CN106266586A - The Chinese medicine composition of a kind of postoperation hemostatic sterilization and preparation and preparation method - Google Patents
The Chinese medicine composition of a kind of postoperation hemostatic sterilization and preparation and preparation method Download PDFInfo
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- CN106266586A CN106266586A CN201510278288.3A CN201510278288A CN106266586A CN 106266586 A CN106266586 A CN 106266586A CN 201510278288 A CN201510278288 A CN 201510278288A CN 106266586 A CN106266586 A CN 106266586A
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Abstract
The present invention relates to the Chinese medicine composition for postoperation hemostatic sterilization, said composition is mainly prepared from than processed by certain part by weight by Radix Notoginseng, Semen Ricini, Oletum Trogopterori, Cacumen Tamaricis, the Pseudobulbus Bletillae (Rhizoma Bletillae), Rhizoma Saururi (Herba Saururi), Pollen Typhae carbon and Folium Artemisiae Argyi；Said composition uses multiple pure natural medical material meticulously to develop, and health environment-friendly, haemostatic effect is good；Additionally having the effect of sterilization antiinflammatory while hemostasis, wound does not infects, and has effect that hemostasis and pain-relieving, effectively sterilization and suppression are infected, surgery operation sterilizing arresting bleeding and healing up ulcer is had good effect.
Description
Technical field
The invention belongs to field of pharmaceutical preparations, the Chinese drug-treated group sterilized particularly to a kind of postoperation hemostatic
Compound.
Background technology
Along with the development of modern medicine, operation becomes the effective remedy measures of some diseases,
On surgical clinical, traumatic hemorrhage, hands intraoperative hemorrhage and postoperative wound are hemorrhage is common disease
Wait, and polyphyly clinic danger, urgency, serious symptom.May result in shock during Massive Bleeding, cause life
Danger, the most hemorrhage also with pain, inflammation etc., outside injury put, operation technique and
During postoperative monitoring, it is necessary to using hemostasis as the most urgent disposal means.On the other hand,
Can not stop blooding in time if hemorrhage, then can deposit in vivo, cause other diseases.Many arts
Postoperative infection forms refractory wound, and wound forms pyogenic infection, causes prolonged not healing, to suffering from
Person brings the most painful and psychological burden.
At present, hemorrhage to trauma wound, the Hemostasis of employing be；During operation
Bleeding part hemostasis general use mosquito forceps to stop blooding temporarily, then use ligation or the side of burning
Method processes；Postoperative wound hemorrhage typically adopting is covered with aseptic cotton after debridement, then with yarn of sterilizing
Cloth is wrapped up, to reach fixing wound, the purpose of hemostasis.These methods possess certain
Effect, but to more situations of losing blood such as large-area wound, deep wound, effect is inadequate
Ideal, healing time is long, postoperative wound delayed healing, increases wound infection probability, and holds
Easily leave ugly cicatrix.Additionally, in terms of sterilization infection after hemostasis, trauma wound
When using wrapping Hemostasis, generally use sterile saline to rinse, be aided with iodine tincture etc. and disappear
Toxic agent infection, such troublesome poeration, inefficiency, sterilize the most thorough；To surgical wound surface
The sterilization of wound generally uses local debridement, disinfection, is aided with antibiotics suppression and infects,
Impact on patient's self immune system is relatively big, and healing time is long, easy infection, carries to patient
Carry out Affliction grade seriously, also increase the weight of the work load of medical worker.
Summary of the invention
It is a feature of the present invention that the Chinese medicine composition that a kind of sterilization of stopping blooding is provided, and preparation
The method of this Chinese medicine composition, utilizes the mutual synergism of active component of multiple Chinese herbal medicine,
Can sterilize again while hemostasis, the hemostasis of surgical operation wound surface can be widely used in.
For achieving the above object, the technical solution used in the present invention is as follows:
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, mainly by the crude drug warp of following weight portion
Processing is prepared from:
The method have the benefit that invention uses multiple pure natural medical material meticulously to develop,
Health environment-friendly, haemostatic effect is good, contains the Chinese medicine ingredients of anti-inflammation simultaneously, and wound does not infects,
There is effect that hemostasis and pain-relieving, effectively sterilization and suppression are infected, surgery disinfecting hemostasis sore is had
There is good effect.
Improve further, the Chinese medicine composition of postoperation hemostatic of the present invention sterilization, also include as
The crude drug of lower weight portion:
Concha Arcae 6-13 Flos Lonicerae 3-10 Herba Houttuyniae 2-8 Colla Corii Asini 2-6.
Add Concha Arcae, Flos Lonicerae, Herba Houttuyniae and Colla Corii Asini, strengthening haemostatic effect simultaneously, having
Effect strengthens sterilization, antibacterial, antiphlogistic effects, evident in efficacy, is a kind of extraordinary external hemostasis
Medicament.
Preferably, the parts by weight preparing the raw materials used medicine of described compositions are:
Further preferably, the parts by weight preparing the raw materials used medicine of described compositions are:
Another aspect of the present invention provides the preparation side of the Chinese medicine composition of described postoperation hemostatic sterilization
Method, the method comprises the steps:
1) weighing the Pollen Typhae of recipe quantity, after cleaning, drying, in putting pot, 100-120 DEG C of stir-fry is to the most dark brown
Color, sustainability, after cooling, caking is rubbed broken, place and l-2 day i.e. obtain Pollen Typhae carbon；
2) weigh the Oletum Trogopterori of recipe quantity, Rhizoma Saururi (Herba Saururi), Cacumen Tamaricis and Folium Artemisiae Argyi, clean, be dried,
It is ground into coarse powder, boiling twice, adds the water of crude drug gross weight 10-15 times for the first time
Decocting 2-3h, second time adds the soak by water 2-3h of crude drug gross weight 6-8 times, after filtration,
Merging filtrate, adds ethyl acetate and extracts three times, merge organic facies, be dried in filtrate, rotation is steamed,
It is standby that removal solvent obtains dry powder；
3) weigh the Pollen Typhae carbon of recipe quantity, Semen Ricini, Radix Notoginseng and the Pseudobulbus Bletillae (Rhizoma Bletillae), pulverize respectively, grind to
Superfine end, after crossing 80-100 mesh sieve, mix homogeneously is standby；
4) by step 2) and step 3) the fine powder mix homogeneously of gained i.e. obtains described compositions.
In order to use and easy to carry, Chinese medicine composition that postoperation hemostatic is sterilized by the present invention and medicine
The unguentum that on, acceptable adjuvant is made, it is characterised in that described adjuvant is by following weight fraction
One-tenth be grouped into: liquid paraffin 65-80, antioxidant 0.01-0.02, emulsifying agent 0.5-1.
Further preferably, described antioxidant be mass ratio be the Butylated hydroxyanisole of 3:1
Mixture with citric acid；Described emulsifying agent be mass ratio be 1:2 anhydrous sorbitol sesquialter oil
Acid esters and the mixture of sorbitan monooleate.
On the other hand, the present invention also provides for the purposes of described compositions and preparation thereof, and it is used for making
Application in standby hemostasis, disinfecting drug.
Chinese medicine composition for postoperation hemostatic sterilization of the present invention uses multiple pure natural medical material
Meticulously develop, can effectively, quickly stop blooding contain in anti-inflammation simultaneously
Medicine composition, wound does not infects, and collects effect of hemostasis, pain relieving, effectively sterilization and suppression infection in one
Body, comprehensively treats wound and nurses one's health, good effect.After making unguentum, use and take
Carry convenient, and further increase bioavailability and the curative effect of compositions.
Detailed description of the invention
Embodiment 1
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, said composition is by the crude drug warp of following weight portion
Processing is prepared from:
Embodiment 2
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, said composition is by the crude drug warp of following weight portion
Processing is prepared from:
Embodiment 3
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, said composition is by the crude drug warp of following weight portion
Processing is prepared from:
Preparation method:
1) Cattail Pollen of clean dry is put in pot, do not stop to stir-fry in 100 DEG C, fry to described Pollen Typhae
Powder is pitchy, but sustainability, after cooling, caking is rubbed broken, place and i.e. obtain Pollen Typhae carbon on 2nd；
2) weigh the Oletum Trogopterori of recipe quantity, Rhizoma Saururi (Herba Saururi), Cacumen Tamaricis and Folium Artemisiae Argyi, clean, dry, pulverize
Become coarse powder, boiling twice, add the soak by water 3h of crude drug gross weight 10 times for the first time,
Second time adds the soak by water 3h of crude drug gross weight 6 times, after filtration, merging filtrate, filtrate
Middle addition ethyl acetate extracts three times, merges organic facies, is dried, and rotation is steamed, and removes solvent and must do
Powder is standby；
3) weigh the Pollen Typhae carbon of recipe quantity, Semen Ricini, Radix Notoginseng and the Pseudobulbus Bletillae (Rhizoma Bletillae), pulverize respectively, grind to superfine
End, after crossing 80-100 mesh sieve, mix homogeneously is standby；
4) by step 2) and step 3) the fine powder mix homogeneously of gained i.e. obtains described compositions.
Embodiment 4
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, said composition is by the crude drug warp of following weight portion
Processing is prepared from:
Embodiment 5
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, said composition is by the crude drug warp of following weight portion
Processing is prepared from:
Embodiment 6
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, said composition is by the crude drug warp of following weight portion
Processing is prepared from:
Embodiment 7
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, said composition is by the crude drug warp of following weight portion
Processing is prepared from:
1) Cattail Pollen of clean dry is put in pot, do not stop to stir-fry in 120 DEG C, fry to described Pollen Typhae
Powder is pitchy, but sustainability, after cooling, caking is rubbed broken, place and i.e. obtain Pollen Typhae carbon on 1st；
2) Herba Houttuyniae of recipe quantity, Flos Lonicerae, Rhizoma Saururi (Herba Saururi), Oletum Trogopterori, Cacumen Tamaricis and Folium Artemisiae Argyi are weighed,
Clean, dry, pulverize into coarse powder, boiling twice, add crude drug gross weight for the first time
The soak by water 2h of 15 times, second time adds the soak by water 2h of crude drug gross weight 8 times, after filtration,
Merging filtrate, adds ethyl acetate and extracts three times, merge organic facies, be dried in filtrate, rotation is steamed,
It is standby that removal solvent obtains dry powder；
3) Pollen Typhae carbon of recipe quantity, Concha Arcae, Radix Notoginseng, the Pseudobulbus Bletillae (Rhizoma Bletillae), Colla Corii Asini and Semen Ricini are weighed, respectively
Pulverizing, grind extremely smalls, after crossing 80-100 mesh sieve, mix homogeneously is standby；
4) by step 2) and step 3) the fine powder mix homogeneously of gained i.e. obtains described compositions.
Embodiment 8
The Chinese medicine composition of a kind of postoperation hemostatic sterilization, said composition is by the crude drug warp of following weight portion
Processing is prepared from:
Preparation method:
1) Cattail Pollen of clean dry is put in pot, do not stop to stir-fry in 110 DEG C, fry to described Pollen Typhae
Powder is pitchy, but sustainability, after cooling, caking is rubbed broken, place and i.e. obtain Pollen Typhae carbon on 1st；
2) Herba Houttuyniae of recipe quantity, Flos Lonicerae, Rhizoma Saururi (Herba Saururi), Oletum Trogopterori, Cacumen Tamaricis and Folium Artemisiae Argyi are weighed,
Clean, dry, pulverize into coarse powder, boiling twice, add crude drug gross weight for the first time
The soak by water 2h of 14 times, second time adds the soak by water 2h of crude drug gross weight 7 times, after filtration,
Merging filtrate, adds ethyl acetate and extracts three times, merge organic facies, be dried in filtrate, rotation is steamed,
It is standby that removal solvent obtains dry powder；
3) Pollen Typhae carbon of recipe quantity, Concha Arcae, Radix Notoginseng, the Pseudobulbus Bletillae (Rhizoma Bletillae), Colla Corii Asini and Semen Ricini are weighed, respectively
Pulverizing, grind extremely smalls, after crossing 80-100 mesh sieve, mix homogeneously is standby；
4) by step 2) and step 3) the fine powder mix homogeneously of gained i.e. obtains described compositions.
Embodiment 9 unguentum
Preparation method:
1) Butylated hydroxyanisole and citric acid are sufficiently mixed, are dissolved in 70 DEG C of distilled water；By liquid
Paraffin body, sorbitan sesquioleate and sorbitan monooleate mixing, be heated to
Adding in distilled water after 70 DEG C, stirring, to mix homogeneously, cools that to make substrate standby；
2) compositions prepared by recipe quantity embodiment 8 and 1/3rd steps 1 are taken) substrate made
Grind well into pasty state, mix homogeneously with residue substrate the most again and obtain unguentum.
Embodiment 10 unguentum
Preparation method: prepared by method as described in embodiment 9
Clinical trial
By Radix Notoginseng, Semen Ricini, Oletum Trogopterori, Cacumen Tamaricis, the Pseudobulbus Bletillae (Rhizoma Bletillae), Rhizoma Saururi (Herba Saururi), Pollen Typhae carbon and
Folium Artemisiae Argyi is Chinese medicine composition 1 by the compositions that recipe quantity is prepared from.
By Radix Notoginseng, Semen Ricini, Oletum Trogopterori, Cacumen Tamaricis, the Pseudobulbus Bletillae (Rhizoma Bletillae), Rhizoma Saururi (Herba Saururi), Pollen Typhae carbon,
The compositions that Folium Artemisiae Argyi, Concha Arcae, Flos Lonicerae, Herba Houttuyniae and Colla Corii Asini are prepared from by recipe quantity
For Chinese medicine composition 2.
Test 1 Chinese medicine composition to clotting time of mice and the impact in bleeding time
Mice docking bleeding time (BT) and capillary tube clotting time (CT) experiment are widely used in
Hemostasis, the screening active ingredients of clot promoting drug, method is directly perceived, easy, easy.This experiment is with hemostasis
Blood coagulation rationale is for instructing, and main employing both approaches evaluates the hemostasis of Chinese medicine composition
Effect.
1 experiment material
1.1 laboratory animals: kunming mice, body weight 18-20g, Beijing dimension tonneau China laboratory animal technology
Company limited provides.
1.2 positive control medicines: YUNNAN BAIYAO, Yunnan Paiyao Group Corp., Ltd, lot number
20090605。
1.3 positive control agent: normal saline.
2 experimental techniques
80 white mice are randomly divided into 8 groups, often group 10.Blood capillary is done with 4 groups
Clotting assay, respectively Chinese medicine composition 1 group, Chinese medicine composition 2 groups, YUNNAN BAIYAO group (sun
Property matched group) and normal saline group (negative control group)；Other 4 groups do white mice docking hemorrhage
Time test, respectively Chinese medicine composition 1 group, Chinese medicine composition 2 groups, YUNNAN BAIYAO group and
Normal saline group, compares with physiology group, is calculated as follows CT LVFS and BT LVFS.
CT LVFS (%)=(normal saline group clotting time-testing sample group clotting time)/
Normal saline group clotting time * 100%
BT LVFS (%)=(normal saline group bleeding time-testing sample group bleeding time)/
Normal saline group bleeding time * 100%.
3 experimental results
Above-mentioned experiment is observed, and records observed data, experimental result part table 1.
Table 1 treatment group and matched group haemostatic effect compare
4 conclusions
Statistical result shows, Chinese medicine composition 1 group and Chinese medicine composition 2 groups and YUNNAN BAIYAO group
Mice blood clotting time (CT) and mice bleeding time (BT) are compared with normal saline group, difference pole
Significantly (p ＜ 0.01), illustrate that Chinese medicine composition 1 and Chinese medicine composition 2 are respectively provided with preferably rush
Enter blood coagulation, shorten the effect of mice bleeding time, i.e. have preferably anastalsis, and it is only
Blood effect is all better than the most conventional commercially available " YUNNAN BAIYAO ", the wherein hemostasis of Chinese medicine composition 2 groups
Effect is better than Chinese medicine extract
Test the bacteriostatic experiment of 2 Chinese medicine compositions
1 experiment material
1.1 experimental strains:
Select staphylococcus aureus, Hemolytic streptococcus, Diplococcus pneumoniae and dysentery bacterium.
1.2 bacterium culture mediums:
Nutrient agar and nutrient broth medium.
1.3 experiment packets:
Bacteriostatic experiment divides experimental group and matched group, and experimental group selects Chinese medicine composition 1 of the present invention
With Chinese medicine composition 2, matched group selects hypochlorous acid disinfectant solution.
2 experiment contents
Above-mentioned four kinds of strains are inoculated on four agar culture mediums respectively, at 37 DEG C, cultivate 48
Hour, respectively from above-mentioned agar culture medium four kinds of bacterium colonies of picking be inoculated in respectively four fresh
In nutrient broth medium, synthermal under, cultivate 24 hours standby.
Take Chinese medicine composition 1 of the present invention and each 0.5g of Chinese medicine composition 2；Hypochlorous acid disinfectant solution 4mL,
Dilute 10 times, above-mentioned three kinds of disinfectant are placed in three containers respectively, are placed in aseptic condition
Under, standby.
The experimental strain of above-mentioned cultivation is diluted 50 times respectively with aseptic nutrient broth, every kind of bacterium
Plant and be sub-packed in three culture dishs, respectively labelling matched group, experimental group 1 and experimental group 2.
Chinese medicine composition 1 of the present invention is added in experimental group 1 culture dish；Chinese medicine composition 2
Add in experimental group 2 culture dish；Hypochlorous acid disinfectant solution dilute solution instills matched group culture dish.
3 experimental results
Above-mentioned experiment is observed, observes four groups of strains and measure strain revolution mark, and remembering
Record observed data, experimental result is shown in Table 2.
Table 2 treatment group and matched group sterilization, fungistatic effect compare
After observation is measured, it is placed in above-mentioned culture dish under aseptic condition standing two days, with
Track is it has been observed that matched group bacterium colony continues breeding, and experimental group bacterium colony is unchanged.
4 conclusions
Chinese medicine composition disinfection effect for postoperation hemostatic sterilization provided by the present invention is relatively
Good, and can substantially suppress bacteria breed；Wherein the bactericidal effect of experimental group 2 is better than experimental group 1.
Model case
The Meng, man, 25 years old, because of the shank of imprudence reaping hook incised wound oneself of ceding territory, bleeds not
Only, carry out emergency treatment and go to a doctor, sprinkle 2 millimeters thick by the Chinese medicine composition of the present invention, stop blooding rapidly, so
After bind up with gauze, share medicine four times, recovery from illness.
Zheng, 32 years old, female, the long 3.2cm × 1.8cm in oxter × big fibroma of 1.5cm, need hands
Art is excised, and after finishing operation stitching, does not arrhea blood at scalpel edge, and amount is relatively big, binder and
Gauze is difficult to stop, and sprinkles Chinese medicine composition 2 millimeters thick of the present invention, binds up with gauze,
Effectively hemostasis.Within 3rd day, changing dressings, the edge of a knife recovers good, without oozing of blood, without inflammation, without pain.
Claims (9)
1. the Chinese medicine composition of postoperation hemostatic sterilization, it is characterised in that described compositions mainly by
The crude drug of following weight portion is processed to be prepared from:
2. the Chinese medicine composition of postoperation hemostatic sterilization as claimed in claim 1, it is characterised in that system
Standby described compositions also includes the crude drug of following weight portion:
Concha Arcae 6-13 Flos Lonicerae 3-10 Herba Houttuyniae 2-8 Colla Corii Asini 2-6.
3. the Chinese medicine composition of postoperation hemostatic sterilization as claimed in claim 2, it is characterised in that system
The weight fraction raw materials used for described compositions is:
4. the Chinese medicine composition of postoperation hemostatic sterilization as claimed in claim 3, it is characterised in that system
The parts by weight of the standby raw materials used medicine of described compositions are:
5. according to the Chinese medicine composition of the arbitrary described postoperation hemostatic sterilization of claim 1-4 with pharmaceutically
The unguentum that acceptable adjuvant is made, it is characterised in that described adjuvant is by following parts by weight
One-tenth is grouped into: liquid paraffin 65-80, antioxidant 0.01-0.02 and emulsifying agent 0.5-1.
6. unguentum as claimed in claim 5, is characterized in that, described antioxidant be mass ratio be 3:1
Butylated hydroxyanisole and the mixture of citric acid.
7. unguentum as claimed in claim 5, is characterized in that, described emulsifying agent be mass ratio be 1:2
Sorbitan sesquioleate and the mixture of sorbitan monooleate.
8. the preparation method of the Chinese medicine composition of postoperation hemostatic sterilization as claimed in claim 1, it is special
Levy and be to comprise the steps:
1) weighing the Pollen Typhae of recipe quantity, after cleaning, drying, in putting pot, 100-120 DEG C of stir-fry is to pitchy,
Sustainability, rubs broken by caking after cooling, place and l-2 day i.e. obtain Pollen Typhae carbon；
2) weigh the Oletum Trogopterori of recipe quantity, Rhizoma Saururi (Herba Saururi), Cacumen Tamaricis and Folium Artemisiae Argyi, clean, dry, pulverize
Become coarse powder, boiling twice, add the soak by water of crude drug gross weight 10-15 times for the first time
2-3h, second time adds the soak by water 2-3h of crude drug gross weight 6-8 times, after filtration, merges
Filtrate, adds ethyl acetate and extracts three times, merge organic facies, be dried in filtrate, rotation is steamed, and goes
Except solvent, to obtain dry powder standby；
3) weigh the Pollen Typhae carbon of recipe quantity, Semen Ricini, Radix Notoginseng and the Pseudobulbus Bletillae (Rhizoma Bletillae), pulverize respectively, grind to superfine
End, after crossing 80-100 mesh sieve, mix homogeneously is standby；
4) by step 2) and step 3) the fine powder mix homogeneously of gained i.e. obtains described compositions.
9. the Chinese medicine composition of postoperation hemostatic sterilization as claimed in claim 1 or 2 preparation hemostasis,
Application in disinfecting drug.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2020133948A1 (en) * | 2018-12-25 | 2020-07-02 | 衢州市益年堂农林科技有限公司 | Composition having whitening and anti-oxidation effects and skin care cream thereof |
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| WO2020133948A1 (en) * | 2018-12-25 | 2020-07-02 | 衢州市益年堂农林科技有限公司 | Composition having whitening and anti-oxidation effects and skin care cream thereof |
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Application publication date: 20170104 |