CN106188732A - A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper and preparation method thereof - Google Patents

A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper and preparation method thereof Download PDF

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Publication number
CN106188732A
CN106188732A CN201610527273.0A CN201610527273A CN106188732A CN 106188732 A CN106188732 A CN 106188732A CN 201610527273 A CN201610527273 A CN 201610527273A CN 106188732 A CN106188732 A CN 106188732A
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China
Prior art keywords
fragrance
aretaining
longaacting
wallpaper
osmanthus flower
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CN201610527273.0A
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Chinese (zh)
Inventor
肖作兵
朱广用
周如隽
牛云蔚
张玉
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Shanghai Institute of Technology
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Shanghai Institute of Technology
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Priority to CN201610527273.0A priority Critical patent/CN106188732A/en
Publication of CN106188732A publication Critical patent/CN106188732A/en
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L21/00Compositions of unspecified rubbers
    • C08L21/02Latex
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • EFIXED CONSTRUCTIONS
    • E04BUILDING
    • E04FFINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
    • E04F13/00Coverings or linings, e.g. for walls or ceilings
    • E04F13/002Coverings or linings, e.g. for walls or ceilings made of webs, e.g. of fabrics, or wallpaper, used as coverings or linings
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

Abstract

One Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper of the present invention, count by weight percentage, the deionized water of Longaacting fragrance-aretaining osmanthus flower fragrance by 1% 10%, the latex of 10% 40% and surplus forms.The preparation method of described a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper is: first disperseed in deionized water by emulsion uniform, it is subsequently adding Longaacting fragrance-aretaining osmanthus flower fragrance to stir, wallpaper is immersed, takes out and be dried, i.e. obtain the fragrant wallpaper with Flos Osmanthi Fragrantis characteristic perfume.The Longaacting fragrance-aretaining osmanthus flower fragrance that the present invention uses, count by weight percentage, the deionized water of osmanthus flower fragrance by 5% 25%, the dextrin of 10% 45%, the pure glue of 1% 4%, the arabic gum of 0.5% 1.5% and surplus forms.The osmanthus flower fragrance of Longaacting fragrance-aretaining is applied to the perfuming of wallpaper by the present invention, has obtained the Flos Osmanthi Fragrantis fragrance wallpaper of Longaacting fragrance-aretaining, has added the aromatic function of wallpaper, improve the added value of wallpaper.

Description

A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper and preparation method thereof
Technical field
The invention belongs to chemical field, relate to a kind of fragrance wallpaper, specifically a kind of Flos Osmanthi Fragrantis fragrance wallpaper and system thereof Preparation Method.
Background technology
Wallpaper, also known as wallpaper, is a kind of material for decorating indoor wall, the main base material of wallpaper be generally divided into papery, Four kinds of plastic sheeting, textile fibre cloth product, expansion type plastics etc..Wallpaper is in the American-European history using existing last 100 years, in city A kind of idea product has been become on field.Wallpaper low cost, purposes is wide, and surface color is various in style, and beautiful decoration is generous, and it is unique Style and distinguished decoration effect, enjoy the favor of people, be widely used in decorated house, public place of entertainment at present Institute, market, hotel etc..Along with improving constantly of people's living standard, the wallpaper with different-style and applicable different needs is new Product are in the urgent need to exploitation.If wallpaper can persistently distribute fragrance, give graceful comfortable fragrance, the attached of wallpaper will be greatly improved Value added and using effect, so the development of fragrance wallpaper has very important significance.
Flos Osmanthi Fragrantis has deep and remote delicate fragrance rhythm and a sweet clear fragrance of a flower, fragrant and sweet soft sweet like violet, has the fresh and sweet of orange blossom and Flos Rosae Rugosae concurrently With pure and sweet, Flos Osmanthi Fragrantis fragrance is the fragrance of a flower that a kind of people generally like.But, it is all, by volatility, there is certain note due to essence Organic compound composition, the lasting of tradition essence is the most lasting, therefore, the fragrance with Flos Osmanthi Fragrantis odor characteristic of Longaacting fragrance-aretaining The development of wallpaper has wide market prospect and important using value.
The preparation of the fragrant wallpaper with the Longaacting fragrance-aretaining of Flos Osmanthi Fragrantis characteristic perfume has no report.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper and Preparation method, described this Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper and preparation method thereof to solve wallpaper of the prior art can not The technical problem of Longaacting fragrance-aretaining.
The invention provides a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, count by weight percentage, its raw materials used composition And content is as follows:
Longaacting fragrance-aretaining osmanthus flower fragrance 1%-10%;
Latex 10%-40%;
First part of deionized water surplus;
Described Longaacting fragrance-aretaining osmanthus flower fragrance, count by weight percentage, its raw material composition and content are as follows:
Concrete, pure glue is commercially available prod, and for a kind of esters modified starch, concrete chemical name is: octenyl succinic Acid esters starch.
Present invention also offers above-mentioned a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, its preparation method is as follows:
1) step of an osmanthus flower fragrance preparing Longaacting fragrance-aretaining is included:
I. osmanthus flower fragrance, dextrin, pure glue, arabic gum and second part of deionized water are weighed according to mass percent;
Add second part of deionized water the most in a reservoir, open stirring, be heated to 60 DEG C;
Iii. being joined by dextrin in the water of step (ii), temperature is maintained at 60 DEG C, continues stirring, makes dextrin dispersion all Even, obtain clear transparent solutions;
Iv. being joined by pure glue in the solution of step (iii) gained, temperature is maintained at 60 DEG C, continues stirring, makes pure glue divide Dissipate uniformly, obtain clear transparent solutions;
V. being joined by arabic gum in the solution of step (iv) gained, temperature is maintained at 60 DEG C, continues stirring, makes me Primary glue is uniformly dispersed, and obtains clear transparent solutions, is cooled to 40 DEG C;
Vi. osmanthus flower fragrance is joined in the solution of step (v) gained, continue stirring, make osmanthus flower fragrance be uniformly dispersed, then Open homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the osmanthus flower fragrance of Longaacting fragrance-aretaining;
2) Longaacting fragrance-aretaining osmanthus flower fragrance, latex and first part of deionized water are weighed according to mass percent;
3) add first part of deionized water in a reservoir, open stirring, be subsequently adding latex, make latex be uniformly dispersed;
4) weigh Longaacting fragrance-aretaining osmanthus flower fragrance, join step 3) in the latex dispersion that obtains, continue stirring, make long-acting Lasting osmanthus flower fragrance is dispersed in latex dispersion;
5) wallpaper is immersed in step 4) in the Longaacting fragrance-aretaining osmanthus flower fragrance dispersion liquid that obtains, infiltrate 1 minute, then by wall Paper takes out and is dried, and i.e. obtains Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper.
The present invention uses dextrin and pure glue to be wall material, is embedded by osmanthus flower fragrance, forms cladding at essence particle surface Film, thus reduce the volatility of essence, improve the thermostability of osmanthus flower fragrance, stability and lasting.
The present invention compares with prior art, and its technological progress is significant.The present invention obtains the Flos Osmanthi Fragrantis of a kind of Longaacting fragrance-aretaining Essence, and by this flavor application in the perfuming of wallpaper, obtained the Flos Osmanthi Fragrantis fragrance wallpaper of Longaacting fragrance-aretaining, added the fragrance of wallpaper Function, improves the added value of wallpaper.
Detailed description of the invention
Below by embodiment, the present invention is further described, but does not affect protection scope of the present invention.
Embodiment 1
A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, count by weight percentage, its raw materials used composition and content are as follows:
Longaacting fragrance-aretaining osmanthus flower fragrance 1%-10% (1g)
Latex 10%-40% (10g)
Deionized water 89% (89g);
Above-mentioned a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper is prepared via a method which:
(1) add a certain amount of deionized water water, in a reservoir, open stirring, be subsequently adding a certain amount of latex, make breast Glue is uniformly dispersed;
(2), weigh a certain amount of Longaacting fragrance-aretaining osmanthus flower fragrance, join in the latex dispersion that step (1) obtains, continue Stirring, makes Longaacting fragrance-aretaining osmanthus flower fragrance be dispersed in latex dispersion;
(3), by wallpaper it is immersed in the Longaacting fragrance-aretaining osmanthus flower fragrance dispersion liquid that step (2) obtains, infiltrates 1 minute, then Wallpaper is taken out and is dried, i.e. obtain Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper.The aroma strength of this fragrance wallpaper is the most weak.This fragrance wallpaper Naturally, after placing 3 months, through sensory evaluation, still there is the odor characteristic of Flos Osmanthi Fragrantis.
The osmanthus flower fragrance of Longaacting fragrance-aretaining used in above-mentioned a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, by weight percentage Calculating, its raw material composition and content are as follows:
The osmanthus flower fragrance of above-mentioned a kind of Longaacting fragrance-aretaining is prepared via a method which:
(1) add a certain proportion of deionized water, in a reservoir, open stirring, be heated to 60 DEG C;
(2), by dextrin joining in the water of step (1), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, Obtain clear transparent solutions;
(3), by pure glue joining in the solution of step (2) gained, temperature is maintained at 60 DEG C, continues stirring, makes pure glue divide Dissipate uniformly, obtain clear transparent solutions;
(4), by arabic gum joining in the solution of step (3) gained, temperature is maintained at 60 DEG C, continue stirring, make Ah Draw primary glue to be uniformly dispersed, obtain clear transparent solutions, be cooled to 40 DEG C;
(5), by osmanthus flower fragrance join in the solution of step (4) gained, continue stirring, make osmanthus flower fragrance be uniformly dispersed, It is then turned on homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the osmanthus flower fragrance of Longaacting fragrance-aretaining, this essence fragrance is strong Spend the most weak.
Embodiment 2
A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, count by weight percentage, its raw materials used composition and content are as follows:
Longaacting fragrance-aretaining osmanthus flower fragrance 10% (10g)
Latex 40% (40g)
Deionized water 50% (50g);
Above-mentioned a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper is prepared via a method which:
(1) add a certain amount of deionized water water, in a reservoir, open stirring, be subsequently adding a certain amount of latex, make breast Glue is uniformly dispersed;
(2), weigh a certain amount of Longaacting fragrance-aretaining osmanthus flower fragrance, join in the latex dispersion that step (1) obtains, continue Stirring, makes Longaacting fragrance-aretaining osmanthus flower fragrance be dispersed in latex dispersion;
(3), by wallpaper it is immersed in the Longaacting fragrance-aretaining osmanthus flower fragrance dispersion liquid that step (2) obtains, infiltrates 1 minute, then Wallpaper is taken out and is dried, i.e. obtain Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper.The aroma strength of this fragrance wallpaper is strong.This fragrance wallpaper is certainly After so placing 3 months, through sensory evaluation, still there is the odor characteristic of Flos Osmanthi Fragrantis.
The osmanthus flower fragrance of Longaacting fragrance-aretaining used in above-mentioned a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, by weight percentage Calculating, its raw material composition and content are as follows:
The osmanthus flower fragrance of above-mentioned a kind of Longaacting fragrance-aretaining is prepared via a method which:
(1) add a certain proportion of deionized water, in a reservoir, open stirring, be heated to 60 DEG C;
(2), by dextrin joining in the water of step (1), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, Obtain clear transparent solutions;
(3), by pure glue joining in the solution of step (2) gained, temperature is maintained at 60 DEG C, continues stirring, makes pure glue divide Dissipate uniformly, obtain clear transparent solutions;
(4), by arabic gum joining in the solution of step (3) gained, temperature is maintained at 60 DEG C, continue stirring, make Ah Draw primary glue to be uniformly dispersed, obtain clear transparent solutions, be cooled to 40 DEG C;
(5), by osmanthus flower fragrance join in the solution of step (4) gained, continue stirring, make osmanthus flower fragrance be uniformly dispersed, It is then turned on homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the osmanthus flower fragrance of Longaacting fragrance-aretaining, this essence fragrance is strong Degree is strong.
Embodiment 3
A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, count by weight percentage, its raw materials used composition and content are as follows:
Longaacting fragrance-aretaining osmanthus flower fragrance 5% (5g)
Latex 30% (30g)
Deionized water 65% (65g);
Above-mentioned a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper is prepared via a method which:
(1) add a certain amount of deionized water water, in a reservoir, open stirring, be subsequently adding a certain amount of latex, make breast Glue is uniformly dispersed;
(2), weigh a certain amount of Longaacting fragrance-aretaining osmanthus flower fragrance, join in the latex dispersion that step (1) obtains, continue Stirring, makes Longaacting fragrance-aretaining osmanthus flower fragrance be dispersed in latex dispersion;
(3), by wallpaper it is immersed in the Longaacting fragrance-aretaining osmanthus flower fragrance dispersion liquid that step (2) obtains, infiltrates 1 minute, then Wallpaper is taken out and is dried, i.e. obtain Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper.The aroma strength of this fragrance wallpaper is moderate.This fragrance wallpaper Naturally, after placing 3 months, through sensory evaluation, still there is the odor characteristic of Flos Osmanthi Fragrantis.
The osmanthus flower fragrance of Longaacting fragrance-aretaining used in above-mentioned a kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, by weight percentage Calculating, its raw material composition and content are as follows:
The osmanthus flower fragrance of above-mentioned a kind of Longaacting fragrance-aretaining is prepared via a method which:
(1) add a certain proportion of deionized water, in a reservoir, open stirring, be heated to 60 DEG C;
(2), by dextrin joining in the water of step (1), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, Obtain clear transparent solutions;
(3), by pure glue joining in the solution of step (2) gained, temperature is maintained at 60 DEG C, continues stirring, makes pure glue divide Dissipate uniformly, obtain clear transparent solutions;
(4), by arabic gum joining in the solution of step (3) gained, temperature is maintained at 60 DEG C, continue stirring, make Ah Draw primary glue to be uniformly dispersed, obtain clear transparent solutions, be cooled to 40 DEG C;
(5), by osmanthus flower fragrance join in the solution of step (4) gained, continue stirring, make osmanthus flower fragrance be uniformly dispersed, It is then turned on homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the osmanthus flower fragrance of Longaacting fragrance-aretaining, this essence fragrance is strong Spend moderate.
Above said content is only the basic explanation under present inventive concept, and according to appointing that technical scheme is done What equivalent transformation, belongs to the scope of protection of the invention.

Claims (2)

1. a Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper, it is characterised in that count by weight percentage, its raw materials used composition and containing Measure as follows:
Longaacting fragrance-aretaining osmanthus flower fragrance 1%-10%;
Latex 10%-40%;
First part of deionized water surplus;
Described Longaacting fragrance-aretaining osmanthus flower fragrance, count by weight percentage, its raw material composition and content are as follows:
A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper the most according to claim 1, it is characterised in that its preparation method is as follows:
1) step of an osmanthus flower fragrance preparing Longaacting fragrance-aretaining is included:
I. osmanthus flower fragrance, dextrin, pure glue, arabic gum and second part of deionized water are weighed according to mass percent;
Add second part of deionized water the most in a reservoir, open stirring, be heated to 60 DEG C;
Iii. being joined by dextrin in the water of step (ii), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, To clear transparent solutions;
Iv. being joined by pure glue in the solution of step (iii) gained, temperature is maintained at 60 DEG C, continues stirring, makes the dispersion of pure glue all Even, obtain clear transparent solutions;
V. being joined by arabic gum in the solution of step (iv) gained, temperature is maintained at 60 DEG C, continues stirring, makes arabic gum It is uniformly dispersed, obtains clear transparent solutions, be cooled to 40 DEG C;
Vi. osmanthus flower fragrance is joined in the solution of step (v) gained, continue stirring, make osmanthus flower fragrance be uniformly dispersed, be then turned on Homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the osmanthus flower fragrance of Longaacting fragrance-aretaining;
2) Longaacting fragrance-aretaining osmanthus flower fragrance, latex and first part of deionized water are weighed according to mass percent;
3) add first part of deionized water in a reservoir, open stirring, be subsequently adding latex, make latex be uniformly dispersed;
4) weigh Longaacting fragrance-aretaining osmanthus flower fragrance, join step 3) in the latex dispersion that obtains, continue stirring, make Longaacting fragrance-aretaining Osmanthus flower fragrance is dispersed in latex dispersion;
5) wallpaper is immersed in step 4) in the Longaacting fragrance-aretaining osmanthus flower fragrance dispersion liquid that obtains, infiltrate 1 minute, then wallpaper is taken Go out dry, i.e. obtain Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper.
CN201610527273.0A 2016-07-06 2016-07-06 A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper and preparation method thereof Pending CN106188732A (en)

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Application Number Priority Date Filing Date Title
CN201610527273.0A CN106188732A (en) 2016-07-06 2016-07-06 A kind of Longaacting fragrance-aretaining Flos Osmanthi Fragrantis fragrance wallpaper and preparation method thereof

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08291500A (en) * 1995-04-19 1996-11-05 Jumoku Chushutsu Seibun Riyou Gijutsu Kenkyu Kumiai Production of fragrance-containing wall paper
CN103801239A (en) * 2014-02-28 2014-05-21 东南大学 Heat-resisting sustained release type osmanthus fragrans essence microcapsule as well as preparation method and application thereof
CN203701480U (en) * 2014-01-16 2014-07-09 福建圣莉雅环保壁纸有限公司 Wallpaper sending forth fragrance for long time
CN105219170A (en) * 2015-10-16 2016-01-06 上海应用技术学院 One smears tea fragrance pencil Oil varnish and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08291500A (en) * 1995-04-19 1996-11-05 Jumoku Chushutsu Seibun Riyou Gijutsu Kenkyu Kumiai Production of fragrance-containing wall paper
CN203701480U (en) * 2014-01-16 2014-07-09 福建圣莉雅环保壁纸有限公司 Wallpaper sending forth fragrance for long time
CN103801239A (en) * 2014-02-28 2014-05-21 东南大学 Heat-resisting sustained release type osmanthus fragrans essence microcapsule as well as preparation method and application thereof
CN105219170A (en) * 2015-10-16 2016-01-06 上海应用技术学院 One smears tea fragrance pencil Oil varnish and preparation method thereof

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