CN106149360A - A kind of silkworm silk swelling agent - Google Patents
A kind of silkworm silk swelling agent Download PDFInfo
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- CN106149360A CN106149360A CN201610519819.8A CN201610519819A CN106149360A CN 106149360 A CN106149360 A CN 106149360A CN 201610519819 A CN201610519819 A CN 201610519819A CN 106149360 A CN106149360 A CN 106149360A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/2243—Mono-, di-, or triglycerides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/285—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acid amides or imides
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
- D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
Abstract
The invention discloses a kind of silkworm silk swelling agent, in units of weight portion, including following raw material: potassium silicate 200 800 parts, 80 100 parts of surfactant, defoamer 6 10 parts, foam stabilizer 35 parts, penetrating agent 24 parts, emulsifying agent 23 parts, dispersant 12 parts, cross-linking agent 24 parts, regulator 23 parts, thickening agent 23 parts, preservative 12 parts, flavouring agent 0.8 1.2 parts, 1,500 9000 parts of water.Silkworm silk swelling agent bactericidal property of the present invention is excellent, and staphylococcus aureus, escherichia coli, the sterilizing rate of Candida albicans are all reached more than 97%；Preparation method of the present invention is simple, it is feasible to facilitate, and silkworm silk swelling agent preparation cost is low, effectively in popularization and application.
Description
[technical field]
The invention belongs to swelling agent preparing technical field, be specifically related to a kind of silkworm silk swelling agent.
[background technology]
The technique of traditional approach processing silkworm silk quilt is simple, and kind is the most single, with the silkworm silk quilt of traditional handicraft processing through making
With rear, silk fiber easy entanglement, adhesion, elastic therewith and warmth retention property will decrease, need often to turn over tear open, garnetting, Cai Nengbao
Hold the original excellent dress ornament performance of silkworm silk quilt.
The performance such as bulk, soft, high-elastic excellent for giving silkworm silk, need to carry out polish to silkworm silk, makes silk fiber empty
Gap is expanded, and the silk cotton made has feature bulk, not knot tying between high resiliency, fiber.By using swelling agent to enter silkworm silk
Row expanding treatment, can increase silk fiber bulkiness, high resiliency, flexibility, can effectively prevent not haircuts, entanglement between silk fiber,
Improve the practicality of silkworm silk quilt.Silkworm silk carries out needing in finishing passes to use silkworm silk swelling agent at present, but effect is not
Very well, the demand of factory's actual production it is not met by.
[summary of the invention]
The present invention provides a kind of silkworm silk swelling agent, and to solve silk fiber easy entanglement, adhesion, elastic therewith and warmth retention property will
The problem such as can decrease.Silkworm silk swelling agent bactericidal property of the present invention is excellent, reads staphylococcus aureus, escherichia coli, white
The sterilizing rate of pearl bacterium all reaches more than 97%；Preparation method of the present invention is simple, it is feasible to facilitate, and silkworm silk swelling agent preparation cost is low,
Strong in popularization and application.
In order to solve above technical problem, the present invention by the following technical solutions:
A kind of silkworm silk swelling agent, in units of weight portion, including following raw material: potassium silicate 200-800 part, surfactant
80-100 part, defoamer 6-10 part, foam stabilizer 3-5 part, penetrating agent 2-4 part, emulsifying agent 2-3 part, dispersant 1-2 part, cross-linking agent
2-4 part, regulator 2-3 part, thickening agent 2-3 part, preservative 1-2 part, flavouring agent 0.8-1.2 part, water 1500-9000 part；
Described surfactant is polyacrylamide；
Described foam stabilizer is polyvinyl alcohol；
Described emulsifying agent is glyceryl monostearate；
Described cross-linking agent diethyl phosphate；
The preparation method of described silkworm silk swelling agent, comprises the following steps:
S1: added by surfactant in 700-1500 part water, be warming up to 44-46 DEG C of stirring and dissolving, prepares mixed liquor I；
S2: the mixed liquor I prepared to step S1 adds penetrating agent, emulsifying agent, dispersant, cross-linking agent, thickening agent, is heated to
58-62 DEG C, under ul-trasonic irradiation, be 200-300r/min stir process 25-30min at rotating speed, prepares mixed liquor II；
S3: stop heating and ul-trasonic irradiation, the mixed liquor II prepared to step S2 adds defoamer and foam stabilizer, is turning
Speed is stirring 5-10min under 100-300r/min, prepares mixed liquor III；
S4: add preservative and flavouring agent in the mixed liquor III that step S3 prepares, under rotating speed is 100-200r/min
Stirring 3-5min, prepares mixed liquor IV；
S5: adding regulator in the mixed liquor IV that step S4 prepares, making pH value is 5-5.4, prepares mixed liquor V；
S6: potassium silicate is added in 800-8000 part water, at being warming up to 65-68 DEG C, stirring and dissolving potassium silicate, prepare mixing
Liquid VI；
Mixed liquor VI mix homogeneously that S7: the mixed liquor V step S5 prepared and step S6 prepare, i.e. prepares silkworm silk swollen
Agent.
Further, described defoamer is silane-modified propionic ester.
Further, described penetrating agent alkyl benzene sulphonate potassium.
Further, described dispersant lauryl alcohol potassium sulfate.
Further, described regulator is acetic acid.
Further, described thickening agent is carrageenan.
Further, described preservative is quinoxyfen.
Further, described flavouring agent is Herba Lysimachiae foenum-graeci quintessence oil.
The method have the advantages that
(1), after using silkworm silk swelling agent of the present invention, silkworm silk has stronger compliance and intensity of colour；
(2) silkworm silk swelling agent bactericidal property of the present invention is excellent, to staphylococcus aureus, escherichia coli, Candida albicans
Sterilizing rate all reaches more than 97%；
(3) preparation method of the present invention is simple, it is feasible to facilitate, and silkworm silk swelling agent preparation cost is low, effectively in popularization and application.
[detailed description of the invention]
For ease of being more fully understood that the present invention, being illustrated by following example, these embodiments belong to the present invention's
Protection domain, but it is not intended to protection scope of the present invention.
In an embodiment, described silkworm silk swelling agent, in units of weight portion, including following raw material: potassium silicate 200-800
Part, surfactant 80-100 part, defoamer 6-10 part, foam stabilizer 3-5 part, penetrating agent 2-4 part, emulsifying agent 2-3 part, dispersant
1-2 part, cross-linking agent 2-4 part, regulator 2-3 part, thickening agent 2-3 part, preservative 1-2 part, flavouring agent 0.8-1.2 part, water 1500-
9000 parts；
Described surfactant is polyacrylamide.
Described defoamer is silane-modified propionic ester.
Described foam stabilizer is polyvinyl alcohol.
Described penetrating agent alkyl benzene sulphonate potassium.
Described emulsifying agent is glyceryl monostearate.
Described dispersant lauryl alcohol potassium sulfate.
Described cross-linking agent diethyl phosphate.
Described regulator is acetic acid.
Described thickening agent is carrageenan.
Described preservative is quinoxyfen.
Described flavouring agent is Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of described silkworm silk swelling agent, comprises the following steps:
S1: added by surfactant in 700-1500 part water, be warming up to 44-46 DEG C of stirring and dissolving, prepares mixed liquor I；
S2: the mixed liquor I prepared to step S1 adds penetrating agent, emulsifying agent, dispersant, cross-linking agent, thickening agent, is heated to
58-62 DEG C, under ul-trasonic irradiation, be 200-300r/min stir process 25-30min at rotating speed, prepares mixed liquor II；
S3: stop heating and ul-trasonic irradiation, the mixed liquor II prepared to step S2 adds defoamer and foam stabilizer, is turning
Speed is stirring 5-10min under 100-300r/min, prepares mixed liquor III；
S4: add preservative and flavouring agent in the mixed liquor III that step S3 prepares, under rotating speed is 100-200r/min
Stirring 3-5min, prepares mixed liquor IV；
S5: adding regulator in the mixed liquor IV that step S4 prepares, making pH value is 5-5.4, prepares mixed liquor V；
S6: potassium silicate is added in 800-8000 part water, at being warming up to 65-68 DEG C, stirring and dissolving potassium silicate, prepare mixing
Liquid VI；
Mixed liquor VI mix homogeneously that S7: the mixed liquor V step S5 prepared and step S6 prepare, i.e. prepares silkworm silk swollen
Agent.
Below by more specifically embodiment, the present invention will be described.
Embodiment 1
A kind of silkworm silk swelling agent, in units of weight portion, including following raw material: potassium silicate 500 parts, surfactant 90
Part, defoamer 8 parts, foam stabilizer 4 parts, penetrating agent 3 parts, emulsifying agent 2 parts, dispersant 2 parts, cross-linking agent 3 parts, regulator 3 parts, thickening
Agent 2 parts, preservative 2 parts, flavouring agent 1 part, 5000 parts of water；
Described surfactant is polyacrylamide.
Described defoamer is silane-modified propionic ester.
Described foam stabilizer is polyvinyl alcohol.
Described penetrating agent alkyl benzene sulphonate potassium.
Described emulsifying agent is glyceryl monostearate.
Described dispersant lauryl alcohol potassium sulfate.
Described cross-linking agent diethyl phosphate.
Described regulator is acetic acid.
Described thickening agent is carrageenan.
Described preservative is quinoxyfen.
Described flavouring agent is Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of described silkworm silk swelling agent, comprises the following steps:
S1: added in 800 parts of water by surfactant, be warming up to 45 DEG C of stirring and dissolving, prepares mixed liquor I；
S2: the mixed liquor I prepared to step S1 adds penetrating agent, emulsifying agent, dispersant, cross-linking agent, thickening agent, is heated to
60 DEG C, under ul-trasonic irradiation, be 300r/min stir process 25min at rotating speed, prepares mixed liquor II；
S3: stop heating and ul-trasonic irradiation, the mixed liquor II prepared to step S2 adds defoamer and foam stabilizer, is turning
Speed is stirring 8min under 200r/min, prepares mixed liquor III；
S4: add preservative and flavouring agent in the mixed liquor III that step S3 prepares, stir under rotating speed is 200r/min
3min, prepares mixed liquor IV；
S5: adding regulator in the mixed liquor IV that step S4 prepares, making pH value is 5.2, prepares mixed liquor V；
S6: added in 4200 parts of water by potassium silicate, be warming up at 66 DEG C, stirring and dissolving potassium silicate, prepares mixed liquor VI；
Mixed liquor VI mix homogeneously that S7: the mixed liquor V step S5 prepared and step S6 prepare, i.e. prepares silkworm silk swollen
Agent.
Embodiment 2
A kind of silkworm silk swelling agent, in units of weight portion, including following raw material: potassium silicate 200 parts, surfactant 80
Part, defoamer 6 parts, foam stabilizer 3 parts, penetrating agent 2 parts, emulsifying agent 2 parts, dispersant 1 part, cross-linking agent 2 parts, regulator 2 parts, thickening
Agent 2 parts, preservative 1 part, flavouring agent 0.8 part, 1500 parts of water；
Described surfactant is polyacrylamide.
Described defoamer is silane-modified propionic ester.
Described foam stabilizer is polyvinyl alcohol.
Described penetrating agent alkyl benzene sulphonate potassium.
Described emulsifying agent is glyceryl monostearate.
Described dispersant lauryl alcohol potassium sulfate.
Described cross-linking agent diethyl phosphate.
Described regulator is acetic acid.
Described thickening agent is carrageenan.
Described preservative is quinoxyfen.
Described flavouring agent is Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of described silkworm silk swelling agent, comprises the following steps:
S1: added in 700 parts of water by surfactant, be warming up to 44 DEG C of stirring and dissolving, prepares mixed liquor I；
S2: the mixed liquor I prepared to step S1 adds penetrating agent, emulsifying agent, dispersant, cross-linking agent, thickening agent, is heated to
58 DEG C, under ul-trasonic irradiation, be 200r/min stir process 30min at rotating speed, prepares mixed liquor II；
S3: stop heating and ul-trasonic irradiation, the mixed liquor II prepared to step S2 adds defoamer and foam stabilizer, is turning
Speed is stirring 10min under 100r/min, prepares mixed liquor III；
S4: add preservative and flavouring agent in the mixed liquor III that step S3 prepares, stir under rotating speed is 1000r/min
5min, prepares mixed liquor IV；
S5: adding regulator in the mixed liquor IV that step S4 prepares, making pH value is 5, prepares mixed liquor V；
S6: added in 800 parts of water by potassium silicate, be warming up at 65 DEG C, stirring and dissolving potassium silicate, prepares mixed liquor VI；
Mixed liquor VI mix homogeneously that S7: the mixed liquor V step S5 prepared and step S6 prepare, i.e. prepares silkworm silk swollen
Agent.
Embodiment 3
A kind of silkworm silk swelling agent, in units of weight portion, including following raw material: potassium silicate 800 parts, surfactant 100
Part, defoamer 10 parts, foam stabilizer 5 parts, penetrating agent 4 parts, emulsifying agent 3 parts, dispersant 2 parts, cross-linking agent 4 parts, regulator 3 parts, increasing
Thick dose 3 parts, preservative 2 parts, flavouring agent 1.2 parts, 9000 parts of water；
Described surfactant is polyacrylamide.
Described defoamer is silane-modified propionic ester.
Described foam stabilizer is polyvinyl alcohol.
Described penetrating agent alkyl benzene sulphonate potassium.
Described emulsifying agent is glyceryl monostearate.
Described dispersant lauryl alcohol potassium sulfate.
Described cross-linking agent diethyl phosphate.
Described regulator is acetic acid.
Described thickening agent is carrageenan.
Described preservative is quinoxyfen.
Described flavouring agent is Herba Lysimachiae foenum-graeci quintessence oil.
The preparation method of described silkworm silk swelling agent, comprises the following steps:
S1: added in 8000 parts of water by surfactant, be warming up to 46 DEG C of stirring and dissolving, prepares mixed liquor I；
S2: the mixed liquor I prepared to step S1 adds penetrating agent, emulsifying agent, dispersant, cross-linking agent, thickening agent, is heated to
62 DEG C, under ul-trasonic irradiation, be 300r/min stir process 25min at rotating speed, prepares mixed liquor II；
S3: stop heating and ul-trasonic irradiation, the mixed liquor II prepared to step S2 adds defoamer and foam stabilizer, is turning
Speed is stirring 5min under 300r/min, prepares mixed liquor III；
S4: add preservative and flavouring agent in the mixed liquor III that step S3 prepares, stir under rotating speed is 200r/min
3min, prepares mixed liquor IV；
S5: adding regulator in the mixed liquor IV that step S4 prepares, making pH value is 5.4, prepares mixed liquor V；
S6: added in 8000 parts of water by potassium silicate, be warming up at 68 DEG C, stirring and dissolving potassium silicate, prepares mixed liquor VI；
Mixed liquor VI mix homogeneously that S7: the mixed liquor V step S5 prepared and step S6 prepare, i.e. prepares silkworm silk swollen
Agent.
Performance test:
(1) use embodiment of the present invention 1-3 product and commercially available common swelling agent that the silkworm silk after refining is carried out expanding treatment,
Its compliance and intensity of colour testing result are as shown in the table.
As seen from the above table, after using silkworm silk swelling agent of the present invention, silkworm silk has stronger compliance and intensity of colour.
(2) bactericidal property detects: detect the bactericidal property of the silkworm silk swelling agent of embodiment of the present invention 1-3,
Its sterilizing power result is: staphylococcus aureus 98%-99%, escherichia coli 97%-98%, Candida albicans 97%-99%.
Above content it cannot be assumed that the present invention be embodied as be confined to these explanation, technology belonging to the present invention is led
For the those of ordinary skill in territory, without departing from the inventive concept of the premise, it is also possible to make some simple deduction or replace,
All should be considered as belonging to the scope of patent protection that the present invention is determined by the claims submitted to.
Claims (8)
1. a silkworm silk swelling agent, it is characterised in that in units of weight portion, including following raw material: potassium silicate 200-800 part,
Surfactant 80-100 part, defoamer 6-10 part, foam stabilizer 3-5 part, penetrating agent 2-4 part, emulsifying agent 2-3 part, dispersant 1-2
Part, cross-linking agent 2-4 part, regulator 2-3 part, thickening agent 2-3 part, preservative 1-2 part, flavouring agent 0.8-1.2 part, water 1500-
9000 parts；
Described surfactant is polyacrylamide；
Described foam stabilizer is polyvinyl alcohol；
Described emulsifying agent is glyceryl monostearate；
Described cross-linking agent diethyl phosphate；
The preparation method of described silkworm silk swelling agent, comprises the following steps:
S1: added by surfactant in 700-1500 part water, be warming up to 44-46 DEG C of stirring and dissolving, prepares mixed liquor I；
S2: the mixed liquor I prepared to step S1 adds penetrating agent, emulsifying agent, dispersant, cross-linking agent, thickening agent, is heated to 58-
62 DEG C, under ul-trasonic irradiation, be 200-300r/min stir process 25-30min at rotating speed, prepares mixed liquor II；
S3: stop heating and ul-trasonic irradiation, the mixed liquor II prepared to step S2 adds defoamer and foam stabilizer, at rotating speed is
Stir 5-10min under 100-300r/min, prepare mixed liquor III；
S4: add preservative and flavouring agent in the mixed liquor III that step S3 prepares, stir under rotating speed is 100-200r/min
3-5min, prepares mixed liquor IV；
S5: adding regulator in the mixed liquor IV that step S4 prepares, making pH value is 5-5.4, prepares mixed liquor V；
S6: potassium silicate is added in 800-8000 part water, at being warming up to 65-68 DEG C, stirring and dissolving potassium silicate, prepare mixed liquor
Ⅵ；
Mixed liquor VI mix homogeneously that S7: the mixed liquor V step S5 prepared and step S6 prepare, i.e. prepares silkworm silk swelling agent.
Silkworm silk swelling agent the most according to claim 1, it is characterised in that described defoamer is silane-modified propionic ester.
Silkworm silk swelling agent the most according to claim 1, it is characterised in that described penetrating agent alkyl benzene sulphonate potassium.
Silkworm silk swelling agent the most according to claim 1, it is characterised in that described dispersant lauryl alcohol potassium sulfate.
Silkworm silk swelling agent the most according to claim 1, it is characterised in that described regulator is acetic acid.
Silkworm silk swelling agent the most according to claim 1, it is characterised in that described thickening agent is carrageenan.
Silkworm silk swelling agent the most according to claim 1, it is characterised in that described preservative is quinoxyfen.
Silkworm silk swelling agent the most according to claim 1, it is characterised in that described flavouring agent is Herba Lysimachiae foenum-graeci quintessence oil.
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| CN201610519819.8A CN106149360A (en) | 2016-06-29 | 2016-06-29 | A kind of silkworm silk swelling agent |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610519819.8A CN106149360A (en) | 2016-06-29 | 2016-06-29 | A kind of silkworm silk swelling agent |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106758400A (en) * | 2016-11-29 | 2017-05-31 | 广西立盛茧丝绸有限公司 | A kind of colouring method of silk |
| CN106757399A (en) * | 2016-11-29 | 2017-05-31 | 广西立盛茧丝绸有限公司 | It is a kind of to improve natural silk degumming agent of degumming rate and preparation method thereof |
| CN106757400A (en) * | 2016-11-29 | 2017-05-31 | 广西立盛茧丝绸有限公司 | A kind of natural silk degumming agent and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105442303A (en) * | 2015-12-18 | 2016-03-30 | 张莘蔓 | Silk expanding agent and preparation method thereof |
| CN105484028A (en) * | 2015-12-18 | 2016-04-13 | 张莘蔓 | Silk bulking method |
| CN105506961A (en) * | 2015-12-18 | 2016-04-20 | 张莘蔓 | Method for puffing refined silk |
| CN105696315A (en) * | 2016-03-10 | 2016-06-22 | 广西立盛茧丝绸有限公司 | Silk swelling method |
-
2016
- 2016-06-29 CN CN201610519819.8A patent/CN106149360A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105442303A (en) * | 2015-12-18 | 2016-03-30 | 张莘蔓 | Silk expanding agent and preparation method thereof |
| CN105484028A (en) * | 2015-12-18 | 2016-04-13 | 张莘蔓 | Silk bulking method |
| CN105506961A (en) * | 2015-12-18 | 2016-04-20 | 张莘蔓 | Method for puffing refined silk |
| CN105696315A (en) * | 2016-03-10 | 2016-06-22 | 广西立盛茧丝绸有限公司 | Silk swelling method |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106758400A (en) * | 2016-11-29 | 2017-05-31 | 广西立盛茧丝绸有限公司 | A kind of colouring method of silk |
| CN106757399A (en) * | 2016-11-29 | 2017-05-31 | 广西立盛茧丝绸有限公司 | It is a kind of to improve natural silk degumming agent of degumming rate and preparation method thereof |
| CN106757400A (en) * | 2016-11-29 | 2017-05-31 | 广西立盛茧丝绸有限公司 | A kind of natural silk degumming agent and preparation method thereof |
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