CN106187081A - A kind of preparation technology of crystallite ink-jet polished bricks - Google Patents
A kind of preparation technology of crystallite ink-jet polished bricks Download PDFInfo
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- CN106187081A CN106187081A CN201610571866.7A CN201610571866A CN106187081A CN 106187081 A CN106187081 A CN 106187081A CN 201610571866 A CN201610571866 A CN 201610571866A CN 106187081 A CN106187081 A CN 106187081A
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- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
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- C04B2235/3472—Alkali metal alumino-silicates other than clay, e.g. spodumene, alkali feldspars such as albite or orthoclase, micas such as muscovite, zeolites such as natrolite
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Abstract
The preparation technology of a kind of crystallite ink-jet polished bricks, belongs to house decoration material technical field.It is characterized in that, preparation process is: then pushs aside after first base substrate raw material ink-jet being starched re-compacted one-tenth base substrate cake and expects filling；Covering end base, after drying pre-burning part be fired, carry out after being warming up to 1090 DEG C ~ 1105 DEG C being incubated 38min ~ 43min for the first time, carry out second time after being warming up to 1207 DEG C ~ 1212 DEG C the most again and be incubated 95min ~ 110min, second time be incubated after with the rate of temperature fall fast cooling of 95 DEG C/10min ~ 120 DEG C/10min to room temperature；After firing, upper base substrate face is polished and get final product.The textured pattern of the crystallite ink-jet polished bricks that this technique is made has randomness, and each piece of brick all has the decorative pattern of oneself uniqueness, and the decorative pattern that decorative pattern is had by whole upper green body layer, brick decorative pattern will be caused to disappear along with friction.
Description
Technical field
The preparation technology of a kind of crystallite ink-jet polished bricks, belongs to house decoration material technical field.
Background technology
Traditional ceramic tile is with fire-resistant metal-oxide and half-metal oxide, via grinding, mix, suppress, glazing,
Sintering process makes and is formed.Decorative pattern on ceramic tile is typically all formed glaze layer by glazing step and shows, but this glaze
If the thickness of the glaze layer of face brick is less, then ceramic tile can will grind glaze layer within the shorter use time so that porcelain
Original decorative pattern hour of brick.And if increase glaze layer thickness, cost can increase considerably, reduce the market competitiveness.Now
Also the ceramic tile having no longer sets glaze layer, but is directly polished, the base substrate of ceramic tile to obtain the ceramic tile of a kind of surface-brightening.But
Being that the surface of this polished bricks cannot form diversified decorative pattern, style is single, does not meets Popular Aesthetics demand.
Summary of the invention
The technical problem to be solved in the present invention is: overcome the deficiencies in the prior art, it is provided that a kind of wear-resisting pattern again is various
The preparation technology of crystallite ink-jet polished bricks.
The technical solution adopted for the present invention to solve the technical problems is: the preparation technology of this crystallite ink-jet polished bricks, its
It is characterised by that preparation process is:
1) random blanking is carried out after first base substrate raw material pulverizing being made base substrate raw meal powder；
2) uniform ink-jet slurry on base substrate raw meal powder, is then compressed to base substrate cake；
3) base substrate cake is pushed aside, cause the random area to be filled of through base substrate cake；
4) blank grog blanking to the most above-mentioned push aside after base substrate cake on fill area to be filled realize thoroughly expect filling；
5) compressing prepared upper base substrate is re-started after thoroughly expecting filling；
6) on upper base substrate, it is coated with end base and obtains pre-burning part, the base substrate raw material composition used by end base and the base substrate raw material group of step 1)
Become identical；
7) pre-burning part is dried 45 min ~ 60min under the baking temperature of 200 DEG C ~ 220 DEG C；
8) being fired pre-burning part, after furnace temperature is preheated to 900 DEG C, pre-burning part enters stove, with 15 DEG C/10min ~ 22 DEG C/10min
Heating rate be gradually heating to 1090 DEG C ~ 1105 DEG C after carry out for the first time being incubated 38min ~ 43min, the most again with 10 DEG C/
The heating rate of 10min ~ 20 DEG C/10min carry out after being gradually heating to 1207 DEG C ~ 1212 DEG C second time be incubated 95min ~
110min, second time be incubated after with the rate of temperature fall fast cooling of 65 DEG C/10min ~ 120 DEG C/10min to room temperature；
9) after firing, upper base substrate face is polished and get final product.
The preparation technology of this crystallite ink-jet polished bricks uses secondary material distributing mode, and upper base substrate and the end base of secondary material distributing are
At the bottom of same base material, brick face and brick, complete unity can reach jade highest quality effect, decreases because bottom surface material does not mates simultaneously
The brick later stage rebound deformation caused.For upper base substrate through step 3), 4) add somehow and between the bottom surface material that formed of ink slurry not
The sintering curve joining the problem present invention drying process by step 7) and step 8) is overcome, and first passes through drying process and makes
Upper base substrate and end base in retain appropriate moisture, then control the crystalline rate in bottom surface is expected by controlling heating rate, reaching
It is incubated with stable crystal form to first carrying out the short time during certain degree of crystallinity at a lower temperature, then reduces heating rate and enter one
Step controls crystal formation and grows up, finally long-time heat preservation under the high temperature of 1207 DEG C ~ 1212 DEG C, stable prod micro structure, the most rapidly
Cooling, makes complete unity at the bottom of brick face and brick can reach jade highest quality effect, thoroughly solves the later stage bounce-back of brick simultaneously
Deformation.The present invention is delineated by unique vivid cloth, colorant, thoroughly expects that filling, powder the big core technology essences of deduction four are cast.Product
The natural texture effects such as formation mountains and rivers, the surface vein of the earth, lava agglomerate, valley ground cleave, rubble distribution.By Grand Canyon rise and fall be continuous, hundred
Turn thousand times, dangerously steep elegant naturally meteorological perfect inscription rubbing, the superb craftsmanship of reduction the Nature.The powder warp of different colours in base substrate
After crossing premix extruding, forming the unbroken mountain range texture that rises and falls, lines are free and easy, enjoyable true to nature.In order to make the three-dimensional higher texture of product
Finer and smoother, the ink throwing atomization process cooperation additionally using ink-jet slurry strikes off step, makes ink throw and is distributed uniformly after atomization
Around lava, agglomerate, form brightly painted stone line, deep or shallow, sketch out the profile of lava agglomerate visually, be rich in
Third dimension.Base substrate cake powder after precompressed, pushs aside with pressure tool hands, forms crisscross valley physical features style and features, then exist
To super expect (somehow) fill therebetween so that texture is more life-like, three-dimensional, the use of super material, makes product more press close to beautiful matter
Texture.Somehow freely to trickle down that cooperation strikes off be somehow the random cloth of powder, deduce the textured pattern that product surface is the most elegant.
The textured pattern of the crystallite ink-jet polished bricks that this technique is made has randomness, and each piece of brick all has the decorative pattern of oneself uniqueness,
And the decorative pattern that decorative pattern is had by whole upper green body layer, brick decorative pattern will be caused to disappear along with friction.
Preferably, base substrate raw meal powder is first compressed to blank bar by described step 1), and blank bar is broken into the longest
The small blocks in irregular shape of diagonal 3cm ~ 10cm, the spacing between adjacent isles body is 2.5cm ~ 15cm；Then proceed to
Unrestrained base substrate raw meal powder is further continued for carrying out step 2 after filling the space between small blocks) operation.Twice base substrate raw material of this technique
Use and the powder of different colours can be carried out independent assortment collocation, through premix precompressed, form color after crushing well arranged,
Agglomerate is not of uniform size, the lava agglomerate that quantity differs, and is randomly distributed on polished bricks surface, more presses close to former stone effect, level
Clearly more demarcated.
Preferably, described base substrate raw material weight portion composition includes: albite 35 ~ 45 parts, potassium feldspar 17 ~ 24 parts, ball clay
20 ~ 28 parts, 3 ~ 7 parts of high alumina stone, 2 ~ 4 parts of Talcum.This formula can reach similar natural jade decorative effect and avoid again simultaneously
The antifouling defects in brick face such as pin hole pore.High-quality selection guarantees Product Green environmental protection and radiationless pollution.Ball clay is because of pressure during exploitation
Glomeration and gain the name, be that be made up of and be mixed with the one of the impurity such as a number of quartz, Muscovitum and organic matter kaolinite plastic
Clay.High alumina stone is also known as bauxite soil or bauxite, and main component is aluminium oxide, is the hydrated alumina containing impurity, is one
Plant earthy mineral.
Described somehow base substrate grog commonly used in the art can be used, all can reach preferable under the technique of the present invention
Effect.
Preferably, the base substrate cake described in step 3) forms the in irregular shape of long-diagonal 10cm ~ 25cm after being pushed aside
Agglomerate body, the spacing between adjacent bulk body is 0.6 cm ~ 3cm.Under this optimum condition, form pattern and more agree with nature,
More attractive in appearance.
Preferably, step 2) described in the weight portion composition of ink slurry include: albite 27 ~ 33 parts, potassium feldspar 27 ~ 33 parts,
Ball clay 13 ~ 17 parts, 8 ~ 12 parts of high alumina stone, pyrophillite 8 ~ 12 parts, 3 ~ 7 parts of Talcum.This ink slurry cooperation present invention process can body
Revealing the unexistent fine and smooth texture of common polished bricks and rich colors, color development is gorgeous and does not haves delayed crazing, deformation completely
Many defects such as pin hole.
Preferably, the pre-burning part described in step 7) is dried 60min under the baking temperature of 200 DEG C.
Preferably, the temperature of the first time insulation described in step 8) is 1100 DEG C, and temperature retention time is 40min.
Preferably, the temperature of the second time insulation described in step 8) is 1210 DEG C, and temperature retention time is 100min.
It is dried and under the above-mentioned optimum condition fired, it is possible to make the polished bricks of the present invention reach optimal state.
Compared with prior art, the preparation technology of a kind of crystallite ink-jet polished bricks of the present invention is had the advantage that
It is: the preparation technology of this crystallite ink-jet polished bricks makes complete unity at the bottom of brick face and brick can reach beautiful by the control of calcining system
Stone highest quality effect, thoroughly solves the later stage rebound deformation of brick simultaneously.The product surface that the present invention prepares forms ground, mountains and rivers
The natural texture effects such as arteries and veins, lava agglomerate, valley ground cleave, rubble distribution.Grand Canyon is risen and fallen be continuous, hundred turns thousand times, dangerously steep waft
Naturally the meteorological perfect inscription rubbing of ease, the superb craftsmanship of reduction the Nature.The texture maps of the crystallite ink-jet polished bricks that this technique is made
Case has randomness, and each piece of brick all has the decorative pattern of oneself uniqueness, and the decorative pattern that decorative pattern is had by whole upper green body layer, no
Brick decorative pattern can be caused to disappear along with friction.
Detailed description of the invention
Below in conjunction with specific embodiment, the preparation technology of a kind of crystallite ink-jet polished bricks of the present invention is described further,
Wherein embodiment 1 is most preferred embodiment.
Embodiment 1:
1) press base substrate raw material weight portion to form: albite 40 parts, potassium feldspar 40 parts, ball clay 25 parts, 5 parts of high alumina stone, Talcum 3
Part weighs material；It is pressed into base substrate bar after base substrate raw material pulverizing；This billet cake is broken into long-diagonal 3cm ~ 10cm again
Small blocks in irregular shape, the spacing between adjacent isles body is 2.5cm ~ 15cm；Then proceed to unrestrained base substrate raw meal powder
Again carry out compacting after filling the space between small blocks and make base substrate cake；
2) uniform ink-jet slurry on base substrate raw meal powder, is then compressed to base substrate cake；The weight portion composition of ink slurry includes: albite 30
Part, potassium feldspar 30 parts, ball clay 15 parts, 10 parts of high alumina stone, pyrophillite 10 parts, 5 parts of Talcum；
3) utilize pressure tool hands to be pushed aside by secondary base substrate cake, cause the area to be filled of through base substrate cake, pressure tool hands to be pushed aside by base substrate cake
The agglomerate body in irregular shape of rear formation long-diagonal 15cm ~ 25cm, the spacing between adjacent bulk body be 0.6 cm ~
3cm；
4) freely trickle down blank chamotte powder on the base substrate cake after above-mentioned pushing aside to realize thoroughly expecting filling；
5) blank grog is re-started compressing prepared upper base substrate；
6) being coated with base substrate raw material identical with step 1) on upper base substrate and form the end base being pressed into, the cutting of professional etiquette of going forward side by side lattice obtains pre-
Burn part；
7) pre-burning part is dried 60min under the baking temperature of 200 DEG C；
8) pre-burning part is fired, the thermograph of every 10min temperature of record: being fired pre-burning part, furnace temperature is pre-
Heat is to after 900 DEG C, and pre-burning part enters stove, with the heating rate of 15 DEG C/10min ~ 22 DEG C/10min be gradually heating to 1100 DEG C laggard
Row insulation 40min for the first time, after being gradually heating to 1220 DEG C with the heating rate of 10 DEG C/10min ~ 20 DEG C/10min the most again
Carrying out second time and be incubated 100min, second time is quick with the rate of temperature fall of 65 DEG C/10min ~ 120 DEG C/10min after being incubated
It is cooled to room temperature；
Thermograph
；
9) after firing, upper base substrate face is polished and get final product.
Embodiment 2:
1) press base substrate raw material weight portion to form: albite 35 parts, potassium feldspar 24 parts, ball clay 20 parts, 7 parts of high alumina stone, Talcum 2
Part weighs material；It is pressed into base substrate bar after base substrate raw material pulverizing；This blank bar is broken into long-diagonal 3cm ~ 10cm again
Small blocks in irregular shape, the spacing between adjacent isles body is 2.5cm ~ 15cm；Then proceed to unrestrained base substrate raw meal powder
Again carry out compacting after filling the space between small blocks and make base substrate cake；
2) uniform ink-jet slurry on base substrate raw meal powder, is then compressed to base substrate cake；The weight portion composition of ink slurry includes: albite 27
Part, potassium feldspar 33 parts, ball clay 13 parts, 12 parts of high alumina stone, pyrophillite 8 parts, 7 parts of Talcum；
3) utilize pressure tool hands to be pushed aside by secondary base substrate cake, cause the area to be filled of through base substrate cake, pressure tool hands to be pushed aside by base substrate cake
The agglomerate body in irregular shape of rear formation long-diagonal 15cm ~ 25cm, the spacing between adjacent bulk body be 0.6 cm ~
3cm；
4) freely trickle down blank chamotte powder on the base substrate cake after above-mentioned pushing aside to realize thoroughly expecting filling；
5) blank grog is re-started compressing prepared upper base substrate；
6) being coated with base substrate raw material identical with step 1) on upper base substrate and form the end base being pressed into, the cutting of professional etiquette of going forward side by side lattice obtains pre-
Burn part；
7) pre-burning part is dried 55min under the baking temperature of 210 DEG C；
8) being fired pre-burning part, every 10min records a temperature sintering curve: be fired pre-burning part, and furnace temperature preheats
After 900 DEG C, pre-burning part enters stove, carries out after being gradually heating to 1105 DEG C with the heating rate of 15 DEG C/10min ~ 22 DEG C/10min
For the first time insulation 38min, the most again with the heating rate of 10 DEG C/10min ~ 20 DEG C/10min be gradually heating to 1222 DEG C laggard
Row second time insulation 95min, with the rate of temperature fall fast cooling of 65 DEG C/10min ~ 120 DEG C/10min after being incubated for the second time
To room temperature；
Thermograph
；
9) after firing, upper base substrate face is polished and get final product.
Embodiment 3:
1) press base substrate raw material weight portion to form: albite 45 parts, potassium feldspar 17 parts, ball clay 28 parts, 3 parts of high alumina stone, Talcum 4
Part weighs material；By the base substrate raw material pulverizing random blanking of laggard row；
2) uniform ink-jet slurry on base substrate raw meal powder, is then compressed to base substrate cake；The weight portion composition of ink slurry includes: albite 33
Part, potassium feldspar 27 parts, ball clay 17 parts, 8 parts of high alumina stone, pyrophillite 12 parts, 3 parts of Talcum；
3) utilize pressure tool hands to be pushed aside by base substrate cake, cause the area to be filled of through base substrate cake, pressure tool hands to push base substrate cake aside rear shape
Becoming the agglomerate body in irregular shape of long-diagonal 10cm ~ 25cm, the spacing between adjacent bulk body is 0.6 cm ~ 3cm；
4) freely trickle down blank chamotte powder on the base substrate cake after above-mentioned pushing aside to realize thoroughly expecting filling；
5) blank grog is re-started compressing prepared upper base substrate；
6) being coated with base substrate raw material identical with step 1) on upper base substrate and form the end base being pressed into, the cutting of professional etiquette of going forward side by side lattice obtains pre-
Burn part；
7) pre-burning part is dried 45 min under the baking temperature of 220 DEG C；
8) being fired pre-burning part, every 10min records a temperature sintering curve: be fired pre-burning part, and furnace temperature preheats
After 900 DEG C, pre-burning part enters stove, carries out after being gradually heating to 1090 DEG C with the heating rate of 15 DEG C/10min ~ 22 DEG C/10min
For the first time insulation 43min, the most again with the heating rate of 10 DEG C/10min ~ 20 DEG C/10min be gradually heating to 1217 DEG C laggard
Row second time insulation 110min, with the fast prompt drop of rate of temperature fall of 65 DEG C/10min ~ 120 DEG C/10min after being incubated for the second time
Warm to room temperature；
Thermograph
；
9) after firing, upper base substrate face is polished and get final product.
The above, be only presently preferred embodiments of the present invention, is not the restriction that the present invention makees other form, appoints
What those skilled in the art changed possibly also with the technology contents of the disclosure above or be modified as equivalent variations etc.
Effect embodiment.But every without departing from technical solution of the present invention content, the technical spirit of the foundation present invention is to above example institute
Any simple modification, equivalent variations and the remodeling made, still falls within the protection domain of technical solution of the present invention.
Claims (8)
1. the preparation technology of a crystallite ink-jet polished bricks, it is characterised in that preparation process is:
1) random blanking is carried out after first base substrate raw material pulverizing being made base substrate raw meal powder；
2) uniform ink-jet slurry on base substrate raw meal powder, is then compressed to base substrate cake；
3) base substrate cake is pushed aside, cause the random area to be filled of through base substrate cake；
4) blank grog blanking to the most above-mentioned push aside after base substrate cake on fill area to be filled realize thoroughly expect filling；
5) compressing prepared upper base substrate is re-started after thoroughly expecting filling；
6) on upper base substrate, it is coated with end base and obtains pre-burning part, the base substrate raw material composition used by end base and the base substrate raw material group of step 1)
Become identical；
7) pre-burning part is dried 45 min ~ 60min under the baking temperature of 200 DEG C ~ 220 DEG C；
8) being fired pre-burning part, after furnace temperature is preheated to 900 DEG C, pre-burning part enters stove, with 15 DEG C/10min ~ 22 DEG C/10min
Heating rate be gradually heating to 1090 DEG C ~ 1105 DEG C after carry out for the first time being incubated 38min ~ 43min, the most again with 10 DEG C/
The heating rate of 10min ~ 20 DEG C/10min carry out after being gradually heating to 1207 DEG C ~ 1212 DEG C second time be incubated 95min ~
110min, second time be incubated after with the rate of temperature fall fast cooling of 65 DEG C/10min ~ 120 DEG C/10min to room temperature；
9) after firing, upper base substrate face is polished and get final product.
The preparation technology of a kind of crystallite ink-jet polished bricks the most according to claim 1, it is characterised in that: described step 1)
Middle first base substrate raw meal powder is compressed to blank bar, and blank bar is broken into the in irregular shape of long-diagonal 3cm ~ 10cm
Small blocks, the spacing between adjacent isles body is 2.5cm ~ 15cm；Then proceed to unrestrained base substrate raw meal powder fill between small blocks
Be further continued for behind space carrying out step 2) operation.
The preparation technology of a kind of crystallite ink-jet polished bricks the most according to claim 1 and 2, it is characterised in that: described base
Body raw material weight portion composition includes: albite 35 ~ 45 parts, potassium feldspar 17 ~ 24 parts, ball clay 20 ~ 28 parts, 3 ~ 7 parts of high alumina stone,
2 ~ 4 parts of Talcum.
The preparation technology of a kind of crystallite ink-jet polished bricks the most according to claim 1, it is characterised in that: described in step 3)
Base substrate cake is formed the agglomerate body in irregular shape of long-diagonal 10cm ~ 25cm after pushing aside, between adjacent bulk body between
Away from for 0.6 cm ~ 3cm.
The preparation technology of a kind of crystallite ink-jet polished bricks the most according to claim 1, it is characterised in that: step 2) described in
The weight portion composition of ink slurry includes: albite 27 ~ 33 parts, potassium feldspar 27 ~ 33 parts, ball clay 13 ~ 17 parts, 8 ~ 12 parts of high alumina stone,
Pyrophillite 8 ~ 12 parts, 3 ~ 7 parts of Talcum.
The preparation technology of a kind of crystallite ink-jet polished bricks the most according to claim 1, it is characterised in that: described in step 7)
Pre-burning part is dried 60min under the baking temperature of 200 DEG C.
The preparation technology of a kind of crystallite ink-jet polished bricks the most according to claim 1, it is characterised in that: described in step 8)
The temperature of insulation is 1100 DEG C for the first time, and temperature retention time is 40min.
The preparation technology of a kind of crystallite ink-jet polished bricks the most according to claim 1, it is characterised in that: described in step 8)
The temperature of second time insulation is 1210 DEG C, and temperature retention time is 100min.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103159497A (en) * | 2011-12-09 | 2013-06-19 | 辽宁金地阳陶瓷有限公司 | Jinyongdong stone polished tile and production method for same |
| CN104944923A (en) * | 2015-06-23 | 2015-09-30 | 淄博成畅建筑陶瓷有限公司 | Polished tile and making method thereof |
| CN105328782A (en) * | 2015-10-22 | 2016-02-17 | 广东宏陶陶瓷有限公司 | Ceramic polished brick and production method and production line of ceramic polished brick |
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2016
- 2016-07-20 CN CN201610571866.7A patent/CN106187081B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103159497A (en) * | 2011-12-09 | 2013-06-19 | 辽宁金地阳陶瓷有限公司 | Jinyongdong stone polished tile and production method for same |
| CN104944923A (en) * | 2015-06-23 | 2015-09-30 | 淄博成畅建筑陶瓷有限公司 | Polished tile and making method thereof |
| CN105328782A (en) * | 2015-10-22 | 2016-02-17 | 广东宏陶陶瓷有限公司 | Ceramic polished brick and production method and production line of ceramic polished brick |
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