CN106190756A - Herba Spinaciae health promoting vinegar and application thereof - Google Patents
Herba Spinaciae health promoting vinegar and application thereof Download PDFInfo
- Publication number
- CN106190756A CN106190756A CN201610544892.0A CN201610544892A CN106190756A CN 106190756 A CN106190756 A CN 106190756A CN 201610544892 A CN201610544892 A CN 201610544892A CN 106190756 A CN106190756 A CN 106190756A
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- fermentation
- vinegar
- herba
- herba spinaciae
- enzymolysis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/28—Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/42—Cucurbitaceae (Cucumber family)
- A61K36/428—Trichosanthes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/54—Lauraceae (Laurel family), e.g. cinnamon or sassafras
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
- A61K36/714—Aconitum (monkshood)
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12J—VINEGAR; PREPARATION OR PURIFICATION THEREOF
- C12J1/00—Vinegar; Preparation or purification thereof
- C12J1/04—Vinegar; Preparation or purification thereof from alcohol
Abstract
The open a kind of Herba Spinaciae health promoting vinegar of the present invention, chooses Herba Spinaciae and cleans, enzyme denaturing, and colloid mill defibrination makes slurry；Aconitum carmichjaelii Debx., Cortex Cinnamomi, Fructus Trichosanthis, Herba Silybi mariani mixing are pulverized, is subsequently adding cellulase and carries out enzymolysis, obtain Chinese medicine enzymolysis solution；Slurry, Spartina alterniflora's extract and Chinese medicine enzymolysis solution through enzymolysis processing is pressed the mass ratio mixing of 17:0.7:1, add the active dry yeast bacterium 0.03 0.05% activated, carry out alcohol fermentation, adjust initial pH=4 5 with citric acid, fermentation temperature is 24 32 DEG C, and fermentation duration is 24 days；In described active dry yeast 5% sucrose solution after sterilization；Acetic fermentation: add Chinese liquor and the initial alcoholic strength of mixed liquor after fermentation first is adjusted to 8%, add acetic acid bacteria 1.5 1.7%, carry out acetic fermentation.The present invention is in good taste, and has good therapeutic effect for emphysema.
Description
Technical field
The present invention relates to a kind of Herba Spinaciae health promoting vinegar and application thereof, belong to food technology field.
Background technology
Dish has the title of " nutrition model student ", and it is rich in carotenoid, vitamin C, vitamin K, mineral (calcareous, irony
Deng), the various nutrients such as coenzyme Q10, emphysema are one of old people's respiratory tract diseases more typically, and its pathogenesis is the completeest
All clear Chu, shows according to relevant clinical data, and emophysematous generation and bronchial obstruction have certain relation, due to long-term smoking and
The factors such as environmental pollution make bronchus be inflamed, and cause bronchus luminal stenosis, the most in the case of infections, it is easier to
Increase internal proteinase activity, thus emphysema occur.Clinical manifestation is that weight declines rapidly, health is weak, appetite not
Shake, upper abdomen distension, merge respiratory symptom and the sign such as cough, expectoration, pulmonary's respiratory murmur attenuating.
Summary of the invention
The problem existed for above-mentioned prior art, the present invention provides a kind of Herba Spinaciae health promoting vinegar, it is possible to effective treatment is burst
The symptom of ulcer colitis, has no side effect.
To achieve these goals, the technical solution used in the present invention is: a kind of Herba Spinaciae health promoting vinegar, described Spinach vinegar former
Material formula includes following component:
(1) raw material: Herba Spinaciae, Spartina alterniflora's extract；
(2) Chinese medicine: Aconitum carmichjaelii Debx., Cortex Cinnamomi, Fructus Trichosanthis, Herba Silybi mariani.
A kind of Herba Spinaciae health promoting vinegar, it is characterised in that described Spinach vinegar follows these steps to carry out:
(1), choose Herba Spinaciae cleaning, enzyme denaturing, colloid mill defibrination, make slurry；Described slurry uses complex enzyme zymohydrolysis, enzyme digestion reaction temperature
It is about 36 DEG C, enzymolysis time about 2h；
(2), Aconitum carmichjaelii Debx., Cortex Cinnamomi, Fructus Trichosanthis, Herba Silybi mariani mixing are pulverized, and sieved with the screen cloth of 10 mesh, discard thick
Raw material forms raw material；The most mixed 20 MPas of homogenizers of merga pass that add water carry out homogenizing, are then spray-dried, obtain powdery
Granule, by above-mentioned powdered granule addition distillation hydro-thermal to about 70-75 DEG C, is subsequently adding cellulase and carries out enzymolysis, during this
Temperature maintains 70-75 DEG C, 100 minutes persistent period, obtains Chinese medicine enzymolysis solution；
(3) the mass ratio mixing of 17:0.7:1, by slurry, Spartina alterniflora's extract and the Chinese medicine enzymolysis solution through enzymolysis processing is pressed,
Adding white sugar makes the initial pol of mixed liquor be adjusted to 12-14%；
(4), alcohol fermentation: add the active dry yeast bacterium 0.03-0.05% activated, carry out alcohol fermentation, adjust with citric acid
Initially
PH=4-5, fermentation temperature is 24-32 DEG C, and fermentation duration is 2-4 days；Described active dry yeast 5% sugarcane after sterilization
30-50min is activated in sugar juice, under 26-32 DEG C of temperature conditions；
(5), acetic fermentation: add Chinese liquor and the initial alcoholic strength of mixed liquor after fermentation first is adjusted to 8%, add acetic acid bacteria
1.5-1.7%, carries out acetic fermentation；Fermentation acid-base value is pH=4-4.5, and fermentation temperature is 28-34 DEG C, ferments 4-5 days, in fermentation
While be stirred, its mixing speed is 120-160r/min；
(6), centrifugal: by the centrifugal 20-30min under the rotating speed of 3000-4000r/min of the fruit vinegar after fermentation, to collect supernatant, remove
Remove macroscopic solid content and impurity；
(7), ultrafiltration: the fruit vinegar fruit vinegar filter ultrafiltration after being centrifuged, operation pressure 0.07-0.108MPa, operation temperature 30-
35 DEG C, feed velocity 4-8L/h, ultrafiltration time 15-20min, remove and cause high molecular weight protein, the color that former fruit vinegar is muddy, precipitate
The impurity components such as element, pectin, Plant fiber, antibacterial, yeast；
(8), fill, sterilizing: the former fruit vinegar filling machine after ultrafiltration is loaded in the carafe cleaned up, 75-80 DEG C of temperature
Sterilize under the conditions of degree 15-20min, obtains finished product.
Described compound enzyme is made up of by the mass ratio of 7:1 pectase and cellulase.
Described composition of raw materials is preferably the composition of following mass parts:
(2) Chinese medicine: Aconitum carmichjaelii Debx. 1-2 part, Cortex Cinnamomi 1-3 part, Fructus Trichosanthis 0.1-0.2 part, Herba Silybi mariani 0.9-2 part.
The application in terms for the treatment of emphysema of a kind of Herba Spinaciae health promoting vinegar.
The fruit vinegar of the present invention by Herba Spinaciae and Chinese medicine with the use of, Chinese medicine includes that Aconitum carmichjaelii Debx., Cortex Cinnamomi, Fructus Trichosanthis, Herba Silybi mariani are by adding
Enter cellulase to carry out enzymolysis and have activated the activity of Chinese medicine, add Spartina alterniflora's extract also the most acute to treatment with Spinach vinegar for carrier
Emphysema can obtain good effect.The synergism of formula so that the present invention can suppress the combination of bacteria cell wall, stable
Antibacterial effect.During antibacterial, there is the highest antibacterial activity in particular for staphylococcus, gram negative bacilli is had
Extremely strong stability.The Spinach vinegar long shelf-life of the present invention, sweet and sour taste, fragrance are tempting, all-ages.
Detailed description of the invention
The invention will be further described below.
Embodiment 1:
A kind of Herba Spinaciae health promoting vinegar, it is characterised in that described Spinach vinegar follows these steps to carry out:
(1), choose Herba Spinaciae cleaning, enzyme denaturing, colloid mill defibrination, make slurry；Described slurry uses complex enzyme zymohydrolysis, enzyme digestion reaction temperature
It is about 36 DEG C, enzymolysis time about 2h；
(2), 1 part of Aconitum carmichjaelii Debx., 1 part of Cortex Cinnamomi, 0.1 part of Fructus Trichosanthis, 0.9 part of Herba Silybi mariani mixing are pulverized, and entered with the screen cloth of 10 mesh
Row sieves, and discards thick raw material and forms raw material；The most mixed 20 MPas of homogenizers of merga pass that add water carry out homogenizing, then spray
Mist is dried, and obtains powdered granule, by above-mentioned powdered granule addition distillation hydro-thermal to about 70-75 DEG C, is subsequently adding cellulase and enters
Row enzymolysis, during this, temperature maintains 70-75 DEG C, 100 minutes persistent period, obtains Chinese medicine enzymolysis solution；
(3) the mass ratio mixing of 17:0.7:1, by slurry, Spartina alterniflora's extract and the Chinese medicine enzymolysis solution through enzymolysis processing is pressed,
Adding white sugar makes the initial pol of mixed liquor be adjusted to 12-14%；
(4), alcohol fermentation: add the active dry yeast bacterium 0.03-0.05% activated, carry out alcohol fermentation, adjust with citric acid
Initial pH=4-5, fermentation temperature is 24-32 DEG C, and fermentation duration is 2-4 days；Described active dry yeast 5% sugarcane after sterilization
30-50min is activated in sugar juice, under 26-32 DEG C of temperature conditions；
(5), acetic fermentation: add Chinese liquor and the initial alcoholic strength of mixed liquor after fermentation first is adjusted to 8%, add acetic acid bacteria
1.5-1.7%, carries out acetic fermentation；Fermentation acid-base value is pH=4-4.5, and fermentation temperature is 28-34 DEG C, ferments 4-5 days, in fermentation
While be stirred, its mixing speed is 120-160r/min；
(6), centrifugal: by the centrifugal 20-30min under the rotating speed of 3000-4000r/min of the fruit vinegar after fermentation, to collect supernatant, remove
Remove macroscopic solid content and impurity；
(7), ultrafiltration: the fruit vinegar fruit vinegar filter ultrafiltration after being centrifuged, operation pressure 0.07-0.108MPa, operation temperature 30-
35 DEG C, feed velocity 4-8L/h, ultrafiltration time 15-20min, remove and cause high molecular weight protein, the color that former fruit vinegar is muddy, precipitate
The impurity components such as element, pectin, Plant fiber, antibacterial, yeast；
(8), fill, sterilizing: the former fruit vinegar filling machine after ultrafiltration is loaded in the carafe cleaned up, 75-80 DEG C of temperature
Sterilize under the conditions of degree 15-20min, obtains finished product.
Described compound enzyme is made up of by the mass ratio of 7:1 pectase and cellulase,
The processing technology of the extract of above-mentioned Spartina alterniflora is: 1) by the Spartina alterniflora after vacuum drying, powder in pulverizer
Broken obtain Spartina alterniflora's powder, Spartina alterniflora, powder are placed in the extraction kettle of supercritical extraction；2) supercritical CO 2 is used to make
For solvent, concentration be 60% ethanol do entrainer；3) extracting pressure is controlled 20～35MPa by regulation extraction kettle, temperature control
System is at 35 DEG C, and CO2 flow-control is at 9L/h, and extraction time controls at 2h, obtains brown paste Spartina alterniflora's extract.
Embodiment 2, identical with embodiment 1 step, difference is: Chinese medicinal components is: Aconitum carmichjaelii Debx. 2 parts, Cortex Cinnamomi 3 parts, melon
Beach wormwood 0.2 part, Herba Silybi mariani 1 part.
Comparative example 1: identical with embodiment 1 step, difference is: do not contain Spartina alterniflora's extract.
Comparative example 2: identical with embodiment 1 step, difference is: by 1 part of Aconitum carmichjaelii Debx., 1 portion of Cortex Cinnamomi, 0.1 part of Fructus Trichosanthis,
The mixing of 0.9 part of Herba Silybi mariani pulverize after without enzymolysis step.
Comparative example 3: 1 part of Aconitum carmichjaelii Debx., 1 part of Cortex Cinnamomi, 0.1 part of Fructus Trichosanthis, 0.9 part of Herba Silybi mariani mixing are carried out pulverizing and boil Chinese medicine.
Experimental Comparison:
The clinical data of 80 example senile emphysema infected patients, is randomly divided into four groups according to different therapeutic modalities, often group
Each 20 examples；Often organize each 20 examples, inclusive criteria: be diagnosed as emphysema generation infected patient through electrocardiogram, x-ray inspection etc., suffer from
The data such as person's age, sex, weight and the course of disease compare, and no significant difference has comparability.
Therapeutic Method:
Observation group: the Spinach vinegar beverage of oral embodiment 1, is administered orally twice, a 50ml every day.
Comparative example 1 group: the Spinach vinegar beverage of oral contrast example 1, is administered orally twice, a 50ml every day.
Comparative example 2 groups: the Spinach vinegar beverage of oral contrast example 2, is administered orally twice, a 50ml every day.
Comparative example 3 groups: take 1 part of Aconitum carmichjaelii Debx., Chinese medicine that 1 part of Cortex Cinnamomi, 0.1 part of Fructus Trichosanthis, 0.9 part of Herba Silybi mariani boil.
Four groups of patients were all a course for the treatment of with continuous 4 weeks, and treatment observes therapeutic effect after 2 courses for the treatment of continuously.
Criterion of therapeutical effect: cure: the clinical symptoms of senile emphysema concurrent infection patient is improved completely, Electrocardioscopy
There is not any pneumonia symptom in display；Effective: patient clinical symptom has to a certain degree to be improved, Electrocardioscopy pulmonary
Inflammatory symptom has a certain degree of alleviation；Invalid: the clinical symptoms of patient is not improved, Electrocardioscopy pneumonia symptom is anti-
And deteriorate.
Statistical method this group data acquisition SPSS13.0 statistics software processes, and carries out X 2 test between group, with
P < 0.05 anticipates for there being statistics.
By table it can be seen that observation group and 1,2,3 groups of total effective rate comparing differences of comparative example notable (P< 0.01), there is statistics
Learn meaning
Being drawn by Experiment on Microbiology, embodiment 1 comparative example 1 is compared, the sterilization effect having had, and the shelf-life can extend 2
Month.
Claims (5)
1. a Herba Spinaciae health promoting vinegar, it is characterised in that the composition of raw materials of described Spinach vinegar includes following component:
(1) raw material: Herba Spinaciae, Spartina alterniflora's extract；
(2) Chinese medicine: Aconitum carmichjaelii Debx., Cortex Cinnamomi, Fructus Trichosanthis, Herba Silybi mariani.
A kind of Herba Spinaciae health promoting vinegar, it is characterised in that described Spinach vinegar follows these steps to carry out:
(1), choose Herba Spinaciae cleaning, enzyme denaturing, colloid mill defibrination, make slurry；Described slurry uses complex enzyme zymohydrolysis, enzyme digestion reaction temperature
It is about 36 DEG C, enzymolysis time about 2h；
(2), Aconitum carmichjaelii Debx., Cortex Cinnamomi, Fructus Trichosanthis, Herba Silybi mariani mixing are pulverized, and sieved with the screen cloth of 10 mesh, discard thick
Raw material forms raw material；The most mixed 20 MPas of homogenizers of merga pass that add water carry out homogenizing, are then spray-dried, obtain powdery
Granule, by above-mentioned powdered granule addition distillation hydro-thermal to about 70-75 DEG C, is subsequently adding cellulase and carries out enzymolysis, during this
Temperature maintains 70-75 DEG C, 100 minutes persistent period, obtains Chinese medicine enzymolysis solution；
(3) the mass ratio mixing of 17:0.7:1, by slurry, Spartina alterniflora's extract and the Chinese medicine enzymolysis solution through enzymolysis processing is pressed,
Adding white sugar makes the initial pol of mixed liquor be adjusted to 12-14%；
(4), alcohol fermentation: add the active dry yeast bacterium 0.03-0.05% activated, carry out alcohol fermentation, adjust with citric acid
Initial pH=4-5, fermentation temperature is 24-32 DEG C, and fermentation duration is 2-4 days；Described active dry yeast 5% sugarcane after sterilization
30-50min is activated in sugar juice, under 26-32 DEG C of temperature conditions；
(5), acetic fermentation: add Chinese liquor and the initial alcoholic strength of mixed liquor after fermentation first is adjusted to 8%, add acetic acid bacteria
1.5-1.7%, carries out acetic fermentation；Fermentation acid-base value is pH=4-4.5, and fermentation temperature is 28-34 DEG C, ferments 4-5 days, in fermentation
While be stirred, its mixing speed is 120-160r/min；
(6), centrifugal: by the centrifugal 20-30min under the rotating speed of 3000-4000r/min of the fruit vinegar after fermentation, to collect supernatant, remove
Remove macroscopic solid content and impurity；
(7), ultrafiltration: the fruit vinegar fruit vinegar filter ultrafiltration after being centrifuged, operation pressure 0.07-0.108MPa, operation temperature 30-
35 DEG C, feed velocity 4-8L/h, ultrafiltration time 15-20min, remove and cause high molecular weight protein, the color that former fruit vinegar is muddy, precipitate
The impurity components such as element, pectin, Plant fiber, antibacterial, yeast；
(8), fill, sterilizing: the former fruit vinegar filling machine after ultrafiltration is loaded in the carafe cleaned up, 75-80 DEG C of temperature
Sterilize under the conditions of degree 15-20min, obtains finished product.
A kind of Herba Spinaciae health promoting vinegar, it is characterised in that described compound enzyme is by pectase and cellulase
Form by the mass ratio of 7:1.
A kind of Herba Spinaciae health promoting vinegar the most according to claim 2, it is characterised in that described composition of raw materials is preferably following quality
The composition of part:
(2) Chinese medicine: Aconitum carmichjaelii Debx. 1-2 part, Cortex Cinnamomi 1-3 part, Fructus Trichosanthis 0.1-0.2 part, Herba Silybi mariani 0.9-2 part.
5. one kind such as claim 1-4 any one Herba Spinaciae health promoting vinegar application in terms for the treatment of emphysema.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610544892.0A CN106190756A (en) | 2016-07-12 | 2016-07-12 | Herba Spinaciae health promoting vinegar and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610544892.0A CN106190756A (en) | 2016-07-12 | 2016-07-12 | Herba Spinaciae health promoting vinegar and application thereof |
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| Publication Number | Publication Date |
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| CN106190756A true CN106190756A (en) | 2016-12-07 |
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ID=57476969
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201610544892.0A Pending CN106190756A (en) | 2016-07-12 | 2016-07-12 | Herba Spinaciae health promoting vinegar and application thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109045104A (en) * | 2018-10-18 | 2018-12-21 | 湘西弘湘醋业有限责任公司 | A kind of river small stream bubble foot vinegar and preparation method thereof |
| CN113403173A (en) * | 2021-07-20 | 2021-09-17 | 北京市老才臣食品有限公司 | Fermentation process of white vinegar and white vinegar |
-
2016
- 2016-07-12 CN CN201610544892.0A patent/CN106190756A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109045104A (en) * | 2018-10-18 | 2018-12-21 | 湘西弘湘醋业有限责任公司 | A kind of river small stream bubble foot vinegar and preparation method thereof |
| CN113403173A (en) * | 2021-07-20 | 2021-09-17 | 北京市老才臣食品有限公司 | Fermentation process of white vinegar and white vinegar |
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| C06 | Publication | ||
| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20161207 |
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| WD01 | Invention patent application deemed withdrawn after publication |