of black matrix erythema pottery glaze, it is made up of black matrix glaze and erythema glaze two parts, described black matrix glaze is prepared by the raw materials in: iron sesquioxide 7 15 parts, silicon dioxide 50 70 parts, aluminium sesquioxide 8 15 parts, calcium oxide 5 10 parts, magnesium oxide 12 parts, potassium oxide 36 parts, sodium oxide 25 parts;Described erythema glaze is prepared by the raw materials in: copper oxide 59 parts, zinc oxide 36 parts, silicon dioxide 50 70 parts, aluminium sesquioxide 8 15 parts, potassium oxide 36 parts, sodium oxide 25 parts, tin ash 12 parts;The black matrix erythema pottery glaze that the present invention makes is the most penetrating, has a third dimension, and good fluidity is the most easy to foaming, good luster;Black matrix glaze is colour-stable, uniform color, after element tire is painted with black matrix glaze, and the local painting erythema glaze can formulated on surface, the black matrix erythema pottery glaze that pattern is basically identical can be fired, hinge structure makes great progress.
Description
Technical field
The invention belongs to pottery manufacturing technology field, be specifically related to a kind of black matrix erythema pottery glaze.
Background technology
Pottery is thick for this with glaze, and at the bottom of its color or heavy glaze or in outstanding glaze or floating glaze table, the thick muddy work of glaze, glaze layer opalescence jade-like stone moistens,
Being administrations with multiplied departments lives is intended to drip, and third dimension is extremely strong.Pottery is with transmutation as god, and natural transmutation is the elite place of pottery art, is also
Pottery is rely the four seas of becoming famous, the rare part of porcelain woods of making a name.With executing a kind of glaze in firing, once burning till in multicoloured it is then
" enter kiln of the same colour, kiln discharge ten thousand is color ".Protean transmutation effect, defines the mystery that colors changing hue is infinite, in red inner purple, purple
During in dark blue, blue or green, residence is white, white general red, five colours imbibition, form a brightening, and have the title of ", without right, transmutation is unparalleled for pottery ".
Making pottery when, although present technology has been achieved for remarkable progress, but there are some defects,
Pottery fires finished product in manufacturing process from selecting materials to, and period experiences tens of roads production process, accidentally also making of an operation
All that has been achieved is spoiled for one-tenth, and this is also the reason that pottery yield all the time is extremely low.Pottery it is critical only that enamel, enamel is being fired
After transmutation chatoyance determine the value of pottery, the pottery of white has bluish white, grey dawn, creamy white, beautiful white etc., and blue pottery has
Sky blue, acid blue, powder are blue, sapphire blue, peacock blue;Additionally because the main component of enamel is Anhydrite and Kaolin so that an ancient unit of weight kiln exists
Easily ftracture after kiln discharge cooling, reduce treasure rate.The difference of enamel formula, the color burnt out is the most variant, and tradition is burnt
During pottery processed, it is to execute one layer of glaze, according to firing environment an ancient unit of weight glaze generation transmutation in kiln, it may appear that some are uncontrollable on element tire surface
The decorative pattern of system or color lump, the more difficult pairing of finished product burnt out or configure complete.Therefore, it is badly in need of one to burn at ad-hoc location
Make the pottery burning process of specific decorative pattern.
In prior art, formula of black matrix erythema pottery glaze and preparation method thereof is the most little, and the black matrix erythema prepared
It is poor that pottery glaze surface easily produces slight crack, glaze wearability and resistance to mechanical ability, beautiful sense deficiency.
Summary of the invention
In order to solve the problems referred to above, the present invention provides a kind of black matrix erythema pottery glaze.
The technical solution used in the present invention is:
A kind of black matrix erythema pottery glaze, is made up of black matrix glaze and erythema glaze two parts, described black matrix glaze be by under
The raw material of row weight portion is made: iron sesquioxide 7-15 part, silicon dioxide 50-70 part, aluminium sesquioxide 8-15 part, calcium oxide
5-10 part, magnesium oxide 1-2 part, potassium oxide 3-6 part, sodium oxide 2-5 part;
Described erythema glaze is prepared by the raw materials in: copper oxide 5-9 part, zinc oxide 3-6 part, silicon dioxide
50-70 part, aluminium sesquioxide 8-15 part, potassium oxide 3-6 part, sodium oxide 2-5 part, tin ash 1-2 part.
A kind of black matrix erythema pottery glaze, described black matrix glaze is prepared by the raw materials in: three oxidations
Two ferrum 10 parts, silicon dioxide 60 parts, aluminium sesquioxide 10 parts, calcium oxide 8 parts, magnesium oxide 1.5 parts, potassium oxide 5 parts, sodium oxide 4
Part;
Described erythema glaze is prepared by the raw materials in: copper oxide 8 parts, zinc oxide 5 parts, silicon dioxide 60
Part, aluminium sesquioxide 10 parts, potassium oxide 5 parts, sodium oxide 4 parts, tin ash 1.5 parts.
The present invention also provides for a kind of method preparing black matrix erythema pottery glaze with above-mentioned black matrix erythema pottery glaze:
(1) glazing: first immersed by base substrate in the glaze slip of black matrix glaze and take out in a moment, utilizes the water absorption of base substrate, makes glaze slip equal
Even is attached to billet surface;After the slurry of black matrix glaze dries, then dip the glaze slip painting of erythema glaze with brush pen or brush
Local at base substrate;After glazing, base substrate is loaded saggar;
(2) the glaze firing oxidizing flame stage: first by saggar loading of kiln, then kiln temperature is gradually raised to 1040 DEG C from 0 DEG C, control ventilation
Chimney casket plate is open, and kiln crown skylight is open, in oxidizing atmosphere in kiln, and organic in moisture in saggar, base substrate and kiln and glaze
Things etc. are discharged, and glaze layer starts fusing, and glaze surface is unsintered fine granularity;
(3) the glaze firing reducing flame stage: kiln temperature is at 1040 DEG C-1150 DEG C, and this stage skylight is closed, the closedown of flue casket door or half
Open, coal can not fully burn, and carbon monoxide increases, and in reducing atmosphere in kiln, glaze layer melts, and glaze gradually closes by porous
Close, form rough state;
(4) the neutral flame stage: kiln temperature is raised to 1270 DEG C by 1150 DEG C, in weakly reducing atmosphere in kiln, along with kiln temperature liter
High glaze layer is fused into thick liquid nano and from top to bottom flows, and the melted of glaze layer makes glaze flatten, and glaze layer forms vitreous;
(5) oxidation cooling stage: when kiln temperature is raised to 1250 DEG C-1300 DEG C, soaking is ceased fire after being incubated 1-2 hour, is opened
Wicket, a large amount of oxygen enter in kiln, and in oxidizing atmosphere in kiln, glaze is aoxidized by oxygen, cooling, and glaze colours is formed.
The invention has the beneficial effects as follows: the black matrix erythema pottery glaze that the present invention makes is the most penetrating, has third dimension, flowing
Property is good, the most easy to foaming, good luster;Black matrix glaze is colour-stable, uniform color, after element tire is painted with black matrix glaze, and Ke Yi
The local painting erythema glaze that surface is formulated, can fire the black matrix erythema pottery glaze that pattern is basically identical, and hinge structure has
The biggest progress.
Detailed description of the invention
A kind of black matrix erythema pottery glaze, is made up of black matrix glaze and erythema glaze two parts, and described black matrix glaze is
It is prepared by the raw materials in: iron sesquioxide 7-15 part, silicon dioxide 50-70 part, aluminium sesquioxide 8-15 part, oxygen
Change calcium 5-10 part, magnesium oxide 1-2 part, potassium oxide 3-6 part, sodium oxide 2-5 part;
Described erythema glaze is prepared by the raw materials in: copper oxide 5-9 part, zinc oxide 3-6 part, silicon dioxide
50-70 part, aluminium sesquioxide 8-15 part, potassium oxide 3-6 part, sodium oxide 2-5 part, tin ash 1-2 part.
A kind of black matrix erythema pottery glaze, described black matrix glaze is prepared by the raw materials in: three oxidations
Two ferrum 10 parts, silicon dioxide 60 parts, aluminium sesquioxide 10 parts, calcium oxide 8 parts, magnesium oxide 1.5 parts, potassium oxide 5 parts, sodium oxide 4
Part;
Described erythema glaze is prepared by the raw materials in: copper oxide 8 parts, zinc oxide 5 parts, silicon dioxide 60
Part, aluminium sesquioxide 10 parts, potassium oxide 5 parts, sodium oxide 4 parts, tin ash 1.5 parts.
The present invention also provides for a kind of method preparing black matrix erythema pottery glaze with above-mentioned black matrix erythema pottery glaze:
(1) glazing: first entered by base substrate in the glaze slip of black matrix glaze and take out in a moment, utilizes the water absorption of base substrate, makes glaze slip equal
Even is attached to billet surface;After the slurry of black matrix glaze dries, then dip the glaze slip painting of erythema glaze with brush pen or brush
Local at base substrate;After glazing, base substrate is loaded saggar;
(2) the glaze firing oxidizing flame stage: first by saggar loading of kiln, then kiln temperature is gradually raised to 1040 DEG C from 0 DEG C, control ventilation
Chimney casket plate is open, and kiln crown skylight is open, in oxidizing atmosphere in kiln, and organic in moisture in saggar, base substrate and kiln and glaze
Thing is discharged, and glaze layer starts fusing, and glaze surface is unsintered fine granularity;
(3) the glaze firing reducing flame stage: kiln temperature is at 1040 DEG C-1150 DEG C, and this stage skylight is closed, the closedown of flue casket door or half
Open, coal can not fully burn, and carbon monoxide increases, and in reducing atmosphere in kiln, glaze layer melts, and glaze gradually closes by porous
Close, form rough state;
(4) the neutral flame stage: kiln temperature is raised to 1270 DEG C by 1150 DEG C, in weakly reducing atmosphere in kiln, along with kiln temperature liter
High glaze layer is fused into thick liquid nano and from top to bottom flows, and the melted of glaze layer makes glaze flatten, and glaze layer forms vitreous;
(5) oxidation cooling stage: when kiln temperature is raised to 1250 DEG C-1300 DEG C, soaking is ceased fire after being incubated 1-2 hour, is opened
Wicket, a large amount of oxygen enter in kiln, and in oxidizing atmosphere in kiln, glaze is aoxidized by oxygen, cooling, and glaze colours is formed.
Embodiment 1
A kind of black matrix erythema pottery glaze, is made up of black matrix glaze and erythema glaze two parts, described black matrix glaze be by under
The raw material of row weight portion is made: iron sesquioxide 10 parts, silicon dioxide 60 parts, aluminium sesquioxide 10 parts, calcium oxide 8 parts, oxygen
Change 1.5 parts of magnesium, potassium oxide 5 parts, sodium oxide 4 parts;
Described erythema glaze is prepared by the raw materials in: copper oxide 8 parts, zinc oxide 5 parts, silicon dioxide 60
Part, aluminium sesquioxide 10 parts, potassium oxide 5 parts, sodium oxide 4 parts, tin ash 1.5 parts.
The present invention also provides for a kind of method preparing black matrix erythema pottery glaze with above-mentioned black matrix erythema pottery glaze:
(1) glazing: first entered by base substrate in the glaze slip of black matrix glaze and take out in a moment, utilizes the water absorption of base substrate, makes glaze slip equal
Even is attached to billet surface;After the slurry of black matrix glaze dries, then dip the glaze slip painting of erythema glaze with brush pen or brush
Local at base substrate;After glazing, base substrate is loaded saggar;
(2) the glaze firing oxidizing flame stage: first by saggar loading of kiln, then kiln temperature is gradually raised to 1040 DEG C from 0 DEG C, control ventilation
Chimney casket plate is open, and kiln crown skylight is open, in oxidizing atmosphere in kiln, and organic in moisture in saggar, base substrate and kiln and glaze
Thing is discharged, and glaze layer starts fusing, and glaze surface is unsintered fine granularity;
(3) the glaze firing reducing flame stage: kiln temperature is at 1040 DEG C-1150 DEG C, and this stage skylight is closed, the closedown of flue casket door or half
Open, coal can not fully burn, and carbon monoxide increases, and in reducing atmosphere in kiln, glaze layer melts, and glaze gradually closes by porous
Close, form rough state;
(4) the neutral flame stage: kiln temperature is raised to 1270 DEG C by 1150 DEG C, in weakly reducing atmosphere in kiln, along with kiln temperature liter
High glaze layer is fused into thick liquid nano and from top to bottom flows, and the melted of glaze layer makes glaze flatten, and glaze layer forms vitreous;
(5) oxidation cooling stage: when kiln temperature is raised to 1250 DEG C-1300 DEG C, soaking is ceased fire after being incubated 1-2 hour, is opened
Wicket, a large amount of oxygen enter in kiln, and in oxidizing atmosphere in kiln, glaze is aoxidized by oxygen, cooling, and glaze colours is formed.
Embodiment 2
A kind of black matrix erythema pottery glaze, is made up of black matrix glaze and erythema glaze two parts, described black matrix glaze be by under
The raw material of row weight portion is made: iron sesquioxide 7 parts, silicon dioxide 50 parts, aluminium sesquioxide 8 parts, calcium oxide 5 parts, oxidation
1 part of magnesium, potassium oxide 3 parts, sodium oxide 2 parts;
Described erythema glaze is prepared by the raw materials in: copper oxide 5 parts, zinc oxide 3 parts, silicon dioxide 50
Part, aluminium sesquioxide 8 parts, potassium oxide 3 parts, sodium oxide 2 parts, tin ash 1 part.
Embodiment 3
A kind of black matrix erythema pottery glaze, is made up of black matrix glaze and erythema glaze two parts, described black matrix glaze be by under
The raw material of row weight portion is made: iron sesquioxide 15 parts, silicon dioxide 70 parts, aluminium sesquioxide 15 parts, calcium oxide 10 parts, oxygen
Change 2 parts of magnesium, potassium oxide 6 parts, sodium oxide 5 parts;
Described erythema glaze is prepared by the raw materials in: copper oxide 9 parts, zinc oxide 6 parts, silicon dioxide 70
Part, aluminium sesquioxide 15 parts, potassium oxide 6 parts, sodium oxide 5 parts, tin ash 2 parts.
Claims (2)
1. a black matrix erythema pottery glaze, is made up of black matrix glaze and erythema glaze two parts, it is characterised in that: described is black
Ground-coat enamel material is prepared by the raw materials in: iron sesquioxide 7-15 part, silicon dioxide 50-70 part, aluminium sesquioxide
8-15 part, calcium oxide 5-10 part, magnesium oxide 1-2 part, potassium oxide 3-6 part, sodium oxide 2-5 part;
Described erythema glaze is prepared by the raw materials in: copper oxide 5-9 part, zinc oxide 3-6 part, silicon dioxide
50-70 part, aluminium sesquioxide 8-15 part, potassium oxide 3-6 part, sodium oxide 2-5 part, tin ash 1-2 part.
A kind of black matrix erythema pottery glaze the most according to claim 1, it is characterised in that: described black matrix glaze be by under
The raw material of row weight portion is made: iron sesquioxide 10 parts, silicon dioxide 60 parts, aluminium sesquioxide 10 parts, calcium oxide 8 parts, oxygen
Change 1.5 parts of magnesium, potassium oxide 5 parts, sodium oxide 4 parts;
Described erythema glaze is prepared by the raw materials in: copper oxide 8 parts, zinc oxide 5 parts, silicon dioxide 60
Part, aluminium sesquioxide 10 parts, potassium oxide 5 parts, sodium oxide 4 parts, tin ash 1.5 parts.
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CN201610680523.4A CN106277785A (en) | 2016-08-18 | 2016-08-18 | A kind of black matrix erythema pottery glaze |
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CN201610680523.4A CN106277785A (en) | 2016-08-18 | 2016-08-18 | A kind of black matrix erythema pottery glaze |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107098677A (en) * | 2017-05-31 | 2017-08-29 | 福建德化陶知然陶瓷文化创意有限公司 | Black matrix erythema droplet temmoku glaze ceramics and its preparation technology |
CN107698151A (en) * | 2017-10-20 | 2018-02-16 | 晋晓瞳 | A kind of pottery brick and preparation method thereof |
CN109455931A (en) * | 2018-12-12 | 2019-03-12 | 湖南德兴瓷业有限公司 | A kind of novel furnace transmutation glaze and its preparation process |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105175019A (en) * | 2015-07-24 | 2015-12-23 | 郏县神前传奇陶瓷钧瓷厂 | Complex Tang-dynasty jun glaze with red spots in black and process for preparing jun porcelain by use of complex Tang-dynasty jun glaze |
-
2016
- 2016-08-18 CN CN201610680523.4A patent/CN106277785A/en active Pending
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105175019A (en) * | 2015-07-24 | 2015-12-23 | 郏县神前传奇陶瓷钧瓷厂 | Complex Tang-dynasty jun glaze with red spots in black and process for preparing jun porcelain by use of complex Tang-dynasty jun glaze |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107098677A (en) * | 2017-05-31 | 2017-08-29 | 福建德化陶知然陶瓷文化创意有限公司 | Black matrix erythema droplet temmoku glaze ceramics and its preparation technology |
CN107098677B (en) * | 2017-05-31 | 2020-07-21 | 福建德化陶知然陶瓷文化创意有限公司 | Black-bottom red-spot oil-drop temmoku glaze ceramic and preparation process thereof |
CN107698151A (en) * | 2017-10-20 | 2018-02-16 | 晋晓瞳 | A kind of pottery brick and preparation method thereof |
CN109455931A (en) * | 2018-12-12 | 2019-03-12 | 湖南德兴瓷业有限公司 | A kind of novel furnace transmutation glaze and its preparation process |
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