CN106188731A - A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper and preparation method thereof - Google Patents

A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper and preparation method thereof Download PDF

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Publication number
CN106188731A
CN106188731A CN201610525870.XA CN201610525870A CN106188731A CN 106188731 A CN106188731 A CN 106188731A CN 201610525870 A CN201610525870 A CN 201610525870A CN 106188731 A CN106188731 A CN 106188731A
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CN
China
Prior art keywords
fragrance
aretaining
longaacting
essence
wallpaper
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CN201610525870.XA
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Chinese (zh)
Inventor
肖作兵
朱广用
周如隽
牛云蔚
徐子淇
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Shanghai Institute of Technology
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Shanghai Institute of Technology
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Priority to CN201610525870.XA priority Critical patent/CN106188731A/en
Publication of CN106188731A publication Critical patent/CN106188731A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L21/00Compositions of unspecified rubbers
    • C08L21/02Latex
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • EFIXED CONSTRUCTIONS
    • E04BUILDING
    • E04FFINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
    • E04F13/00Coverings or linings, e.g. for walls or ceilings
    • E04F13/002Coverings or linings, e.g. for walls or ceilings made of webs, e.g. of fabrics, or wallpaper, used as coverings or linings
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/02Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

Abstract

A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, count by weight percentage, the deionized water of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence by 1% 10%, the latex of 10% 40% and surplus forms.Additionally provide the preparation method of above-mentioned Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, first emulsion uniform is disperseed in deionized water, be subsequently adding Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence and stir, wallpaper is immersed, further take out dry, i.e. obtain the fragrant wallpaper with fragrance of a flower delicate fragrance characteristic perfume.Described Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence, count by weight percentage, the deionized water of fragrance of a flower delicate fragrance essence by 5% 25%, the dextrin of 10% 45%, the pure glue of 1% 4%, the arabic gum of 0.5% 1.5% and surplus forms.The fragrance of a flower delicate fragrance flavor application of Longaacting fragrance-aretaining in the perfuming of wallpaper, has been obtained the fragrance of a flower delicate fragrance fragrance wallpaper of Longaacting fragrance-aretaining, has added the aromatic function of wallpaper, improve the added value of wallpaper by the present invention.

Description

A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper and preparation method thereof
Technical field
The invention belongs to chemical field, relate to a kind of fragrance wallpaper, specifically a kind of fragrance of a flower delicate fragrance fragrance wallpaper and Its preparation method.
Background technology
Wallpaper, also known as wallpaper, is a kind of material for decorating indoor wall, the main base material of wallpaper be generally divided into papery, Four kinds of plastic sheeting, textile fibre cloth product, expansion type plastics etc..Wallpaper is in the American-European history using existing last 100 years, in city A kind of idea product has been become on field.Wallpaper low cost, purposes is wide, and surface color is various in style, and beautiful decoration is generous, and it is unique Style and distinguished decoration effect, enjoy the favor of people, be widely used in decorated house, public place of entertainment at present Institute, market, hotel etc..Along with improving constantly of people's living standard, the wallpaper with different-style and applicable different needs is new Product are in the urgent need to exploitation.If wallpaper can persistently distribute fragrance, give graceful comfortable fragrance, the attached of wallpaper will be greatly improved Value added and using effect, so the development of fragrance wallpaper has very important significance.
Fragrance of a flower delicate fragrance is a kind of composite fragrant, has the feature of the fragrance of a flower and delicate fragrance concurrently, and fragrance of a flower delicate fragrance composite fragrant is a kind of people The odor type generally liked.But, the organic compound all being had certain note by volatility due to essence forms, and tradition is fragrant The lasting of essence is the most lasting, and therefore, the development of the fragrant wallpaper with fragrance of a flower delicate fragrance odor characteristic of Longaacting fragrance-aretaining has wide Market prospect and important using value.
The preparation of the fragrant wallpaper with the Longaacting fragrance-aretaining of fragrance of a flower delicate fragrance characteristic perfume has no report.
Summary of the invention
For above-mentioned technical problem of the prior art, the invention provides a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper And preparation method thereof, described this Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper and preparation method thereof to solve of the prior art Wallpaper can not the technical problem of Longaacting fragrance-aretaining.
The invention provides a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, count by weight percentage, it is raw materials used Composition and content are as follows:
Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence 1%-10%;
Latex 10%-40%;
First part of deionized water surplus;
The fragrance of a flower delicate fragrance essence of described Longaacting fragrance-aretaining, count by weight percentage, its raw material composition and content are as follows:
Concrete, pure glue is commercially available prod, and for a kind of esters modified starch, concrete chemical name is: octenyl succinic Acid esters starch.
Present invention also offers the preparation method of above-mentioned a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, including walking as follows Rapid:
1) step of the fragrance of a flower delicate fragrance essence preparing Longaacting fragrance-aretaining;
I. fragrance of a flower delicate fragrance essence, dextrin, pure glue, arabic gum, second part of deionized water are weighed according to mass percent;
Add second part of deionized water the most in a reservoir, open stirring, be heated to 60 DEG C;
Iii. being joined by dextrin in the water of step (i), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, Obtain clear transparent solutions;
Iv. being joined by pure glue in the solution of step (ii) gained, temperature is maintained at 60 DEG C, continues stirring, makes pure glue divide Dissipate uniformly, obtain clear transparent solutions;
V. being joined by arabic gum in the solution of step (iii) gained, temperature is maintained at 60 DEG C, continue stirring, make Ah Draw primary glue to be uniformly dispersed, obtain clear transparent solutions, be cooled to 40 DEG C;
Vi. fragrance of a flower delicate fragrance essence is joined in the solution of step (iv) gained, continue stirring, make fragrance of a flower delicate fragrance essence divide Dissipate uniformly, be then turned on homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the fragrance of a flower delicate fragrance essence of Longaacting fragrance-aretaining.
2) Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence, latex and first part of deionized water are weighed according to mass percent;
3) add first part of deionized water water in a reservoir, open stirring, be subsequently adding latex, make latex be uniformly dispersed;
4) by Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence, step 3 is joined) in the latex dispersion that obtains, continue stirring, make long Effect lasting fragrance of a flower delicate fragrance essence is dispersed in latex dispersion;
5) wallpaper is immersed in step 4) in the Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence dispersion liquid that obtains, infiltrate 1 minute, then Wallpaper is taken out and is dried, i.e. obtain Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper.
The present invention uses dextrin and pure glue to be wall material, is embedded by fragrance of a flower delicate fragrance essence, is formed at essence particle surface Coating film, thus reduce the volatility of essence, improve the thermostability of fragrance of a flower delicate fragrance essence, stability and lasting.
The present invention compares with prior art, and its technological progress is significant.The present invention obtains the fragrance of a flower of a kind of Longaacting fragrance-aretaining Delicate fragrance essence, and by this flavor application in the perfuming of wallpaper, obtained the fragrance of a flower delicate fragrance fragrance wallpaper of Longaacting fragrance-aretaining, added wall The aromatic function of paper, improves the added value of wallpaper.
Detailed description of the invention
Below by embodiment, the present invention is further described, but does not affect protection scope of the present invention.
Embodiment 1
A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, count by weight percentage, its raw materials used composition and content are such as Under:
Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence 1%-10% (1g)
Latex 10%-40% (10g)
Deionized water 89% (89g);
Above-mentioned a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper is prepared via a method which:
(1) add a certain amount of deionized water water, in a reservoir, open stirring, be subsequently adding a certain amount of latex, make breast Glue is uniformly dispersed;
(2), weigh a certain amount of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence, join in the latex dispersion that step (1) obtains, Continue stirring, make Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence be dispersed in latex dispersion;
(3), by wallpaper it is immersed in the Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence dispersion liquid that step (2) obtains, infiltrates 1 minute, Then wallpaper is taken out and be dried, i.e. obtain Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper.The aroma strength of this fragrance wallpaper is the most weak.Should After fragrance wallpaper is placed 3 months naturally, through sensory evaluation, still there is the odor characteristic of fragrance of a flower delicate fragrance.
The fragrance of a flower delicate fragrance essence of Longaacting fragrance-aretaining used in above-mentioned a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, by weight Amount percentage calculation, its raw material composition and content are as follows:
The fragrance of a flower delicate fragrance essence of above-mentioned a kind of Longaacting fragrance-aretaining is prepared via a method which:
(1) add a certain proportion of deionized water, in a reservoir, open stirring, be heated to 60 DEG C;
(2), by dextrin joining in the water of step (1), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, Obtain clear transparent solutions;
(3), by pure glue joining in the solution of step (2) gained, temperature is maintained at 60 DEG C, continues stirring, makes pure glue divide Dissipate uniformly, obtain clear transparent solutions;
(4), by arabic gum joining in the solution of step (3) gained, temperature is maintained at 60 DEG C, continue stirring, make Ah Draw primary glue to be uniformly dispersed, obtain clear transparent solutions, be cooled to 40 DEG C;
(5), by fragrance of a flower delicate fragrance essence join in the solution of step (4) gained, continue stirring, make fragrance of a flower delicate fragrance essence divide Dissipate uniformly, be then turned on homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the fragrance of a flower delicate fragrance essence of Longaacting fragrance-aretaining, This essence aroma strength is the most weak.
Embodiment 2
A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, count by weight percentage, its raw materials used composition and content are such as Under:
Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence 10% (10g)
Latex 40% (40g)
Deionized water 50% (50g);
Above-mentioned a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper is prepared via a method which:
(1) add a certain amount of deionized water water, in a reservoir, open stirring, be subsequently adding a certain amount of latex, make breast Glue is uniformly dispersed;
(2), weigh a certain amount of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence, join in the latex dispersion that step (1) obtains, Continue stirring, make Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence be dispersed in latex dispersion;
(3), by wallpaper it is immersed in the Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence dispersion liquid that step (2) obtains, infiltrates 1 minute, Then wallpaper is taken out and be dried, i.e. obtain Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper.The aroma strength of this fragrance wallpaper is strong.This virtue After fragrant wallpaper is placed 3 months naturally, through sensory evaluation, still there is the odor characteristic of fragrance of a flower delicate fragrance.
The fragrance of a flower delicate fragrance essence of Longaacting fragrance-aretaining used in above-mentioned a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, by weight Amount percentage calculation, its raw material composition and content are as follows:
The fragrance of a flower delicate fragrance essence of above-mentioned a kind of Longaacting fragrance-aretaining is prepared via a method which:
(1) add a certain proportion of deionized water, in a reservoir, open stirring, be heated to 60 DEG C;
(2), by dextrin joining in the water of step (1), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, Obtain clear transparent solutions;
(3), by pure glue joining in the solution of step (2) gained, temperature is maintained at 60 DEG C, continues stirring, makes pure glue divide Dissipate uniformly, obtain clear transparent solutions;
(4), by arabic gum joining in the solution of step (3) gained, temperature is maintained at 60 DEG C, continue stirring, make Ah Draw primary glue to be uniformly dispersed, obtain clear transparent solutions, be cooled to 40 DEG C;
(5), by fragrance of a flower delicate fragrance essence join in the solution of step (4) gained, continue stirring, make fragrance of a flower delicate fragrance essence divide Dissipate uniformly, be then turned on homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the fragrance of a flower delicate fragrance essence of Longaacting fragrance-aretaining, This essence aroma strength is strong.
Embodiment 3
A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, count by weight percentage, its raw materials used composition and content are such as Under:
Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence 5% (5g)
Latex 30% (30g)
Deionized water 65% (65g);
Above-mentioned a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper is prepared via a method which:
(1) add a certain amount of deionized water water, in a reservoir, open stirring, be subsequently adding a certain amount of latex, make breast Glue is uniformly dispersed;
(2), weigh a certain amount of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence, join in the latex dispersion that step (1) obtains, Continue stirring, make Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence be dispersed in latex dispersion;
(3), by wallpaper it is immersed in the Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence dispersion liquid that step (2) obtains, infiltrates 1 minute, Then wallpaper is taken out and be dried, i.e. obtain Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper.The aroma strength of this fragrance wallpaper is moderate.Should After fragrance wallpaper is placed 3 months naturally, through sensory evaluation, still there is the odor characteristic of fragrance of a flower delicate fragrance.
The fragrance of a flower delicate fragrance essence of Longaacting fragrance-aretaining used in above-mentioned a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, by weight Amount percentage calculation, its raw material composition and content are as follows:
The fragrance of a flower delicate fragrance essence of above-mentioned a kind of Longaacting fragrance-aretaining is prepared via a method which:
(1) add a certain proportion of deionized water, in a reservoir, open stirring, be heated to 60 DEG C;
(2), by dextrin joining in the water of step (1), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, Obtain clear transparent solutions;
(3), by pure glue joining in the solution of step (2) gained, temperature is maintained at 60 DEG C, continues stirring, makes pure glue divide Dissipate uniformly, obtain clear transparent solutions;
(4), by arabic gum joining in the solution of step (3) gained, temperature is maintained at 60 DEG C, continue stirring, make Ah Draw primary glue to be uniformly dispersed, obtain clear transparent solutions, be cooled to 40 DEG C;
(5), by fragrance of a flower delicate fragrance essence join in the solution of step (4) gained, continue stirring, make fragrance of a flower delicate fragrance essence divide Dissipate uniformly, be then turned on homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the fragrance of a flower delicate fragrance essence of Longaacting fragrance-aretaining, This essence aroma strength is moderate.
Above said content is only the basic explanation under present inventive concept, and according to appointing that technical scheme is done What equivalent transformation, belongs to the scope of protection of the invention.

Claims (2)

1. a Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper, it is characterised in that count by weight percentage, its raw materials used composition And content is as follows:
Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence 1%-10%;
Latex 10%-40%;
First part of deionized water surplus;
The fragrance of a flower delicate fragrance essence of described Longaacting fragrance-aretaining, count by weight percentage, its raw material composition and content are as follows:
The preparation method of a kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper the most according to claim 1, it is characterised in that bag Include following steps:
1) step of the fragrance of a flower delicate fragrance essence preparing Longaacting fragrance-aretaining;
I. fragrance of a flower delicate fragrance essence, dextrin, pure glue, arabic gum, second part of deionized water are weighed according to mass percent;
Add second part of deionized water the most in a reservoir, open stirring, be heated to 60 DEG C;
Iii. being joined by dextrin in the water of step (i), temperature is maintained at 60 DEG C, continues stirring, makes dextrin be uniformly dispersed, obtain Clear transparent solutions;
Iv. being joined by pure glue in the solution of step (ii) gained, temperature is maintained at 60 DEG C, continues stirring, makes the dispersion of pure glue all Even, obtain clear transparent solutions;
V. being joined by arabic gum in the solution of step (iii) gained, temperature is maintained at 60 DEG C, continues stirring, makes Arab Glue is uniformly dispersed, and obtains clear transparent solutions, is cooled to 40 DEG C;
Vi. fragrance of a flower delicate fragrance essence is joined in the solution of step (iv) gained, continue stirring, make the dispersion of fragrance of a flower delicate fragrance essence all Even, it is then turned on homogenizer, homogenizing 30 minutes under the conditions of 10000rph, i.e. obtain the fragrance of a flower delicate fragrance essence of Longaacting fragrance-aretaining.
2) Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence, latex and first part of deionized water are weighed according to mass percent;
3) add first part of deionized water water in a reservoir, open stirring, be subsequently adding latex, make latex be uniformly dispersed;
4) by Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence, step 3 is joined) in the latex dispersion that obtains, continue stirring, make long-acting staying Fragrant flower perfume (or spice) delicate fragrance essence is dispersed in latex dispersion;
5) wallpaper is immersed in step 4) in the Longaacting fragrance-aretaining fragrance of a flower delicate fragrance essence dispersion liquid that obtains, infiltrate 1 minute, then by wall Paper takes out and is dried, and i.e. obtains Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper.
CN201610525870.XA 2016-07-06 2016-07-06 A kind of Longaacting fragrance-aretaining fragrance of a flower delicate fragrance fragrance wallpaper and preparation method thereof Pending CN106188731A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110593013A (en) * 2019-09-19 2019-12-20 上海应用技术大学 Apple-flavored aromatic wallpaper and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08291500A (en) * 1995-04-19 1996-11-05 Jumoku Chushutsu Seibun Riyou Gijutsu Kenkyu Kumiai Production of fragrance-containing wall paper
CN101708451A (en) * 2009-12-25 2010-05-19 陕西科技大学 Method for preparing high-temperature resistant essence microcapsules
CN103801239A (en) * 2014-02-28 2014-05-21 东南大学 Heat-resisting sustained release type osmanthus fragrans essence microcapsule as well as preparation method and application thereof
CN203701480U (en) * 2014-01-16 2014-07-09 福建圣莉雅环保壁纸有限公司 Wallpaper sending forth fragrance for long time
CN103949196A (en) * 2014-05-12 2014-07-30 东南大学 Osmanthus essence microcapsule powder as well as preparation method and application thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08291500A (en) * 1995-04-19 1996-11-05 Jumoku Chushutsu Seibun Riyou Gijutsu Kenkyu Kumiai Production of fragrance-containing wall paper
CN101708451A (en) * 2009-12-25 2010-05-19 陕西科技大学 Method for preparing high-temperature resistant essence microcapsules
CN203701480U (en) * 2014-01-16 2014-07-09 福建圣莉雅环保壁纸有限公司 Wallpaper sending forth fragrance for long time
CN103801239A (en) * 2014-02-28 2014-05-21 东南大学 Heat-resisting sustained release type osmanthus fragrans essence microcapsule as well as preparation method and application thereof
CN103949196A (en) * 2014-05-12 2014-07-30 东南大学 Osmanthus essence microcapsule powder as well as preparation method and application thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110593013A (en) * 2019-09-19 2019-12-20 上海应用技术大学 Apple-flavored aromatic wallpaper and preparation method thereof

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